KR101748093B1 - Skin Moisturizing Mist Composition with Hydogen water and Ozone - Google Patents

Abstract

The present invention discloses a skin moisturizing mist composition capable of preventing and improving skin aging through ozone having an effect on skin tissue regeneration by removing active oxygen which is a main factor of skin aging through hydrogen peroxide having an antioxidative effect, And a manufacturing method thereof. Such a skin moisturizing mist composition may further comprise a plant extract, and provides a cosmetic spray device using the same.

Description

{Skin Moisturizing Mist Composition with Hydogen water and Ozone}

The present disclosure relates to a skin moisturizing mist composition containing water, ozone, natural essential oil, and gamma-polyglutamic acid, which provides moisture and nutrition to the skin and has excellent antioxidant effect for removing active oxygen causing skin aging And a manufacturing method thereof.

The skin of a person is continuously aged due to a decrease in the ability of the cell naturally since the 20th generation. As a result, the elasticity of the skin is reduced and the wrinkles are generated and the visual beauty is decreased. Especially, The facial skin, which is a critical factor in perception, is a part that makes much effort to look younger and beautiful by delaying aging.

Skin aging, as mentioned above, is a natural biological phenomenon as the age goes on, but the rate of skin aging is greatly influenced by the stimulation of the external environment. Typical causes are the effects of active oxygen generated on the skin and ultraviolet Exposure and other external factors.

Therefore, it is difficult to artificially control skin aging according to age, but in the case of external factors, it is possible to remove or inhibit, for example, to remove active oxygen generated on skin, to block ultraviolet rays, It is possible to slow down the progress of skin aging and to look younger and younger than age.

On the other hand, active oxygen, which is the most representative cause of skin aging, is a highly oxidative oxygen scum that is naturally generated in the body of a human body as oxygen which is introduced into the body through respiration is used as an energy source in a normal metabolic process, Sometimes it occurs in the body, but the skin is exposed to ultraviolet rays, and active oxygen is generated. Or by external factors such as X-rays, tobacco smoke and air pollution electromagnetic waves, pesticide residues and stress.

These reactive oxygen species contain peroxides in the form of oxygen ions and are highly reactive substances, such as oxidizing other substances in the body due to unpaired electrons. They attack normal DNA and cellular tissues of the body, Destroys information, collapses cell membranes and forms abnormal cellular proteins.

In particular, facial skin, which is easily exposed to ultraviolet rays in the body, is more easily oxidized than active oxygen, and oxidizes the lipid of the facial skin cell membrane to produce peroxidized lipid, which is converted to an aged pigment by binding with protein, It also causes melanin pigment, which causes stain or freckles on the facial skin. It also causes collagen, which is the elastic fiber of the skin, to change and cause skin sagging and wrinkles. When active oxygen enters our body, normal cells and DNA are attacked. Direct and indirect diseases are cancer, leukemia, heart disease, arteriosclerosis, stroke, angina, hypertension, rheumatism, atopic dermatitis, dandruff, Wrinkles, and stains.

This harmful active oxygen is highly reactive and can easily bind to hydrogen atoms. When bound to hydrogen atoms, active oxygen can be easily removed while changing to water. Thus, attempts to remove active oxygen of skin using this principle There has been a skin aging prevention device in which water in air is converted into hydrogen ions and superoxide ions and then supplied to the skin to remove active oxygen.

However, although the skin aging prevention device succeeded in inducing the ionizing gas of the skin to be ejected, the amount of the generated ionizing gas was small, and the effect was insignificant because the ejected ionizing gas disappeared into the air immediately after contact with the skin.

