KR20220164564A - (메트)아크릴산을 정제하기 위한 방법 - Google Patents

(메트)아크릴산을 정제하기 위한 방법 Download PDF

Info

Publication number
KR20220164564A
KR20220164564A KR1020227038652A KR20227038652A KR20220164564A KR 20220164564 A KR20220164564 A KR 20220164564A KR 1020227038652 A KR1020227038652 A KR 1020227038652A KR 20227038652 A KR20227038652 A KR 20227038652A KR 20220164564 A KR20220164564 A KR 20220164564A
Authority
KR
South Korea
Prior art keywords
column
stream
acrylic acid
ppm
less
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
KR1020227038652A
Other languages
English (en)
Korean (ko)
Inventor
서지 트레작
아우렐리엔 휴브
Original Assignee
아르끄마 프랑스
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 아르끄마 프랑스 filed Critical 아르끄마 프랑스
Publication of KR20220164564A publication Critical patent/KR20220164564A/ko
Pending legal-status Critical Current

Links

Images

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C57/00—Unsaturated compounds having carboxyl groups bound to acyclic carbon atoms
    • C07C57/02—Unsaturated compounds having carboxyl groups bound to acyclic carbon atoms with only carbon-to-carbon double bonds as unsaturation
    • C07C57/03—Monocarboxylic acids
    • C07C57/04—Acrylic acid; Methacrylic acid
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • B01D3/143—Fractional distillation or use of a fractionation or rectification column by two or more of a fractionation, separation or rectification step
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/34—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/42—Regulation; Control
    • B01D3/4205—Reflux ratio control splitter
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C07C51/44—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C07C51/44—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
    • C07C51/46—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation by azeotropic distillation

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
KR1020227038652A 2020-04-06 2021-03-23 (메트)아크릴산을 정제하기 위한 방법 Pending KR20220164564A (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
FRFR2003402 2020-04-06
FR2003402A FR3108906B1 (fr) 2020-04-06 2020-04-06 Procede de purification d’acide (meth)acrylique
PCT/FR2021/050490 WO2021205090A1 (fr) 2020-04-06 2021-03-23 Procede de purification d'acide (meth)acrylique

Publications (1)

Publication Number Publication Date
KR20220164564A true KR20220164564A (ko) 2022-12-13

Family

ID=71094530

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1020227038652A Pending KR20220164564A (ko) 2020-04-06 2021-03-23 (메트)아크릴산을 정제하기 위한 방법

Country Status (8)

Country Link
US (1) US12116339B2 (https=)
EP (1) EP4132898B8 (https=)
JP (1) JP2023520711A (https=)
KR (1) KR20220164564A (https=)
CN (1) CN115397801A (https=)
BR (1) BR112022018198A2 (https=)
FR (1) FR3108906B1 (https=)
WO (1) WO2021205090A1 (https=)

Family Cites Families (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3725208A (en) 1971-08-20 1973-04-03 Nippon Kayaku Kk Process for purification of acrylic acid from aldehydes by distillation with a reagent
JPS6054939B2 (ja) * 1977-08-04 1985-12-03 住友化学工業株式会社 粗製アクリル酸の精製方法
TW305830B (https=) 1993-03-26 1997-05-21 Sulzer Chemtech Ag
JP3991873B2 (ja) * 2002-01-29 2007-10-17 三菱化学株式会社 （メタ）アクリル酸の製造方法
JP3957298B2 (ja) * 2003-06-05 2007-08-15 株式会社日本触媒 アクリル酸の製造方法
US7393976B2 (en) 2003-11-26 2008-07-01 Rohm And Haas Company Process for manufacturing reduced water content (meth)acrylic acid
US8242308B2 (en) 2006-09-15 2012-08-14 Arkema Inc. Process for producing acrylic acid
FR2948365B1 (fr) 2009-07-22 2011-09-09 Arkema France Procede de fabrication d'acide acrylique bio-ressource a partir de glycerol
KR102327728B1 (ko) 2014-02-20 2021-11-18 알케마 인코포레이티드 아크릴산의 제조 공정 및 시스템
FR3033558B1 (fr) 2015-03-12 2017-02-24 Arkema France Procede ameliore de production d'acide (meth)acrylique
FR3041958B1 (fr) * 2015-10-06 2019-06-14 Arkema France Procede ameliore de production d’acide (meth)acrylique de grade polymere
FR3064630B1 (fr) * 2017-04-04 2019-09-13 Arkema France Procede de purification d'acide (meth)acrylique incluant une colonne de distillation a paroi separatrice
FR3094716B1 (fr) 2019-04-02 2021-06-04 Arkema France Production d’acide acrylique de grade polymere

