CN114191359A - Shower gel containing paris polyphylla extract and preparation method thereof - Google Patents
Shower gel containing paris polyphylla extract and preparation method thereof Download PDFInfo
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- CN114191359A CN114191359A CN202111565989.7A CN202111565989A CN114191359A CN 114191359 A CN114191359 A CN 114191359A CN 202111565989 A CN202111565989 A CN 202111565989A CN 114191359 A CN114191359 A CN 114191359A
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- paris polyphylla
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- rhizoma paridis
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- 241000244987 Daiswa polyphylla Species 0.000 title claims abstract description 135
- 239000000284 extract Substances 0.000 title claims abstract description 135
- 238000002360 preparation method Methods 0.000 title claims abstract description 29
- 238000000605 extraction Methods 0.000 title description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 39
- 241000727169 Prinsepia utilis Species 0.000 claims abstract description 33
- 239000000463 material Substances 0.000 claims abstract description 15
- 239000002699 waste material Substances 0.000 claims abstract description 5
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 45
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 45
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 40
- 239000000843 powder Substances 0.000 claims description 38
- 238000002156 mixing Methods 0.000 claims description 35
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 28
- 239000004094 surface-active agent Substances 0.000 claims description 24
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- 235000017709 saponins Nutrition 0.000 claims description 23
- 150000007949 saponins Chemical class 0.000 claims description 22
- MRUAUOIMASANKQ-UHFFFAOYSA-N cocamidopropyl betaine Chemical compound CCCCCCCCCCCC(=O)NCCC[N+](C)(C)CC([O-])=O MRUAUOIMASANKQ-UHFFFAOYSA-N 0.000 claims description 20
- 229940073507 cocamidopropyl betaine Drugs 0.000 claims description 20
- 238000010438 heat treatment Methods 0.000 claims description 19
- 239000002904 solvent Substances 0.000 claims description 19
- 239000008367 deionised water Substances 0.000 claims description 18
- 229910021641 deionized water Inorganic materials 0.000 claims description 18
- 239000000706 filtrate Substances 0.000 claims description 18
- 238000000227 grinding Methods 0.000 claims description 18
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- 238000001816 cooling Methods 0.000 claims description 15
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- 239000004299 sodium benzoate Substances 0.000 claims description 15
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- 239000011780 sodium chloride Substances 0.000 claims description 14
- 238000000265 homogenisation Methods 0.000 claims description 13
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 12
- TVACALAUIQMRDF-UHFFFAOYSA-N dodecyl dihydrogen phosphate Chemical compound CCCCCCCCCCCCOP(O)(O)=O TVACALAUIQMRDF-UHFFFAOYSA-N 0.000 claims description 12
- 238000000034 method Methods 0.000 claims description 12
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- 239000000654 additive Substances 0.000 claims description 7
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- 235000010663 Lavandula angustifolia Nutrition 0.000 claims description 6
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- LQZZUXJYWNFBMV-UHFFFAOYSA-N dodecan-1-ol Chemical compound CCCCCCCCCCCCO LQZZUXJYWNFBMV-UHFFFAOYSA-N 0.000 claims description 6
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- UFVKGYZPFZQRLF-UHFFFAOYSA-N hydroxypropyl methyl cellulose Chemical compound OC1C(O)C(OC)OC(CO)C1OC1C(O)C(O)C(OC2C(C(O)C(OC3C(C(O)C(O)C(CO)O3)O)C(CO)O2)O)C(CO)O1 UFVKGYZPFZQRLF-UHFFFAOYSA-N 0.000 claims description 6
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- QZXSMBBFBXPQHI-UHFFFAOYSA-N N-(dodecanoyl)ethanolamine Chemical compound CCCCCCCCCCCC(=O)NCCO QZXSMBBFBXPQHI-UHFFFAOYSA-N 0.000 claims description 5
- 229910019142 PO4 Inorganic materials 0.000 claims description 5
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims description 5
- 238000004090 dissolution Methods 0.000 claims description 5
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- 239000010452 phosphate Substances 0.000 claims description 5
- 229910052700 potassium Inorganic materials 0.000 claims description 5
- 239000011591 potassium Substances 0.000 claims description 5
- RFVNOJDQRGSOEL-UHFFFAOYSA-N 2-hydroxyethyl octadecanoate Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCCO RFVNOJDQRGSOEL-UHFFFAOYSA-N 0.000 claims description 4
- 238000001914 filtration Methods 0.000 claims description 4
- IUCHKMAZAWJNBJ-RCYXVVTDSA-N oleanolic acid 3-O-beta-D-glucosiduronic acid Chemical compound O([C@H]1CC[C@]2(C)[C@H]3CC=C4[C@@]([C@@]3(CC[C@H]2C1(C)C)C)(C)CC[C@]1(CCC(C[C@H]14)(C)C)C(O)=O)[C@@H]1O[C@H](C(O)=O)[C@@H](O)[C@H](O)[C@H]1O IUCHKMAZAWJNBJ-RCYXVVTDSA-N 0.000 claims description 4
- 239000003755 preservative agent Substances 0.000 claims description 4
- 230000002335 preservative effect Effects 0.000 claims description 4
- 239000002994 raw material Substances 0.000 claims description 4
- 230000001502 supplementing effect Effects 0.000 claims description 4
- 239000002671 adjuvant Substances 0.000 claims description 3
- 230000002421 anti-septic effect Effects 0.000 claims description 3
- 239000010445 mica Substances 0.000 claims description 3
- 229910052618 mica group Inorganic materials 0.000 claims description 3
- 239000001509 sodium citrate Substances 0.000 claims description 3
- NLJMYIDDQXHKNR-UHFFFAOYSA-K sodium citrate Chemical compound O.O.[Na+].[Na+].[Na+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O NLJMYIDDQXHKNR-UHFFFAOYSA-K 0.000 claims description 3
- 239000003814 drug Substances 0.000 abstract description 12
- 230000000694 effects Effects 0.000 abstract description 11
- 241000196324 Embryophyta Species 0.000 abstract description 8
- 238000004659 sterilization and disinfection Methods 0.000 abstract description 5
- 239000000499 gel Substances 0.000 description 44
- 239000006210 lotion Substances 0.000 description 7
- 230000000844 anti-bacterial effect Effects 0.000 description 6
- 239000000047 product Substances 0.000 description 6
- 239000000126 substance Substances 0.000 description 5
- 230000003385 bacteriostatic effect Effects 0.000 description 4
- 238000004140 cleaning Methods 0.000 description 4
- 150000001875 compounds Chemical class 0.000 description 4
- 230000036541 health Effects 0.000 description 4
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 3
- 238000001514 detection method Methods 0.000 description 3
- 241000411851 herbal medicine Species 0.000 description 3
- 238000003287 bathing Methods 0.000 description 2
- WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 description 2
- 230000006378 damage Effects 0.000 description 2
- 208000017520 skin disease Diseases 0.000 description 2
- GEHJYWRUCIMESM-UHFFFAOYSA-L sodium sulfite Chemical compound [Na+].[Na+].[O-]S([O-])=O GEHJYWRUCIMESM-UHFFFAOYSA-L 0.000 description 2
