CN113925810A - Whitening and blue light resisting composition, mask and preparation method of mask - Google Patents
Whitening and blue light resisting composition, mask and preparation method of mask Download PDFInfo
- Publication number
- CN113925810A CN113925810A CN202111230630.4A CN202111230630A CN113925810A CN 113925810 A CN113925810 A CN 113925810A CN 202111230630 A CN202111230630 A CN 202111230630A CN 113925810 A CN113925810 A CN 113925810A
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- whitening
- butanediol
- blue
- light
- water
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- 239000000203 mixture Substances 0.000 title claims abstract description 83
- 230000002087 whitening effect Effects 0.000 title claims abstract description 75
- 238000002360 preparation method Methods 0.000 title claims abstract description 12
- 239000006166 lysate Substances 0.000 claims abstract description 31
- 238000000855 fermentation Methods 0.000 claims abstract description 27
- 230000004151 fermentation Effects 0.000 claims abstract description 27
- 241001673954 Magnolia sieboldii Species 0.000 claims abstract description 26
- 235000017587 Medicago sativa ssp. sativa Nutrition 0.000 claims abstract description 26
- JKMHFZQWWAIEOD-UHFFFAOYSA-N 2-[4-(2-hydroxyethyl)piperazin-1-yl]ethanesulfonic acid Chemical compound OCC[NH+]1CCN(CCS([O-])(=O)=O)CC1 JKMHFZQWWAIEOD-UHFFFAOYSA-N 0.000 claims abstract description 18
- ZGSCRDSBTNQPMS-UJURSFKZSA-N 3-O-Ethylascorbic acid Chemical compound CCOC1=C(O)C(=O)O[C@@H]1[C@@H](O)CO ZGSCRDSBTNQPMS-UJURSFKZSA-N 0.000 claims abstract description 18
- SCVVSSZVLZQUDZ-UHFFFAOYSA-N 3-methyl-2,6-dihydro-1H-pyrimidine-2-carboxylic acid Chemical compound CN1C(NCC=C1)C(=O)O SCVVSSZVLZQUDZ-UHFFFAOYSA-N 0.000 claims abstract description 14
- 229940120145 3-o-ethylascorbic acid Drugs 0.000 claims abstract description 14
- CBTVGIZVANVGBH-UHFFFAOYSA-N aminomethyl propanol Chemical compound CC(C)(N)CO CBTVGIZVANVGBH-UHFFFAOYSA-N 0.000 claims abstract description 14
- 229940089468 hydroxyethylpiperazine ethane sulfonic acid Drugs 0.000 claims abstract description 14
- 240000004658 Medicago sativa Species 0.000 claims abstract description 8
- DFPAKSUCGFBDDF-ZQBYOMGUSA-N [14c]-nicotinamide Chemical compound N[14C](=O)C1=CC=CN=C1 DFPAKSUCGFBDDF-ZQBYOMGUSA-N 0.000 claims abstract description 7
- 240000004808 Saccharomyces cerevisiae Species 0.000 claims abstract description 6
- CDQSJQSWAWPGKG-UHFFFAOYSA-N butane-1,1-diol Chemical compound CCCC(O)O CDQSJQSWAWPGKG-UHFFFAOYSA-N 0.000 claims description 84
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 63
- 241000219823 Medicago Species 0.000 claims description 25
- 150000001875 compounds Chemical class 0.000 claims description 20
- TXFPEBPIARQUIG-UHFFFAOYSA-N 4'-hydroxyacetophenone Chemical group CC(=O)C1=CC=C(O)C=C1 TXFPEBPIARQUIG-UHFFFAOYSA-N 0.000 claims description 18
- DFPAKSUCGFBDDF-UHFFFAOYSA-N Nicotinamide Chemical compound NC(=O)C1=CC=CN=C1 DFPAKSUCGFBDDF-UHFFFAOYSA-N 0.000 claims description 18
- 239000003906 humectant Substances 0.000 claims description 17
- 239000002562 thickening agent Substances 0.000 claims description 17
- 239000003963 antioxidant agent Substances 0.000 claims description 16
- 230000003078 antioxidant effect Effects 0.000 claims description 16
- 235000006708 antioxidants Nutrition 0.000 claims description 16
- 239000002738 chelating agent Substances 0.000 claims description 16
- 125000003118 aryl group Chemical group 0.000 claims description 14
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- 239000003755 preservative agent Substances 0.000 claims description 12
- 230000002335 preservative effect Effects 0.000 claims description 12
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 claims description 11
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 11
- NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 claims description 11
- 229920002385 Sodium hyaluronate Polymers 0.000 claims description 11
- 229920006037 cross link polymer Polymers 0.000 claims description 11
- 229960003966 nicotinamide Drugs 0.000 claims description 11
- 235000005152 nicotinamide Nutrition 0.000 claims description 11
- 239000011570 nicotinamide Substances 0.000 claims description 11
- 229940010747 sodium hyaluronate Drugs 0.000 claims description 11
- YWIVKILSMZOHHF-QJZPQSOGSA-N sodium;(2s,3s,4s,5r,6r)-6-[(2s,3r,4r,5s,6r)-3-acetamido-2-[(2s,3s,4r,5r,6r)-6-[(2r,3r,4r,5s,6r)-3-acetamido-2,5-dihydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-2-carboxy-4,5-dihydroxyoxan-3-yl]oxy-5-hydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-3,4,5-trihydroxyoxane-2- Chemical compound [Na+].CC(=O)N[C@H]1[C@H](O)O[C@H](CO)[C@@H](O)[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@H](O[C@H]2[C@@H]([C@@H](O[C@H]3[C@@H]([C@@H](O)[C@H](O)[C@H](O3)C(O)=O)O)[C@H](O)[C@@H](CO)O2)NC(C)=O)[C@@H](C(O)=O)O1 YWIVKILSMZOHHF-QJZPQSOGSA-N 0.000 claims description 11
- 229920001285 xanthan gum Polymers 0.000 claims description 11
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- 229940082509 xanthan gum Drugs 0.000 claims description 11
