CN115367748B - 一种高比表面积成型炭材料及其制备方法 - Google Patents
一种高比表面积成型炭材料及其制备方法 Download PDFInfo
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- CN115367748B CN115367748B CN202110549046.9A CN202110549046A CN115367748B CN 115367748 B CN115367748 B CN 115367748B CN 202110549046 A CN202110549046 A CN 202110549046A CN 115367748 B CN115367748 B CN 115367748B
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- 239000003575 carbonaceous material Substances 0.000 title claims abstract description 24
- 238000002360 preparation method Methods 0.000 title claims abstract description 10
- 235000013312 flour Nutrition 0.000 claims abstract description 43
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 33
- 239000002245 particle Substances 0.000 claims abstract description 27
- 229920003023 plastic Polymers 0.000 claims abstract description 22
- 239000004033 plastic Substances 0.000 claims abstract description 22
- 239000011148 porous material Substances 0.000 claims abstract description 16
- 238000001035 drying Methods 0.000 claims abstract description 15
- 238000004898 kneading Methods 0.000 claims abstract description 13
- 238000005299 abrasion Methods 0.000 claims abstract description 8
- 230000003213 activating effect Effects 0.000 claims abstract description 8
- 238000001125 extrusion Methods 0.000 claims abstract description 8
- 238000010335 hydrothermal treatment Methods 0.000 claims abstract description 8
- 238000007789 sealing Methods 0.000 claims abstract description 8
- 238000003756 stirring Methods 0.000 claims abstract description 8
- 238000002156 mixing Methods 0.000 claims abstract description 6
- 241000209094 Oryza Species 0.000 claims description 16
- 235000007164 Oryza sativa Nutrition 0.000 claims description 16
- 235000009566 rice Nutrition 0.000 claims description 16
- 238000010438 heat treatment Methods 0.000 claims description 15
- 238000000034 method Methods 0.000 claims description 14
- 239000000463 material Substances 0.000 claims description 12
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 claims description 8
- 241000209140 Triticum Species 0.000 claims description 7
- 235000021307 Triticum Nutrition 0.000 claims description 7
- 230000004913 activation Effects 0.000 claims description 7
- 241000894006 Bacteria Species 0.000 claims description 6
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims description 6
- 239000000203 mixture Substances 0.000 claims description 6
- 238000000465 moulding Methods 0.000 claims description 6
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 5
- 241000235342 Saccharomycetes Species 0.000 claims description 5
- 239000012298 atmosphere Substances 0.000 claims description 5
- 238000000855 fermentation Methods 0.000 claims description 5
- 230000004151 fermentation Effects 0.000 claims description 5
- 239000000843 powder Substances 0.000 claims description 5
- 229920002472 Starch Polymers 0.000 claims description 4
- 229910052786 argon Inorganic materials 0.000 claims description 4
- 235000019698 starch Nutrition 0.000 claims description 4
- 239000008107 starch Substances 0.000 claims description 4
- 239000001569 carbon dioxide Substances 0.000 claims description 3
- 229910002092 carbon dioxide Inorganic materials 0.000 claims description 3
- 229910052757 nitrogen Inorganic materials 0.000 claims description 3
- 239000002202 Polyethylene glycol Substances 0.000 claims description 2
- 239000001307 helium Substances 0.000 claims description 2
- 229910052734 helium Inorganic materials 0.000 claims description 2
- SWQJXJOGLNCZEY-UHFFFAOYSA-N helium atom Chemical compound [He] SWQJXJOGLNCZEY-UHFFFAOYSA-N 0.000 claims description 2
- 229920000609 methyl cellulose Polymers 0.000 claims description 2
- 239000001923 methylcellulose Substances 0.000 claims description 2
- 229920001223 polyethylene glycol Polymers 0.000 claims description 2
- 244000275012 Sesbania cannabina Species 0.000 claims 1
- 239000008187 granular material Substances 0.000 claims 1
- 238000006555 catalytic reaction Methods 0.000 abstract description 5
- 238000000926 separation method Methods 0.000 abstract description 5
- 238000001179 sorption measurement Methods 0.000 abstract description 5
- 230000000694 effects Effects 0.000 abstract description 4
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 35
- 229910052799 carbon Inorganic materials 0.000 description 12
- 241000219793 Trifolium Species 0.000 description 10
- 238000001816 cooling Methods 0.000 description 6
- 239000002994 raw material Substances 0.000 description 5
- 241000219782 Sesbania Species 0.000 description 4
- 239000011230 binding agent Substances 0.000 description 4
- 238000010000 carbonizing Methods 0.000 description 4
- 239000003795 chemical substances by application Substances 0.000 description 4
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 3
- 240000004808 Saccharomyces cerevisiae Species 0.000 description 3
- 238000010025 steaming Methods 0.000 description 3
- KXGFMDJXCMQABM-UHFFFAOYSA-N 2-methoxy-6-methylphenol Chemical compound [CH]OC1=CC=CC([CH])=C1O KXGFMDJXCMQABM-UHFFFAOYSA-N 0.000 description 2
- 239000002028 Biomass Substances 0.000 description 2