- DSSYKIVIOFKYAU-XCBNKYQSSA-N (R)-camphor Chemical compound C1C[C@@]2(C)C(=O)C[C@@H]1C2(C)C DSSYKIVIOFKYAU-XCBNKYQSSA-N 0.000 description 1
- MFYSUUPKMDJYPF-UHFFFAOYSA-N 2-[(4-methyl-2-nitrophenyl)diazenyl]-3-oxo-n-phenylbutanamide Chemical compound C=1C=CC=CC=1NC(=O)C(C(=O)C)N=NC1=CC=C(C)C=C1[N+]([O-])=O MFYSUUPKMDJYPF-UHFFFAOYSA-N 0.000 description 1
- FJKROLUGYXJWQN-UHFFFAOYSA-N 4-hydroxybenzoic acid Chemical compound OC(=O)C1=CC=C(O)C=C1 FJKROLUGYXJWQN-UHFFFAOYSA-N 0.000 description 1
- 244000215068 Acacia senegal Species 0.000 description 1
- NIXOWILDQLNWCW-UHFFFAOYSA-N Acrylic acid Chemical compound OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 1
- 241000213006 Angelica dahurica Species 0.000 description 1
- 206010003399 Arthropod bite Diseases 0.000 description 1
- 239000005711 Benzoic acid Substances 0.000 description 1
- 235000019224 Camellia sinensis var Qingmao Nutrition 0.000 description 1
- 229920002134 Carboxymethyl cellulose Polymers 0.000 description 1
- 241000050051 Chelone glabra Species 0.000 description 1
- 241000723346 Cinnamomum camphora Species 0.000 description 1
- 244000060011 Cocos nucifera Species 0.000 description 1
- 235000013162 Cocos nucifera Nutrition 0.000 description 1
- 241000186427 Cutibacterium acnes Species 0.000 description 1
- QXNVGIXVLWOKEQ-UHFFFAOYSA-N Disodium Chemical compound [Na][Na] QXNVGIXVLWOKEQ-UHFFFAOYSA-N 0.000 description 1
- KCXVZYZYPLLWCC-UHFFFAOYSA-N EDTA Chemical compound OC(=O)CN(CC(O)=O)CCN(CC(O)=O)CC(O)=O KCXVZYZYPLLWCC-UHFFFAOYSA-N 0.000 description 1
- FPVVYTCTZKCSOJ-UHFFFAOYSA-N Ethylene glycol distearate Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCCOC(=O)CCCCCCCCCCCCCCCCC FPVVYTCTZKCSOJ-UHFFFAOYSA-N 0.000 description 1
- 229920002907 Guar gum Polymers 0.000 description 1
- 229920000084 Gum arabic Polymers 0.000 description 1
- 244000048199 Hibiscus mutabilis Species 0.000 description 1
- 235000003973 Hibiscus mutabilis Nutrition 0.000 description 1
- 241000234280 Liliaceae Species 0.000 description 1
- 241000220317 Rosa Species 0.000 description 1
- 229920002125 Sokalan® Polymers 0.000 description 1
- 235000002594 Solanum nigrum Nutrition 0.000 description 1
- 240000002307 Solanum ptychanthum Species 0.000 description 1
- 241000219784 Sophora Species 0.000 description 1
- 241000191967 Staphylococcus aureus Species 0.000 description 1
- 241000191963 Staphylococcus epidermidis Species 0.000 description 1
- 229920002472 Starch Polymers 0.000 description 1
- 208000027418 Wounds and injury Diseases 0.000 description 1
- 239000000205 acacia gum Substances 0.000 description 1
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- 239000002253 acid Substances 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 239000006286 aqueous extract Substances 0.000 description 1
- 239000013040 bath agent Substances 0.000 description 1
- 235000010233 benzoic acid Nutrition 0.000 description 1
- 230000003115 biocidal effect Effects 0.000 description 1
- 229960000846 camphor Drugs 0.000 description 1
- 229930008380 camphor Natural products 0.000 description 1
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- 239000008112 carboxymethyl-cellulose Substances 0.000 description 1
- 229940126678 chinese medicines Drugs 0.000 description 1
- 230000000295 complement effect Effects 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 239000006071 cream Substances 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 229960001484 edetic acid Drugs 0.000 description 1
- 238000002481 ethanol extraction Methods 0.000 description 1
- BEFDCLMNVWHSGT-UHFFFAOYSA-N ethenylcyclopentane Chemical compound C=CC1CCCC1 BEFDCLMNVWHSGT-UHFFFAOYSA-N 0.000 description 1
- 150000002191 fatty alcohols Chemical class 0.000 description 1
- 239000006260 foam Substances 0.000 description 1
- 238000005187 foaming Methods 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 150000004676 glycans Chemical class 0.000 description 1
- 239000004519 grease Substances 0.000 description 1
- 239000000665 guar gum Substances 0.000 description 1
- 235000010417 guar gum Nutrition 0.000 description 1
- 229960002154 guar gum Drugs 0.000 description 1
- 239000003906 humectant Substances 0.000 description 1
- 230000000977 initiatory effect Effects 0.000 description 1
- 208000014674 injury Diseases 0.000 description 1
- 230000007794 irritation Effects 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 239000002398 materia medica Substances 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- 230000003020 moisturizing effect Effects 0.000 description 1
- 239000003605 opacifier Substances 0.000 description 1
- 229940084806 paris polyphylla root extract Drugs 0.000 description 1
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- 238000012503 pharmacopoeial method Methods 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- 235000010482 polyoxyethylene sorbitan monooleate Nutrition 0.000 description 1
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- 229920000053 polysorbate 80 Polymers 0.000 description 1
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- 229940055019 propionibacterium acne Drugs 0.000 description 1
- 235000020339 pu-erh tea Nutrition 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 229940083542 sodium Drugs 0.000 description 1
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- 229960002668 sodium chloride Drugs 0.000 description 1
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- 235000010199 sorbic acid Nutrition 0.000 description 1
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- 229940075582 sorbic acid Drugs 0.000 description 1
- 235000013599 spices Nutrition 0.000 description 1
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- 230000000638 stimulation Effects 0.000 description 1
- 230000008961 swelling Effects 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
- 229940126680 traditional chinese medicines Drugs 0.000 description 1
- LWIHDJKSTIGBAC-UHFFFAOYSA-K tripotassium phosphate Chemical compound [K+].[K+].[K+].[O-]P([O-])([O-])=O LWIHDJKSTIGBAC-UHFFFAOYSA-K 0.000 description 1
- XPFJYKARVSSRHE-UHFFFAOYSA-K trisodium;2-hydroxypropane-1,2,3-tricarboxylate;2-hydroxypropane-1,2,3-tricarboxylic acid Chemical group [Na+].[Na+].[Na+].OC(=O)CC(O)(C(O)=O)CC(O)=O.[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O XPFJYKARVSSRHE-UHFFFAOYSA-K 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Dermatology (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Cosmetics (AREA)
Abstract
The invention provides a medicine containing rhizoma paridis (rhizoma paridis yunnanensis)Paris polyphylla Smith var.yunnanensis(Franch.) hand-Mazz) extract and its preparation method are provided. The shower gel containing the paris polyphylla extract is composed of 0.1-2.0% of paris polyphylla extract, 0.1-1.0% of prinsepia utilis royle oil, conventional shower gel auxiliary materials and water. The product of the invention has the effects of bacteriostasis and disinfection, increases the utilization of waste plant resources, has low cost and has good application value and prospect. In addition, the invention lays a certain foundation for the application of folk plant resourcesThe preparation method is simple, easy to implement and has a good application prospect.