According to a recent study, the activity of superoxide dismutase, an enzyme neutralizing free radicals, which is originally present in the body but gradually decreases from about 30 years of age and decreases in proportion to age, causing rapid aging progression , It is considered that hydrogen having an antioxidant effect sufficiently complements the function of the superoxide dismutase,

On the other hand, it has been confirmed that when water is electrolyzed, atomic hydrogen having high reactivity is dissolved in the reduced water generated on the cathode side. Hydrogen is usually present in the molecular state, but the active hydrogen in the atomic state is unstable. Therefore, when bound to minerals such as metal nano-colloids, it can stay stable for a long time. Hydrogen is a powerful toxic active oxygen that can not remove many antioxidants Hydroxy radicals. ≪ / RTI > This is a reaction in which a nano-sized hydrogen molecule aggregate dissolved in water reacts with a hydroxyl radical, which is an active oxygen, into water. It can not be removed by hydrogen gas bubbles that are large enough to be seen, Hydrogen atoms, that is, the active hydrogen is most likely to react with active oxygen.

On the other hand, ozone is an oxygen isotope having a structure in which three oxygen atoms are bonded, and has not only strong anti-skin effect against bacterial, viral and fungal infectious diseases but also excellent in skin tissue regeneration through rapid healing ability As the results of research on the effect of ozone are known, there is an increasing tendency to use ozone to improve skin aging.

1. KR Patent Registration No. 10-1055472 C1 (2011.08.02) 2. KR Registration Utility Model Bulletin 20-0469698 C1 (March 10, 2013)

To provide moisture and nutrition to the user's skin, and to provide a skin moisturizing mist composition capable of preventing and improving skin aging in advance.

The present disclosure has the following features in order to achieve the above object.

The mist moisturizing composition for skin moisturizing according to the present invention is characterized by containing hydrogen peroxide, ozone dissolved in oil, natural essential oil and gamma-polyglutamic acid. And at least one selected from the group consisting of

The composition for skin moisturizing mist of the present disclosure is characterized by further comprising a vegetable extract, wherein the vegetable extract comprises at least one kind of at least one or two or more kinds of extracts selected from the group consisting of locust bean leaves, golden roots, The extract is characterized by containing at least one selected from the group consisting of lavender extract, rosemary extract, sunflower extract, borage extract, sage extract, jasmine extract and chemomail extract.

The present invention relates to a method for producing a mist moisturizing composition for skin moisturizing, which contains hydrogen peroxide, ozone dissolved in oil, natural essential oil and gamma-polyglutamic acid. (a) preparing the hydrogenated water; (b) producing ozone dissolved in the oil; (c) mixing the aqueous hydrogen peroxide produced in the steps (a) and (b) with ozone dissolved in the oil, extracted natural essential oil, gamma-polyclutamate and vegetable extract do.
The step of producing hydrofluoric acid may include the steps of: (T1) combining one of alternating current and direct current; (T2) electrolysis through a selected electricity for electrolysis; And (T3) electrolyzing the electrolyzed water to obtain the hydrogenated water, wherein the electricity for electrolysis comprises: (1) a method of reversing direct current electricity at an arbitrary cycle; (2) a method of using high frequency alternating current; (3) a method in which DC or DC inversion and AC electricity are simultaneously used in the same electrolysis tank; (4) a method in which DC or DC inversion and AC electricity are alternately used in the same electrolysis tank; And (5) a method in which a plurality of electrolytic tanks are used to separately use a direct current or direct current inversion electrolytic tank and an alternating electrolytic tank separately, and the voltage or inversion period is varied widely to improve the efficiency of electrolysis, PH is neutral and has a high reducing power, and the concentration of active hydrogen is increased.
The step of producing dissolved ozone in the oil may include the steps of: (S1) generating ozone by using an ozone generator through a plasma, a high voltage discharge, a corona discharge, or a UV method; (S2) bubbling the ozone generated in the step S1 in the oil at a low temperature until the ozone dissolved amount in the oil becomes 400 to 1,100 meq / kg peroxide; And (S3) changing the viscosity of the oil by increasing the bubbling temperature after the primary bubble discharge in the step S2, and then decreasing the bubbling temperature so that the ozone dissolved amount in the oil becomes 1400 to 2900 meq / kg of peroxide Wherein the oil contains an unsaturated fatty acid, the ozone reacts with the double bond structure between the carbon atoms of the unsaturated fatty acid to produce an ozonized oil, and the unsaturated fatty acid is oleic acid, palmitoleic acid , Linoleic acid, and arachidonic acid.
The cosmetic spray device of the present disclosure is characterized by comprising a mist composition for skin moisturizing.

