CN113876682B - Pearl powder self-foaming cleansing composition and preparation method and application thereof - Google Patents
Pearl powder self-foaming cleansing composition and preparation method and application thereof Download PDFInfo
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- CN113876682B CN113876682B CN202111181035.6A CN202111181035A CN113876682B CN 113876682 B CN113876682 B CN 113876682B CN 202111181035 A CN202111181035 A CN 202111181035A CN 113876682 B CN113876682 B CN 113876682B
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- pearl powder
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- foaming
- pearl
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- 229910001415 sodium ion Inorganic materials 0.000 description 1
- 239000002689 soil Substances 0.000 description 1
- 230000002269 spontaneous effect Effects 0.000 description 1
- 239000012086 standard solution Substances 0.000 description 1
- 210000000434 stratum corneum Anatomy 0.000 description 1
- 239000006228 supernatant Substances 0.000 description 1
- 230000002936 tranquilizing effect Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/008—Preparations for oily skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/41—Particular ingredients further characterized by their size
- A61K2800/412—Microsized, i.e. having sizes between 0.1 and 100 microns
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Dermatology (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Zoology (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Gerontology & Geriatric Medicine (AREA)
- Cosmetics (AREA)
Abstract
The invention provides a pearl powder self-foaming cleansing composition, which consists of, by weight, 0.01-10% of pearl powder, 1-50% of acid, 1-30% of carbonate, 1-50% of surfactant, 1-20% of thickener and the balance of starch; wherein the acid is selected from organic acid and/or inorganic acid; the invention provides a method for adding carbonic acid to the traditional formula system of the clean flour and further adding pearl powder on the basis of the carbonic acid self-foaming performance; therefore, in the self-foaming process of the clean flour, the components such as rich amino acids, microelements, calcium ions and the like in the pearl powder can be effectively dissolved out; the multiple active ingredients act together; the natural pearl powder adopted by the invention can effectively avoid severe reaction generated when high-content carbonate and inorganic acid are mixed, so that the self-foaming speed of the formula can be regulated and controlled, the irritation to skin is reduced, and the stability of the product is improved.
Description
Technical Field
Relates to the field of skin external preparations, in particular to a cleansing composition, a preparation method and application thereof.
Background
From ancient times, women had the habit of using clean flour to remove facial soils until the rise of fatty acid salt surfactant materials and the popular use of solid soaps, the clean flour gradually disappeared from the human field of vision. In recent years, however, clean flour has become a consumer choice again, gaining a great deal of acceptance and acceptance.
The pearl is a classical beauty medicinal material since ancient times, the great medical trails of the ancient times such as the compendium of materia medica, the miscellaneous records of famous doctors, the Kaibao grass and the like indicate that the pearl has the effects of tranquillizing, detoxifying, retaining youthful looks, moistening and tendering skin and the like, and the skin is glossy and white, the beauty mechanism is that the pearl contains various amino acids and microelements required by human bodies, the nutrition components of the pearl are close to the nutrients required by human skins, the pearl is easy to be absorbed by human bodies, and the pearl has good beauty and health care effects.