- 235000010493 xanthan gum Nutrition 0.000 claims description 11
- 241001530056 Athelia rolfsii Species 0.000 claims description 10
- 241000235347 Schizosaccharomyces pombe Species 0.000 claims description 10
- 238000001816 cooling Methods 0.000 claims description 9
- QCDWFXQBSFUVSP-UHFFFAOYSA-N 2-phenoxyethanol Chemical group OCCOC1=CC=CC=C1 QCDWFXQBSFUVSP-UHFFFAOYSA-N 0.000 claims description 8
- ANZUDYZHSVGBRF-UHFFFAOYSA-N 3-ethylnonane-1,2,3-triol Chemical compound CCCCCCC(O)(CC)C(O)CO ANZUDYZHSVGBRF-UHFFFAOYSA-N 0.000 claims description 8
- 239000003921 oil Substances 0.000 claims description 8
- 229960005323 phenoxyethanol Drugs 0.000 claims description 8
- 235000010624 Medicago sativa Nutrition 0.000 claims description 7
- 244000181025 Rosa gallica Species 0.000 claims description 7
- 239000002537 cosmetic Substances 0.000 claims description 7
- 150000002148 esters Chemical class 0.000 claims description 7
- LXAHHHIGZXPRKQ-UHFFFAOYSA-N 5-fluoro-2-methylpyridine Chemical group CC1=CC=C(F)C=N1 LXAHHHIGZXPRKQ-UHFFFAOYSA-N 0.000 claims description 4
- 238000004321 preservation Methods 0.000 claims description 4
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- 239000003109 Disodium ethylene diamine tetraacetate Substances 0.000 description 5
- ZGTMUACCHSMWAC-UHFFFAOYSA-L EDTA disodium salt (anhydrous) Chemical group [Na+].[Na+].OC(=O)CN(CC([O-])=O)CCN(CC(O)=O)CC([O-])=O ZGTMUACCHSMWAC-UHFFFAOYSA-L 0.000 description 5
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- WQXNXVUDBPYKBA-YFKPBYRVSA-N ectoine Chemical compound CC1=[NH+][C@H](C([O-])=O)CCN1 WQXNXVUDBPYKBA-YFKPBYRVSA-N 0.000 description 4
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- PUPZLCDOIYMWBV-UHFFFAOYSA-N (+/-)-1,3-Butanediol Chemical compound CC(O)CCO PUPZLCDOIYMWBV-UHFFFAOYSA-N 0.000 description 1
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Images
Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/41—Amines
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
- A61K8/4953—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom containing pyrimidine ring derivatives, e.g. minoxidil
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/673—Vitamin B group
- A61K8/675—Vitamin B3 or vitamin B3 active, e.g. nicotinamide, nicotinic acid, nicotinyl aldehyde
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
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- A61K8/676—Ascorbic acid, i.e. vitamin C
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9728—Fungi, e.g. yeasts
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- A—HUMAN NECESSITIES
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- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
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- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A—HUMAN NECESSITIES
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
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- Biotechnology (AREA)
- Engineering & Computer Science (AREA)
- Emergency Medicine (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a whitening and blue light resisting composition, a mask and a preparation method thereof. The whitening anti-blue-light composition comprises the following components in percentage by weight: hydroxyethyl piperazine ethanesulfonic acid, nicotinamide, aminomethyl propanol, a yeast fermentation lysate of Schizosaccharomyces cerevisiae, alfalfa extract, 3-o-ethyl ascorbic acid, tetrahydro methyl pyrimidine carboxylic acid, Magnolia sieboldii extract. The whitening blue-light-resistant composition disclosed by the invention is whitening and blue-light-resistant, and has a remarkable effect.
Description
Technical Field
The invention relates to the technical field of cosmetics, and particularly relates to a whitening and blue light resisting composition, a mask and a preparation method of the mask.
Background
Skin aging includes physiological aging and photoaging. The wavelengths of the ultraviolet light, the visible light and the infrared light are sequentially from short to long. Compared with ultraviolet rays, visible light has stronger penetrating power and can reach the dermis of human skin, so that the visible light can cause deeper damage to the skin. The visible light is composed of seven colors of light such as purple, blue, cyan, green, yellow, orange, red and the like, wherein the energy of the blue light wave band with the wavelength of 400-500 nm is the highest, and the harm to human bodies is the greatest. Blue light can penetrate into the dermis of skin, mitochondria in cells can generate active oxygen free radicals under the irradiation of the blue light, and the active oxygen free radicals can generate oxidation reaction with the mitochondria, DNA and cell structures containing lipid to damage the mitochondria and the DNA, cause cell membrane dysfunction, influence the growth and development of the cells, damage the cell structures, cause cell damage to cause apoptosis, and lead to the premature aging of the skin. Currently, anti-blue light products have become a research hotspot in the cosmetic field.