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As described above, the composition for skin moisturizing mist is formed by addition of water and ozone. Since the chemical composition is not contained as a main component, it is excellent in terms of function as well as cosmetics, It is a mixture with natural extract without side effects. It has the advantage of preventing aging of skin and improving skin by removing active oxygen which is the most important factor of skin aging.

FIG. 1 is a flow chart showing steps of a method for producing hydrogenated water. FIG.
FIG. 2 is a flowchart showing steps of a method for producing ozonized oil.

Will be apparent as the same becomes better understood by reference to the advantages and features of the disclosure herein, and the embodiments described below which achieve them. It should be understood, however, that the present disclosure is not limited to the embodiments disclosed herein but may be embodied in many different forms and should not be construed to limit the scope of the present disclosure to those skilled in the art, To fully disclose the scope of the disclosure, which is defined by the scope of the claims and is not intended to be limiting. The singular forms herein include plural forms unless the context clearly dictates otherwise.

In the following description of the embodiments of the present invention, a detailed description of known functions and configurations incorporated herein will be omitted when it may obscure the subject matter of the present disclosure. The terms used herein are defined in consideration of functions in the embodiments of the present disclosure, which may vary depending on the user, the intention or custom of the operator, and the like. Therefore, the definition should be based on the contents throughout this specification.

Hereinafter, preferred embodiments of the present disclosure will be described in detail. BRIEF DESCRIPTION OF THE DRAWINGS The above and other features and advantages of the present invention will be more clearly understood from the following detailed description taken in conjunction with the accompanying drawings, in which: FIG.

This disclosure relates to a mist moisturizing composition for skin moisturizing, and a cosmetic spray device comprising the same, and in one aspect, the disclosure relates to a mist moisturizing composition for skin moisturizing.

More specifically, the composition for skin moisturizing mist according to the present disclosure is characterized by containing hydrogen water, ozone, natural essential oil and gamma-polyglutamic acid as main components.

The composition for skin moisturizing according to the present disclosure has an active oxygen eliminating function which is excellent in electrolytic reduced water in which hydrogen having atomic state of high reactivity is present when water is electrolyzed and has an antioxidative action and is effective for preventing skin aging .

As a result of analyzing water of the world's miracles, the electrolytic reduced water has been found to contain a large amount of hydrogen which is not contained in general water, and researches that hydrogen combines with active oxygen to prevent the disease of the body (Hereinafter referred to as "hydrogenated water") in the industry as a result of analysis based on not only the composition of water, but also the amount of hydrogen dissolved.

The active oxygen is divided into a good active oxygen used in the immune function and a bad active oxygen (hereinafter referred to as active oxygen) which is too active and toxic to damage cells. Here, the generation of active oxygen is the conversion of 1% to 2% of the inhaled oxygen, although most of the oxygen inhaled by a person for energy production of the body is converted into water. When the burden of mitochondria increases due to excessive exercise or stress, active oxygen becomes unnecessary and becomes unstable. There are many factors that cause active oxygen, such as ultraviolet and intense exercise, as well as stress, overeating, drinking, smoking, radiation, ultrasound and environmental pollution, and ultimately cause cell disease and promote senescence do. Other factors include ultraviolet rays, nitrogen monoxide, chemical fertilizers, medicines, residual pesticides, peroxides, and metal ions. These free radicals cause a free radical reaction that destroys the membranes of cell membranes and intracellular organelles, resulting in scars on DNA that cause cancer, adult disease, and aging.

On the other hand, hydrogen is the only antioxidant capable of selectively removing only active oxygen and reaching the organs and brain cells of the body. In addition, the cells of the body are composed of water and oil. Since hydrogen is dissolved in both water and oil, it can reach the corners of cells and remove active oxygen. Many people know that hydrogen reacts intensely, but in fact, hydrogen molecules do not burn well. This is due to the diffusivity of hydrogen. Diffusivity refers to the property of flying quickly into the air when dispersed. Hydrogen diffuses quickly when left in the air due to its diffusibility, but when absorbed into the body, it does not accumulate without active oxygen and is not discharged out of the body.

