CN114946321A - Pelleting formula for isatis tinctoria seeds and preparation method thereof - Google Patents
Pelleting formula for isatis tinctoria seeds and preparation method thereof Download PDFInfo
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- CN114946321A CN114946321A CN202210643483.1A CN202210643483A CN114946321A CN 114946321 A CN114946321 A CN 114946321A CN 202210643483 A CN202210643483 A CN 202210643483A CN 114946321 A CN114946321 A CN 114946321A
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- seeds
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- isatis tinctoria
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- 238000002360 preparation method Methods 0.000 title claims abstract description 17
- 241000334154 Isatis tinctoria Species 0.000 title claims description 29
- 239000000853 adhesive Substances 0.000 claims abstract description 22
- 230000001070 adhesive effect Effects 0.000 claims abstract description 22
- 239000008188 pellet Substances 0.000 claims abstract description 18
- 239000000654 additive Substances 0.000 claims abstract description 16
- 230000000996 additive effect Effects 0.000 claims abstract description 16
- 238000011049 filling Methods 0.000 claims abstract description 15
- 229920002472 Starch Polymers 0.000 claims abstract description 14
- 239000008107 starch Substances 0.000 claims abstract description 14
- 235000019698 starch Nutrition 0.000 claims abstract description 14
- 108010020346 Polyglutamic Acid Proteins 0.000 claims abstract description 12
- 229920002643 polyglutamic acid Polymers 0.000 claims abstract description 12
- 241000219000 Populus Species 0.000 claims abstract description 11
- 239000000440 bentonite Substances 0.000 claims abstract description 11
- 229910000278 bentonite Inorganic materials 0.000 claims abstract description 11
- SVPXDRXYRYOSEX-UHFFFAOYSA-N bentoquatam Chemical compound O.O=[Si]=O.O=[Al]O[Al]=O SVPXDRXYRYOSEX-UHFFFAOYSA-N 0.000 claims abstract description 11
- 239000000843 powder Substances 0.000 claims abstract description 11
- 239000011248 coating agent Substances 0.000 claims abstract description 10
- 238000000576 coating method Methods 0.000 claims abstract description 10
- 229920002134 Carboxymethyl cellulose Polymers 0.000 claims abstract description 9
- 239000001768 carboxy methyl cellulose Substances 0.000 claims abstract description 9
- 235000010948 carboxy methyl cellulose Nutrition 0.000 claims abstract description 9
- 239000008112 carboxymethyl-cellulose Substances 0.000 claims abstract description 9
- 229920000591 gum Polymers 0.000 claims abstract description 9
- 125000005270 trialkylamine group Chemical group 0.000 claims abstract description 9
- 244000005700 microbiome Species 0.000 claims abstract description 7
- 239000003086 colorant Substances 0.000 claims abstract description 5
- 239000003999 initiator Substances 0.000 claims abstract description 5
- 239000000575 pesticide Substances 0.000 claims abstract description 5
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 4
- FPAFDBFIGPHWGO-UHFFFAOYSA-N dioxosilane;oxomagnesium;hydrate Chemical compound O.[Mg]=O.[Mg]=O.[Mg]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O FPAFDBFIGPHWGO-UHFFFAOYSA-N 0.000 claims abstract description 4
- 239000006187 pill Substances 0.000 claims description 48
- 238000000034 method Methods 0.000 claims description 17
- 239000000463 material Substances 0.000 claims description 16
- 238000012216 screening Methods 0.000 claims description 16
- 239000000203 mixture Substances 0.000 claims description 15
- 239000005900 Flonicamid Substances 0.000 claims description 12
- RLQJEEJISHYWON-UHFFFAOYSA-N flonicamid Chemical compound FC(F)(F)C1=CC=NC=C1C(=O)NCC#N RLQJEEJISHYWON-UHFFFAOYSA-N 0.000 claims description 12
- 230000005484 gravity Effects 0.000 claims description 8
- 238000004806 packaging method and process Methods 0.000 claims description 8
- 238000005498 polishing Methods 0.000 claims description 8
- 239000004576 sand Substances 0.000 claims description 8
- 238000005507 spraying Methods 0.000 claims description 8
- 230000001954 sterilising effect Effects 0.000 claims description 8
- 239000005886 Chlorantraniliprole Substances 0.000 claims description 7
- PSOVNZZNOMJUBI-UHFFFAOYSA-N chlorantraniliprole Chemical compound CNC(=O)C1=CC(Cl)=CC(C)=C1NC(=O)C1=CC(Br)=NN1C1=NC=CC=C1Cl PSOVNZZNOMJUBI-UHFFFAOYSA-N 0.000 claims description 7