Disclosure of Invention
The invention aims to overcome the defects in the prior art and provide a whitening anti-blue-light composition.
The invention also aims to provide a whitening blue-light-resistant facial mask containing the whitening blue-light-resistant composition.
The invention further aims to provide a preparation method of the whitening blue-light-resistant mask.
The purpose of the invention is realized by the following technical scheme: a whitening anti-blue-light composition comprises the following components in percentage by weight: hydroxyethylpiperazineethanesulfonic acid, nicotinamide, aminomethylpropanol, a Saccharomyces bifidus fermentation product lysate, Medicago SATIVA (MEDICAGO SATIVA) extract, 3-o-ethyl ascorbic acid, tetrahydro-methylpyrimidine carboxylic acid, and Magnolia sieboldii (MAGNOLIASIEBELBII) extract.
Preferably, the whitening blue-light-resistant composition further comprises an auxiliary material compounded with the active substances: the lysate of the secondary fission yeast fermentation product is compounded with butanediol; compounding the alfalfa extract with butanediol and water; the magnolia sieboldii extract is compounded with butanediol and water.
Preferably, in the whitening blue-light resistant composition, the components are calculated according to the following weight percentage: 4 to 6 percent of hydroxyethyl piperazine ethane sulfonic acid, 18 to 24 percent of nicotinamide, 0.8 to 1.3 percent of aminomethyl propanol, 35 to 47 percent of a compound of a schizosaccharomyces cerevisiae fermentation product lysate and butanediol, 8 to 10 percent of a compound of alfalfa extract, butanediol and water, 4 to 12 percent of 3-o-ethyl ascorbic acid, 0.4 to 1 percent of tetrahydro-methyl pyrimidine carboxylic acid, and 11 to 14 percent of a compound of a magnolia sieboldii extract, butanediol and water; more preferably, 4.5% of hydroxyethyl piperazine ethanesulfonic acid, 22.5% of nicotinamide, 0.9% of aminomethyl propanol, 45% of a mixture of a schizosaccharomyces cerevisiae fermentation product lysate and butanediol, 9% of a mixture of alfalfa extract, butanediol and water, 5% of 3-o-ethyl ascorbic acid, 0.7% of tetrahydro-methyl pyrimidine carboxylic acid and 13.5% of a mixture of magnolia sieboldii extract, butanediol and water.
Preferably, the weight percentage of the two in the compound of the schizosaccharomyces cerevisiae fermentation product lysate and butanediol is 25% -30% and 70% -75% in sequence.
Preferably, the weight percentages of the alfalfa extract, the butanediol and the water in the compound are 4.5-5%, 45-50% and 40-45% in sequence.
Preferably, in the complex of the magnolia sieboldii extract, the butanediol and the water, the weight percentages of the magnolia sieboldii extract, the butanediol and the water are 0.4-0.5%, 39.5-45.5% and 54-60.1% in sequence.
The whitening anti-blue-light composition is applied to the preparation of cosmetics.
The cosmetic comprises lotion, cream, spray, essence and essential oil.
Preferably, the whitening anti-blue light composition is added into the cosmetic in an amount of 1-25 wt%.
The whitening anti-blue-light facial mask comprises the following components in percentage by weight: 10-25% of whitening blue-light resistant composition, 5-9% of humectant, 0.3-0.5% of antioxidant, 0.01-0.03% of chelating agent, 0.1-0.45% of thickening agent, 0.1-0.4% of preservative, 0.001-0.005% of aromatic and the balance of water; preferably, the composition comprises the following components in percentage by weight: 16-23% of whitening blue-light resistant composition, 7-9% of humectant, 0.5% of antioxidant, 0.03% of chelating agent, 0.45% of thickening agent, 0.4% of preservative, 0.005% of aromatic and the balance of water; more preferably, the composition comprises the following components in percentage by weight: 22.35% of whitening blue-light resistant composition, 7.1% of humectant, 0.5% of antioxidant, 0.03% of chelating agent, 0.45% of thickening agent, 0.4% of preservative, 0.005% of aromatic and the balance of water.
Preferably, the humectant is butanediol, polyglycerol-10, sodium hyaluronate; more preferably, the weight percentages of the three are as follows: 4 to 6 percent of butanediol, 101.5 to 3 percent of polyglycerol and 0.05 to 0.1 percent of sodium hyaluronate.
Preferably, the thickener is xanthan gum, hydrolyzed SCLEROTIUM rolfsii (scleritium rolfsii) gum, acrylic acid/C10-30 alkanol acrylate crosspolymer; more preferably, the weight percentages of the three are as follows: 0.08 to 0.2 percent of xanthan gum, 0.03 to 0.05 percent of hydrolyzed sclerotium rolfsii gum and 0.1 to 0.2 percent of acrylic acid (ester)/C10 to 30 alkanol acrylate cross-linked polymer.
Preferably, the antioxidant is p-hydroxyacetophenone.
Preferably, the chelating agent is disodium EDTA.
Preferably, the preservative is phenoxyethanol or ethylhexyl glycerol.