Description
Technical Field
The invention belongs to the technical field of cosmetics, and particularly relates to shower gel containing a paris polyphylla extract, and more particularly to traditional Chinese medicine shower gel containing a paris polyphylla root extract, a paris polyphylla stem and leaf extract and prinsepia utilis royle oil and a preparation method thereof.
Background
The shower gel, also called bath agent and shower cream, is a liquid washing and protecting product for cleaning the whole body skin when people take a bath, and is a common cleaning product for modern people. Chemical essence and chemical raw materials are mainly added into shower gel on the market, and to a certain extent, although the shower gel has a good cleaning function and a certain disinfection and antibiosis effect, most of the shower gel has certain toxic and side effects, can cause great damage to skin after long-time use, and chemical substances are not thoroughly cleaned in the use process, enter the deep layer of the skin or are introduced into the mouth through hands, and cause deep injury to the human body. However, with the development of economic society, some traditional Chinese medicine shower gels with health care function have been developed and applied in China, but the health care effect is not ideal. Paris polyphylla and prinsepia utilis royle are used as mountain plants produced in Yunnan Lijiang in folk life for health preserving and health care, and have a long history of thousands of years. According to the Chinese pharmacopoeia (2020 edition), the Paris polyphylla is dried rhizome of Paris polyphylla Smith var.yunnanensis (Franch.) hand. -mazz. or Paris polyphylla Smith var.chinensis (Franch.) Hara of Liliaceae, and the content of Paris polyphylla saponin I (C) is limited to be calculated according to the dried rhizome44H70O16) Rhizoma paridis Saponin II (C)51H82O20) And rhizoma paridis saponin VII (C)51H82O21) The total amount of (A) should not be less than 0.60%. The paris polyphylla serving as a folk prescription has the effects of sterilization and disinfection in folk use, and the material basis is mainlySaponins compound [ reference 1: the medicinal value and chemical substance basis of the plants of Paris genus, Chinese traditional medicine journal 2015,40(5),833 + 839; reference 2: chinese herbal medicine 2016,47(18), 3301-one 3323; reference 3: tuxin, Liheoshi, Piaozheng, Wangyou, Wanyingying, Vanming, Wanshuang, Zhang Haizhu, Xiayinglonggong, research progress of pharmacological action and predictive analysis of quality markers Chinese herbal medicine, 2019,50(19), 4838-plus 4852.]. The bacteriostatic activity of prinsepia utilis royle oil is also widely used in folk [ reference 4: economic value and cultivation technique of wild Prinsepia utilis Royle of Dali, forestry survey planning, 2004,29(S1):287-289.]Experimental studies show that prinsepia utilis royle oil has a certain bacteriostatic function [ reference 5: comparison research of antibacterial effects of the giarine, Shiyundong, Lixiang, Zhouyanqing, Luolan, Prinsepia utilis Royle oil and Pu' er tea water, grain and oil food technology 2010,18(5) 31-33; reference 6: zhangrongxi, revenge, Zhaojia, Yangxiang, grand group, the bacteriostatic effect of the water extract of different parts of the Prinsepia utilis Ino agricultural science 2007,35(2), 408-doped wine 411.]。
Chinese patent CN112618463A discloses "a bacteriostatic skin-care bath foam containing traditional Chinese medicine extract", which contains traditional Chinese medicine extract, and contains 7 kinds of Chinese herbal medicines: the camphor leaves, the cotton rose leaves, the paris polyphylla, the black nightshade, the lightyellow sophora root, the dahurian angelica root and the baical skullcap root are prepared according to the proportion of 2:2:1:1:2:1:2, and the extraction is carried out according to the step one in the claim 6, but only the liquid medicine is concentrated and filtered in the step one, so that the traditional Chinese medicine extracting solution is obtained. However, the concentrated solution is not limited in the end, and the amount of ethanol contained in the extract solution is not clearly described. Therefore, although the amount of the Chinese medicinal extract added is limited in the end of this patent, the degree of concentration is not limited, and the amount of the Chinese medicinal extract added is not determined. Although paris polyphylla is added in the patent, paris polyphylla is only one of 7 traditional Chinese medicinal materials, and the mass ratio is 1/11. Finally, paris plants, which are perennial herbaceous plants belonging to the family trillioniaceae, have 26 and 14 varieties [ reference 1], and different varieties of steroid saponin compounds contained in paris plants [ reference 7: wei JC, Gao WY, Yan XD, Wang Y, lacing SS, Xiao PG, chemical Constitutes of Plants from the Genus Paris, chem, Biodiversity,2014,11(9), 1277-. The 7 Chinese medicines used in the patent contain the paris polyphylla, but the specific variety is not limited, and the content of saponin is not limited.
Chinese patent CN108309883A discloses an antibacterial health-care shower gel containing Yuzhou radix Rhapontici and a preparation method thereof, wherein the shower gel comprises 5 traditional Chinese medicine extracts, one of the traditional Chinese medicine extracts is a water extract of rhizoma paridis, and the rhizoma paridis is limited to dried rhizome of Yunnan rhizoma paridis or paris polyphylla. Different extraction solvents can lead to inconsistency of extracted compounds, according to the regulations of Chinese pharmacopoeia (2020 edition), the extraction of saponin is mainly concentrated in an ethanol extraction part, and an aqueous extraction part is mainly some water-soluble compounds and mainly contains polysaccharide. Secondly, although the patent contains the extract of the paris polyphylla, the paris polyphylla is not the main traditional Chinese medicine extract and is only one of 5 traditional Chinese medicine extracts. Therefore, the rhizoma paridis aqueous extract used in the patent has low saponin content and is only one of 5 traditional Chinese medicines.