Also Published As

Publication number Publication date
FR3108906B1 (fr) 2022-03-04
US12116339B2 (en) 2024-10-15
EP4132898B1 (fr) 2025-04-23
EP4132898A1 (fr) 2023-02-15
FR3108906A1 (fr) 2021-10-08
CN115397801A (zh) 2022-11-25
WO2021205090A1 (fr) 2021-10-14
BR112022018198A2 (pt) 2022-10-25
US20230109749A1 (en) 2023-04-13
EP4132898B8 (fr) 2025-10-22
JP2023520711A (ja) 2023-05-18

Similar Documents

Publication Publication Date Title
CN101516820B (zh) 制备丙烯酸的方法
KR100269194B1 (ko) 메틸 메타크릴레이트의 제조 방법
US10112885B2 (en) Process and system for producing acrylic acid
KR102263549B1 (ko) 개선된 (메트)아크릴산 제조 방법
US7799946B2 (en) Process for separating methacrolein from methacrylic acid in a gas phase product from the partial oxidation of isobutene
JP2012232996A (ja) （メタ）アクリル酸の製造方法
KR102641477B1 (ko) 분리벽을 갖는 증류 컬럼을 포함하는 (메트)아크릴산의 정제 방법
KR102698594B1 (ko) 폴리머 등급의 (메트)아크릴산의 개선된 제조 방법
KR20170128262A (ko) (메트)아크릴산의 개선된 제조 방법
KR20160036627A (ko) 미정제 에스테르-등급 아크릴산의 에스테르화에 의한 경질 아크릴레이트의 연속 제조 방법
JP3681285B2 (ja) メタクリル酸メチルの製造方法
JP5368673B2 (ja) （メタ）アクリル酸の製造方法
US20020177728A1 (en) Refining processes
KR20150115878A (ko) 프로펜의 불균질 촉매화 산화의 공정 가스로부터 아크롤레인을 제거하는 방법
KR20220164564A (ko) (메트)아크릴산을 정제하기 위한 방법

Legal Events

Date Code Title Description
PA0105 International application

St.27 status event code: A-0-1-A10-A15-nap-PA0105

PG1501 Laying open of application

St.27 status event code: A-1-1-Q10-Q12-nap-PG1501

A201 Request for examination
PA0201 Request for examination

St.27 status event code: A-1-2-D10-D11-exm-PA0201

R17-X000 Change to representative recorded

St.27 status event code: A-3-3-R10-R17-oth-X000

R18 Changes to party contact information recorded

Free format text: ST27 STATUS EVENT CODE: A-3-3-R10-R18-OTH-X000 (AS PROVIDED BY THE NATIONAL OFFICE)

R18-X000 Changes to party contact information recorded

St.27 status event code: A-3-3-R10-R18-oth-X000

D21 Rejection of application intended

Free format text: ST27 STATUS EVENT CODE: A-1-2-D10-D21-EXM-PE0902 (AS PROVIDED BY THE NATIONAL OFFICE)

PE0902 Notice of grounds for rejection

St.27 status event code: A-1-2-D10-D21-exm-PE0902

P11 Amendment of application requested

Free format text: ST27 STATUS EVENT CODE: A-2-2-P10-P11-NAP-X000 (AS PROVIDED BY THE NATIONAL OFFICE)

P11-X000 Amendment of application requested

St.27 status event code: A-2-2-P10-P11-nap-X000