The direct effect of the pearl powder on skin cells is shown as providing an extracellular environment with sufficient nutrition; thereby achieving the effects of whitening skin, removing spots, eliminating scars, restoring skin elasticity, reducing skin wrinkles, and the like. A large number of pharmacological experiments show that the pearl powder can create a good environment for regenerating epithelial cells and promote the healing of skin wounds; the pearl powder has strong inhibition effect on staphylococcus aureus and the like, has anti-inflammatory and antibacterial effects, and can regulate skin flora and enhance skin repair activity. The fine solid particles of the pearl powder can absorb and reflect a part of ultraviolet rays and various radiation rays, have a protective effect on radiation ray damage, can avoid sunburn and have a good sun-screening effect. It is considered that the biochemical reaction induced by free radicals and the increase of intracellular lipid peroxides are important factors for the aging of human cells. The pearl powder can reduce the content of Malondialdehyde (MDA) which is a lipid peroxide degradation product, improve the activity of superoxide dismutase (SOD), inhibit the peroxidation of biomembrane lipid caused by free radicals, thereby achieving the effects of resisting oxidation, delaying aging and the like. And the keratin contained in the pearl and the lipid of the keratinocyte together form a cell membrane for protecting the natural moisturizing factor, so that the loss of the natural moisturizing factor is well prevented, and the outward diffusion of moisture from the skin is properly controlled, so that the stratum corneum maintains a certain moisture content within a certain period of time. In addition, the pearl contains various microelements which can permeate the gaps of surface cells and the glands to be absorbed by the dermis, thereby playing the roles of improving skin nutrition and circulation, regulating the pH value of the skin, enhancing the elasticity of the skin cells and the like. In addition, researches show that free calcium ions have great importance to skin, and the important basis for living cells is that the intracellular calcium ions have low concentration and the extracellular calcium ions have high concentration, so that a transmembrane activity state is formed when a certain concentration gradient exists inside and outside a membrane, and secretion, contraction and excitation of the transmembrane activity state depend on the concentration gradient of the calcium ions. Calcium ions enter human body cell interstitium, can promote the activity of Adenosine Triphosphate (ATP) enzyme, regulate acid-base balance and participate in the action of a cell buffer system. More importantly, the concentration gradient of calcium ions inside and outside the cell membrane can ensure that external information can be accurately and stably transferred into the cell to maintain the metabolic balance state of the cell, thereby delaying the aging of the cell.
Patent CN201580080271.5 discloses a foamable personal care composition and its use, which produces a large amount of dense foam by means of surfactants and thickeners and maintains its stability for a long period of time, the ingredients of which do not contain pearl powder or calcium carbonate.
Patent CN200710035583.1 discloses a skin care multi-effect bath powder, a production method and a use method thereof, which contain herbal essence powder and pearl powder. Wherein the pearl powder is instant pearl powder prepared by enzymolysis. The composition has complex components, the action mechanism of the compatible components of the traditional Chinese medicine is not completely clear, and the composition is difficult to be applied to skin-sensitive people or facial skin. The dry flowable powder is extremely easy to dissolve in water, can not be foamed, has small cleaning strength, can not be applied to the skin surface, is difficult to clean and use locally on the skin, has long use time and is not simple and convenient.
The existing commercial carbonic acid self-foaming cleansing faces mainly comprise high-content carbonate, high-content inorganic acid or organic acid and fatty acid salt surfactant, have the advantages of high self-foaming speed, difficult control, strong cleaning power, irritation burden on skin and poor product stability.
Disclosure of Invention
In order to overcome the defects in the prior art, in a first aspect, the invention provides a pearl powder self-foaming facial cleaning composition which comprises, by weight, 0.01-10% of pearl powder, 1-50% of acid, 1-30% of carbonate, 1-50% of surfactant, 1-20% of thickener and the balance of starch; wherein the acid is selected from organic acid and/or inorganic acid.
The invention provides a method for adding carbonic acid to the traditional formula system of the clean flour and further adding pearl powder on the basis of the carbonic acid self-foaming performance; therefore, in the self-foaming process of the clean flour, the components such as rich amino acids, microelements, calcium ions and the like in the pearl powder can be effectively dissolved out; the dissolved active ingredients act together, such as trace elements penetrate through the gaps of surface cells and glands are absorbed by dermis, so that skin nutrition and circulation are improved, and skin cell elasticity is enhanced; the dissolved calcium ions reach the surface layer of the skin, act on the skin after percutaneous absorption, improve the number of mature keratinocytes, regulate and control the differentiation of epidermal cells and the like; can nourish the skin and strengthen the restoration of the skin barrier while cleaning the skin. In addition, the natural pearl powder adopted by the invention can effectively slow down the severe reaction generated when the high-content sodium bicarbonate and the inorganic acid are mixed, so that the self-foaming speed of the formula can be regulated and controlled, the irritation to the skin is reduced, and the stability of the product is improved.
The pearl powder self-foaming cleansing composition provided by the invention has the advantages of good self-foaming effect, moderate foaming speed, uniform, fine and dense foam, long foam stability duration, fresh and non-dry skin feel, excellent product stability, and has the effects of cleaning, oil control, moisture preservation, oxidation resistance, skin brightening, freckle removing, whitening, aging resistance, wrinkle resistance, tightening, soothing, moistening and sun protection.
