CN114870056B - Antibacterial deodorant and preparation method thereof - Google Patents

Antibacterial deodorant and preparation method thereof Download PDF

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CN114870056B
CN114870056B CN202210610921.4A CN202210610921A CN114870056B CN 114870056 B CN114870056 B CN 114870056B CN 202210610921 A CN202210610921 A CN 202210610921A CN 114870056 B CN114870056 B CN 114870056B
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CN114870056A (en
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吴明
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Zhejiang Weihua Jujiu Technology Co ltd
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    • A61L9/00—Disinfection, sterilisation or deodorisation of air
    • A61L9/01—Deodorant compositions
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
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    • A01N37/40—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a singly bound oxygen or sulfur atom attached to the same carbon skeleton, this oxygen or sulfur atom not being a member of a carboxylic group or of a thio analogue, or of a derivative thereof, e.g. hydroxy-carboxylic acids having at least one oxygen or sulfur atom attached to an aromatic ring system having at least one carboxylic group or a thio analogue, or a derivative thereof, and one oxygen or sulfur atom attached to the same aromatic ring system
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
    • A01N47/08—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having one or more single bonds to nitrogen atoms
    • A01N47/10—Carbamic acid derivatives, i.e. containing the group —O—CO—N<; Thio analogues thereof
    • A01N47/12—Carbamic acid derivatives, i.e. containing the group —O—CO—N<; Thio analogues thereof containing a —O—CO—N< group, or a thio analogue thereof, neither directly attached to a ring nor the nitrogen atom being a member of a heterocyclic ring
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/34—Chemical or biological purification of waste gases
    • B01D53/74—General processes for purification of waste gases; Apparatus or devices specially adapted therefor
    • B01D53/77—Liquid phase processes
    • B01D53/78—Liquid phase processes with gas-liquid contact
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
    • C08G77/60—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule in which all the silicon atoms are connected by linkages other than oxygen atoms
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    • A61L2101/00—Chemical composition of materials used in disinfecting, sterilising or deodorising
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    • A61L2209/00—Aspects relating to disinfection, sterilisation or deodorisation of air
    • A61L2209/20—Method-related aspects
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2257/00—Components to be removed
    • B01D2257/90—Odorous compounds not provided for in groups B01D2257/00 - B01D2257/708
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
    • Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change

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Abstract

The invention relates to the field of macromolecules, in particular to an antibacterial deodorant and a preparation method thereof; the method provides the existing chemical deodorization technology, and generally can not effectively inhibit the reproductive metabolism of bacteria; the antibacterial agent adopted by the invention has strong capability of killing bacteria, broad spectrum, high efficiency, stable chemical property, low toxicity, no stimulation to skin mucosa, good combination with other types of bactericides and no damage to sterilized articles; the sterilization process is rapid, no harmful substance is generated, and no selective sterilization mode exists, so that the bacteria can not generate drug resistance; in addition, the macromolecular silicon-based odor removing agent prepared by carrying out hydrosilylation reaction on 1, 1-iron dimethyl silicon, diallyl dimethyl ammonium chloride and zinc ricinoleate has high temperature resistance and high humidity resistance, is suitable for being used in the south with damp and warm water, and has lasting use effect.