- 238000009472 formulation Methods 0.000 claims description 7
- 238000005453 pelletization Methods 0.000 claims description 6
- 238000004659 sterilization and disinfection Methods 0.000 claims description 6
- 235000009328 Amaranthus caudatus Nutrition 0.000 claims description 5
- 240000001592 Amaranthus caudatus Species 0.000 claims description 5
- 235000012735 amaranth Nutrition 0.000 claims description 5
- 239000004178 amaranth Substances 0.000 claims description 5
- 239000000975 dye Substances 0.000 claims description 4
- 238000004519 manufacturing process Methods 0.000 claims description 4
- 238000002791 soaking Methods 0.000 claims description 4
- 235000005979 Citrus limon Nutrition 0.000 claims description 3
- 244000131522 Citrus pyriformis Species 0.000 claims description 3
- 235000000177 Indigofera tinctoria Nutrition 0.000 claims description 3
- 239000005941 Thiamethoxam Substances 0.000 claims description 3
- IINNWAYUJNWZRM-UHFFFAOYSA-L erythrosin B Chemical compound [Na+].[Na+].[O-]C(=O)C1=CC=CC=C1C1=C2C=C(I)C(=O)C(I)=C2OC2=C(I)C([O-])=C(I)C=C21 IINNWAYUJNWZRM-UHFFFAOYSA-L 0.000 claims description 3
- 235000012732 erythrosine Nutrition 0.000 claims description 3
- 239000004174 erythrosine Substances 0.000 claims description 3
- 229940011411 erythrosine Drugs 0.000 claims description 3
- 229940097275 indigo Drugs 0.000 claims description 3
- COHYTHOBJLSHDF-UHFFFAOYSA-N indigo powder Natural products N1C2=CC=CC=C2C(=O)C1=C1C(=O)C2=CC=CC=C2N1 COHYTHOBJLSHDF-UHFFFAOYSA-N 0.000 claims description 3
- NWWZPOKUUAIXIW-FLIBITNWSA-N thiamethoxam Chemical compound [O-][N+](=O)\N=C/1N(C)COCN\1CC1=CN=C(Cl)S1 NWWZPOKUUAIXIW-FLIBITNWSA-N 0.000 claims description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 3
- 235000012756 tartrazine Nutrition 0.000 claims description 2
- 239000004149 tartrazine Substances 0.000 claims description 2
- UJMBCXLDXJUMFB-GLCFPVLVSA-K tartrazine Chemical compound [Na+].[Na+].[Na+].[O-]C(=O)C1=NN(C=2C=CC(=CC=2)S([O-])(=O)=O)C(=O)C1\N=N\C1=CC=C(S([O-])(=O)=O)C=C1 UJMBCXLDXJUMFB-GLCFPVLVSA-K 0.000 claims description 2
- 229960000943 tartrazine Drugs 0.000 claims description 2
- 230000000694 effects Effects 0.000 abstract description 12
- 238000009331 sowing Methods 0.000 abstract description 5
- 241000334160 Isatis Species 0.000 abstract description 3
- 230000007226 seed germination Effects 0.000 abstract description 2
- 239000000126 substance Substances 0.000 abstract 2
- 241000976416 Isatis tinctoria subsp. canescens Species 0.000 abstract 1
- 238000010899 nucleation Methods 0.000 description 5
- 230000008569 process Effects 0.000 description 4
- 241000196324 Embryophyta Species 0.000 description 3
- 238000004040 coloring Methods 0.000 description 3
- 230000035784 germination Effects 0.000 description 3
- 230000012010 growth Effects 0.000 description 3
- 239000004480 active ingredient Substances 0.000 description 2
- 239000013543 active substance Substances 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 2
- 239000002917 insecticide Substances 0.000 description 2
- 235000015097 nutrients Nutrition 0.000 description 2
- 235000016068 Berberis vulgaris Nutrition 0.000 description 1
- 241000335053 Beta vulgaris Species 0.000 description 1
- 241000219193 Brassicaceae Species 0.000 description 1
- 241000238631 Hexapoda Species 0.000 description 1
- 244000061176 Nicotiana tabacum Species 0.000 description 1
- 235000002637 Nicotiana tabacum Nutrition 0.000 description 1
- 241000607479 Yersinia pestis Species 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 239000011149 active material Substances 0.000 description 1
- 230000004075 alteration Effects 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 239000003899 bactericide agent Substances 0.000 description 1
- 239000011230 binding agent Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 230000003111 delayed effect Effects 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 239000003337 fertilizer Substances 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000005648 plant growth regulator Substances 0.000 description 1
- 239000002689 soil Substances 0.000 description 1
- 239000010902 straw Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 230000004083 survival effect Effects 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01C—PLANTING; SOWING; FERTILISING
- A01C1/00—Apparatus, or methods of use thereof, for testing or treating seed, roots, or the like, prior to sowing or planting
