CN115006325A - Anti-aging cosmetic emulsion containing nanogold and preparation method thereof - Google Patents
Anti-aging cosmetic emulsion containing nanogold and preparation method thereof Download PDFInfo
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- A61K2800/82—Preparation or application process involves sonication or ultrasonication
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- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
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- Emergency Medicine (AREA)
- Gerontology & Geriatric Medicine (AREA)
- Cosmetics (AREA)
Abstract
The invention relates to anti-aging cosmetic emulsion containing nanogold and a preparation method thereof, belonging to the technical field of daily necessities. The anti-aging cosmetic emulsion containing the nanogold comprises the following raw materials in parts by mass: 0.2-1 part of nanogold gel concentrated particles, 0.2-0.5 part of edible tulip extracting solution, 0.5-1 part of essential oil, 0.5-2 parts of hyaluronic acid, 5-10 parts of butanediol and 5-15 parts of solvent. The preparation method of the anti-aging cosmetic emulsion containing the nano gold comprises the following steps: mixing the above raw materials, and performing ultrasonic treatment to obtain anti-aging cosmetic emulsion containing nanogold. The anti-aging cosmetic emulsion can delay the failure of the nano-gold, is beneficial to ensuring the long-acting effect of the nano-gold, can relieve the aging of skin and improve the nutrition metabolism of the skin.
Description
Technical Field
The invention relates to the technical field of daily supplies, in particular to anti-aging cosmetic emulsion containing nanogold and a preparation method thereof.
Background
With the improvement of living standard of people, beauty and health are more and more concerned. The ever-increasing change of the cosmetic industry has strengthened the attention of people to health and beauty.
The nano gold applied to cosmetics can enter the deep layer of skin, not only can activate cells, but also can eliminate free radicals and resist oxidation, but the addition of the gold can cause the cost increase of the cosmetics. The nano gold is used as an antioxidant, and the capability of eliminating free radicals plays a role in enhancing the antioxidation effect, so that the effect of the nano gold is determined.
At present, in cosmetics, only the prepared nanogold gel is mixed with other components to prepare cosmetic emulsion, the efficacy is single, and the nanogold directly enters deep layers of skin to eliminate free radicals, so that the antioxidant effect is poor.
Disclosure of Invention
The invention provides a nano-gold-containing anti-aging cosmetic emulsion and a preparation method thereof for solving the technical problems. The edible tulip extracting solution is added into the anti-aging cosmetic emulsion, so that the failure of the nano-gold can be delayed, the long-acting effect of the nano-gold can be ensured, the aging of skin can be relieved, and the nutrition metabolism of the skin can be improved.
The technical scheme for solving the technical problems is as follows:
the invention provides a preparation method for the composite material, which comprises the following raw materials in parts by mass: 0.2-1 part of nanogold gel concentrated particles, 0.2-0.5 part of edible tulip extracting solution, 0.5-1 part of essential oil, 0.5-2 parts of hyaluronic acid, 5-10 parts of butanediol and 5-15 parts of solvent.
The principle of the invention is as follows:
nanogold gel concentrate particles capable of scavenging free radicals; the Pseudobulbus Cremastrae Seu pleiones extract has effects of activating tyrosinase, inhibiting cell division, and resisting radiation; hyaluronic acid has effects of keeping moisture, resisting aging, resisting ultraviolet, promoting wound healing, and resisting bacteria and inflammation.
The beneficial effects of the invention are: the invention can delay the invalidation of the nano-gold, is beneficial to ensuring the long-acting effect of the nano-gold, can relieve the aging of skin and improve the nutrition metabolism of the skin.
Furthermore, the particle size of the nanogold gel concentrated particles is 50-100 mu m.
The beneficial effect of adopting the further scheme is that: under the particle size, the nanogold gel concentrated particles can enter the deep layer of the skin, can effectively improve the skin and play a role in resisting aging.
Further, the nanogold gel particles are prepared from the following raw materials in parts by mass: 0.02-0.08 part of gold nanoparticles, 0.05-0.5 part of gel factors, 5-20 parts of hyaluronic acid and 5-20 parts of collagen membrane liquid.
