CN113876682A - Pearl powder self-foaming cleansing composition and preparation method and application thereof - Google Patents
Pearl powder self-foaming cleansing composition and preparation method and application thereof Download PDFInfo
- Publication number
- CN113876682A CN113876682A CN202111181035.6A CN202111181035A CN113876682A CN 113876682 A CN113876682 A CN 113876682A CN 202111181035 A CN202111181035 A CN 202111181035A CN 113876682 A CN113876682 A CN 113876682A
- Authority
- CN
- China
- Prior art keywords
- acid
- pearl powder
- cleansing composition
- self
- foaming
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- 238000012430 stability testing Methods 0.000 description 1
- 238000011105 stabilization Methods 0.000 description 1
- 239000012086 standard solution Substances 0.000 description 1
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- 230000037072 sun protection Effects 0.000 description 1
- 229940126680 traditional chinese medicines Drugs 0.000 description 1
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Images
Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/008—Preparations for oily skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/41—Particular ingredients further characterized by their size
- A61K2800/412—Microsized, i.e. having sizes between 0.1 and 100 microns
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- Public Health (AREA)
- Veterinary Medicine (AREA)
- Dermatology (AREA)
- Birds (AREA)
- Epidemiology (AREA)
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- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Gerontology & Geriatric Medicine (AREA)
- Cosmetics (AREA)
Abstract
The invention provides a pearl powder self-foaming cleansing composition, which consists of 0.01 to 10 percent of pearl powder, 1 to 50 percent of acid, 1 to 30 percent of carbonate, 1 to 50 percent of surfactant, 1 to 20 percent of thickening agent and the balance of starch according to weight percentage; wherein the acid is selected from organic acid and/or inorganic acid; the invention provides a formula system of traditional face cleaning powder, which is added with carbonic acid self-foaming performance, and further added with pearl powder on the basis; therefore, during the self-foaming process of the flour, the rich amino acids, trace elements, calcium ions and other components in the pearl powder can be effectively dissolved out; the multiple active ingredients act together; the natural pearl powder adopted by the invention can effectively avoid violent reaction generated when high-content carbonate and inorganic acid are mixed, so that the self-foaming speed of the formula can be regulated and controlled, the irritation to skin is reduced, and the stability of the product is improved.
Description
Technical Field
Relates to the field of skin external preparations, in particular to a cleansing composition and a preparation method and application thereof.
Background
Since ancient times, women have had the habit of using face cleansers to remove facial soils, until the rise of fatty acid salt surfactant materials and the widespread use of solid soaps, face cleansers gradually disappeared from the visual field of people. However, in recent years, face cleansers have become the choice of consumers again, and have gained a great deal of acceptance and appreciation.
The pearl has the effects of calming the nerves, detoxifying, retaining youthful looks, moistening and tendering skin and the like and makes the skin glossy and white, and the beauty mechanism is that the pearl contains various amino acids and trace elements required by a human body, and the nutrient components of the pearl are close to the nutrient required by the human skin, so that the pearl is easily absorbed by the human body and has good beauty and health care effects.
The direct effect of pearl powder on skin cells is shown in providing an extracellular environment with sufficient nutrition; thereby achieving the effects of whitening skin, removing spots, eliminating scars, restoring skin elasticity, relieving skin wrinkles and the like. A large number of pharmacological experiments show that the pearl powder can create a good environment for epithelial cell regeneration and promote the healing of skin wound; the pearl powder has strong inhibiting effect on staphylococcus aureus and the like, has the anti-inflammatory and antibacterial effects, and can regulate skin flora and enhance skin repairing activity. The fine solid particles of the pearl powder can absorb and reflect a part of ultraviolet rays and various radiant rays, has the protection effect on the damage of the radiant rays, can avoid the formation of sunburn and has better sun-proof effect. The biochemical reaction induced by free radicals and the increase of lipid peroxides in cells are considered to be important factors of human cell aging. The Margarita powder can reduce Malondialdehyde (MDA) content of lipid peroxide degradation product, improve superoxide dismutase (SOD) activity, and inhibit lipid peroxidation of biomembrane caused by free radicals, thereby achieving effects of resisting oxidation and delaying aging. Moreover, the keratin contained in the pearl and the lipid of the horny cell can jointly form a cell membrane for protecting the natural moisturizing factor, thereby well preventing the loss of the natural moisturizing factor and properly controlling the outward diffusion of water from the skin, so that the horny layer can keep a certain water content within a certain time. In addition, various microelements contained in Margarita can permeate into the interstitial space of superficial layer cells and glands to be absorbed by dermis to improve skin nutrition and circulation, regulate skin pH value, and enhance skin cell elasticity. Other researches show that free calcium ions have great importance to skin, and the important basis for living cells is that the concentration of calcium ions in cells is low, the concentration of calcium ions in cells is high, and certain concentration gradient exists between the inside and the outside of the membrane to form a transmembrane active state, and secretion, contraction and excitation of the membrane are all determined by the concentration gradient of the calcium ions. The calcium ions enter into the intercellular substance of human body, can promote the activity of Adenosine Triphosphate (ATP) enzyme, regulate acid-base balance, and participate in the action of cell buffer system. More importantly, the concentration gradient of calcium ions inside and outside the cell membrane enables external information to be accurately and stably transmitted into the cell to maintain the metabolic balance state of the cell, thereby delaying the cell aging.