- A01C1/06—Coating or dressing seed
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01C—PLANTING; SOWING; FERTILISING
- A01C1/00—Apparatus, or methods of use thereof, for testing or treating seed, roots, or the like, prior to sowing or planting
- A01C1/08—Immunising seed
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/34—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom
- A01N43/40—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom six-membered rings
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/48—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with two nitrogen atoms as the only ring hetero atoms
- A01N43/56—1,2-Diazoles; Hydrogenated 1,2-diazoles
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N51/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds having the sequences of atoms O—N—S, X—O—S, N—N—S, O—N—N or O-halogen, regardless of the number of bonds each atom has and with no atom of these sequences forming part of a heterocyclic ring
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01P—BIOCIDAL, PEST REPELLANT, PEST ATTRACTANT OR PLANT GROWTH REGULATORY ACTIVITY OF CHEMICAL COMPOUNDS OR PREPARATIONS
- A01P7/00—Arthropodicides
- A01P7/04—Insecticides
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Environmental Sciences (AREA)
- Wood Science & Technology (AREA)
- Pest Control & Pesticides (AREA)
- Plant Pathology (AREA)
- Engineering & Computer Science (AREA)
- Zoology (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Dentistry (AREA)
- Agronomy & Crop Science (AREA)
- Soil Sciences (AREA)
- Insects & Arthropods (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Pretreatment Of Seeds And Plants (AREA)
Abstract
The invention discloses a pelleting formula for isatis tinctoria seeds and a preparation method thereof, wherein the pelleting formula comprises an adhesive, an initiator, an inert filling substance, an additive, a pesticide and a coloring agent, the adhesive is carboxymethyl cellulose, starch and gum, the initiator is one or more of trialkylamine, trialkylphosphine and alcohol, the inert filling substance is one or more of pure poplar powder, talcum powder and bentonite, and the additive is a biological colony, a super halophilic microorganism and a polyglutamic acid solution. The invention utilizes the matching of adhesives with different types and proportions to enhance the adhesiveness of the coating to the seed pellets, improves the seed quality and activity, solves the problems of small woad seeds, difficult sowing, large sowing quantity, time and labor consumption, ensures that the preparation method is simple and convenient, solves the problem of poor adhesion effect or difficult disintegration caused by poor effect of the adhesive in the traditional seed pelleting, and achieves the effect of improving the seed germination rate.
Description
Technical Field
The invention relates to the technical field of agriculture, in particular to a pelleting formula for isatis tinctoria seeds and a preparation method thereof.
Background
The seed pelleting is to utilize an adhesive to adhere pesticides, bactericides, fertilizers, plant growth regulators, fillers and the like on the surface of seeds and process the seeds into spherical single seeds without obvious difference in size and shape. The method is mainly used for small-sized seeds of vegetables, rapes, tobaccos, beet and the like. The pelleted seeds have regular shapes and consistent sizes, mechanical precision seeding is easier to realize, and one or two seeds in one hole are thoroughly realized. After the seed pelleting treatment, the seeding of the seed tape with the nutrient and the pesticide is realized, the seedling survival rate is high, the growth is robust, and the occurrence of plant diseases and insect pests can be effectively reduced; a "dead" micro-active material pool is formed around the seed. The seeded pelleting agent absorbs water to expand and form cracks, and the active ingredients are slowly contacted with seeds and surrounding soil through the cracks, so that the active ingredients can better participate in the growth process of the plants in the seedling stage. Because the release of the active substance is a slow process, the active substance cannot be greatly lost in a short time due to leaching or dissolving action, and the toxic action cannot be formed due to instant accumulation of pesticide and nutrient.