Preferably, the fragrance is rosebush (rosamascena) flower oil.
The preparation method of the whitening blue-light-resistant mask comprises the following steps:
(1) mixing butanediol, polyglycerol-10, sodium hyaluronate, xanthan gum, hydrolyzed sclerotium rolfsii gum, acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, p-hydroxyacetophenone, EDTA disodium and water, homogenizing at 82-85 ℃, and preserving heat to obtain a mixture A;
(2) cooling the mixture A obtained in the step (1) to 60-65 ℃, and vacuumizing and mixing the mixture A with hydroxyethyl piperazine ethanesulfonic acid, nicotinamide and aminomethyl propanol in the whitening blue-light-resistant composition to obtain a mixture B;
(3) cooling the mixture B in the step (2) to 40-42 ℃, and mixing the mixture B with a composition of a cracked yeast fermentation product lysate and butanediol and a composition of a medicago sativa extract, butanediol and water in the whitening blue-light resistant composition to obtain a mixture C;
(4) and (3) cooling the mixture C obtained in the step (3) to 35-38 ℃, and mixing the mixture C with 3-o-ethyl ascorbic acid, tetrahydro-methyl pyrimidine carboxylic acid, a compound of magnolia sieboldii extract, butanediol and water, phenoxyethanol, ethylhexyl glycerol and rosa damascena flower oil in the whitening and blue light resisting composition to obtain the whitening and blue light resisting mask.
Preferably, the homogenization in the step (1) adopts a stirring mode.
Preferably, the heat preservation in the step (1) is stirring heat preservation for 20-30 min.
Preferably, the mixing manner in the steps (2), (3) and (4) is stirring; more preferably, the mixing in steps (2) and (3) is 20-30 Hz stirring for 15-20min, and the mixing in step (4) is 10-20 Hz stirring for 20-30 min.
Preferably, the pressure of the vacuum pumping in the step (2) is 0.2 MPa.
Preferably, in steps (2) and (4), the raw materials mixed with the mixture A, C, respectively, are mixed and dissolved in advance.
Compared with the prior art, the invention has the following beneficial effects:
at present, the whitening products on the market only carry out repair and whitening, and neglect the damage of ultraviolet rays to skin during whitening. The whitening and blue light resisting mask provided by the invention has the advantages of whitening, blue light resisting and obvious effect.
Drawings
Fig. 1 is a graph of the whitening test results of the whitening blue-light-resistant mask of example 2; wherein, a is before use, and b is after use.
FIG. 2 is a graph showing the results of blue light resistance tests of the masks of examples 1 to 3 and comparative examples 1 to 3; where a is comparative example 1, b is example 1, c is example 2, d is comparative example 2, e is example 3, and f is comparative example 3.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example 1
The whitening anti-blue-light facial mask comprises the following components in percentage by weight: 10.75% of whitening blue-light resistant composition, 5.55% of humectant, 0.3% of antioxidant, 0.02% of chelating agent, 0.21% of thickening agent, 0.3% of preservative, 0.003% of aromatic and the balance of water.
The humectant comprises 4 wt% of butanediol, 1.5 wt% of polyglycerol-10 and 0.05 wt% of sodium hyaluronate.
The thickener comprises 0.08 wt% xanthan gum (KELTROL CG-SFT), 0.03 wt% hydrolyzed Sclerotin (BIOEVEN HGS), and 0.1 wt% acrylic acid (ester)/C10-30 alkanol acrylate cross-linked POLYMER (CARBOPOL ULTREZ 20 POLYMER).
The antioxidant is p-hydroxyacetophenone (Symsave II).
The chelating agent is disodium EDTA (Dissolvine NA 2).
The antiseptic is phenoxyethanol and ethylhexyl glycerol.
The aromatic agent is Rosa damascena flower oil.
The whitening blue-light-resistant composition comprises the following components in percentage by weight: 5.58% of hydroxyethyl piperazine ethane sulfonic acid (Unowlobe HEPES), 18.6% of nicotinamide (Niacinamide USP PC, Guangzhou Henan), 0.93% of aminomethyl propanol (AMP-ULTRAPC 2000, Neutralizing Amine), 46.5% of a complex of a fermentation product lysate of binary fission yeast and butanediol (lysate of fermentation product of binary fission yeast, Guangzhou Zhengsu/Sichuan China), 46.5% of a complex of alfalfa extract and butanediol, water (alfalfa leaf, Urb juice MS, Guangzhou folium), 9.3% of 3-o-ethyl ascorbic acid (vitamin C ethyl ether, Gwhite VCE, Guangzhou folium), 4.65% of tetrahydro methylpyrimidine carboxylic acid (ECTOIN, Huaxi organism), 0.47% of extract of Magnolia sieboldii, and 13.95% of a complex of water (Magnolvax extract, Guangzhou good).
In the compound of the lysate of the fermentation product of the saccharomyces bifidus and the butanediol, the weight percentage of the lysate and the butanediol is 30 percent and 70 percent in sequence.
In the compound of the alfalfa extract, the butanediol and the water, the weight percentages of the alfalfa extract, the butanediol and the water are 5%, 50% and 45% in sequence.
In the complex of the magnolia sieboldii extract, butanediol and water, the weight percentages of the magnolia sieboldii extract, the butanediol and the water are 0.5 percent, 39.5 percent and 60 percent in sequence.