Patent CN201580080271.5 discloses a foamable personal care composition and its use, which produces a large amount of dense foam and maintains its stability for a long time by means of surfactants and thickeners, which do not contain pearl powder or calcium carbonate in its ingredients.
Patent CN200710035583.1 discloses a skin care multi-effect bath powder, a production method and a use method thereof, wherein the bath powder contains traditional Chinese medicine herbal essence powder and pearl powder. Wherein the Margarita powder is instant Margarita powder obtained by enzymolysis. The composition has complex components, the action mechanism of the compatible ingredients of the traditional Chinese medicines is not completely clear, and the composition is difficult to be applied to people with sensitive skin or facial skin. The dry flowable powder is very easy to dissolve in water, cannot bubble, has small cleaning force, cannot be applied to the surface of skin, is difficult to locally clean the skin, is long in use time and is not simple and convenient enough.
Most of the existing commercial carbonic acid self-foaming cleansing noodles mainly comprise high-content carbonate, high-content inorganic acid or organic acid and fatty acid salt surfactant, have high self-foaming speed, are difficult to control, have excessively strong cleaning power, have stimulation burden on skin and have poor product stability.
Disclosure of Invention
Aiming at the defects in the prior art, the first aspect of the invention provides a pearl powder self-foaming cleansing composition which comprises 0.01-10% of pearl powder, 1-50% of acid, 1-30% of carbonate, 1-50% of surfactant, 1-20% of thickener and the balance of starch in percentage by weight; wherein the acid is selected from organic acid and/or inorganic acid.
The invention provides a formula system of traditional face cleaning powder, which is added with carbonic acid self-foaming performance, and further added with pearl powder on the basis; therefore, during the self-foaming process of the flour, the rich amino acids, trace elements, calcium ions and other components in the pearl powder can be effectively dissolved out; the dissolved active ingredients act together, such as trace elements are absorbed by the dermis through the gaps of surface cells and glands, so that the nutrition and circulation of the skin are improved, and the elasticity of skin cells is enhanced; the dissolved calcium ions reach the surface layer of the skin, and can act on the skin after being absorbed by the skin, improve the quantity of mature keratinocytes, regulate and control the differentiation of epidermal cells and the like; the skin care product can nourish the skin and strengthen the repair of the skin barrier while cleaning the skin. In addition, the natural pearl powder adopted by the invention can effectively slow down the violent reaction generated when the high-content sodium bicarbonate and the inorganic acid are mixed, thereby regulating and controlling the self-foaming speed of the formula, reducing the irritation to the skin and improving the stability of the product.
The pearl powder self-foaming face-cleaning composition provided by the invention has a good self-foaming effect, moderate foaming speed, uniform, fine and dense foam, long foam stabilization duration, fresh and cool skin feel without dryness, and excellent product stability, and has the effects of cleaning, oil control, moisture retention, oxidation resistance, skin brightening, freckle removing, whitening, aging resistance, wrinkle resistance, compactness, relaxation, moistening and sun protection.