Pearl is a rare traditional Chinese medicine, contains various amino acids and microelements such as calcium, magnesium and the like, and has various effects of whitening, moisturizing and nourishing skin and the like. The Concha Margaritifera is nacre Pteria margaritifera (L.), pteria martensii (Dunker) or Concha Margaritifera shell of Pteriidae. The nacreous layer and the pearl are formed by the mantle of the mother shell and the nacreous layer secreted by the epidermal cells of the pearl sac, and the luster, the color and the components of the nacreous layer and the pearl are basically consistent. When people use pearls to protect skin, the pearls are generally required to be crushed firstly so as to be beneficial to the absorption of the active ingredients of the pearls, and the absorption rate of the active ingredients of the pearls by a human body is dependent on the particle size of the crushed pearls, so that the absorption rate and the bioavailability can reach the optimal values when the particle size of the pearl powder is in a certain range; based on this, in some preferred embodiments, the weight percentage of the pearl powder is 1-5%, the pearl powder source is pearl and/or mother of pearl, and the particle size is 50-2000 nm.
In some embodiments, the carbonate is sodium bicarbonate and/or potassium bicarbonate solid powder.
In some embodiments, the organic acid is selected from at least one of water-soluble solid powders having a moisture content of 5% or less, such as citric acid, tartaric acid, succinic acid, lactobionic acid, modified salicylic acid, modified ascorbic acid, and the like.
In some embodiments, the mineral acid is an acid salt; in some preferred embodiments, the acid salt is selected from the group consisting of dihydrogen phosphate and/or hydrogen sulfate; still further preferably, the acid salt is at least one of potassium dihydrogen phosphate, sodium dihydrogen phosphate, ammonium dihydrogen phosphate, potassium hydrogen sulfate, and sodium hydrogen sulfate.
In some embodiments, the surfactant is an amino acid surfactant or a fatty acid salt; in some preferred embodiments, the surfactant is at least one of water-soluble solid powders of cocoyl glutamate, lauroyl glutamate, cocoyl glycinate, lauroyl methyl taurate, lauroyl sarcosinate, laurate, myristate, palmitate, sulfate, isostearate, stearate, and the like.
In some embodiments, the thickening agent is at least one of xanthan gum, pullulanase polysaccharide, carrageenan water-soluble natural polysaccharide powder, carbomer, PEG polymer, sodium hyaluronate, erythritol, xylitol, sorbitol, inositol.
In some embodiments, the starch is at least one of corn starch, tapioca starch, sweet potato starch, potato starch.
In a second aspect, the present invention provides an external preparation for skin comprising the above-described pearl powder self-foaming cleansing composition.
In a third aspect, the present invention provides a method for preparing the pearl powder self-foaming cleansing composition, which comprises the following steps: pulverizing the above materials respectively, mixing with Margarita powder, carbonate, surfactant, thickener, and starch at 10-100rpm, stirring at low speed for 1-10min, adding pre-pulverized acid, and stirring at 10-100rpm for 1-10 min.
The preparation process provided by the invention is simple and convenient to operate.
In a fourth aspect, the invention applies the pearl powder self-foaming facial cleanser composition to the preparation of external skin preparations; the skin external agent has good self-foaming effect, fresh and non-dry skin feel, good product stability, and has effects of cleaning, controlling oil, keeping moisture, resisting oxidation, brightening skin, removing speckle, whitening skin, resisting aging, resisting wrinkle, tightening, relieving, moistening, and preventing sunburn.
Compared with the prior art, the invention has the following beneficial effects:
the invention provides a method for adding carbonic acid to the traditional formula system of the clean flour and further adding pearl powder on the basis of the carbonic acid self-foaming performance; therefore, in the self-foaming process of the clean flour, the components such as rich amino acids, microelements, calcium ions and the like in the pearl powder can be effectively dissolved out; the dissolved active ingredients act together, such as trace elements penetrate through the gaps of surface cells and glands are absorbed by dermis, so that skin nutrition and circulation are improved, and skin cell elasticity is enhanced; the dissolved calcium ions reach the surface layer of the skin, act on the skin after percutaneous absorption, improve the number of mature keratinocytes, regulate and control the differentiation of epidermal cells and the like; can nourish the skin and strengthen the restoration of the skin barrier while cleaning the skin. In addition, the invention uses natural pearl powder to minimize the severe reaction generated when high-content sodium bicarbonate and inorganic acid are mixed, so that the self-foaming speed of the formula can be regulated and controlled, and the irritation to skin is reduced.