The preparation method of the whitening blue-light-resistant mask comprises the following steps:
(1) adding butanediol, polyglycerol-10, sodium hyaluronate, xanthan gum, hydrolyzed sclerotium rolfsii gum, acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, p-hydroxyacetophenone, EDTA disodium and water into an emulsifying pot, heating to 82-85 ℃, stirring, homogenizing, and keeping the temperature for 20min to obtain a mixture A;
(2) cooling the mixture A obtained in the step (1) to 65 ℃, adding hydroxyethyl piperazine ethanesulfonic acid, nicotinamide and aminomethyl propanol (pre-dissolved) in the whitening blue-light-resistant composition, vacuumizing at 0.2Mpa, and stirring at 30 Hz for 20min to be uniform to obtain a mixture B;
(3) cooling the mixture B in the step (2) to 42 ℃, adding a compound of a lysis product of a fission yeast fermentation product and butanediol and a compound (pre-dissolving) of a medicago sativa extract, butanediol and water in the whitening anti-blue light composition, and stirring for 20min at 30 Hz until the mixture is uniform to obtain a mixture C;
(4) and (3) cooling the mixture C obtained in the step (3) to 38 ℃, adding 3-o-ethyl ascorbic acid, tetrahydro-methyl pyrimidine carboxylic acid, a compound of magnolia sieboldii extract, butanediol and water, phenoxyethanol, ethylhexyl glycerol and rosa damascena flower oil (pre-dissolved) into the whitening and blue light resisting composition, and stirring for 30min at 15 Hz to obtain the whitening and blue light resisting mask.
Example 2
The whitening anti-blue-light facial mask comprises the following components in percentage by weight: 22.35% of whitening blue-light resistant composition, 7.1% of humectant, 0.5% of antioxidant, 0.03% of chelating agent, 0.45% of thickening agent, 0.4% of preservative, 0.005% of aromatic and the balance of water.
The humectant comprises 5 wt% of butanediol, 2 wt% of polyglycerol-10 and 0.1 wt% of sodium hyaluronate.
The thickener comprises 0.2 wt% of xanthan gum (KELTROL CG-SFT), 0.05 wt% of hydrolyzed sclerotium rolfsii (BIOEVEN HGS), and 0.2 wt% of acrylic acid/C10-30 alkanol acrylate cross-linked POLYMER (CARBOPOL ULTREZ 20 POLYMER).
The antioxidant is p-hydroxyacetophenone (Symsave II).
The chelating agent is disodium EDTA (Dissolvine NA 2).
The antiseptic is phenoxyethanol and ethylhexyl glycerol.
The aromatic agent is Rosa damascena flower oil.
The whitening blue-light-resistant composition comprises the following components in percentage by weight: 4.4% of hydroxyethyl piperazine ethane sulfonic acid (Unowpure HEPES), 22.4% of nicotinamide (Niacinamide USP PC, Guangzhou Henan), 0.9% of aminomethyl propanol (AMP-ULTRA PC 2000, Neutralizing Amine), 44.75% of a complex of a fermentation product lysate of binary fission yeast and butanediol (lysate of fermentation product of binary fission yeast, Guangzhou Zheng/Sichuan), 44.75% of a complex of alfalfa EXTRACT and butanediol, water (alfalfa juice MS, Guangzhou Gaojia leaves), 9% of 3-o-ethyl ascorbic acid (vitamin C ethyl ether, Gwhite VCE, Guangzhou Gaojia leaves), 4.5% of tetrahydro methylpyrimidine carboxylic acid (ECTOIN, Huaxi bio), 0.7% of Tiannu EXTRACT and butanediol, water complex (MAGNOOLIA EXTRACIAN EXTRACT, CT Guangzhou Ganbao EXTRACT) 13.4%.
In the compound of the lysate of the fermentation product of the saccharomyces bifidus and the butanediol, the weight percentage of the lysate and the butanediol is 30 percent and 70 percent in sequence.
In the compound of the alfalfa extract, the butanediol and the water, the weight percentages of the alfalfa extract, the butanediol and the water are 5%, 50% and 45% in sequence.
In the complex of the magnolia sieboldii extract, butanediol and water, the weight percentages of the magnolia sieboldii extract, the butanediol and the water are 0.5 percent, 39.5 percent and 60 percent in sequence.
The preparation method of the whitening blue-light-resistant mask is the same as that of the embodiment 1.
Example 3
The whitening anti-blue-light facial mask comprises the following components in percentage by weight: 16.85% of whitening blue-light resistant composition, 9.1% of humectant, 0.5% of antioxidant, 0.03% of chelating agent, 0.45% of thickening agent, 0.4% of preservative, 0.005% of aromatic and the balance of water.
The humectant comprises 6 wt% of butanediol, 3 wt% of polyglycerol-10 and 0.1 wt% of sodium hyaluronate.
The thickener comprises 0.2 wt% of xanthan gum (KELTROL CG-SFT), 0.05 wt% of hydrolyzed sclerotium rolfsii (BIOEVEN HGS), and 0.2 wt% of acrylic acid/C10-30 alkanol acrylate cross-linked POLYMER (CARBOPOL ULTREZ 20 POLYMER).
The antioxidant is p-hydroxyacetophenone (Symsave II).