Specifically, the method for producing the hydrogenated water will be described. Hydrogen is generated by electrolysis, so that water can be electrolyzed to generate hydrogen atoms and be held in a state of hydrogen atoms in the water. In this case, (T1) of combining one of the alternating currents and the inverse of the direct current as follows; A step (T2) of electrolyzing through a selected electricity for electrolysis; And a step (T3) of obtaining hydrogenated water through electrolysis.

(1) A method in which DC electricity is inverted at an arbitrary cycle.

(2) a method using high-frequency alternating current.

(3) Direct current or direct current inversion and alternating current are used simultaneously in the same electrolysis tank.

(4) A method in which DC or DC inversion and AC electricity are alternately used in the same electrolysis tank.

(5) A method in which a plurality of electrolysis tanks are used, and a direct current or direct current inversion electrolysis tank and an alternating electrolysis tank are separately used.

As described above, when the alternating current or the direct current inversion is used in combination, the PH becomes neutral and has a high reducing power, and if the voltage or the inversion period is widely varied, the concentration of active hydrogen is increased and the efficiency of electrolysis is increased.

More specifically, in the composition of the present disclosure, the hydrophobic water is preferably 90 to 98% by weight based on the total weight of the composition for moisturizing the skin. Active hydrogen in the hydrophobic water contacts the skin to remove active oxygen, to enhance nutrition and vitality of the cells, and to prevent cell death due to aging of the cells. Therefore, the user's skin tone becomes clear, It is possible to obtain an effect of preventing aging as well as promotion of skin production.

On the other hand, in the composition according to the present disclosure, the ozone is an ozonized oil dissolved in an oil that is a gaseous state in a gaseous state, or is contained in a micro / nano bubble. Ozone itself is decomposed by oxygen in the air and strong ultraviolet It is an active gas which has no concern about secondary pollution because of its nature to return to oxygen after the reaction. It can generate gas regardless of its location if there is only air or oxygen, emits oxygen in a short time in water, There is no fear of car pollution. In addition, it has a strong oxidative power next to fluorine in natural materials, and it has strong sterilizing action.

Generally, the ozone is an isotope of oxygen, which is generated by the action of active oxygen on oxygen molecules in principle. There are several ways to obtain oxygen on this atom. The most common recipe is a method of causing silent discharge in clean dry air or oxygen through the ozone generator. Other methods include electrolysis of dilute sulfuric acid at low temperature and heating of liquid oxygen. It also occurs when ultraviolet rays are applied to the air, when fluorine reacts with water, or when phosphorus is oxidized.

In addition, ozone has a pale blue color in a gaseous state, a black-blue color in a liquid state, a dark purple color in a solid state, a peculiar smell, and a smell can be felt even when 1/500000 capacity exists in the air. The melting point is -193 ° C, the boiling point is -111.9 ° C, the critical temperature is -5 ° C, and the critical pressure is 92.3 atm. In the gaseous state, it does not dissolve well in water. Solubility dissolves in liquid nitrogen, carbon tetrachloride, and chloroform at 9.4 mL / 100 mL at 40 ° C and is well absorbed in turpentine oil and cinnamon oil.

Specifically, the method for producing the ozonized oil will be described. Ozone, which is a very unstable gas having a structure in which three oxygen atoms are bonded, has a strong nature to dissociate naturally. Ozone with unstable structure has the ability to dissociate the bacteria by taking away the electrons of the fundamental RNN / DNN structure. In addition, oxygen atoms generated by the decomposition of ozone have a strong oxidizing power, and react easily with other compounds to oxidize and decompose the compounds. However, since ozone easily escapes from the hydrophilic material and is released into the air, the function of ozone can not be sufficiently used. In recent years, ozone is dissolved in oil, which is a hydrophobic material, Ozone oil was produced by the method, and the function of ozone was effectively used.