The beneficial effect of adopting the further scheme is that: the nano gold gel particles contain hyaluronic acid and collagen, and have good effect of improving the skin.
Furthermore, the edible tulip extracting solution contains 0.02-0.1% of active ingredients and the balance of ethanol.
The beneficial effect of adopting the above further scheme is: the active ingredients of the edible tulip extracting solution comprise leucine, di (2-ethyl) hexyl phthalate, gastrodin and daucosterol, and the edible tulip extracting solution adopting the active ingredients can effectively improve the performance of skin cells.
Further, the essential oil is any one of rose essential oil, lavender essential oil and camellia essential oil.
The beneficial effect of adopting the further scheme is that: the essential oil can impart fragrance to cosmetic emulsion.
Further, the solvent is any one of deionized water.
The beneficial effect of adopting the above further scheme is: the raw materials can be sufficiently dissolved by using the solvent.
The invention also provides a preparation method of the anti-aging cosmetic emulsion containing the nanogold, which comprises the following steps: mixing 0.2-1 part by mass of nanogold gel concentrated particles, 0.2-0.5 part by mass of edible tulip extracting solution, 0.5-1 part by mass of essential oil, 0.5-2 parts by mass of hyaluronic acid, 5-10 parts by mass of butanediol and 5-15 parts by mass of solvent, and carrying out ultrasonic treatment until the mixture is uniform, thus obtaining the nanogold-containing anti-aging cosmetic emulsion.
The beneficial effect who adopts above-mentioned scheme is: the cosmetic emulsion prepared by the method has good uniformity.
Further, the nanogold gel concentrated particles are prepared by the following steps:
s11: fully mixing 0.02-0.08 part by mass of nano gold particles, 0.05-0.5 part by mass of gel factors and 5-20 parts by mass of hyaluronic acid to obtain an initial mixed solution;
s12: pressurizing and atomizing the initial mixed solution obtained in the step S11 to obtain initial droplets, and freeze-drying the initial droplets to obtain freeze-dried droplets;
s13: and (5) mixing the freeze-dried microdroplets obtained in the step (S12) with 5-20 parts by mass of collagen membrane liquid to obtain a membrane-coated mixed solution, and then carrying out pressurization and atomization treatment to obtain the nanogold gel concentrated particles.
The beneficial effect of adopting the further scheme is that: the initial microdroplet can be solidified at low temperature through freeze-drying, after the initial microdroplet is mixed with collagen membrane liquid, a collagen membrane can be attached to the outer surface of the initial microdroplet, and then the nano-gold gel concentrated particles can be obtained after atomization treatment, wherein both collagen and hyaluronic acid can be used for assisting nano-gold particles to improve the skin.
Further, in step S12, the temperature of the freeze-drying is-25 to-30 ℃.
The beneficial effect of adopting the further scheme is that: at the temperature, the initial microdroplets can be freeze-dried, and the freeze-drying effect is good.
Further, in step S13, the mixing temperature is 0 to 5 ℃.
The beneficial effect of adopting the further scheme is that: at the temperature, the freeze-dried microdroplets and the collagen membrane liquid have good mixing effect, and the freeze-dried microdroplets are wrapped by the collagen.
Detailed Description
The principles and features of this invention are described below in conjunction with examples which are set forth to illustrate, but are not to be construed to limit the scope of the invention.
Example 1
In this example, the anti-aging cosmetic emulsion containing nanogold was prepared from 0.5 parts by mass of nanogold gel-concentrated fine particles, 0.3 parts by mass of an edible tulip extract, 0.8 parts by mass of essential oil, 1.5 parts by mass of hyaluronic acid, 8 parts by mass of butylene glycol, and 8 parts by mass of deionized water; wherein the average particle diameter of the nanogold gel concentrated particles is 60 mu m, and the nanogold gel concentrated particles are prepared from 0.05 part by mass of nanogold particles, 0.2 part by mass of gel factors, 15 parts by mass of hyaluronic acid and 15 parts by mass of collagen membrane liquid.
And (3) taking and mixing the raw materials according to the parts by mass, and carrying out ultrasonic treatment to homogenize the mixture to obtain the anti-aging cosmetic emulsion containing the nanogold.
