CN114288703B - 一种硼酸生产结晶分离设备 - Google Patents
一种硼酸生产结晶分离设备 Download PDFInfo
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- CN114288703B CN114288703B CN202210085012.3A CN202210085012A CN114288703B CN 114288703 B CN114288703 B CN 114288703B CN 202210085012 A CN202210085012 A CN 202210085012A CN 114288703 B CN114288703 B CN 114288703B
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- 238000002425 crystallisation Methods 0.000 title claims abstract description 100
- 230000008025 crystallization Effects 0.000 title claims abstract description 100
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 title claims abstract description 16
- 239000004327 boric acid Substances 0.000 title claims abstract description 16
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 12
- 238000000926 separation method Methods 0.000 title claims abstract description 10
- 239000002245 particle Substances 0.000 claims abstract description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 5
- 239000007788 liquid Substances 0.000 claims description 37
- 238000007789 sealing Methods 0.000 claims description 24
- 238000009434 installation Methods 0.000 claims description 20
- 239000013078 crystal Substances 0.000 claims description 14
- 238000003756 stirring Methods 0.000 claims description 12
- 239000011229 interlayer Substances 0.000 claims description 11
- 238000007790 scraping Methods 0.000 claims description 9
- 238000001816 cooling Methods 0.000 claims description 5
- 230000002349 favourable effect Effects 0.000 claims description 3
- 239000011159 matrix material Substances 0.000 claims description 3
- 230000009286 beneficial effect Effects 0.000 claims description 2
- 238000004064 recycling Methods 0.000 claims 1
- 238000005192 partition Methods 0.000 abstract description 4
- 239000000243 solution Substances 0.000 description 7
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 4
- 239000011521 glass Substances 0.000 description 4
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 2
- 239000003365 glass fiber Substances 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 229910021538 borax Inorganic materials 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 150000002170 ethers Chemical class 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 235000011187 glycerol Nutrition 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 239000011810 insulating material Substances 0.000 description 1
- 239000002932 luster Substances 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 239000012528 membrane Substances 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 239000005304 optical glass Substances 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000004328 sodium tetraborate Substances 0.000 description 1
- 235000010339 sodium tetraborate Nutrition 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000000341 volatile oil Substances 0.000 description 1
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/10—Process efficiency
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- Crystals, And After-Treatments Of Crystals (AREA)
Abstract
Description
Claims (3)
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CN202210085012.3A CN114288703B (zh) | 2022-01-25 | 2022-01-25 | 一种硼酸生产结晶分离设备 |