Isatis indigotica (Isatis indigotica) is a plant of Isatis indigotica of Cruciferae, dry roots and leaves are used as medicines, and the Isatis indigotica and Isatis indigotica are respectively called as Isatis root and dyers woad leaf, and are traditional bulk medicinal materials in China, and have the effects of dispelling wind, dissipating heat, clearing heat and removing toxicity.
Disclosure of Invention
The invention aims to provide a pelleting formula for isatis tinctoria seeds and a preparation method thereof, which have the effects of good bonding effect and high disintegration speed, and solve the problems of seedling shortage, ridge breaking, excessive single-hole seeding quantity and the like, reduced yield and commodity performance, delayed emergence of seedlings, irregularity and the like caused by the fact that a seeder is easily blocked during seeding due to the fact that a large amount of cluster straws are accompanied during seeding, and the multifunctional compound pelleting formula is to be developed and is more suitable for pelleting isatis tinctoria seeds.
To achieve the above object, the present invention provides a pelletization formulation for isatis tinctoria seeds, comprising: the adhesive comprises carboxymethyl cellulose, starch and gum, the initiator is one or more of trialkylamine, trialkylphosphine and alcohol, the inert filling material is one or more of pure poplar powder, talcum powder and bentonite, the additive is one or more of biological colony, super halophilic microorganism and polyglutamic acid solution, the insecticide is one or more of thiamethoxam, flonicamid and chlorantraniliprole, the amount of the carboxymethyl cellulose, the starch and the gum in the adhesive is 8.2-9.4 g, 5.2-6.8 g and 7.2-8.8 g, the amount of the biological colony, the super halophilic microorganism and the polyglutamic acid solution in the additive is 8 parts, 10 parts and 6 parts, and the seed: starch: trialkylamine: poplar powder: bentonite: polyglutamic acid solution: the usage ratio of flonicamid is 1: 3-5: 2-4: 4-5: 3-6: 3-4: 4-5.
Optionally, the colorant is amaranth, erythrosine, tartrazine and indigo.
Optionally, the inert filling materials are pure poplar wood powder with the granularity of 140 meshes and bentonite with the granularity of 120 meshes.
Optionally, the use amount of the carboxymethyl cellulose, the starch and the gum in the adhesive is 8.4-9.2 g, 5.6-6.2 g and 7.8-8.2 g.
Optionally, the mass ratio of the seeds to the coloring agent is 1: 1.2-2.6; the concentration of amaranth is 80 mg/L; the concentration of lemon yellow is 100 mg/L.
Optionally, the seed: starch: trialkylamine: poplar powder: bentonite: polyglutamic acid solution: the usage ratio of flonicamid is 1:3.8:2.8:4.2:3.6:3.2: 4.2.
The invention provides a preparation method which comprises the following steps: a method for preparing isatis tinctoria seeds in a pelleting mode comprises the following steps:
s1, selecting full seeds as basic seeds, polishing, winnowing and specific gravity concentration;
s2, purifying and selecting the seeds to be pelletized, and removing sand grains, stones or foreign crop seeds possibly doped in the seeds;
s3, sterilizing the purified seeds to be pelletized, wherein the sterilized seeds comprise the following components in parts by weight: adding adhesive and additive in the ratio of 6:2 to uniformly adhere the mixture to the surface of the seeds;
s4, putting a certain amount of seeds into a pelleting coating machine with the rotating speed of 120rpm, adding an inert filling material while rotating, and performing the operation once every 120 seconds;
s5, after the seeds form pills, screening the pills by using a vibration screening device with a specific screen hole, separating the pills with different sizes, and continuously pelleting the smaller pills, wherein the qualified pills enter the next procedure;
s6, spraying different dyes on the surface of the moving pill to color;
s7, putting the colored pellets into a dryer to be baked for 2-7h and observing whether the moisture content reaches the specified moisture content;
and S8, packaging the dried and colored pellets and warehousing.
Optionally, in the seed disinfection process, the disinfection solution may be prepared by soaking flonicamid and chlorantraniliprole.