Example 2
In this example, the anti-aging cosmetic emulsion containing nanogold was prepared from 0.4 parts by mass of nanogold gel concentrated particles, 0.2 parts by mass of an edible tulip extract, 0.7 parts by mass of essential oil, 1.8 parts by mass of hyaluronic acid, 10 parts by mass of butylene glycol, and 13 parts by mass of deionized water; wherein the average particle diameter of the nanogold gel concentrated particles is 75 microns, and the nanogold gel concentrated particles are prepared from 0.06 part by mass of nanogold particles, 0.4 part by mass of gel factors, 16 parts by mass of hyaluronic acid and 15 parts by mass of collagen membrane liquid.
And (3) taking and mixing the raw materials according to the parts by mass, and carrying out ultrasonic treatment to homogenize the mixture to obtain the anti-aging cosmetic emulsion containing the nanogold.
Example 3
In this example, the anti-aging cosmetic emulsion containing nanogold was prepared from 0.8 parts by mass of nanogold gel-concentrated fine particles, 0.4 parts by mass of an edible tulip extract, 0.8 parts by mass of essential oil, 1.8 parts by mass of hyaluronic acid, 10 parts by mass of butylene glycol, and 13 parts by mass of deionized water; wherein the average particle diameter of the nanogold gel concentrated particles is 55 mu m, and the nanogold gel concentrated particles are prepared from 0.08 mass part of nanogold particles, 0.4 mass part of gel factors, 20 mass parts of hyaluronic acid and 20 mass parts of collagen membrane liquid.
And (3) taking and mixing the raw materials according to the parts by mass, and carrying out ultrasonic treatment to homogenize the mixture to obtain the anti-aging cosmetic emulsion containing the nanogold.
Comparative example 1
In the comparative example, the anti-aging cosmetic emulsion containing no nanogold was prepared from 0.3 part by mass of an extractive solution of pseudobulbus cremastrae seu pleiones, 0.8 part by mass of essential oil, 1.5 parts by mass of hyaluronic acid, 8 parts by mass of butylene glycol and 8 parts by mass of deionized water.
And (3) taking and mixing the raw materials according to the parts by mass, and carrying out ultrasonic treatment to homogenize the mixture to obtain the anti-aging cosmetic emulsion without containing the nanogold.
Comparative example 2
In the comparative example, the anti-aging cosmetic emulsion containing nanogold was prepared from 0.5 part by mass of nanogold gel concentrated particles, 0.8 part by mass of essential oil, 1.5 parts by mass of hyaluronic acid, 8 parts by mass of butylene glycol and 8 parts by mass of deionized water; wherein the average particle diameter of the nanogold gel concentrated particles is 60 mu m, and the nanogold gel concentrated particles are prepared from 0.05 part by mass of nanogold particles, 0.2 part by mass of gel factors, 15 parts by mass of hyaluronic acid and 15 parts by mass of collagen membrane liquid.
And (2) taking and mixing the materials according to the parts by weight of the raw materials of the anti-aging cosmetic emulsion containing the nanogold, and carrying out ultrasonic treatment until the mixture is homogenized to obtain the anti-aging cosmetic emulsion containing the nanogold.
The performance analysis and inspection are carried out according to the cosmetic hygiene standard, and the inspection method is as follows:
respectively mixing the emulsions of the examples 1-3 and the comparative examples 1-2 with deionized water according to a volume ratio of 1:5, adding 0.1mL of 0.01% hydrogen peroxide into 20mL of the mixed emulsion for reaction, dipping a sample by a glass rod, and testing the complete decomposition of the hydrogen peroxide by using an acid ferrous chloride test paper; adding 0.1mL of hydrogen peroxide with the mass concentration of 0.01% into the sample for reaction, and testing by using acid ferrous chloride test paper; and repeating the steps until the hydrogen peroxide is not completely decomposed by testing with the acidic ferrous chloride test paper, and recording the final times of adding the hydrogen peroxide.