The chelating agent is disodium EDTA (Dissolvine NA 2).
The antiseptic is phenoxyethanol and ethylhexyl glycerol.
The aromatic agent is Rosa damascena flower oil.
The whitening blue-light-resistant composition comprises the following components in percentage by weight: 5.9% of hydroxyethyl piperazine ethane sulfonic acid (Unowlobe HEPES), 23.7% of nicotinamide (Niacinamide USP PC, Guangzhou Henan), 1.2% of aminomethylpropanol (AMP-ULTRAPC 2000, Neutralizing Amine), 35.6% of a complex of a fermentation product lysate of binary fission yeast and butanediol (lysate of fermentation product of binary fission yeast, Guangzhou Zhengsu/Sichuan China), 35.6% of a complex of alfalfa EXTRACT and butanediol, water (alfalfa juice MS, Guangzhou folium), 8.9% of 3-o-ethyl ascorbic acid (vitamin C ethyl ether, Gwhite VCE, Guangzhou folium), 11.8% of tetrahydro methylpyrimidine carboxylic acid (ECTOIN, Huaxi bio), 0.9% of Magnolia sieboldii EXTRACT and butanediol, and a complex of water (MAGNOPENIA EXOLIA CAN EXTRACT, Guangzhou BAO) 12%.
In the compound of the lysate of the fermentation product of the saccharomyces bifidus and the butanediol, the weight percentage of the lysate and the butanediol is 30 percent and 70 percent in sequence.
In the compound of the alfalfa extract, the butanediol and the water, the weight percentages of the alfalfa extract, the butanediol and the water are 5%, 50% and 45% in sequence.
In the complex of the magnolia sieboldii extract, butanediol and water, the weight percentages of the magnolia sieboldii extract, the butanediol and the water are 0.5 percent, 39.5 percent and 60 percent in sequence.
The preparation method of the whitening blue-light-resistant mask is the same as that of the embodiment 1.
Comparative example 1
The whitening anti-blue-light facial mask comprises the following components in percentage by weight: 2.56% of whitening blue-light resistant composition, 4.01% of humectant, 0.1% of antioxidant, 0.01% of chelating agent, 0.11% of thickening agent, 0.1% of preservative, 0.001% of aromatic and the balance of water.
The humectant comprises 3 wt% of butanediol, 1 wt% of polyglycerol-10 and 0.01 wt% of sodium hyaluronate.
The thickener comprises 0.05 wt% of xanthan gum (KELTROL CG-SFT), 0.01 wt% of hydrolyzed sclerotium rolfsii (BIOEVEN HGS), and 0.05 wt% of acrylic acid/C10-30 alkanol acrylate cross-linked POLYMER (CARBOPOL ULTREZ 20 POLYMER).
The antioxidant is p-hydroxyacetophenone (Symsave II).
The chelating agent is disodium EDTA (Dissolvine NA 2).
The whitening blue-light-resistant composition comprises the following components in percentage by weight: hydroxyethyl piperazine ethane sulfonic acid (Unowpure HEPES) 11.8%, nicotinamide (Niacinamide USP PC, Guangzhou Henan) 19.5%, aminomethyl propanol (AMP-ULTRA PC 2000, Neutralizing Amine) 1.95%, a complex of the yeast fermentation lysate and butanediol (Zusabunya koensis fermentation lysate, Guangzhou Zheng/Sichuan) 39%, alfalfa EXTRACT and butanediol, a complex of water (alfalfa Urb juice MS, Guangzhou Jia Ye) 3.9%, 3-o-ethyl ascorbic acid (vitamin C ethyl ether, Gwhite VCE, Guangzhou Jia Ye), tetrahydro methylpyrimidine carboxylic acid (ECTOIN, Huaxi bio) 0.39%, a complex of the Carya paniculata EXTRACT and butanediol, water (MAGNOOLIA EXTRACLAMAN, CT Guangzhou Bo EXTRACT) 19.5%.
In the compound of the lysate of the fermentation product of the saccharomyces bifidus and the butanediol, the weight percentage of the lysate and the butanediol is 30 percent and 70 percent in sequence.
In the compound of the alfalfa extract, the butanediol and the water, the weight percentages of the alfalfa extract, the butanediol and the water are 5%, 50% and 45% in sequence.
In the complex of the magnolia sieboldii extract, butanediol and water, the weight percentages of the magnolia sieboldii extract, the butanediol and the water are 0.5 percent, 39.5 percent and 60 percent in sequence.
The preparation method of the whitening blue-light-resistant mask is the same as that of the embodiment 1.
Comparative example 2
Comparative example 2 differs from example 2 in that no split yeast fermentation lysate plus butanediol formulation was added.
Comparative example 3
Comparative example 3 differs from example 2 in that no alfalfa extract plus butylene glycol, water formulation was added.
TABLE 1 raw materials and amounts (in weight%) in examples and comparative examples
The appearance and physical and chemical indexes of the whitening blue-light-resistant mask meet the following requirements:
1. appearance was yellowish transparent liquid, pH (direct test): 5.0-6.5.
2. The heat resistance (45 +/-2 ℃) is 3 months, the room temperature is recovered, and no abnormality exists.
3. Cold resistance (-18 +/-2 ℃): the room temperature was returned to 3 months without abnormality.
4. The high-low temperature cold-hot circulating box is adopted to circularly test for three months (45 ℃ and minus 18 ℃), and no abnormality is found.