Disclosure of Invention
The technical problem to be solved by the invention is as follows: aiming at the problems in the prior art, the invention provides shower gel containing paris polyphylla extract and a preparation method thereof.
In order to achieve the above purpose of the present invention, the present invention provides the following technical solutions:
a shower gel containing a paris polyphylla extract comprises 0.1-2.0% of paris polyphylla extract, 0.1-1.0% of prinsepia utilis royle oil and conventional shower gel auxiliary materials in percentage by weight, the auxiliary materials are added in the range of the conventional shower gel auxiliary materials, and the balance is complemented to 100% by deionized water. The content of total saponins in the rhizoma paridis Yunnanensis extract is higher than 0.60%.
The shower gel containing the Paris polyphylla extract is characterized in that the Paris polyphylla (Paris polyphylla Smith var. yunnanensis (Franch)) extract is one or two of Paris polyphylla root tuber extract and Paris polyphylla stem and leaf extract;the rhizoma paridis extract is prepared from dried root tuber, and is determined by the method specified in Chinese pharmacopoeia (2020 edition) to limit the content of rhizoma paridis saponin I (C)44H70O16) Rhizoma paridis Saponin II (C)51H82O20) And rhizoma paridis saponin VII (C)51H82O21) The total amount of (A) should not be less than 0.60%; the raw material used by the paris polyphylla stem and leaf extract is the overground stem and leaf part which is directly discarded after the seeds are harvested every year.
A shower gel containing paris polyphylla extract is prepared by the following method:
dissolving the conventional solid thickening agent as adjuvant in water at 40-60 deg.C, adding solid surfactant to dissolve, cooling, adding liquid surfactant, cosolvent, antioxidant, antiseptic, and other additives, mixing, adding rhizoma paridis extract and Prinsepia utilis oil, mixing, measuring pH, adding pH regulator as required, and mixing. The content of total saponins in the rhizoma paridis Yunnanensis extract is higher than 0.60%.
A shower gel containing paris polyphylla extract is prepared by the following method:
(1) grinding the medicinal part tuber root of the paris polyphylla or the waste overground part stem leaves of the paris polyphylla in each year into powder by a grinder and a grinder, and sieving the powder by a sieve of 20-80 meshes;
(2) extracting with 50-100% ethanol solution, heating and refluxing, and ultrasonic extracting for 2-3 times (each time for 1-5 hr) at a material-to-liquid ratio of 1:2-1: 20;
(3) filtering the extractive solution, enriching the filtrate, and removing solvent by rotary evaporator to obtain solvent-free extract of rhizoma paridis Yunnanensis, wherein the total saponin content in the extract is higher than 0.60%.
The invention also provides a preparation method of the shower gel containing the paris polyphylla extract, which comprises the following steps:
(1) grinding medicinal part of rhizoma paridis Yunnanensis, i.e. root tuber or waste aerial parts of rhizoma paridis Yunnanensis every year, stem and leaf into powder by a grinder, and sieving with 20-80 mesh sieve;
(2) extracting with 50-100% ethanol solution, heating and refluxing, and ultrasonic extracting for 2-3 times (each time for 1-5 hr) at a material-to-liquid ratio of 1:2-1: 20;
(3) filtering each extractive solution, enriching filtrate, and removing solvent by rotary evaporator to obtain solvent-free extract of rhizoma paridis Yunnanensis.
Another preparation method of shower gel containing paris polyphylla extract comprises the following steps: dissolving the conventional solid thickening agent as adjuvant in water at 40-60 deg.C, adding solid surfactant to dissolve, cooling, adding liquid surfactant, cosolvent, antioxidant, antiseptic, and other additives, mixing, adding rhizoma paridis Yunnanensis extract and Prinsepia utilis oil, mixing, measuring pH, adding pH regulator as required, and mixing.
A preparation method of shower gel containing paris polyphylla extract comprises the following steps:
(1) preparing the Yunnan paris polyphylla stem and leaf extract: grinding the stem and leaf parts of the paris polyphylla into powder by a grinder, and sieving the powder by a 40-mesh sieve; secondly, heating and refluxing for 3 times with 80% ethanol solution, and each time for 2 h; finally, collecting the extracting solution for 3 times, and removing the solvent from the filtrate by a rotary evaporator to obtain solvent-free Yunnan rhizoma paridis stem and leaf extract;
(2) preparing the shower gel: mixing surfactant 10.0 wt% of cocamidopropyl betaine, 8.0 wt% of potassium lauryl alcohol ether phosphate and 7.0 wt% of cocamidopropyl hydroxysulfobetaine; secondly, 1.0 percent of propylene glycol, 9.0 percent of glycerol, 1.0 percent of sodium chloride and 0.1 percent of sodium benzoate are added in sequence for dissolving and mixing evenly; finally, 0.1 percent of Yunnan paris polyphylla stem and leaf extract is added, 0.1 percent of prinsepia utilis royle oil is slowly added under the homogenization condition, and finally, deionized water is used for complementing to 100 percent and the mixture is evenly mixed.
A preparation method of shower gel containing paris polyphylla extract comprises the following steps:
(1) preparing the paris polyphylla root tuber extract: grinding the rhizoma paridis yunnanensis root tuber part into powder by a grinder, and sieving the powder with a 80-mesh sieve; secondly, heating and refluxing for 2h by using 60% ethanol solution (1:2), and then carrying out ultrasonic treatment for 1h for 2 times; finally, collecting the extracting solution for 2 times, and removing the solvent from the filtrate by a rotary evaporator to obtain a solvent-free paris polyphylla root tuber extract;
(2) preparing the shower gel: according to the weight percentage, 0.6 percent of hydroxypropyl methyl cellulose is dissolved by adding a proper amount of water at the temperature of 60 ℃, and then 5.0 percent of surfactant monolauryl phosphate is added to be dissolved at the temperature of 60 ℃; after cooling, 10.0 percent of cocamidopropyl betaine, 12.0 percent of disodium fatty alcohol polyoxyethylene ether sulfosuccinate, 4.0 percent of propylene glycol, 4.0 percent of glycerol, 1.5 percent of sodium chloride and 0.1 percent of sodium benzoate are sequentially added for dissolving and mixing evenly; and finally, adding 1.1% of paris polyphylla root tuber extract, 0.2% of lavender essence and 0.1% of lavender purple mica powder, slowly adding 0.5% of prinsepia utilis royle oil under the homogenization condition, adding 0.1% of sodium citrate, finally supplementing to 100% with deionized water, and uniformly mixing.