This is a method of injecting oxygen into oil and irradiating ultraviolet rays thereto to react oxygen with oil. The present disclosure relates to a method of producing ozone using an ozone generator (S1); Bubbling the ozone generated in the oil at 5 to 32 DEG C in the oil so as to carry out a primary bubble ejection step (S2) until the amount of dissolved ozone in the oil becomes 400 to 1100 meq / kg peroxide; After the primary bubble ejection, the bubbling temperature is increased to 26 to 62 ° C to change the viscosity of the oil, and then the bubbling temperature is reduced to 5 to 32 ° C, so that the ozone dissolution amount in the oil becomes 1400 to 2900 meq / kg peroxide And a step (S3) of discharging the secondary bubbles until the bubbles are discharged.

First, since ozone is generated by the ozone generator, it may be difficult to provide the required amount of ozone by only the ozone generator. Therefore, in this step (S1), liquefied oxygen and oxygen generator are additionally added before ozone generation, The efficiency of the generator can be increased. Ozone can be generated by plasma, high voltage discharge, corona discharge, and UV method by injecting a high concentration of oxygen gas into a conventional ozone generator.

Then, the ozone generated in the step (S1) is bubbled and injected into the oil. The oil includes an unsaturated fatty acid because the double bond structure and ozone react between the carbon atoms of the unsaturated fatty acid to produce an ozonized oil. The unsaturated fatty acid may be oleic acid, palmitoleic acid, linoleic acid, arachidonic acid, But is not limited thereto, and may be contained in an amount of 50 wt% or more, and more preferably 50 to 90 wt%, based on 100 wt% of the oil. When the content is less than 50% by weight, even if ozone is dissolved for a long time, there is a limit in the amount of the dissolution, namely, the increase in the peroxide value, and dissociation can be more easily caused even when stored. Continuously bubble ozone until ozone is fully saturated and let it dissolve until maximum is maintained.

In general, ozone is sensitive to external stimuli such as light, humidity, temperature, etc., so it is preferable to remove the moisture during bubbling and increase the temperature during ozone dissolution. The ozone injection according to the primary bubble ejection is preferably carried out at a low temperature of 5 to 32 DEG C, and particularly preferably at 13 to 16 DEG C for an increase in the peroxide value, so that a separate cooling device It can also be used. If the bubbling temperature is less than 5 ° C, the oil may rapidly solidify to become a semi-solid state, and the peroxide value of the ozone may not be properly discharged. If the temperature exceeds 32 ° C, . At this time, the injection time is about 50 to 200 hours for a long time, but if it is carried out for a long time, the fluid oil is changed to a semi-solid state cream. If the oil turns into a viscous cream, the ozone bubbling effect can no longer be expected. Therefore, in the primary bubble discharging step S2, it is preferable to set the peroxide value in the oil to about 400 to 1100 meq / kg.

In order to lower the viscosity of the oil which has been changed into the cream form by injecting ozone for a long time in the primary bubble discharging step (S2), the bubbling temperature of the ozone is increased for a certain period of time so that the ozone is further dissolved in the oil, In the discharging step S3, a separate heating device may be used to allow the ozone to bubble in the heated state. At this time, the bubbling temperature is preferably 26 to 62 占 폚. When the bubbling temperature is less than 26 캜, the oil does not change from a semi-solid cream state to a liquid state, so that the oil does not dissolve well. When the temperature exceeds 62 캜, it may be difficult to preserve the peroxide value. Unlike the primary bubble discharge step (S2), when the temperature is increased, the liquid phase is changed to increase the dissolution efficiency and increase the peroxide value.

However, if the viscosity of the oil is changed, the amount of the gas discharged to the gas is also increased. Therefore, it is preferable to lower the viscosity to the same temperature as that of the primary bubble discharging step (S2). After the secondary bubble discharging step (S3), the ozone dissolution amount is preferably 1400 to 2900 meq / kg of peroxide. When the dissolved amount of ozone is less than 1400 meq / kg, the value of peroxide value in the final produced ozonized oil does not reach the desired range, and when it exceeds 2900 meq / kg, ozone injection in oil may be difficult and cytotoxicity is induced according to the user Skin sensitization can occur.