The pearl is a precious traditional Chinese medicine, contains various amino acids and trace elements such as calcium, magnesium and the like, and has various effects of whitening, moistening skin, beautifying and the like. The Concha Margaritifera is Pteria margaritifera (L.) of Pteria of Pteriidae, Pteria martensii (Dunker) of Pteria Margaritifera, or Concha Margaritifera of several kinds of freshwater mussels of Unionidae. The pearl layer and pearl are formed by nacrum secreted by mantle of mother shell and epidermal cell of pearl sac, and their luster, color and components are basically identical. When people use pearls for skin care, the pearls are generally required to be firstly crushed to be beneficial to the absorption of effective components of the pearls, and because the absorption rate of human bodies to the effective components of the pearls depends on the particle size of the crushed pearls, when the particle size of the pearl powder is in a certain range, the absorption rate and the bioavailability can reach the optimal values; based on the above, in some preferred embodiments, the weight percentage of the pearl powder is 1-5%, the pearl powder source is pearl and/or mother-of-pearl, and the particle size is 50-2000 nm.
In some embodiments, the carbonate salt is a solid powder of sodium bicarbonate and/or potassium bicarbonate.
In some embodiments, the organic acid is selected from at least one of water-soluble solid powders of citric acid, tartaric acid, succinic acid, lactobionic acid, modified salicylic acid, modified ascorbic acid, and the like having a moisture content of less than 5%.
In some embodiments, the inorganic acid is an acid salt; in some preferred embodiments, the acid salt is selected from dihydrogen phosphate and/or hydrogen sulfate; still more preferably, the acid salt is at least one of potassium dihydrogen phosphate, sodium dihydrogen phosphate, ammonium dihydrogen phosphate, potassium hydrogen sulfate, and sodium hydrogen sulfate.
In some embodiments, the surfactant is an amino acid surfactant or a fatty acid salt; in some preferred embodiments, the surfactant is at least one of water soluble solid powders of cocoyl glutamate, lauroyl glutamate, cocoyl glycinate, lauroyl methyl taurate, lauroyl sarcosinate, laurate, myristate, palmitate, sulfate, isostearate, stearate, and the like.
In some embodiments, the thickener is at least one of xanthan gum, pullulanase, carrageenan water-soluble natural polysaccharide powder, carbomer, PEG polymer, sodium hyaluronate, erythritol, xylitol, sorbitol, inositol.
In some embodiments, the starch is at least one of corn starch, tapioca starch, sweet potato starch, potato starch.
In a second aspect, the present invention provides an external preparation for skin comprising the pearl powder self-foaming cleansing composition described above.
In a third aspect, the present invention provides a preparation method of the pearl powder self-foaming cleansing composition, which comprises the following steps: pulverizing the above materials respectively, stirring Margarita powder, carbonate, surfactant, thickener and starch at 10-100rpm for 1-10min, adding pulverized acid, and stirring at 10-100rpm for 1-10 min.
The preparation process provided by the invention is simple and convenient to operate.
In a fourth aspect, the pearl powder self-foaming cleansing composition is applied to preparing a skin external agent; the skin external preparation has good self-foaming effect, refreshing and non-dry skin feeling, and good product stability, and has effects of cleaning, controlling oil, keeping moisture, resisting oxidation, brightening skin, resolving macula, whitening, resisting aging, resisting wrinkle, tightening, relieving, moistening, and preventing sunburn.
Compared with the prior art, the invention has the following beneficial effects:
the invention provides a formula system of traditional face cleaning powder, which is added with carbonic acid self-foaming performance, and further added with pearl powder on the basis; therefore, during the self-foaming process of the flour, the rich amino acids, trace elements, calcium ions and other components in the pearl powder can be effectively dissolved out; the dissolved active ingredients act together, such as trace elements are absorbed by the dermis through the gaps of surface cells and glands, so that the nutrition and circulation of the skin are improved, and the elasticity of skin cells is enhanced; the dissolved calcium ions reach the surface layer of the skin, and can act on the skin after being absorbed by the skin, improve the quantity of mature keratinocytes, regulate and control the differentiation of epidermal cells and the like; the skin care product can nourish the skin and strengthen the repair of skin barriers while cleaning the skin. In addition, the invention uses the natural pearl powder to reduce the violent reaction generated when the high-content sodium bicarbonate and the inorganic acid are mixed as much as possible, thereby regulating and controlling the self-foaming speed of the formula and reducing the irritation to the skin.
The preparation process provided by the invention is simple and convenient to operate.
The pearl essence-containing skin care product contains pearl powder active ingredients, has good self-foaming effect, fresh and cool skin feeling without dryness after use, has excellent product stability, and has the effects of cleaning, controlling oil, preserving moisture, resisting oxidation, brightening skin, removing freckles, whitening, resisting aging, resisting wrinkles, compacting, relaxing, moistening and preventing sun.