A preparation method of shower gel containing paris polyphylla extract comprises the following steps:
(1) preparing the paris polyphylla root tuber extract: grinding the rhizoma paridis yunnanensis root tuber part into powder by a grinder, and sieving the powder with a 80-mesh sieve; secondly, heating and refluxing for 2 times by using 95% ethanol solution, and each time lasts for 4 hours; finally, collecting the extracting solution for 2 times, and removing the solvent from the filtrate by a rotary evaporator to obtain a solvent-free paris polyphylla root tuber extract;
(2) preparing the shower gel: according to the weight percentage, 10.0 percent of monolauryl phosphate as a surfactant is added with a proper amount of water to be dissolved at the temperature of 60 ℃; after cooling, sequentially adding 5.0% of cocamidopropyl betaine, 2.0% of propylene glycol, 5.0% of glycerol, 1.5% of sodium chloride and 0.1% of sodium benzoate, and uniformly dissolving and mixing; finally, 2.0 percent of paris polyphylla root tuber extract is added, 0.2 percent of prinsepia utilis royle oil is slowly added under the homogenization condition, deionized water is used for complementing to 100 percent, and the mixture is uniformly mixed.
A preparation method of shower gel containing paris polyphylla extract comprises the following steps:
(1) preparing the Yunnan paris polyphylla stem and leaf extract: grinding the stem and leaf parts of the paris polyphylla into powder by a grinder, and sieving the powder by a 20-mesh sieve; secondly, heating and refluxing for 1h by using 50% ethanol solution, and then performing ultrasonic treatment for 1h for 3 times; finally, collecting the extracting solution for 3 times, and removing the solvent from the filtrate by a rotary evaporator to obtain solvent-free Yunnan rhizoma paridis stem and leaf extract;
(2) preparing the shower gel: according to the weight percentage, 2.0 percent of coconut monoethanolamide as a surfactant is added with a proper amount of water to be dissolved at the temperature of 60 ℃, then 0.8 percent of pearling agent ethylene glycol monostearate is added to be heated and dissolved at the temperature of 60 ℃, and if the dissolution is not thorough, a homogenizer is used for assisting the dissolution; after cooling, 6.0 percent of cocamidopropyl betaine, 9.0 percent of disodium fatty alcohol polyoxyethylene ether sulfosuccinate, 2.0 percent of propylene glycol, 5.0 percent of glycerol, 13.0 percent of sodium chloride and 0.1 percent of sodium benzoate are sequentially added and evenly mixed; finally, 1.1 percent of paris polyphylla stem and leaf extract is added, 1.0 percent of prinsepia utilis royle oil is slowly added under the homogenization condition, deionized water is used for complementing to 100 percent, and the mixture is uniformly mixed.
The medicinal materials used in the invention are as follows: yunnan rhizoma paridis medicinal material (origin: Lijiang Yunxin Green biological development Co., Ltd.); prinsepia utilis Royle oil (origin: Lijiang City, Yunnan province).
The auxiliary materials comprise a surfactant, a thickening agent, a pH regulator, a cosolvent, a preservative and other additives, wherein:
the surfactant is two or more of fatty alcohol polyoxyethylene ether sulfosuccinate monoester disodium (AEMES), monolauryl phosphate (MAP), lauryl alcohol ether phosphate potassium (MAEPK), Coconut Monoethanolamide (CMEA), cocamidopropyl betaine (CAB-35) and Cocamidopropyl Hydroxysulfobetaine (CHSB).
The thickening agent is one or more of hydroxypropyl methyl cellulose, carboxymethyl cellulose, sodium carboxymethyl starch, gum arabic, carbomer, guar gum and sodium chloride, and the addition range of the thickening agent is 0.1-2.0%.
The pH regulator is citric acid-sodium citrate, and the addition range of the pH regulator is properly added according to the required pH.
The cosolvent is one or a combination of propylene glycol, tween 80, glycerol and deionized water, the addition range of the cosolvent is adjusted according to actual conditions, and finally the deionized water is used for supplementing 100%.
The preservative is one or a combination of more of sodium benzoate, sorbic acid, benzoic acid and paraben, and the addition range of the preservative is 0.1-1.0%.
The other additives are pearling agent, aromatizing agent, opacifier, pigment, humectant, extract, antioxidant, etc. for regulating the appearance of the product. The other additives mainly increase the additional functions and market competitiveness of the product, and the addition range is 0-2%. The aromatizer is one or more of essence, spice and extract used for covering the odor of partial grease or surfactant in the matrix, enabling the product to emit fresh and pleasant aroma and increasing the use feeling of the product. The pearling agent is one or the combination of two of ethylene glycol monostearate and ethylene glycol distearate. The antioxidant is one or two of ethylene diamine tetraacetic acid and sodium sulfite.
The use method of the shower gel containing the paris polyphylla extract comprises the following steps:
firstly, the body skin is wetted by warm water, rich bubbles are made by the shower gel containing the paris polyphylla extract by means of a foaming tool and are spread on the whole body, then the skin is massaged by two hands properly, and finally, the bubbles on the body and the shower gel containing the paris polyphylla extract are thoroughly washed clean.
Compared with the prior art, the shower gel containing the paris polyphylla extract has the following advantages:
(1) according to the invention, the paris polyphylla extract is added into the formula, so that the shower gel has good antibacterial and disinfection effects. As paris polyphylla is widely used in folk for the treatment of various skin diseases and antibacterial functions (propionibacterium acnes, staphylococcus epidermidis, staphylococcus aureus, etc.) [ reference 8: yan Xiuhuang, Panqidong, Sun Haoyun, Gaolu, Yanrong, Yanglixin and Yunnan manyleaf paris rhizomeBasic research on application and traditional efficacy, journal of Chinese materia medica, 2021,1-12,https:// doi.org/10.19540/j.cnki.cjcmm.20210901.101network initiation]The bath lotion can be used for improving the skin state, relieving or even radically treating slight skin diseases, red swelling caused by mosquito bites and the like after long-term use, and has mild properties, antibacterial and disinfection effects, small irritation to the skin and good using effect.
(2) The Paris polyphylla (Paris polyphylla Smith var. yunnanensis (Franch.) hand. -Mazz.) used by the invention is provided by Lijiang Xinxin Green biological development Co., Ltd., and the raw materials are detected according to a detection method provided by pharmacopeia, so that the content of total saponins is far higher than 0.60%. The compound having the main medicinal function in the paris polyphylla is a saponin compound, and the paris polyphylla extract used in the invention is extracted by ethanol, is consistent with a pharmacopeia method, has high saponin content and can achieve the optimal medicinal function of the paris polyphylla.
(3) According to the invention, the prinsepia utilis royle oil is added in the formula, and due to good skin care and antibacterial activity [ references 4, 5 and 6], the prinsepia utilis royle oil has good cleaning effect by using the similarity and intermiscibility of the oil during bathing; secondly, after bathing, the prinsepia utilis royle oil can be adhered to the surface of the skin, so that the water locking and moisturizing effects are good, the stimulation effect on the skin is small, and the using effect is good.