The preparation process provided by the invention is simple and convenient to operate.
The pearl powder-containing skin care cream contains pearl powder active ingredients, has good spontaneous foaming effect, fresh and dry skin feel after use, and good product stability, and has the effects of cleaning, controlling oil, moisturizing, resisting oxidation, brightening skin, removing freckles, whitening skin, resisting aging, resisting wrinkles, tightening, relieving, moistening and preventing sunburn.
Drawings
FIG. 1 is a schematic diagram of foaming of the product of example 1 (left panel) and the product of comparative example 1 (right panel).
Detailed Description
Example 1 Pearl powder self-foaming cleansing composition A
The pearl powder self-foaming facial cleaning composition A is prepared according to the following components in percentage by mass.
TABLE 1 pearl powder self foaming cleansing composition A composition Table
The preparation method comprises the following steps: pulverizing the above materials, stirring at low speed for 1min at 100rpm for B, C, D, E, F, adding A, and stirring at low speed for 10min at 100 rpm.
Example 2 Pearl powder self-foaming cleansing composition B
The pearl powder self-foaming facial cleaning composition B is prepared according to the following components in percentage by mass.
TABLE 2 composition of pearl powder self-foaming facial cleanser B
The preparation method is the same as in example 1.
Comparative example 1 comparative self foaming cleansing composition
The comparative self-foaming cleansing composition was prepared from the following components in mass percent.
Table 3 comparative self foaming cleansing composition ingredients Table
The preparation method is the same as in example 1.
Test example 1 product foaming Performance test
The pearl powder prepared in example 1 was taken from the foaming cleansing composition a (left side of the figure) and the foaming cleansing composition prepared in comparative example 1 (right side of the figure) after foaming at room temperature for 20 seconds. The foaming speed is moderate in the left drawing, the foam is uniform, fine and dense, and the foam stability duration is long; the right drawing shows rapid foaming, uneven foam size, short foam duration, instability and easy defoaming.
The results show that the pearl powder self-foaming facial cleansing composition has small reaction and stable foaming when in use; the invention proves that the natural pearl powder can obviously reduce the severe reaction generated when the high-content sodium bicarbonate and the inorganic acid are mixed, reduce the irritation to the skin and be milder.
Test example 2 product stability test
The pearl powder self-foaming facial cleansing composition prepared according to examples 1-2 was subjected to stability tests of heat resistance, cold resistance, alternation, light irradiation and the like, wherein,
the heat resistance test conditions were: constant temperature and light shielding at 45+/-1 ℃;
the cold resistance test conditions are as follows: -20+/-1 ℃ and keeping the temperature away from light;
the alternating test conditions were: transferring from-20deg.C constant temperature for 3.5 days to 45deg.C constant temperature for 3.5 days, and keeping away from light;
the illumination test conditions are as follows: illumination constant temperature and humidity test box (1.47 x 10) 6 Lux·hr)；
The test results are shown in table 4 below.
Table 4 product stability test
The results show that the pearl powder self-foaming facial cleansing composition has excellent stability under various conditions. The addition of pearl powder makes the system of the composition more stable.
Test example 3 measurement of calcium ion content in self-foaming lysate
Test sample: sample 1: pearl powder self-foaming cleansing composition prepared according to example 1,
Sample 2: self-foaming cleansing composition prepared according to comparative example 1,
Sample 3: pearl powder
The reference method comprises the following steps: ion chromatography for measuring sodium, potassium, magnesium and calcium ions in water sample
Reagent: methane sulfonic acid, anhydrous calcium chloride, purified water and hydrochloric acid.
Instrument: thermo scientific ICS-900 ion chromatograph.