Optionally, the ratio of the flonicamid to the chlorantraniliprole to the seeds is 1:2:300, the soaking time is set to be 2-3 hours, and the seeds are washed with clean water and dried after being soaked to complete disinfection.
Compared with the prior art, the invention has the following beneficial effects:
according to the method, the adhesion of the coating to the seed pellets is enhanced by utilizing the matching of the adhesives with different types and proportions, the seed quality and the activity are improved, the problems of small woad seeds, difficult sowing, large sowing amount, time and labor consumption are solved, the method is more beneficial to field production and mechanical precision sowing, the seed consumption is greatly reduced, the production cost is reduced, the used materials are environment-friendly, economical and safe, the seeds subjected to pelleting germination are neat and have high germination rate, the germination accelerating effect is achieved, and the growth index and the quality are greatly improved.
The preparation method is simple and convenient, solves the problem of poor bonding effect or difficult disintegration caused by poor bonding effect of the traditional seed pelleting adhesive, and achieves the effect of improving the seed germination rate.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
The invention provides a pelleting formula for isatis tinctoria seeds, which comprises the following components in part by weight: the adhesive comprises carboxymethyl cellulose, starch and gum, the initiator is one or more of trialkylamine, trialkylphosphine and alcohol, the inert filling material is one or more of pure poplar powder, talcum powder and bentonite, the additive is one or more of biological colony, super halophilic microorganism and polyglutamic acid solution, the insecticide is one or more of thiamethoxam, flonicamid and chlorantraniliprole, the amount of the carboxymethyl cellulose, the starch and the gum in the adhesive is 8.2-9.4 g, 5.2-6.8 g and 7.2-8.8 g, the amount of the biological colony, the super halophilic microorganism and the polyglutamic acid solution in the additive is 8 parts, 10 parts and 6 parts, and the seed: starch: trialkylamine: poplar powder: bentonite: polyglutamic acid solution: the usage ratio of flonicamid is 1: 3-5: 2-4: 4-5: 3-6: 3-4: 4-5.
Example 1
The invention provides a pelleting preparation method of isatis tinctoria seeds, which comprises the following steps:
s1, selecting full seeds as basic seeds, polishing, winnowing and specific gravity concentration;
s2, purifying and selecting the seeds to be pelletized, and removing sand grains, stones or foreign crop seeds possibly doped in the seeds;
s3, sterilizing the purified seeds to be pelletized, wherein the sterilized seeds comprise the following components in parts by weight: adding adhesive and additive in the ratio of 6:2 to uniformly adhere the mixture to the surface of the seeds;
s4, putting a certain amount of seeds into a pelleting coating machine with the rotating speed of 120rpm, adding an inert filling material while rotating, and performing the operation once every 120 seconds;
s5, after the seeds form pills, screening the pills by using a vibration screening device with a specific screen hole, separating the pills with different sizes, and continuously pelleting the smaller pills, wherein the qualified pills enter the next procedure;
s6, spraying different dyes on the surface of the moving pill to color;
s7, putting the colored pellets into a dryer to be baked for 2 hours and observing whether the moisture content reaches the specified moisture content;
and S8, packaging the dried and colored pellets and warehousing.
Example 2
The invention provides a preparation method which comprises the following steps: a pelleting preparation method of isatis tinctoria seeds comprises the following steps:
s1, selecting full seeds as basic seeds, polishing, winnowing and specific gravity concentration;
s2, purifying and selecting the seeds to be pelletized, and removing sand grains, stones or foreign crop seeds possibly doped in the seeds;
s3, sterilizing the purified seeds to be pelletized, wherein the sterilized seeds comprise the following components in parts by weight of 1: adding a binder and an additive in a ratio of 3:1, and uniformly adhering the mixture to the surface of the seeds;
s4, putting a certain amount of seeds into a pelleting coating machine with the rotating speed of 100rpm, adding an inert filling material while rotating, and performing the operation once every 80 seconds;
s5, after the seeds form pills, screening the pills by using a vibration screening device with a specific screen hole, separating the pills with different sizes, and continuously pelleting the smaller pills, wherein the qualified pills enter the next procedure;
s6, spraying amaranth on the surface of the moving pill for coloring;
s7, putting the colored pellets into a dryer to be baked for 3 hours and observing whether the moisture content reaches the specified moisture content;
and S8, packaging the dried and colored pellets and warehousing.