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CN202210085012.3A CN114288703B (zh) | 2022-01-25 | 2022-01-25 | 一种硼酸生产结晶分离设备 |
Publications (2)
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CN114288703A CN114288703A (zh) | 2022-04-08 |
CN114288703B true CN114288703B (zh) | 2023-08-25 |
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CN202210085012.3A Active CN114288703B (zh) | 2022-01-25 | 2022-01-25 | 一种硼酸生产结晶分离设备 |
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CN (1) | CN114288703B (zh) |
Citations (22)
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---|---|---|---|---|
GB571527A (en) * | 1941-06-27 | 1945-08-29 | American Cyanamid Co | Improvements in or relating to the production of crystalline nitroguanidine in an extremely fine state of subdivision |
FR1113884A (fr) * | 1953-12-07 | 1956-04-05 | Standard Oil Dev Co | Procédé de cristallisation et de récupération d'hydrocarbures |
CH347819A (de) * | 1955-10-27 | 1960-07-31 | Schneider Carlos | Verfahren und Einrichtung zum kontinuierlichen Konzentrieren von Lösungen durch Gefrieren eines Lösungsmittels und Trennung des flüssigen vom erstarrten Anteil |
US3389974A (en) * | 1964-06-10 | 1968-06-25 | Montedison Spa | Process and apparatus for harvesting crystals |
GB1172959A (en) * | 1967-07-11 | 1969-12-03 | Inst Francais Du Petrole | Crystallization Process and Apparatus |
GB1188542A (en) * | 1967-01-27 | 1970-04-15 | Distington Engineering Co | Continuous Crystallising Equipment |
CN1030065A (zh) * | 1987-03-03 | 1989-01-04 | 北京市建筑材料科学研究所 | 硼矿制取硼酸联产硝酸钠 |
CN1061728A (zh) * | 1990-11-27 | 1992-06-10 | 苏舍兄弟有限公司 | 通过结晶从液体混合物中分离物质的装置 |
JPH0565685A (ja) * | 1991-09-06 | 1993-03-19 | Toho Aen Kk | 陽極スライム除去装置 |
CA2300437A1 (en) * | 1999-03-11 | 2000-09-11 | Goudsche Machinefabriek B.V. | Crystallizer with cooling element and sweeping element with sweeping parts, and sweeping element and sweeping part for such a crystallizer |
JP2004154619A (ja) * | 2002-11-01 | 2004-06-03 | Tsukishima Kikai Co Ltd | 被処理液循環型掻取式晶析装置 |
CN108525341A (zh) * | 2018-03-22 | 2018-09-14 | 孙学中 | 一种用于医药原料制备的植物有效成分提取设备 |
CN108585088A (zh) * | 2018-05-17 | 2018-09-28 | 庄艺婷 | 一种基于工业污水再利用的结晶处理装置 |
CN109603192A (zh) * | 2018-12-18 | 2019-04-12 | 申恒杰 | 一种重质纯碱大批量生产用结晶罐 |
CN209322767U (zh) * | 2018-11-30 | 2019-08-30 | 东莞市杉杉电池材料有限公司 | 一种双草酸硼酸锂的纯化装置 |
CN210159233U (zh) * | 2019-06-18 | 2020-03-20 | 江苏德邦多菱健康科技有限公司 | 一种磷酸盐生产用结晶装置 |
CN211659309U (zh) * | 2019-12-31 | 2020-10-13 | 昆明弘承食品科技有限公司 | 一种桶状结构的溶液用冷冻浓缩装置 |
CN112112572A (zh) * | 2020-09-07 | 2020-12-22 | 中石化石油机械股份有限公司 | 上振荡滑片射流增程水力振荡器 |
CN213031900U (zh) * | 2020-08-26 | 2021-04-23 | 山东皓皓环保科技有限公司 | 一种具有防堵结构的氯化亚铁结晶釜 |
CN213221022U (zh) * | 2020-06-05 | 2021-05-18 | 苏州友硼光电材料有限公司 | 一种制取硼酸的酸化反应结晶器 |
CN113893571A (zh) * | 2021-11-10 | 2022-01-07 | 许妙飞 | 一种氨基葡萄糖盐酸结晶设备 |
CN113952759A (zh) * | 2021-10-19 | 2022-01-21 | 高桂双 | 一种叶黄素提纯结晶系统 |
-
2022
- 2022-01-25 CN CN202210085012.3A patent/CN114288703B/zh active Active
Patent Citations (22)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB571527A (en) * | 1941-06-27 | 1945-08-29 | American Cyanamid Co | Improvements in or relating to the production of crystalline nitroguanidine in an extremely fine state of subdivision |