Through detection, the facial masks of the examples 1-3 and the comparative examples 1-3 meet the above standards.
Whitening test
1. The experimental requirements are as follows: male and female volunteers 18-45 years old meeting the requirements of the test were selected as subjects.
2. And (3) testing a sample: the facial masks prepared in examples 1-3 and comparative examples 1-3 of the present invention.
3. The experimental method comprises the following steps: 120 male and female volunteers (25-45 years old) were selected and divided into 6 groups of 20 persons, and the samples of examples 1-3 and comparative examples 1-3 of the present invention were applied, respectively. The samples were soaked with a mask cloth and applied to the face for 15 minutes before observing skin changes. Photographs were taken before and after use. Group 1 application example 1, group 2 application example 2, group 3 application example 3, group 4 application comparative example 1, group 5 application comparative example 2, group 6 application comparative example 3. The score is between 0 and 10 according to the using effect: the results are shown in Table 2, where the scores from 9 to 10 were good, the scores from 7 to 8 were good, the scores from 5 to 6 were general, the scores from 3 to 4 were poor, and the scores from 1 to 2 were poor, and the average was taken.
TABLE 2
| Sample (I) | Scoring |
| Example 1 | 7 |
| Example 2 | 10 |
| Example 3 | 8 |
| Comparative example 1 | 5 |
| Comparative example 2 | 6 |
| Comparative example 3 | 6 |
The results show that examples 1 to 3 all have whitening efficacy, with the whitening effect of example 2 being the best (fig. 1).
Anti-blue light test
1. The experimental requirements are as follows: male and female volunteers 18-45 years old meeting the requirements of the test were selected as subjects.
2. And (3) testing a sample: the facial masks prepared in examples 1-3 and comparative examples 1-3 of the present invention.
3. The experimental method comprises the following steps: 120 male and female volunteers (25-45 years old) were selected and divided into 6 groups of 20 persons, and the samples of examples 1-3 and comparative examples 1-3 of the present invention were applied, respectively. The volunteers washed the inner skin of the forearm, smeared the sample on the skin, and applied blue light (30J/cm)2) Illumination was carried out for 7min, using a VISIA skin detector measurement (reduction of skin damage by blue light) and photographed (fig. 2). The results show that examples 1-3 are significantly effective against blue light.
While the foregoing is directed to the preferred embodiment of the present invention, it will be understood by those skilled in the art that various changes and modifications may be made without departing from the spirit and scope of the invention.
Claims (10)
1. The whitening anti-blue-light composition is characterized by comprising the following components in percentage by weight: hydroxyethyl piperazine ethanesulfonic acid, nicotinamide, aminomethyl propanol, a saccharomyces cerevisiae fermentation product lysate, alfalfa extract, 3-o-ethyl ascorbic acid, tetrahydro methyl pyrimidine carboxylic acid, magnolia sieboldii extract;
the whitening blue-light-resistant composition also comprises auxiliary materials compounded with active substances: the lysate of the secondary fission yeast fermentation product is compounded with butanediol; compounding the alfalfa extract with butanediol and water; the magnolia sieboldii extract is compounded with butanediol and water.
2. The whitening and blue-light-resisting composition of claim 1, wherein the composition comprises 4% -6% of hydroxyethyl piperazine ethanesulfonic acid, 18% -24% of nicotinamide, 0.8% -1.3% of aminomethyl propanol, 35% -47% of a diclazyte fermentation product lysate and butanediol complex, 8% -10% of a medicago sativa extract and butanediol complex, water complex, 4% -12% of 3-o-ethyl ascorbic acid, 0.4% -1% of tetrahydro-methyl pyrimidine carboxylic acid, and 11% -14% of a magnolia sieboldii extract and butanediol complex, water complex.
3. The whitening and blue-light-resisting composition of claim 2, wherein the composition comprises 4.5% of hydroxyethyl piperazine ethanesulfonic acid, 22.5% of nicotinamide, 0.9% of aminomethyl propanol, 45% of a diclazaromyces fermentation product lysate and butanediol, 9% of a medicago sativa extract, butanediol, and water, 5% of 3-o-ethyl ascorbic acid, 0.7% of tetrahydro-methyl pyrimidinecarboxylic acid, and 13.5% of a magnolia sieboldii extract, butanediol, and water.
4. The whitening anti-blue light composition of claim 2 or 3,
in the compound of the lysate of the secondary fission yeast fermentation product and the butanediol, the weight percentages of the lysate and the butanediol are 25 to 30 percent and 70 to 75 percent in sequence;
in the compound of the alfalfa extract, the butanediol and the water, the weight percentages of the alfalfa extract, the butanediol and the water are 4.5-5%, 45-50% and 40-45% in sequence;
in the complex of the magnolia sieboldii extract, butanediol and water, the weight percentages of the magnolia sieboldii extract, the butanediol and the water are 0.4-0.5%, 39.5-45.5% and 54-60.1% in sequence.
5. Use of the whitening anti-blue-light composition according to any one of claims 1 to 4, for the preparation of a cosmetic comprising an emulsion, a cream, a spray, a serum, an essential oil; the addition amount of the whitening blue-light-resistant composition in the cosmetic is 1-25% by weight.