The analysis step: preparing a methane sulfonic acid aqueous solution with the concentration of 20mmol/L as a eluent; calcium chloride is used for preparing the calcium ion standard solution. Sample 1, sample 2 and sample 3 were each diluted 100-fold with purified water and after complete disappearance of the foam, the supernatants were filtered to give samples to be tested.
The measuring process comprises the following steps:
opening an argon gas bottle, regulating the pressure gauge to 0.2MPa, regulating the pressure reducing valve on the leaching solution bottle to 5psi, switching on an instrument power supply, opening a host computer and a computer, and opening a software system. Unscrewing the pump head waste liquid valve to remove bubbles, and then closing the waste liquid valve. The pump was turned on, run for about 10min, the suppressor was turned on (one day of suppressor activation in advance), and a baseline was collected.
After the baseline is stable, sample injection analysis can be performed, the flow rate of the leaching solution is set to be 0.8mL/min, and a blank sample needs to be fed before the sample injection of the first standard sample and after the sample injection of the last standard sample. And drawing a spectrogram of each component by an instrument data processing system within 30 minutes after one sample injection, and obtaining the calcium ion concentration of the sample after data processing.
Test results: sample 1 had a free calcium ion concentration of 406ppm. Sample 2 and sample 3 were free of free calcium ions.
The results show that the pearl powder self-foaming facial cleanser composition contains the pearl powder active ingredients, has good self-foaming effect, is mild and non-irritating, has fresh and non-dry skin feel and excellent product stability, can effectively dissolve calcium ions, amino acids, trace elements and the like in the pearl powder through the self-foaming process in the use process of the product, and achieves the effects of cleaning, oil control, moisturizing, antioxidation, skin brightening, freckle removing, whitening, aging resistance, wrinkle resistance, tightening, relieving, moistening, sun protection and the like under the combined action of various active ingredients.
Claims (8)
1. The pearl powder self-foaming facial cleaning composition is characterized by comprising, by weight, 1-5% of pearl powder, 1-50% of acid, 1-30% of carbonate, 1-50% of surfactant, 1-20% of thickener and the balance of starch; wherein the acid is selected from organic acid and/or inorganic acid;
the inorganic acid is acid salt; the acid salt is selected from dihydrogen phosphate and/or hydrogen sulfate;
the surfactant is an amino acid surfactant or a fatty acid salt;
the organic acid is one or more than two of citric acid, tartaric acid, succinic acid and lactobionic acid; the carbonate is sodium bicarbonate and/or potassium bicarbonate; the pearl powder is pearl and/or mother of pearl, and the grain size is 50-2000 nm.
2. The pearl powder self-foaming facial cleansing composition of claim 1 wherein the acid salt is at least one of potassium dihydrogen phosphate, sodium dihydrogen phosphate, ammonium dihydrogen phosphate, potassium hydrogen sulfate, sodium hydrogen sulfate.
3. The pearl powder self-foaming facial cleanser composition of claim 1, wherein the surfactant is at least one of cocoyl glutamate, lauroyl glutamate, cocoyl glycinate, lauroyl methyl taurate, lauroyl sarcosinate, laurate, myristate, palmitate, isostearate, stearate.
4. The pearl powder self-foaming facial cleanser composition of claim 1, wherein the thickening agent is at least one of xanthan gum, pullulanase polysaccharide, carrageenan water-soluble natural polysaccharide powder, carbomer, PEG polymer, sodium hyaluronate, erythritol, xylitol, sorbitol, inositol.
5. The self-foaming pearl powder cleansing composition according to claim 1, wherein the starch is at least one of corn starch, tapioca starch, sweet potato starch, potato starch.
6. A skin external preparation comprising the pearl powder self-foaming facial cleansing composition according to any one of claims 1 to 5.
7. The method for preparing a pearl powder self-foaming facial cleansing composition according to any one of claims 1 to 5, comprising the steps of: pulverizing the above materials respectively, mixing with Margarita powder, carbonate, surfactant, thickener, and starch at 10-100rpm, stirring at low speed for 1-10min, adding pre-pulverized acid, and stirring at 10-100rpm for 1-10 min.
8. Use of the pearl powder self-foaming facial cleanser according to any one of claims 1 to 5 in the preparation of an external skin preparation.
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