The test results were as follows:
example 1: the times are 20 times in total;
example 2: the number of times is 19 times in total;
example 3: the times are 21 times in total;
comparative example 1: the times are 12 times in total;
comparative example 2: the number of times was 5 times in total.
The test result shows that: the emulsions containing gold nanoparticles used in examples 1 to 3 and comparative example 1 each have a longer oxidation resistance, and the addition of the Pseudobulbus Cremastrae Seu pleiones extract can prolong the oxidation resistance of the emulsions; the nano gold gel concentrated particles are not added in the comparative example 2, so that the oxidation resistance is low; the nano gold gel concentrated particles and the edible tulip extract can mutually promote and cooperate with each other, so that the duration of the oxidation resistance of the cosmetic emulsion can be prolonged.
The above description is only for the purpose of illustrating the preferred embodiments of the present invention and is not to be construed as limiting the invention, and any modifications, equivalents, improvements and the like that fall within the spirit and principle of the present invention are intended to be included therein.
Claims (10)
1. The anti-aging cosmetic emulsion containing the nanogold is characterized by comprising the following raw materials in parts by mass: 0.2-1 part of nanogold gel concentrated particles, 0.2-0.5 part of edible tulip extracting solution, 0.5-1 part of essential oil, 0.5-2 parts of hyaluronic acid, 5-10 parts of butanediol and 5-15 parts of solvent.
2. The anti-aging cosmetic emulsion containing nanogold according to claim 1, wherein the particle size of the nanogold gel concentrated particles is 50 to 100 μm.
3. The anti-aging cosmetic emulsion containing nanogold according to claim 1, wherein the nanogold gel particles consist of the following raw materials in parts by mass: 0.02-0.08 part of nano gold particles, 0.05-0.5 part of gel factors, 5-20 parts of hyaluronic acid and 5-20 parts of collagen membrane liquid.
4. The anti-aging cosmetic emulsion containing nanogold according to claim 1, wherein the iphigenia indica extracting solution contains 0.02-0.1% of active ingredients, and the balance of ethanol.
5. The anti-aging cosmetic emulsion containing nanogold according to claim 1, wherein the essential oil is any one of rose essential oil, lavender essential oil and camellia essential oil.
6. The anti-aging cosmetic emulsion containing nanogold according to claim 1, wherein the solvent is any one of deionized water.
7. The method for preparing the anti-aging cosmetic emulsion containing nanogold according to any one of claims 1 to 6, comprising the steps of: mixing 0.2-1 part by mass of nanogold gel concentrated particles, 0.2-0.5 part by mass of edible tulip extracting solution, 0.5-1 part by mass of essential oil, 0.5-2 parts by mass of hyaluronic acid, 5-10 parts by mass of butanediol and 5-15 parts by mass of solvent, and carrying out ultrasonic treatment until the mixture is uniform, thus obtaining the nanogold-containing anti-aging cosmetic emulsion.
8. The method for preparing the anti-aging cosmetic emulsion containing nanogold according to claim 7, wherein the nanogold gel concentrated particles are prepared by the following steps:
s11: fully mixing 0.02-0.08 part by mass of nano gold particles, 0.05-0.5 part by mass of gel factors and 5-20 parts by mass of hyaluronic acid to obtain an initial mixed solution;
s12: pressurizing and atomizing the initial mixed solution obtained in the step S11 to obtain initial droplets, and freeze-drying the initial droplets to obtain freeze-dried droplets;
s13: and (5) mixing the freeze-dried microdroplets obtained in the step (S12) with 5-20 parts by mass of collagen membrane liquid to obtain a membrane-coated mixed solution, and then carrying out pressurization and atomization treatment to obtain the nanogold gel concentrated particles.
9. The method for preparing the anti-aging cosmetic emulsion containing nano-gold according to claim 8, wherein the temperature of the freeze-drying is-25 to-30 ℃ in the step S12.
10. The method for preparing the anti-aging cosmetic emulsion containing nanogold according to claim 8, wherein the mixing temperature is 0 to 5 ℃ in step S13.
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| CN116672291B (en) * | 2023-06-20 | 2024-02-13 | 广州家化化学有限公司 | Private care solution containing nano gold and preparation method thereof |
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