Drawings
FIG. 1 is the report of the detection of the total saponin content in the extract of Paris polyphylla of the present invention.
Detailed Description
The invention will be further explained with reference to specific embodiments in the following description, with reference to the drawings. It should be understood that the embodiments described herein are only for explaining the present invention, and are not intended to limit the technical solutions of the present invention.
Example 1
A bath lotion containing extract of Parispyphyllia Smith var. yunnanensis (Franch.) hand. -Mazz) and its preparation method comprises the following steps:
(1) preparing the Yunnan paris polyphylla stem and leaf extract: grinding the stem and leaf parts of the paris polyphylla into powder by a grinder, and sieving the powder by a 40-mesh sieve; secondly, heating and refluxing for 3 times with 80% ethanol solution (1:10) for 2h each time; finally, collecting the extracting solution for 3 times, and removing the solvent from the filtrate by a rotary evaporator to obtain solvent-free Yunnan rhizoma paridis stem and leaf extract;
(2) the preparation method of the shower gel comprises the following steps: mixing surfactant cocamidopropyl betaine (CAB-35, 10.0%), potassium lauryl alcohol ether phosphate (MAEPK, 8.0%), and cocamidopropyl hydroxysulfobetaine (CHSB, 7.0%); secondly, sequentially adding propylene glycol (1.0%), glycerol (9.0%), sodium chloride (1.0%) and sodium benzoate (0.1%) to dissolve and mix uniformly; and finally, adding the paris polyphylla stem and leaf extract (0.1%), slowly adding the prinsepia utilis royle oil (0.1%) under the homogenization condition, finally, complementing the obtained mixture to 100% with deionized water, and uniformly mixing to obtain the shower gel containing the paris polyphylla extract.
Example 2
A bath lotion containing extract of Paris polyphylla (Paris polyphylla Smith var. yunnanensis (Franch.) hand. -Mazz.) and its preparation method comprises the following steps:
(1) preparing the Yunnan paris polyphylla stem and leaf extract: grinding the stem and leaf parts of the paris polyphylla into powder by a grinder, and sieving the powder by a 80-mesh sieve; secondly, heating and refluxing for 2 times with 95% ethanol solution (1:20) for 5 hours each time; finally, collecting the extracting solution for 2 times, and removing the solvent from the filtrate by a rotary evaporator to obtain solvent-free paris polyphylla stem and leaf extract;
(2) the preparation method of the shower gel comprises the following steps: dissolving hydroxypropyl methylcellulose (0.5%) in appropriate amount of water at 60 deg.C, adding surfactant monolauryl phosphate (MAP, 5.0%) and dissolving at 60 deg.C; after cooling, adding cocamidopropyl betaine (CAB-35, 10.0%), potassium lauryl alcohol ether phosphate (MAEPK, 4.0%), propylene glycol (1.0%), glycerol (6.0%), sodium chloride (1.5%) and sodium benzoate (0.1%) in sequence, dissolving and mixing uniformly; and finally, adding 2.0 percent of paris polyphylla stem and leaf extract, slowly adding 0.5 percent of prinsepia utilis royle oil under the homogenization condition, finally, complementing the mixture to 100 percent by deionized water, and uniformly mixing to obtain the shower gel containing the paris polyphylla extract.
Example 3
A bath lotion containing extract of Paris polyphylla (Paris polyphylla Smith var. yunnanensis (Franch.) hand. -Mazz.) and its preparation method comprises the following steps:
(1) preparing the Yunnan paris polyphylla stem and leaf extract: grinding the stem and leaf parts of the paris polyphylla into powder by a grinder, and sieving the powder by a 20-mesh sieve; secondly, heating and refluxing for 1h by using 50% ethanol solution (1:2), and then carrying out ultrasonic treatment for 1h for 3 times; finally, collecting the extracting solution for 3 times, and removing the solvent from the filtrate by a rotary evaporator to obtain solvent-free Yunnan rhizoma paridis stem and leaf extract;
(2) the preparation method of the shower gel comprises the following steps: dissolving surfactant cocoanut oil acid monoethanolamide (CMEA, 2.0%) in water at 60 deg.C, adding pearling agent (ethylene glycol monostearate, 0.8%) at 60 deg.C, heating to dissolve, and dissolving with homogenizer if dissolution is not complete; after cooling, adding cocamidopropyl betaine (CAB-35, 6.0%), disodium fatty alcohol polyoxyethylene ether sulfosuccinate (AEMES, 9.0%), propylene glycol (2.0%), glycerol (5.0%), sodium chloride (13.0%) and sodium benzoate (0.1%) in sequence, and mixing uniformly; and finally, adding the paris polyphylla stem and leaf extract (1.1%), slowly adding the prinsepia utilis royle oil (1.0%) under the homogenization condition, complementing the rest materials to 100% by using deionized water, and uniformly mixing to obtain the shower gel containing the paris polyphylla extract.
Example 4
A bath lotion containing extract of Paris polyphylla (Paris polyphylla Smith var. yunnanensis (Franch.) hand. -Mazz.) and its preparation method comprises the following steps:
(1) preparing the paris polyphylla root tuber extract: preparing the paris polyphylla root tuber extract: grinding the rhizoma paridis yunnanensis root tuber part into powder by a grinder, and sieving the powder by a 40-mesh sieve; secondly, heating and refluxing for 3 times with 75% ethanol solution (1:10) for 3 hours each time; finally, collecting the extracting solution for 3 times, and removing the solvent from the filtrate by a rotary evaporator to obtain a solvent-free paris polyphylla root tuber extract;
(2) the preparation method of the shower gel comprises the following steps: dissolving hydroxypropyl methylcellulose (0.5%) in appropriate amount of water at 60 deg.C, cooling, sequentially adding potassium lauryl alcohol ether phosphate (MAEPK, 12.0%) and cocamidopropyl hydroxysulfobetaine (CHSB, 10.0%), and mixing; secondly, sequentially adding propylene glycol (2.0%), glycerol (5.0%), sodium benzoate (0.1%) and rose essence (0.2%) and uniformly mixing; and finally, adding the paris polyphylla root tuber extract (0.1%), slowly adding the prinsepia utilis royle oil (0.2%), the citric acid (0.1%) and deionized water to complement to 100% under the homogenizing condition, and uniformly mixing to obtain the shower gel containing the paris polyphylla extract.