- 102000010911 Enzyme Precursors Human genes 0.000 description 2
- 108010062466 Enzyme Precursors Proteins 0.000 description 2
- 239000004372 Polyvinyl alcohol Substances 0.000 description 2
- 239000000853 adhesive Substances 0.000 description 2
- 239000003822 epoxy resin Substances 0.000 description 2
- 238000011049 filling Methods 0.000 description 2
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 2
- 229920001568 phenolic resin Polymers 0.000 description 2
- 239000005011 phenolic resin Substances 0.000 description 2
- 229920000647 polyepoxide Polymers 0.000 description 2
- 229920002451 polyvinyl alcohol Polymers 0.000 description 2
- 239000002243 precursor Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 238000004438 BET method Methods 0.000 description 1
- 230000001070 adhesive effect Effects 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 238000003763 carbonization Methods 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 229910021385 hard carbon Inorganic materials 0.000 description 1
- 238000001027 hydrothermal synthesis Methods 0.000 description 1
- 230000008595 infiltration Effects 0.000 description 1
- 238000001764 infiltration Methods 0.000 description 1
- 238000011068 loading method Methods 0.000 description 1
- 239000008204 material by function Substances 0.000 description 1
- 244000005700 microbiome Species 0.000 description 1
- 238000001000 micrograph Methods 0.000 description 1
- 229910021392 nanocarbon Inorganic materials 0.000 description 1
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- 238000004321 preservation Methods 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 238000004626 scanning electron microscopy Methods 0.000 description 1
- 238000007493 shaping process Methods 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/30—Active carbon
- C01B32/312—Preparation
- C01B32/318—Preparation characterised by the starting materials
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/30—Active carbon
- C01B32/312—Preparation
- C01B32/336—Preparation characterised by gaseous activating agents
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Carbon And Carbon Compounds (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
Abstract
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US20220411270A1 (en) * | 2021-06-24 | 2022-12-29 | Nippon Kornmeyer Carbon Group Gmbh | Method for producing carbon- or graphite-foam parts |
Citations (8)
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CN101054171A (zh) * | 2006-04-12 | 2007-10-17 | 中国科学院金属研究所 | 不同尺度纳米孔可控层次组合的碳材料及制备方法和应用 |
CN104477879A (zh) * | 2014-12-05 | 2015-04-01 | 辽宁石油化工大学 | 一种淀粉基碳材料的制备方法 |
CN104709906A (zh) * | 2013-12-17 | 2015-06-17 | 中国科学院过程工程研究所 | 一种三维分级多孔活性炭材料的制备方法 |
CN106946250A (zh) * | 2017-03-31 | 2017-07-14 | 北京化工大学 | 一种具有三维分级多孔结构的紫菜基炭材料及其制备方法和应用 |
CN107651960A (zh) * | 2017-10-27 | 2018-02-02 | 哈尔滨工业大学 | 一种基于淀粉发酵原理制作泡沫碳材料的方法 |
CN108262077A (zh) * | 2017-01-03 | 2018-07-10 | 中国科学院大连化学物理研究所 | 一种具有多级孔高强度氮掺杂炭整体式催化材料及制备方法和催化应用 |
CN109650371A (zh) * | 2019-01-11 | 2019-04-19 | 大连理工大学 | 一种制备多孔掺杂碳电极的通用方法 |
CN110813270A (zh) * | 2018-08-09 | 2020-02-21 | 南京大学 | 一种分级孔固体碱材料及其合成方法 |
Family Cites Families (1)
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CN108136364B (zh) * | 2016-07-22 | 2021-08-27 | 中国石油化工股份有限公司 | 碳基多孔材料及其制备方法和应用 |
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- 2021-05-20 CN CN202110549046.9A patent/CN115367748B/zh active Active
Patent Citations (8)
Publication number | Priority date | Publication date | Assignee | Title |
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CN101054171A (zh) * | 2006-04-12 | 2007-10-17 | 中国科学院金属研究所 | 不同尺度纳米孔可控层次组合的碳材料及制备方法和应用 |
CN104709906A (zh) * | 2013-12-17 | 2015-06-17 | 中国科学院过程工程研究所 | 一种三维分级多孔活性炭材料的制备方法 |
CN104477879A (zh) * | 2014-12-05 | 2015-04-01 | 辽宁石油化工大学 | 一种淀粉基碳材料的制备方法 |
CN108262077A (zh) * | 2017-01-03 | 2018-07-10 | 中国科学院大连化学物理研究所 | 一种具有多级孔高强度氮掺杂炭整体式催化材料及制备方法和催化应用 |
CN106946250A (zh) * | 2017-03-31 | 2017-07-14 | 北京化工大学 | 一种具有三维分级多孔结构的紫菜基炭材料及其制备方法和应用 |
CN107651960A (zh) * | 2017-10-27 | 2018-02-02 | 哈尔滨工业大学 | 一种基于淀粉发酵原理制作泡沫碳材料的方法 |
CN110813270A (zh) * | 2018-08-09 | 2020-02-21 | 南京大学 | 一种分级孔固体碱材料及其合成方法 |
CN109650371A (zh) * | 2019-01-11 | 2019-04-19 | 大连理工大学 | 一种制备多孔掺杂碳电极的通用方法 |
Non-Patent Citations (2)
Title |
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上海科学院等.《多孔材料 奇妙的微结构》.上海科学普及出版社,2018,(第1版),第31页第1-2段. * |
轻质多功能多孔碳材料的制备及性能研究;袁野;《中国博士学位论文全文数据库 工程科技Ⅰ辑》(第01期);第39页倒数第2段、第41页第1段、第42页图3-6、第44页第1段、第49页倒数第1段、第39页倒数第1段、第17页第2段、第20页第2段 * |
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Effective date of registration: 20240201 Address after: 100728 No. 22 North Main Street, Chaoyang District, Beijing, Chaoyangmen Applicant after: CHINA PETROLEUM & CHEMICAL Corp. Country or region after: China Applicant after: Sinopec (Dalian) Petrochemical Research Institute Co.,Ltd. Address before: 100728 No. 22 North Main Street, Chaoyang District, Beijing, Chaoyangmen Applicant before: CHINA PETROLEUM & CHEMICAL Corp. Country or region before: China Applicant before: DALIAN RESEARCH INSTITUTE OF PETROLEUM AND PETROCHEMICALS, SINOPEC Corp. |
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