On the other hand, micro-nano bubbles including ozone have a diameter of nm to μm and can be manufactured using conventional techniques. Further, it can be manufactured by sending a pressurized gas into a composition by using a porous body having fine pores of micrometers or less such as a nanofiltration membrane or a gas separation membrane. The electromagnetic fluid phenomenon and the resonance resonance using the Bernoulli's lens and Faraday's law Thereby inducing development.

In one aspect of the present disclosure, the diameter of the micro-nano bubbles may be 0.005 to 2.5 μm, specifically preferably 0.01 to 1.5 μm, more specifically 0.05 to 1 μm. The diameter of the micro / nano bubbles refers to the average diameter of the micro / nano bubbles contained in the composition. When the micro / nano bubbles have diameters in the range as described above, excellent stability and effects can be exhibited in the composition.

According to the embodiment described above, the ozone dissolved in the ozone or ozone contained in the micro / nano bubble may be contained in an amount of 5 to 300 μg / mL, specifically 10 to 150 μg / mL, It is possible to minimize deterioration or discoloration of the container containing the composition and the composition, with a better skin disease-improving effect.

In the composition according to the present disclosure, in particular, natural essential oils are required to be a directional substance, that is, natural fragrance collected from vegetable tissues, in comparison with synthetic fragrances which have adverse side effects on the production characteristics of cosmetics and fragrance products. A non-volatile solvent extraction method, a leaching solvent extraction method, a liquefied gas extraction method, and a steam distillation method.

In addition, in the skin lotion composition of the present disclosure, the natural essential oil may be any one or more selected from the group consisting of plants harmoniously harmonizing with natural fragrances, for example, a group consisting of a country, a citron, a citron, , And preferably 0.01 to 0.1% by weight based on the total weight of the composition. The natural essential oils thus prepared are known to provide an aromatherapy effect and are also effective in water supply, pore size reduction, alleviation of keratin and wrinkles, and inhibition of pigment deposition.

On the other hand, in the composition according to the present disclosure, specifically, the moisturizing agent is more effective than the hyaluronic acid used in the prior art moisturizing agent, and has an advantage of being environmentally friendly, having little side effects, It is preferable to use gamma-polyglutamic acid extracted from soybeans. The gamma-polyglutamic acid penetrates the skin layer of the skin to inhibit the activity of the hyaluronic acid degrading enzyme in the skin tissue, maintains the concentration of the hyaluronic acid constantly, plays a role of making the skin healthy, Inflammation and necrosis.

Specifically, in the composition of the present disclosure, the gamma-polyglutamic acid is preferably 0.05 to 0.5% by weight based on the total weight of the skin moisturizing mist composition.

The cosmetic spray device according to the composition disclosed herein may further include vegetable extracts, vegetable oils, preservatives, additives, etc. in addition to the above-mentioned hydrogenated water, ozone, natural essential oil and gamma-polyglutamic acid, It can be manufactured into any type of formulation conventionally manufactured in the art according to the control. For example, various types of cosmetics such as cream type, lotion type, emulsion type and skin type can be manufactured.

For example, in the case of producing a mist type cosmetic for use in a cosmetic spray device, it is preferable to use an aqueous solution containing 90 to 98% by weight of hydrogen peroxide, 5 to 300 μg / ml of ozone (B) of mixing and homogenizing the natural essential oil, 0.01 to 0.1 wt.% Of gamma-polyglutamic acid, 0.05 to 0.5 wt.% Of gamma-polyglutamic acid and 0.1 to 2 wt.% Of vegetable extract, It can be applied to spray devices.

The plant extract may contain various extracting methods known in the art to provide moisture and nutrition to the skin, as well as to prevent aging of the skin and to produce extracts of plants and the like which are effective for improvement. For example, it can reduce the pores, moisturize and soothe the position of the hosel leaves, moisturize the skin, relieve the irritation and golden roots that are effective in sedation, prevent the dryness of the skin, The present invention may contain one or more kinds of plants, fruits and herbal extracts or oils which are well known to be effective in the art besides goat's ginseng containing a large amount of ginsenoside showing good effects on moisturizing, 2% by weight, and the like.

The herb extract may include at least one selected from the group consisting of lavender extract, rosemary extract, sunflower extract, borage extract, sage extract, jasmine extract and kemomilla extract.