Description

Antibacterial deodorant and preparation method thereof
Technical Field
The invention relates to the field of polymers, in particular to an antibacterial deodorant and a preparation method thereof.
Background
At present, the foot hygiene products on the market are more, and can be generally divided into direct soaking liquid, water-soluble powder, ointment for treating tinea pedis and a pad body placed in a shoe. The commonly used products generally adopt miconazole nitrate as a main raw material, and some products are also prepared into foot care products by adopting Chinese medicinal preparations. These products have the following problems: the foot care product is used for treating foot diseases, is easy to decompose and has short time effect; the use process is complex; can not be treated by shoe materials and socks; the paste must be applied to the affected part; has no function of deodorizing and decomposing foreign odor molecules.
CN200610018259.4: the invention relates to an antibacterial deodorant for shoes and socks, which can effectively kill the growth of bacterial microorganisms in the shoes and socks so as to eliminate the peculiar smell of the shoes and socks. An antibacterial deodorant for shoes and socks comprises the following components in percentage by weight: and (3) chitosan: 0.1-5%, acetic acid: 10-40%, betaine: 0.2-4%, thymol: 0.05-2%, tween-80: 10-40%, essence: 0.1-4%, deionized water: the balance, the sum of all the components is 100 percent. The main raw materials selected by the invention are all from green organisms, and the invention has the characteristics of no toxicity, environmental protection, low cost, good sterilization effect and long effective time.
CN200710017892.6: the invention relates to a preparation method of a biological antibacterial deodorant, which has the advantages of simple manufacturing method, low cost, obvious deodorization and sterilization effects, no toxicity, no corrosion and difficult secondary pollution. The invention is prepared from the following raw materials in parts by weight: one or more of citric acid, malic acid and lactic acid, the content of which is more than or equal to 1 weight part; water, the content of which is less than or equal to 990 weight portions; filtering the above components on a copper mesh, aseptically mixing with water at room temperature, fully dissolving, and standing to obtain the antibacterial deodorant.
CN200910230771.9: the invention discloses a nano composite micro-emulsion type antibacterial deodorant, which comprises the following raw materials of water, hinoki incense, vanillin, aqueous polyurethane resin, span-80 and nano antibacterial powder dispersion liquid, wherein the proportioning relation of the raw materials is as follows: water: 1000ml; hinoki fragrance: 55ml to 125ml; vanillin: 55ml to 125ml; aqueous polyurethane resin: 11.2ml to 12.8ml; span-80: 5.58ml to 6.28ml; nano antibacterial powder dispersion liquid: 40ml to 60ml. Compared with the prior art, the nano composite micro emulsion type antibacterial deodorant has the following functions: 1) The use amount is small, the cost is low, the adhesive force is strong, and no toxic or side effect exists; 2) Has the functions of no decomposition and long-acting sterilization; 3) Has the functions of decomposing foreign odor molecules and releasing fragrance.
The above patents and prior art generally adopt chemical deodorizing techniques, which convert the odor functional group in the odor substance into a non-odor substance by a series of chemical reactions such as acid-base neutralization, oxidation-reduction, etc. between the deodorizing component and the odor molecule; the chemical deodorization technology can decompose and recombine odor molecules, and meanwhile, the deodorization effect is rapid and obvious, so that the technology is a thorough deodorization technology; the disadvantage is that the reproductive metabolism of bacteria is generally not effectively inhibited.
Disclosure of Invention
In order to solve the problems, the invention provides an antibacterial deodorant and a preparation method thereof, and the preparation method comprises the following operation steps:
according to the mass parts, 25-35 parts of antibacterial agent, 40-60 parts of odor removing agent, 5-7 parts of mildew preventive, 1-4 parts of additive, 0.5-1 part of essence and 100-120 parts of water are stirred and mixed fully under the aseptic condition at room temperature, and then the mixture is kept stand to obtain the antibacterial deodorant.
The invention also provides a preparation method of the special smell removing agent, which comprises the following steps:
according to the mass parts, 30-60 parts of 1, 1-dimethyl silicon-based iron, 20-35 parts of diallyl dimethyl ammonium chloride, 5-12 parts of zinc ricinoleate and 0.02-0.6 part of Kaster platinum catalyst (CAS: 68478-92-2) are heated to 40-50 ℃, and stirred to react for 100-180min to obtain the odor removing agent.
Further, the mildew preventive is methylisothiazolinone, 3-iodine-2-propynyl butyl carbamate or p-hydroxybenzoate.
Further, the additive is ethanol.
Further, the essence is mint-flavored essence or green tea-flavored essence.
Further, the stirring time is 10-30min.
Further, the stirring speed is 600-1000r/min
Further, the standing time is 2-5h.
The invention also provides a preparation method of the antibacterial agent, which comprises the following steps:
the antibacterial agent is obtained by fully stirring and mixing 16-20 parts of benzalkonium chloride, 8-12 parts of ethanol and 3-7 parts of isopropanol according to the parts by weight.
Further, it is characterized in that: the stirring time is 10-15min.
The innovation points of the invention are as follows:
the 1, 1-dimethyl silicon-based iron, diallyl dimethyl ammonium chloride and zinc ricinoleate undergo hydrosilylation reaction to obtain the odor removing agent with the synergistic effect of silicon base and zinc ester.
The invention has the beneficial effects that:
the invention relates to an antibacterial deodorant and a preparation method thereof, and the antibacterial deodorant has the following obvious beneficial effects:
(1) The adopted antibacterial agent has strong capability of killing bacteria, broad spectrum, high efficiency, stable chemical property, low toxicity, no stimulation to skin mucosa, good compounding property with other types of bactericides and no damage to sterilized articles; the sterilization process is rapid, no harmful substance is generated, and no selective sterilization mode exists, so that the bacteria can not generate drug resistance.