Example 5
A bath lotion containing extract of Paris polyphylla (Paris polyphylla Smith var. yunnanensis (Franch.) hand. -Mazz.) and its preparation method comprises the following steps:
(1) preparing the paris polyphylla root tuber extract: preparing the paris polyphylla root tuber extract: grinding the rhizoma paridis yunnanensis root tuber part into powder by a grinder, and sieving the powder with a 80-mesh sieve; secondly, heating and refluxing for 2 times with 95% ethanol solution (1:15) for 4 hours each time; finally, collecting the extracting solution for 2 times, and removing the solvent from the filtrate by a rotary evaporator to obtain a solvent-free paris polyphylla root tuber extract;
(2) the preparation method of the shower gel comprises the following steps: dissolving surfactant monolauryl phosphate (MAP, 10.0%) in appropriate amount of water at 60 deg.C; after cooling, adding cocamidopropyl betaine (CAB-35, 5.0%), propylene glycol (2.0%), glycerol (5.0%), sodium chloride (1.5%) and sodium benzoate (0.1%) in sequence, dissolving and mixing uniformly; and finally, adding the paris polyphylla root tuber extract (2.0%), slowly adding the prinsepia utilis royle oil (0.2%) under the homogenization condition, complementing the rest materials to 100% by using deionized water, and uniformly mixing to obtain the shower gel containing the paris polyphylla extract.
Example 6
A bath lotion containing extract of Paris polyphylla (Paris polyphylla Smith var. yunnanensis (Franch.) hand. -Mazz.) and its preparation method comprises the following steps:
(1) preparing the paris polyphylla root tuber extract: preparing the paris polyphylla root tuber extract: grinding the rhizoma paridis yunnanensis root tuber part into powder by a grinder, and sieving the powder with a 80-mesh sieve; secondly, heating and refluxing for 2h by using 60% ethanol solution (1:2), and then carrying out ultrasonic treatment for 1h for 2 times; finally, collecting the extracting solution for 2 times, and removing the solvent from the filtrate by a rotary evaporator to obtain a solvent-free paris polyphylla root tuber extract;
(2) the preparation method of the shower gel comprises the following steps: dissolving hydroxypropyl methylcellulose (0.6%) in appropriate amount of water at 60 deg.C, adding surfactant monolauryl phosphate (MAP, 5.0%) and dissolving at 60 deg.C; after cooling, adding cocamidopropyl betaine (CAB-35, 10.0%), disodium fatty alcohol polyoxyethylene ether sulfosuccinate (AEMES, 12.0%), propylene glycol (4.0%), glycerol (4.0%), sodium chloride (1.5%) and sodium benzoate (0.1%) in sequence, dissolving and mixing uniformly; and finally, adding the paris polyphylla root tuber extract (1.1%), lavender essence (0.2%) and lavender purple mica powder (0.1%), slowly adding the prinsepia utilis royle oil (0.5%) under the homogenization condition, adding sodium citrate (0.1%), finally supplementing to 100% with deionized water, and uniformly mixing to obtain the shower gel containing the paris polyphylla extract.
The average data of the total saponins content of the paris polyphylla extracted by the method disclosed by the invention is far more than 0.6% specified in Chinese pharmacopoeia (2020 edition). The content of total saponins (rhizoma paridis saponin I, rhizoma paridis saponin II, rhizoma paridis saponin VII) detected recently (rhizoma paridis extract extracted in example 6) was 1.5973% (see figure 1 for detection report).
Claims (10)
1. The shower gel containing the paris polyphylla extract is characterized by consisting of the paris polyphylla extract, prinsepia utilis royle oil and conventional shower gel auxiliary materials, wherein the paris polyphylla extract is 0.1-2.0 percent, the prinsepia utilis royle oil is 0.1-1.0 percent, the auxiliary materials are added in the addition range of the conventional shower gel auxiliary materials, the balance is made up to 100 percent by deionized water, and the total saponin content in the paris polyphylla extract is higher than 0.60 percent.
2. The shower gel containing the paris polyphylla extract as claimed in claim 1, wherein the paris polyphylla extract is extracted from paris polyphyllaThe extract is one or two of rhizoma paridis extract, and caulis et folium Parthenocissi Tricuspidatae extract; the rhizoma paridis extract is prepared from dried root tuber, and is determined by the method specified in Chinese pharmacopoeia (2020 edition) to limit the content of rhizoma paridis saponin I (C)44H70O16) Rhizoma paridis Saponin II (C)51H82O20) And rhizoma paridis saponin VII (C)51H82O21) The total amount of (A) should not be less than 0.60%; the raw material used by the paris polyphylla stem and leaf extract is the overground stem and leaf part which is directly discarded after the seeds are harvested every year.
3. A shower gel containing paris polyphylla extract is characterized by being prepared according to the following method:
dissolving a solid thickening agent as an auxiliary material for a shower gel routine in a proper amount of water at 40-60 ℃, adding a solid surfactant to dissolve the solid thickening agent, cooling, adding a liquid surfactant, a cosolvent, an antioxidant, a preservative and other additives, uniformly mixing, adding the paris polyphylla extract and prinsepia utilis royle oil, uniformly mixing, measuring the pH value, adding a pH regulator as required to adjust the pH value, and uniformly mixing, wherein the total saponin content in the paris polyphylla extract is higher than 0.60%.
4. A shower gel containing paris polyphylla extract is characterized by being prepared according to the following method:
(1) grinding the medicinal part tuber root of the paris polyphylla or the waste overground part stem leaves of the paris polyphylla in each year into powder by a grinder and a grinder, and sieving the powder by a sieve of 20-80 meshes;
(2) extracting with 50-100% ethanol solution, heating and refluxing, and ultrasonic extracting for 2-3 times (each time for 1-5 hr) at a material-to-liquid ratio of 1:2-1: 20;
(3) filtering the extractive solution, enriching the filtrate, and removing solvent by rotary evaporator to obtain solvent-free extract of rhizoma paridis Yunnanensis; the content of total saponins in the rhizoma paridis Yunnanensis extract is higher than 0.60%.
5. The method for preparing a shower gel containing a paris polyphylla extract as claimed in claim 1 or 2, which comprises the steps of:
(1) grinding the medicinal part tuber root of the paris polyphylla or the waste overground part stem leaves of the paris polyphylla in each year into powder by a grinder and a grinder, and sieving the powder by a sieve of 20-80 meshes;
(2) extracting with 50-100% ethanol solution, heating and refluxing, and ultrasonic extracting for 2-3 times (each time for 1-5 hr) at a material-to-liquid ratio of 1:2-1: 20;
(3) filtering each extractive solution, enriching filtrate, and removing solvent by rotary evaporator to obtain solvent-free extract of rhizoma paridis Yunnanensis.
6. The method for preparing a shower gel containing a paris polyphylla extract as claimed in claim 1 or 2, which comprises the following steps: dissolving the conventional solid thickening agent as adjuvant in water at 40-60 deg.C, adding solid surfactant to dissolve, cooling, adding liquid surfactant, cosolvent, antioxidant, antiseptic, and other additives, mixing, adding rhizoma paridis Yunnanensis extract and Prinsepia utilis oil, mixing, measuring pH, adding pH regulator as required, and mixing.