FR1113884A (fr) * | 1953-12-07 | 1956-04-05 | Standard Oil Dev Co | Procédé de cristallisation et de récupération d'hydrocarbures |
CH347819A (de) * | 1955-10-27 | 1960-07-31 | Schneider Carlos | Verfahren und Einrichtung zum kontinuierlichen Konzentrieren von Lösungen durch Gefrieren eines Lösungsmittels und Trennung des flüssigen vom erstarrten Anteil |
US3389974A (en) * | 1964-06-10 | 1968-06-25 | Montedison Spa | Process and apparatus for harvesting crystals |
GB1188542A (en) * | 1967-01-27 | 1970-04-15 | Distington Engineering Co | Continuous Crystallising Equipment |
GB1172959A (en) * | 1967-07-11 | 1969-12-03 | Inst Francais Du Petrole | Crystallization Process and Apparatus |
CN1030065A (zh) * | 1987-03-03 | 1989-01-04 | 北京市建筑材料科学研究所 | 硼矿制取硼酸联产硝酸钠 |
CN1061728A (zh) * | 1990-11-27 | 1992-06-10 | 苏舍兄弟有限公司 | 通过结晶从液体混合物中分离物质的装置 |
JPH0565685A (ja) * | 1991-09-06 | 1993-03-19 | Toho Aen Kk | 陽極スライム除去装置 |
CA2300437A1 (en) * | 1999-03-11 | 2000-09-11 | Goudsche Machinefabriek B.V. | Crystallizer with cooling element and sweeping element with sweeping parts, and sweeping element and sweeping part for such a crystallizer |
JP2004154619A (ja) * | 2002-11-01 | 2004-06-03 | Tsukishima Kikai Co Ltd | 被処理液循環型掻取式晶析装置 |
CN108525341A (zh) * | 2018-03-22 | 2018-09-14 | 孙学中 | 一种用于医药原料制备的植物有效成分提取设备 |
CN108585088A (zh) * | 2018-05-17 | 2018-09-28 | 庄艺婷 | 一种基于工业污水再利用的结晶处理装置 |
CN209322767U (zh) * | 2018-11-30 | 2019-08-30 | 东莞市杉杉电池材料有限公司 | 一种双草酸硼酸锂的纯化装置 |
CN109603192A (zh) * | 2018-12-18 | 2019-04-12 | 申恒杰 | 一种重质纯碱大批量生产用结晶罐 |
CN210159233U (zh) * | 2019-06-18 | 2020-03-20 | 江苏德邦多菱健康科技有限公司 | 一种磷酸盐生产用结晶装置 |
CN211659309U (zh) * | 2019-12-31 | 2020-10-13 | 昆明弘承食品科技有限公司 | 一种桶状结构的溶液用冷冻浓缩装置 |
CN213221022U (zh) * | 2020-06-05 | 2021-05-18 | 苏州友硼光电材料有限公司 | 一种制取硼酸的酸化反应结晶器 |
CN213031900U (zh) * | 2020-08-26 | 2021-04-23 | 山东皓皓环保科技有限公司 | 一种具有防堵结构的氯化亚铁结晶釜 |
CN112112572A (zh) * | 2020-09-07 | 2020-12-22 | 中石化石油机械股份有限公司 | 上振荡滑片射流增程水力振荡器 |
CN113952759A (zh) * | 2021-10-19 | 2022-01-21 | 高桂双 | 一种叶黄素提纯结晶系统 |
CN113893571A (zh) * | 2021-11-10 | 2022-01-07 | 许妙飞 | 一种氨基葡萄糖盐酸结晶设备 |
Non-Patent Citations (1)
Title |
---|
高纯硼酸制备过程中的结晶动力学;龚殿婷等;《过程工程学报》;20081231;全文 * |
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PB01 | Publication | ||
PB01 | Publication | ||
SE01 | Entry into force of request for substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
TA01 | Transfer of patent application right | ||
TA01 | Transfer of patent application right |
Effective date of registration: 20230724 Address after: Room 211-214, Floor 2, Building 1, No. 69, Aoti Street, Jianye District, Nanjing City, Jiangsu Province, 210000 Applicant after: Nanjing Jicaihui Technology Co.,Ltd. Address before: 330001 No. 88 Hangkong Road, Qingyunpu District, Nanchang City, Jiangxi Province Applicant before: Che Qiang |
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TR01 | Transfer of patent right |
Effective date of registration: 20240521 Address after: 361000 No. 728, Yangming Road, Haicang District, Xiamen City, Fujian Province Patentee after: Zhuo Mimi Country or region after: China Address before: Room 211-214, Floor 2, Building 1, No. 69, Aoti Street, Jianye District, Nanjing City, Jiangsu Province, 210000 Patentee before: Nanjing Jicaihui Technology Co.,Ltd. Country or region before: China |