The additive may be prepared by dissolving the following components in an alkaline ionized water having a pH of 3 to 9 as a solvent. Examples of the additive include peptides, acetylhexapeptide-8, dipeptide diaminobutyroylbenzyl, amide diacetate, dipeptide Thianobutyryl benzyl amide diacetate, sodium hyaluronate, coco betaine, dipropylene glycol, butylene glycol, disodium dithia, polysorbate, panthenol, caprylic glycol, Lecosyltrehalose, hydrogenated tachydyrrolesate, glucamate, dimethicone, disodium laureth sulfosuccinate, glycerin, polyquaternium-10, phage-100 stearate, collagen, ethylcellulose, betaglucan And may include one or more selected ones.

On the other hand, the composition for skin moisturizing mist of the present disclosure may further comprise components commonly used in the technical field to which this disclosure belongs. For example, liposomes composed of lipo DPG (dipotassium glycyrrhizate), EDTA-2Na, amino coat, 1,3-butylene glycol, glycerin, HCO-60 hydrogenated castor oil, ethanol, And at least one selected from the group consisting of

Hereinafter, the present disclosure relates to a cosmetic spray device (hereinafter referred to as a mist device) including a mist composition for skin moisturizing, and the mist is a cosmetic material in which cosmetic water is sprayed more finely than spray. The general mist is used for moisture and nutrient supply, whereas the skin moisturizing mist composition of the present invention transmits moisture and nutrients to the skin, and at the same time, the active ingredient effective for removing active oxygen, which is an important external factor of skin aging And is characterized by being a new concept skin moisturizing mist composition capable of preventing and improving aging and additionally exhibiting an aromatherapy effect.

Test Example  1: antioxidant effect

Based on the total weight of the composition, 90 to 98% by weight of hydrogen peroxide, 5 to 300 μg / ml of ozone, 0.01 to 0.1% by weight of natural essential oil, 0.05 to 0.5% by weight of gamma-polyglutamic acid %, And 0.1 to 2% by weight of a vegetable extract were blended and homogenized and mixed with an additive (B) to prepare a mist type cosmetic product, and a DPPH radical scavenging experiment was conducted. This test method can test the direct action of antioxidant effect by testing the scavenging ability of 1,1-Diphenyl-2-picryhydrazyl (DPPH, Sigma D9132-1G) on free radicals generated on ethanol. Compound DPPH produced free radicals in ethanol, and it was mixed with a certain concentration of extract to determine the amount of free radicals to be reduced to some extent. Specifically, 0.5 ml of a 0.1 mM DPPH solution and 0.4 ml of a skin moisturizing mist composition diluted to a predetermined concentration were added to 0.4 ml of ethanol. After vortexing for 10 seconds, the reaction was allowed to proceed for 30 minutes in a dark place. The absorbance was measured at 517 nm using an ELISA. The degree of antioxidant activity was expressed as a percentage based on the absorbance of the control group using ethanol. The resulting free radical scavenging ability was calculated by the following equation (1).

A: absorbance of the control well without treatment of the composition sample

B: absorbance of the experimental group well treated with the composition sample

Control group Experimental group Free radical scavenging ability (%) 95.4 92.5

As shown in the results of Table 1 above, it can be seen that free radical scavenging was observed in the experimental group treated with the composition sample.

Test Example  2: Moisturizing effect

Based on the total weight of the composition, 90 to 98% by weight of hydrogen peroxide, 5 to 300 μg / ml of ozone, 0.01 to 0.1% by weight of natural essential oil, 0.05 to 0.5% by weight of gamma-polyglutamic acid (B) mixed and homogenized with 0.1 to 2% by weight of a vegetable extract and mixed with an additive (B). The cosmetic spray device manufactured by applying the mist type cosmetic was applied to dry the skin, or 20 , And the moisture content of the test site was measured again after 30 minutes, 1 hour and 2 hours in the constant temperature and humidity chamber to test the moisturizing effect. Specifically, 20 applicants were tested. Before 30 minutes, 1 hour, and 2 hours after application and before application, the volunteers' skin moisture content increase rate %) Were measured. The results are shown in Table 2.