(2) The macromolecular silicon-based odor removing agent is prepared by carrying out hydrosilylation reaction on 1, 1-dimethyl silicon-based iron, diallyl dimethyl ammonium chloride and zinc ricinoleate, is high-temperature resistant and strong in humidity resistance, is suitable for being used in the south with humidity and warmth, and has lasting using effect.
Detailed Description
The invention is further illustrated by the following specific examples:
the odor content determination method adopts GB/T14675-93 to determine; the antibacterial effect is measured by GB/T20944.1.2.
Example 1
An antibacterial deodorant and a preparation method thereof comprise the following operation steps:
the antibacterial deodorant is prepared by mixing 25g of antibacterial agent, 40g of odor removing agent, 5g of mildew preventive, 1g of additive, 0.5g of essence and 100g of water under sterile conditions at room temperature, stirring thoroughly, and standing.
The invention also provides a preparation method of the special smell removing agent, which comprises the following steps:
30g of 1, 1-dimethyl silicon-based iron, 20g of diallyl dimethyl ammonium chloride, 5g of zinc ricinoleate and 0.02g of Kastet platinum catalyst (CAS: 68478-92-2) are heated to 40 ℃ and stirred to react for 100min to obtain the odor removing agent.
Furthermore, the mildew preventive is methylisothiazolinone.
Further, the additive is ethanol.
Further, the essence is mint-flavored essence.
Further, the stirring time is 10min.
Further, the stirring speed is 600r/min
Further, the standing time is 2 hours.
The invention also provides a preparation method of the antibacterial agent, which comprises the following steps:
the antibacterial agent is obtained by mixing 16g benzalkonium chloride, 8g ethanol and 3g isopropanol under stirring.
Further, it is characterized in that: the stirring time is 10min.
Example 2
An antibacterial deodorant and a preparation method thereof comprise the following operation steps:
28g of antibacterial agent, 45g of odor removing agent, 6g of mildew preventive, 2g of additive, 0.6g of essence and 105g of water are stirred and mixed fully under the aseptic condition at room temperature, and then the mixture is kept stand to obtain the antibacterial deodorant.
The invention also provides a preparation method of the odor removing agent, which comprises the following steps:
40g of 1, 1-dimethyl silicon-based iron, 25g of diallyl dimethyl ammonium chloride, 7g of zinc ricinoleate and 0.1g of Kanster platinum catalyst (CAS: 68478-92-2) are heated to 44 ℃ and stirred to react for 120min to obtain the odor removing agent.
Furthermore, the mildew inhibitor is 3-iodine-2-propynyl butyl carbamate.
Further, the additive is ethanol.
Further, the essence is mint-flavored essence.
Further, the stirring time is 15min.
Further, the stirring speed is 700r/min
Further, the standing time is 3 hours.
The invention also provides a preparation method of the antibacterial agent, which comprises the following steps:
the antibacterial agent was obtained by thoroughly mixing 17g of benzalkonium chloride, 9g of ethanol, and 4g of isopropyl alcohol with stirring.
Further, it is characterized in that: the stirring time is 12min.
Example 3
An antibacterial deodorant and a preparation method thereof comprise the following operation steps:
32g of antibacterial agent, 55g of odor removing agent, 6g of mildew preventive, 3g of additive, 0.8g of essence and 115g of water are fully stirred and mixed under the aseptic condition at room temperature, and then the mixture is kept stand to obtain the antibacterial deodorant.
The invention also provides a preparation method of the odor removing agent, which comprises the following steps:
50g of 1, 1-dimethyl silicon-based iron, 30g of diallyl dimethyl ammonium chloride, 10g of zinc ricinoleate and 0.4g of Kastet platinum catalyst (CAS: 68478-92-2) are heated to 48 ℃, and stirred to react for 160min to obtain the odor removing agent.
Further, the mildew preventive is 3-iodine-2-propynyl butyl carbamate.
Further, the additive is ethanol.
Further, the essence is green tea flavor essence.
Further, the stirring time is 25min.
Further, the stirring speed is 900r/min
Further, the standing time is 4 hours.
The invention also provides a preparation method of the antibacterial agent, which comprises the following steps:
the antibacterial agent was obtained by thoroughly mixing 19g of benzalkonium chloride, 11g of ethanol, and 6g of isopropyl alcohol with stirring.
Further, it is characterized in that: the stirring time is 14min.
Example 4
An antibacterial deodorant and a preparation method thereof comprise the following operation steps:
the antibacterial deodorant is prepared by mixing 35g of antibacterial agent, 60g of odor removing agent, 7g of mildew preventive, 4g of additive, 1g of essence and 120g of water under the aseptic condition at room temperature, fully stirring, and standing.
The invention also provides a preparation method of the odor removing agent, which comprises the following steps:
60g of 1, 1-dimethyl silicon-based iron and 35g of diallyl dimethyl ammonium chloride, 12g of zinc ricinoleate and 0.6g of Kastet platinum catalyst (CAS: 68478-92-2) are heated to 48 ℃, and stirred to react for 160min to obtain the odor removing agent.
Further, the mildew preventive is p-hydroxybenzoate.
Further, the additive is ethanol.
Further, the essence is green tea flavor essence.
Further, the stirring time is 30min.
Further, the stirring rotating speed is 1000r/min
Further, the standing time is 5 hours.
The invention also provides a preparation method of the antibacterial agent, which comprises the following steps:
20g of benzalkonium chloride, 12g of ethanol and 7g of isopropanol are fully stirred and mixed to obtain the antibacterial agent.
Further, it is characterized in that: the stirring time is 15min.
Comparative example 1
The same procedure as in example 3 was repeated except that 1, 1-dimethylsilyloxy iron was not added;
comparative example 2
The procedure is as in example 3 except that diallyldimethylammonium chloride is not added; comparative example 3
Benzalkonium chloride was not added, as in example 3;
Figure BDA0003671961720000051