Drawings
FIG. 1 is a schematic of the foaming of the product of example 1 (left panel) versus the product of comparative example 1 (right panel).
Detailed Description
EXAMPLE 1 Pearl powder self-foaming cleansing composition A
The pearl powder self-foaming cleansing composition A is prepared from the following components in percentage by mass.
TABLE 1 Pearl powder self-foaming cleansing composition A ingredient table
The preparation method comprises the following steps: respectively pulverizing the above materials, stirring B, C, D, E, F at 100rpm for 1min, adding A, and stirring at 100rpm for 10 min.
EXAMPLE 2 Pearl powder self-foaming cleansing composition B
The pearl powder self-foaming cleansing composition B is prepared from the following components in percentage by mass.
TABLE 2 Pearl powder self-foaming cleansing composition B ingredient table
The preparation method is the same as example 1.
Comparative example 1 comparative self-foaming cleansing composition
The comparative self-foaming cleansing composition was prepared with the following components in mass percent.
Table 3 comparative self-foaming cleansing composition ingredient table
The preparation method is the same as example 1.
Test example 1 foaming Property test of product
The pearl powder self-foaming cleansing composition a prepared in example 1 (left of the figure) and the self-foaming cleansing composition prepared in comparative example 1 (right of the figure) were photographed for foaming after 20 seconds at room temperature. The foaming speed at the left side of the graph is moderate and mild, the foam is uniform, fine and thick, and the foam is stable and has long duration; the right side of the figure has rapid foaming, uneven foam size, short foam duration, instability and easy defoaming.
The results show that the pearl powder self-foaming cleansing composition has small reaction and stable foaming when in use; thus, the natural pearl powder is proved to be capable of remarkably reducing the violent reaction generated when high-content sodium bicarbonate and inorganic acid are mixed, reducing the stimulation to the skin and being milder.
Test example 2 product stability test
The pearl powder self-foaming cleansing composition prepared according to the examples 1-2 is subjected to stability tests such as heat resistance, cold resistance, alternation, illumination and the like, wherein,
the heat resistance test conditions were: keeping the temperature at 45 +/-1 ℃ and keeping out of the sun;
the cold resistance test conditions are as follows: keeping the temperature at minus 20 +/-1 ℃ and keeping out of the sun;
the alternating test conditions were: keeping the temperature at minus 20 ℃ for 3.5 days, changing the temperature at 45 ℃ for 3.5 days, and keeping out of the sun;
the illumination test conditions were: illumination constant temperature and humidity test box (1.47X 10)6Lux·hr)；
The test results are shown in table 4 below.
Table 4 product stability testing
The above results show that the pearl powder self-foaming cleansing composition of the present invention has excellent stability under various conditions. The addition of pearl powder makes the system of the composition more stable.
Test example 3 calcium ion content test in self-foaming extract
Test samples: sample 1: pearl powder self-foaming cleansing composition prepared according to example 1,
Sample 2: self-foaming cleansing composition prepared according to comparative example 1,
Sample 3: pearl powder
The reference method comprises the following steps: ion chromatography for measuring sodium, potassium, magnesium and calcium ions in water sample
Reagent: methane sulfonic acid, anhydrous calcium chloride, purified water and hydrochloric acid.
The instrument comprises the following steps: thermo scientific ICS-900 ion chromatograph.
And (3) an analysis step: preparing 20mmol/L methane sulfonic acid aqueous solution as leacheate; calcium chloride is used for preparing calcium ion standard solution. And respectively diluting the sample 1, the sample 2 and the sample 3 by 100 times by using purified water, and taking supernate to filter the supernate to be used as a sample to be detected after foams completely disappear.
The determination process comprises the following steps:
opening an argon gas cylinder, adjusting a partial pressure meter to 0.2MPa, adjusting a pressure reducing valve on the leaching solution bottle to 5psi, switching on an instrument power supply, turning on a host computer and a computer, and opening a software system. And loosening the pump head waste liquid valve to remove bubbles, and then closing the waste liquid valve. The pump was turned on, run for about 10min, the suppressor power was turned on (one day suppressor was previously activated), and baseline was collected.