Example 3
The invention provides a preparation method which comprises the following steps: a pelleting preparation method of isatis tinctoria seeds comprises the following steps:
s1, selecting full seeds as basic seeds, polishing, winnowing and specific gravity concentration;
s2, purifying and selecting the seeds to be pelletized, and removing sand grains, stones or foreign crop seeds possibly doped in the seeds;
s3, sterilizing the purified seeds to be pelletized, wherein the sterilized seeds comprise the following components in parts by weight: adding adhesive and additive in a ratio of 9:3 to uniformly adhere the mixture to the surface of the seeds;
s4, putting a certain amount of seeds into a pelleting coating machine with the rotating speed of 140rpm, adding an inert filling material while rotating, and carrying out the operation once every 100 seconds;
s5, after the seeds form pills, screening the pills by using a vibration screening device with a specific screen hole, separating the pills with different sizes, and continuously pelleting the smaller pills, wherein the qualified pills enter the next procedure;
s6, spraying erythrosine on the surface of the moving pill for coloring;
s7, putting the colored pellets into a dryer to be baked for 4 hours and observing whether the moisture content reaches the specified moisture content;
and S8, packaging the dried and colored pellets and warehousing.
Example 4
The invention provides a technical scheme that: a pelleting preparation method of isatis tinctoria seeds comprises the following steps:
s1, selecting full seeds as basic seeds, polishing, winnowing and specific gravity concentration;
s2, purifying and selecting the seeds to be pelletized, and removing sand grains, stones or foreign crop seeds possibly doped in the seeds;
s3, sterilizing the purified seeds to be pelletized, wherein the sterilized seeds comprise the following components in parts by weight: adding adhesive and additive in the ratio of 12:4 to make the mixture uniformly adhered on the surface of the seeds;
s4, putting a certain amount of seeds into a pelleting coating machine with the rotating speed of 160rpm, adding an inert filling material while rotating, and carrying out the operation once every 140 seconds;
s5, after the seeds form pills, screening the pills by using a vibration screening device with a specific screen hole, separating the pills with different sizes, and continuously pelleting the smaller pills, wherein the qualified pills enter the next procedure;
s6, spraying lemon yellow on the surface of the moving pill to color;
s7, putting the colored pellets into a dryer to be baked for 5 hours and observing whether the moisture content reaches the specified moisture content;
and S8, packaging the dried and colored pellets and warehousing.
Example 5
The invention provides a technical scheme that: a pelleting preparation method of isatis tinctoria seeds comprises the following steps:
s1, selecting full seeds as basic seeds, polishing, winnowing and specific gravity concentration;
s2, purifying and selecting the seeds to be pelletized, and removing sand grains, stones or foreign crop seeds possibly doped in the seeds;
s3, sterilizing the purified seeds to be pelletized, wherein the sterilized seeds comprise the following components in parts by weight: adding adhesive and additive in the ratio of 14:5 to make the mixture uniformly adhere to the surface of the seeds;
s4, putting a certain amount of seeds into a pelleting coating machine with the rotating speed of 120rpm, adding an inert filling material while rotating, and performing the operation once every 120 seconds;
s5, after the seeds form pills, screening the pills by using a vibration screening device with a specific screen hole, separating the pills with different sizes, and continuously pelleting the smaller pills, wherein the qualified pills enter the next procedure;
s6, spraying indigo on the surface of the moving pill grains for coloring;
s7, putting the colored pellets into a dryer to be baked for 6 hours and observing whether the moisture content reaches the specified moisture content;
and S8, packaging the dried and colored pellets and warehousing.