Claims (9)

1. a preparation method of an antibacterial deodorant comprises the following operation steps:
according to the mass parts, 25-35 parts of antibacterial agent, 40-60 parts of odor removing agent, 5-7 parts of mildew preventive, 1-4 parts of additive, 0.5-1 part of essence and 100-120 parts of water are fully stirred and mixed under the aseptic condition at room temperature, and then are kept stand to obtain the antibacterial deodorant;
the preparation method of the odor removing agent comprises the following steps:
according to the mass parts, 30-60 parts of 1, 1' -di (dimethyl silicon-based) iron, 20-35 parts of diallyl dimethyl ammonium chloride, 5-12 parts of zinc ricinoleate, 0.02-0.6 part of Karster platinum catalyst, CAS:68478-92-2 heating to 40-50 deg.C, stirring, and reacting
And (3) obtaining the odor removing agent after 100-180 min.
2. The method for preparing an antibacterial deodorant according to claim 1, characterized in that: the mildew preventive is methylisothiazolinone, 3-iodine-2-propynyl butyl carbamate or p-hydroxybenzoate.
3. The method for preparing an antibacterial deodorant according to claim 1, characterized in that: the additive is ethanol.
4. The method for preparing an antibacterial deodorant according to claim 1, characterized in that: the essence is mint-flavored essence or green tea-flavored essence.
5. The method for preparing an antibacterial deodorant according to claim 1, characterized in that: the stirring time is 10-30min.
6. The method for preparing an antibacterial deodorant according to claim 1, characterized in that: the stirring speed is 600-1000r/min.
7. The method for preparing an antibacterial deodorant according to claim 1, characterized in that: the standing time is 2-5h.
8. The method for preparing an antibacterial deodorant according to claim 1, characterized in that: the preparation method of the antibacterial agent comprises the following steps: the antibacterial agent is obtained by fully stirring and mixing 16-20 parts of benzalkonium chloride, 8-12 parts of ethanol and 3-7 parts of isopropanol according to the parts by weight.
9. The method for preparing an antibacterial deodorant according to claim 8, characterized in that: the stirring time is 10-15min.
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Denomination of invention: An antibacterial and deodorizing agent and its preparation method

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Pledgee: Zhejiang Dongyang Rural Commercial Bank Co.,Ltd. Weishan Sub branch

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