Before application 30 minutes 1 hours 2 hours Control group 25.3 25.25 25.23 25.2 Experimental group 24.8 52.7 47.7 45.6

As shown in the results of Table 2 above, it can be seen that the moisture content of the experimental group to which the cosmetic spray device was applied was increased as compared with the control group to which the cosmetic spray device was not applied.

The foregoing has outlined rather broadly the features and technical advantages of the present disclosure in order that the claims of the invention to be described below may be better understood. Those skilled in the art will appreciate that the present disclosure can be embodied in other specific forms without departing from the spirit or essential characteristics thereof. Therefore, it is to be understood that the present invention is not limited to the above-described specific example, and various changes and modifications may be made by those skilled in the art without departing from the scope of the present invention. The present invention is not limited to the embodiment of Figs. The scope of the present disclosure is defined by the appended claims rather than the foregoing detailed description, and all changes or modifications derived from the appended claims and their equivalents shall be construed as being included within the scope of the present disclosure.

Claims (6)

Water, ozone dissolved in oil, natural essential oil and gamma-polyglutamic acid,
Wherein the natural essential oil comprises at least one member selected from the group consisting of a country of origin, citron, guinea-pig mugwort, dog mugwort, and ginseng.
The method according to claim 1,
Characterized by further comprising a vegetable extract,
The plant extracts include one or more species selected from the group consisting of Huzel leaves, golden roots,
Wherein the herbal extract comprises at least one selected from the group consisting of lavender extract, rosemary extract, sunflower extract, borage extract, sage extract, jasmine extract and kemomilla extract.
The present invention relates to a method for producing a mist-removing composition for skin moisturizing, which contains hydrogenated water, dissolved ozone in oil, natural essential oil and gamma-polyglutamic acid.
(a) preparing the hydrogenated water;
(b) producing ozone dissolved in the oil; And
(c) mixing the aqueous hydrogen peroxide produced in the steps (a) and (b) with ozone dissolved in the oil, and extracted natural essential oil, gamma-polyglutamic acid and vegetable extract. A method for producing a mist composition for moisturizing.
The method of claim 3,
The step of producing the hydrogenated water comprises:
(T1) combining AC or DC inversion and selecting one of them;
(T2) electrolysis through a selected electricity for electrolysis; And
(T3) electrolysis to obtain said hydrogenated water,
The electricity for electrolysis
(1) a method in which direct current is inverted at an arbitrary cycle;
(2) a method of using high frequency alternating current;
(3) a method in which DC or DC inversion and AC electricity are simultaneously used in the same electrolysis tank;
(4) a method in which DC or DC inversion and AC electricity are alternately used in the same electrolysis tank; And
(5) By using one of a plurality of electrolytic tanks and a method of separately using a direct current or direct current inversion electrolytic tank and an alternating electrolytic tank separately, the voltage or inversion period can be widely varied to increase the efficiency of electrolysis, Wherein the concentration of active hydrogens is higher than that of the active ingredient.
The method of claim 3,
The step of producing dissolved ozone in the oil comprises:
(S1) generating ozone using an ozone generator through a plasma, a high-voltage discharge, a corona discharge, and a UV method;
(S2) bubbling the ozone generated in the step S1 in the oil at a low temperature until the ozone dissolved amount in the oil becomes 400 to 1,100 meq / kg peroxide; And
(S3) After the primary bubble ejection in step S2, the bubbling temperature is increased to change the viscosity of the oil, and then the bubbling temperature is decreased until the amount of ozone dissolved in the oil becomes 1400 to 2900 meq / kg of peroxide And discharging secondary bubbles,
The oil contains an unsaturated fatty acid, and the ozone reacts with the double bond structure between the carbon atoms of the unsaturated fatty acid to generate an ozonized oil,
Wherein the unsaturated fatty acid is oleic acid, palmitoleic acid, linoleic acid, or arachidonic acid.
A cosmetic spraying device characterized by comprising the skin moisturizing mist composition of claim 1 or 2.

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