Example 6
The invention provides a technical scheme that: a pelleting preparation method of isatis tinctoria seeds comprises the following steps:
s1, selecting full seeds as basic seeds, polishing, winnowing and specific gravity concentration;
s2, purifying and selecting the seeds to be pelletized, and removing sand grains, stones or foreign crop seeds possibly doped in the seeds;
s3, sterilizing the purified seeds to be pelletized, wherein the sterilized seeds comprise the following components in parts by weight: adding adhesive and additive in the ratio of 6:2 to uniformly adhere the mixture to the surface of the seeds;
s4, putting a certain amount of seeds into a pelleting coating machine with the rotating speed of 120rpm, adding an inert filling material while rotating, and performing the operation once every 100 seconds;
s5, after the seeds form pills, screening the pills by using a vibration screening device with a specific screen hole, separating the pills with different sizes, and continuously pelleting the smaller pills, wherein the qualified pills enter the next procedure;
s6, spraying different dyes on the surface of the moving pill to color;
s7, putting the colored pellets into a dryer to be baked for 7 hours and observing whether the moisture content reaches the specified moisture content;
and S8, packaging the dried and colored pellets and warehousing.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (9)
1. A pelleted formulation for isatis tinctoria seeds comprising: the adhesive is carboxymethyl cellulose, starch and gum, the initiator is one or more of trialkylamine, trialkylphosphine and alcohol, and the inert filling material is one or more of pure poplar powder, talcum powder and bentonite;
the additive is a biological colony, a super halophilic microorganism and a polyglutamic acid solution, the pesticide is one or more of thiamethoxam, flonicamid and chlorantraniliprole, the usage amount of carboxymethyl cellulose, starch and gum in the adhesive is 8.2-9.4 g, 5.2-6.8 g and 7.2-8.8 g, the usage amount of the biological colony, the super halophilic microorganism and the polyglutamic acid solution in the additive is 8 parts, 10 parts and 6 parts, and the seed: starch: trialkylamine: poplar powder: bentonite: polyglutamic acid solution: the usage ratio of flonicamid is 1: 3-5: 2-4: 4-5: 3-6: 3-4: 4-5.
2. A pelletization formulation for isatis tinctoria seeds according to claim 1, characterized in that: the colorant is amaranth, erythrosine, tartrazine and indigo.
3. A pelletization formulation for isatis tinctoria seeds according to claim 1, characterized in that: the inert filling materials are pure poplar powder with the granularity of 140 meshes and bentonite with the granularity of 120 meshes.
4. A pelletization formulation for isatis tinctoria seeds according to claim 1, characterized in that: the use amount of the carboxymethyl cellulose, the starch and the gum in the adhesive is 8.4-9.2 g, 5.6-6.2 g and 7.8-8.2 g.
5. A pelletization formulation for isatis tinctoria seeds according to claim 1, characterized in that: the mass ratio of the seeds to the coloring agent is 1: 1.2-2.6; the concentration of amaranth is 80 mg/L; the concentration of lemon yellow is 100 mg/L.
6. A pelletization formulation for isatis tinctoria seeds according to claim 1, characterized in that: the seed: starch: trialkylamine: poplar powder: bentonite: polyglutamic acid solution: the usage ratio of flonicamid is 1:3.8:2.8:4.2:3.6:3.2: 4.2.
7. A pelleting preparation method of isatis tinctoria seeds is characterized by comprising the following steps:
s1, selecting full seeds as basic seeds, polishing, winnowing and specific gravity concentration;
s2, purifying and selecting the seeds to be pelletized, and removing sand grains, stones or foreign crop seeds possibly doped in the seeds;
s3, sterilizing the purified seeds to be pelletized, wherein the sterilized seeds comprise the following components in parts by weight: adding adhesive and additive in the ratio of 6:2 to uniformly adhere the mixture to the surface of the seeds;
s4, putting a certain amount of seeds into a pelleting coating machine with the rotating speed of 120rpm, adding an inert filling material while rotating, and performing the operation once every 120 seconds;
s5, after the seeds form pills, screening the pills by using a vibration screening device with a specific screen hole, separating the pills with different sizes, and continuously pelleting the smaller pills, wherein the qualified pills enter the next procedure;
s6, spraying different dyes on the surface of the moving pill to color;
s7, baking the colored pellets in a dryer for 2-7h and observing whether the moisture content reaches the specified moisture content;
and S8, packaging the dried and colored pellets and warehousing.
8. The method for producing Isatis tinctoria seeds according to claim 7, wherein: in the seed disinfection procedure, the materials of the disinfection solution can be soaked by flonicamid and chlorantraniliprole.
9. The method for producing Isatis tinctoria seeds according to claim 7, wherein: the using amount ratio of flonicamid to chlorantraniliprole to seeds is 1:2:300, the soaking time is set to be 2-3 hours, and after soaking, the seeds are cleaned with clear water and dried to finish disinfection.
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