6. The whitening and blue light resisting mask is characterized by comprising the following components in percentage by weight: 10-25% of whitening blue-light resistant composition, 5-9% of humectant, 0.3-0.5% of antioxidant, 0.01-0.03% of chelating agent, 0.1-0.45% of thickening agent, 0.1-0.4% of preservative, 0.001-0.005% of aromatic and the balance of water.
7. The whitening blue-light-resistant mask of claim 6, which comprises the following components in percentage by weight: 16-23% of whitening blue-light resistant composition, 7-9% of humectant, 0.5% of antioxidant, 0.03% of chelating agent, 0.45% of thickening agent, 0.4% of preservative, 0.005% of aromatic and the balance of water.
8. The whitening blue-light-resistant mask of claim 7, which comprises the following components in percentage by weight: 22.35% of whitening blue-light resistant composition, 7.1% of humectant, 0.5% of antioxidant, 0.03% of chelating agent, 0.45% of thickening agent, 0.4% of preservative, 0.005% of aromatic and the balance of water;
the humectant is butanediol, polyglycerol-10 and sodium hyaluronate;
the thickening agent is xanthan gum, hydrolyzed sclerotium rolfsii gum and acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer;
the antioxidant is p-hydroxyacetophenone;
the chelating agent is EDTA disodium;
the preservative is phenoxyethanol and ethylhexyl glycerol;
the aromatic is Rosa damascena flower oil.
9. The whitening blue-light-resistant mask of claim 8,
in the humectant, the weight percentages of the three are as follows: 4% -6% of butanediol, 101.5% -3% of polyglycerol and 0.05% -0.1% of sodium hyaluronate;
in the thickener, the weight percentages of the three are as follows: 0.08 to 0.2 percent of xanthan gum, 0.03 to 0.05 percent of hydrolyzed sclerotium rolfsii gum and 0.1 to 0.2 percent of acrylic acid (ester)/C10 to 30 alkanol acrylate cross-linked polymer.
10. The method for preparing the whitening blue-light-resistant mask of claims 6-9, comprising the steps of:
(1) mixing butanediol, polyglycerol-10, sodium hyaluronate, xanthan gum, hydrolyzed sclerotium rolfsii gum, acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, p-hydroxyacetophenone, EDTA disodium and water, homogenizing at 82-85 ℃, and preserving heat to obtain a mixture A;
(2) cooling the mixture A obtained in the step (1) to 60-65 ℃, and vacuumizing and mixing the mixture A with hydroxyethyl piperazine ethanesulfonic acid, nicotinamide and aminomethyl propanol in the whitening blue-light-resistant composition to obtain a mixture B;
(3) cooling the mixture B in the step (2) to 40-42 ℃, and mixing the mixture B with a composition of a cracked yeast fermentation product lysate and butanediol and a composition of a medicago sativa extract, butanediol and water in the whitening blue-light resistant composition to obtain a mixture C;
(4) cooling the mixture C obtained in the step (3) to 35-38 ℃, and mixing the mixture C with 3-o-ethyl ascorbic acid, tetrahydro-methyl pyrimidine carboxylic acid, a compound of magnolia sieboldii extract, butanediol and water, phenoxyethanol, ethylhexyl glycerol and rosa damascena flower oil in the whitening blue-light-resistant composition to obtain a whitening blue-light-resistant mask;
the heat preservation in the step (1) is stirring and heat preservation for 20-30 min;
stirring in the mixing modes of the steps (2), (3) and (4), stirring for 15-20min at 20-30 Hz in the steps (2) and (3), and stirring for 20-30min at 10-20 Hz in the step (4);
in steps (2) and (4), the raw materials mixed with the mixture A, C, respectively, are mixed and dissolved in advance.
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| CN109528592A (en) * | 2018-12-31 | 2019-03-29 | 广州御艾化妆品有限公司 | Facial mask and preparation method thereof is repaired in a kind of moisturizing whitening |
| CN109589285A (en) * | 2019-01-31 | 2019-04-09 | 广州艾蓓生物科技有限公司 | A kind of Whitening, spot essence and preparation method thereof |
| CN111297745A (en) * | 2019-12-16 | 2020-06-19 | 宁波久瑞生物工程有限公司 | Absorption-promoting whitening composition and production process and application thereof |
| CN111557875A (en) * | 2020-06-02 | 2020-08-21 | 华熙生物科技股份有限公司 | Skin care composition for resisting light pollution and light injury and preparation method and application thereof |
| CN111671685A (en) * | 2020-06-15 | 2020-09-18 | 广州市科昂贸易有限公司 | Whitening and freckle-removing composition, whitening and freckle-removing cream and preparation method thereof |
| CN112891269A (en) * | 2021-01-28 | 2021-06-04 | 广州科丽德日化科技有限公司 | Beauty essence capable of effectively improving skin quality and processing technology thereof |
| CN113476353A (en) * | 2021-07-07 | 2021-10-08 | 广州天然国度生物科技有限公司 | Whitening essence suitable for long-term storage and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN116035985A (en) * | 2022-06-30 | 2023-05-02 | 广州凡岛网络科技有限公司 | Preparation method and application of composition with whitening, repairing and acne mark fading functions |
| CN116392405A (en) * | 2023-04-10 | 2023-07-07 | 深圳市护家科技有限公司 | Whitening composition and external skin preparation |
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