And after the baseline is stable, sample injection analysis can be performed, the flow rate of the eluent is set to be 0.8mL/min, and a blank sample is added before the first standard sample and after the last sample. And drawing the spectrogram of each component by an instrument data processing system within 30min after one sample injection, and obtaining the calcium ion concentration of the sample after data processing.
And (3) testing results: sample 1 had a free calcium ion concentration of 406 ppm. Samples 2 and 3 had no free calcium ions.
The results show that the pearl powder self-foaming cleansing composition disclosed by the invention contains the active ingredients of the pearl powder, has a good self-foaming effect, is mild and non-irritating, has fresh and cool skin feel and excellent stability, can effectively dissolve out calcium ions, amino acids, trace elements and the like in the pearl powder in the self-foaming process in the using process of the product, and achieves the effects of cleaning, controlling oil, moisturizing, resisting oxidation, brightening skin, removing freckles, whitening, resisting aging, resisting wrinkles, compacting, relieving, moistening, preventing sunburn and the like under the combined action of various active ingredients.
Claims (10)
1. The pearl powder self-foaming cleansing composition is characterized by comprising 0.01-10 wt% of pearl powder, 1-50 wt% of acid, 1-30 wt% of carbonate, 1-50 wt% of surfactant, 1-20 wt% of thickener and the balance of starch; wherein the acid is selected from organic acid and/or inorganic acid.
2. The pearl powder self-foaming cleansing composition according to claim 1, wherein the weight percentage of the pearl powder is 1-5%, the pearl powder source is pearl and/or mother-of-pearl, and the particle size is 50-2000 nm.
3. The pearl powder self-foaming cleansing composition according to claim 1, wherein the carbonate is sodium bicarbonate and/or potassium bicarbonate.
4. The pearl powder self-foaming cleansing composition according to claim 1, wherein the inorganic acid is an acid salt; preferably, the acid salt is selected from dihydrogen phosphate and/or hydrogen sulfate; still further preferably, the acid salt is at least one of potassium dihydrogen phosphate, sodium dihydrogen phosphate, ammonium dihydrogen phosphate, potassium hydrogen sulfate and sodium hydrogen sulfate;
the organic acid is one or more selected from citric acid, tartaric acid, succinic acid, lactobionic acid, modified salicylic acid, and modified ascorbic acid.
5. The pearl powder self-foaming cleansing composition according to claim 1, wherein the surfactant is an amino acid surfactant or a fatty acid salt; preferably, the surfactant is at least one of cocoyl glutamate, lauroyl glutamate, cocoyl glycinate, lauroyl methyl taurate, lauroyl sarcosinate, laurate, myristate, palmitate, sulfate, isostearate, stearate.
6. The pearl powder self-foaming cleansing composition according to claim 1, wherein the thickener is at least one of xanthan gum, pullulanase, carrageenan water-soluble natural polysaccharide powder, carbomer, PEG polymer, sodium hyaluronate, erythritol, xylitol, sorbitol, and inositol.
7. The pearl powder self-foaming cleansing composition according to claim 1, wherein the starch is at least one of corn starch, tapioca starch, sweet potato starch, and potato starch.
8. An external preparation for skin, characterized in that it comprises the pearl powder self-foaming cleansing composition according to any one of claims 1 to 7.
9. The preparation method of the pearl powder self-foaming cleansing composition according to any one of claims 1 to 7, which is characterized by comprising the following steps: pulverizing the above materials respectively, stirring Margarita powder, carbonate, surfactant, thickener and starch at 10-100rpm for 1-10min, adding pulverized acid, and stirring at 10-100rpm for 1-10 min.
10. The use of the pearl powder self-foaming cleansing composition according to any one of claims 1 to 7 in the preparation of a skin external preparation.
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| CN115518024A (en) * | 2022-10-13 | 2022-12-27 | 欧诗漫生物股份有限公司 | Foaming face cleaning composition, foaming face cleaning agent, preparation method and using method thereof |
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| CN115518024A (en) * | 2022-10-13 | 2022-12-27 | 欧诗漫生物股份有限公司 | Foaming face cleaning composition, foaming face cleaning agent, preparation method and using method thereof |
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| CN113876682B (en) | 2023-11-03 |
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Denomination of invention: A pearl powder self foaming cleansing composition and its preparation method and application Granted publication date: 20231103 Pledgee: Agricultural Bank of China Limited Deqing County sub branch Pledgor: OSMUN BIOLOGICAL Co.,Ltd. Registration number: Y2024980023335 |