7. A preparation method of shower gel containing paris polyphylla extract is characterized by comprising the following steps:
(1) preparing the Yunnan paris polyphylla stem and leaf extract: grinding the stem and leaf parts of the paris polyphylla into powder by a grinder, and sieving the powder by a 40-mesh sieve; secondly, heating and refluxing for 3 times with 80% ethanol solution, and each time for 2 h; finally, collecting the extracting solution for 3 times, and removing the solvent from the filtrate by a rotary evaporator to obtain solvent-free Yunnan rhizoma paridis stem and leaf extract;
(2) preparing the shower gel: mixing surfactant 10.0 wt% of cocamidopropyl betaine, 8.0 wt% of potassium lauryl alcohol ether phosphate and 7.0 wt% of cocamidopropyl hydroxysulfobetaine; secondly, 1.0 percent of propylene glycol, 9.0 percent of glycerol, 1.0 percent of sodium chloride and 0.1 percent of sodium benzoate are added in sequence for dissolving and mixing evenly; finally, 0.1 percent of Yunnan paris polyphylla stem and leaf extract is added, 0.1 percent of prinsepia utilis royle oil is slowly added under the homogenization condition, and finally, deionized water is used for complementing to 100 percent and the mixture is evenly mixed.
8. A preparation method of shower gel containing paris polyphylla extract is characterized by comprising the following steps:
(1) preparing the paris polyphylla root tuber extract: grinding the rhizoma paridis yunnanensis root tuber part into powder by a grinder, and sieving the powder with a 80-mesh sieve; secondly, heating and refluxing for 2h by using 60% ethanol solution (1:2), and then carrying out ultrasonic treatment for 1h for 2 times; finally, collecting the extracting solution for 2 times, and removing the solvent from the filtrate by a rotary evaporator to obtain a solvent-free paris polyphylla root tuber extract;
(2) preparing the shower gel: according to the weight percentage, 0.6 percent of hydroxypropyl methyl cellulose is dissolved by adding a proper amount of water at the temperature of 60 ℃, and then 5.0 percent of surfactant monolauryl phosphate is added to be dissolved at the temperature of 60 ℃; after cooling, 10.0 percent of cocamidopropyl betaine, 12.0 percent of disodium fatty alcohol polyoxyethylene ether sulfosuccinate, 4.0 percent of propylene glycol, 4.0 percent of glycerol, 1.5 percent of sodium chloride and 0.1 percent of sodium benzoate are sequentially added for dissolving and mixing evenly; and finally, adding 1.1% of paris polyphylla root tuber extract, 0.2% of lavender essence and 0.1% of lavender purple mica powder, slowly adding 0.5% of prinsepia utilis royle oil under the homogenization condition, adding 0.1% of sodium citrate, finally supplementing to 100% with deionized water, and uniformly mixing.
9. A preparation method of shower gel containing paris polyphylla extract is characterized by comprising the following steps:
(1) preparing the paris polyphylla root tuber extract: grinding the rhizoma paridis yunnanensis root tuber part into powder by a grinder, and sieving the powder with a 80-mesh sieve; secondly, heating and refluxing for 2 times by using 95% ethanol solution, and each time lasts for 4 hours; finally, collecting the extracting solution for 2 times, and removing the solvent from the filtrate by a rotary evaporator to obtain a solvent-free paris polyphylla root tuber extract;
(2) preparing the shower gel: according to the weight percentage, 10.0 percent of monolauryl phosphate as a surfactant is added with a proper amount of water to be dissolved at the temperature of 60 ℃; after cooling, sequentially adding 5.0% of cocamidopropyl betaine, 2.0% of propylene glycol, 5.0% of glycerol, 1.5% of sodium chloride and 0.1% of sodium benzoate, and uniformly dissolving and mixing; finally, 2.0 percent of paris polyphylla root tuber extract is added, 0.2 percent of prinsepia utilis royle oil is slowly added under the homogenization condition, deionized water is used for complementing to 100 percent, and the mixture is uniformly mixed.
10. A preparation method of shower gel containing paris polyphylla extract is characterized by comprising the following steps:
(1) preparing the Yunnan paris polyphylla stem and leaf extract: grinding the stem and leaf parts of the paris polyphylla into powder by a grinder, and sieving the powder by a 20-mesh sieve; secondly, heating and refluxing for 1h by using 50% ethanol solution, and then performing ultrasonic treatment for 1h for 3 times; finally, collecting the extracting solution for 3 times, and removing the solvent from the filtrate by a rotary evaporator to obtain solvent-free Yunnan rhizoma paridis stem and leaf extract;
(2) preparing the shower gel: according to the weight percentage, 2.0 percent of coconut monoethanolamide as a surfactant is added with a proper amount of water to be dissolved at the temperature of 60 ℃, then 0.8 percent of pearling agent ethylene glycol monostearate is added to be heated and dissolved at the temperature of 60 ℃, and if the dissolution is not thorough, a homogenizer is used for assisting the dissolution; after cooling, 6.0 percent of cocamidopropyl betaine, 9.0 percent of disodium fatty alcohol polyoxyethylene ether sulfosuccinate, 2.0 percent of propylene glycol, 5.0 percent of glycerol, 13.0 percent of sodium chloride and 0.1 percent of sodium benzoate are sequentially added and evenly mixed; finally, 1.1 percent of paris polyphylla stem and leaf extract is added, 1.0 percent of prinsepia utilis royle oil is slowly added under the homogenization condition, deionized water is used for complementing to 100 percent, and the mixture is uniformly mixed.
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Citations (3)
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|---|---|---|---|---|
| CN102406576A (en) * | 2011-10-28 | 2012-04-11 | 何黎 | Prinsepia utilis Royle oil-containing functional skin care product and preparation method thereof |
| WO2018184250A1 (en) * | 2017-04-08 | 2018-10-11 | 格兰比圣（深圳）科技有限公司 | Body wash and preparation method therefor |
| CN112618463A (en) * | 2021-01-19 | 2021-04-09 | 北京圣永制药有限公司 | Bacteriostatic skin-care bath foam containing traditional Chinese medicine extract |
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- 2021-12-21 CN CN202111565989.7A patent/CN114191359A/en active Pending
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|---|---|---|---|---|
| CN102406576A (en) * | 2011-10-28 | 2012-04-11 | 何黎 | Prinsepia utilis Royle oil-containing functional skin care product and preparation method thereof |
| WO2018184250A1 (en) * | 2017-04-08 | 2018-10-11 | 格兰比圣（深圳）科技有限公司 | Body wash and preparation method therefor |
| CN112618463A (en) * | 2021-01-19 | 2021-04-09 | 北京圣永制药有限公司 | Bacteriostatic skin-care bath foam containing traditional Chinese medicine extract |
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