CN113876679B - Multi-effect composition with moisturizing and sensitive skin relieving functions, essence and preparation method - Google Patents
Multi-effect composition with moisturizing and sensitive skin relieving functions, essence and preparation method Download PDFInfo
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- CN113876679B CN113876679B CN202111310237.6A CN202111310237A CN113876679B CN 113876679 B CN113876679 B CN 113876679B CN 202111310237 A CN202111310237 A CN 202111310237A CN 113876679 B CN113876679 B CN 113876679B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/42—Amides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/005—Preparations for sensitive skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
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- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
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- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Abstract
The invention belongs to the field of cosmetics, and in particular relates to a multi-effect composition with the functions of moisturizing and relieving sensitive skin, an essence and a preparation method thereof, wherein the multi-effect composition comprises the following components in parts by mass of 0.1-3 parts of panthenol,1-6 parts of ASIA, 0.1-3 parts of skin-nourishing medicine, 0.1-5 parts of purslane extract and 0.05-0.5 part of Xihenjing. The invention selects a specific combination, panthenol,ASIA, yufuning, herba Portulacae extract and Ximanpu can make the composition achieve the effects of keeping moisture and relieving, and has the advantages of multiple effects, cooperation, natural and simple collocation, and high safety.
Description
Technical Field
The invention belongs to the field of cosmetics, and particularly relates to a multi-effect composition with functions of moisturizing and relieving sensitive skin, an essence and a preparation method.
Background
Sensitive muscles are the skin symptoms that most countries' females and nearly half of males consider themselves to have, and sensitive muscles severely affect quality of life.
The cause of sensitive skin is not a single one, but rather a combination of factors. Such as personal factors and external factors. Personal factors are affected by genetics, sex, endocrine, age, disease, mental stress, etc.; external factors are mainly unsuitable skin care products, incorrect skin care products can cause damage to skin, sun light, temperature and seasonal change, air pollution can make skin sensitive, and life habits such as eating and work habits, and eating spicy food, staying up night and alcohol effect can cause skin sensitivity. Because the skin is damaged, the moistening degree is reduced, the skin immunity is reduced, and finally the skin barrier is too weak and cannot resist external stimulus, so that various uncomfortable symptoms such as redness, peeling, tightening, stinging, tingling, burning, continuous itching feeling and the like are caused. Sensitive skin is the most difficult of all to care, so it is not dare to try easily for general skin care products.
Based on the special condition of sensitive muscles, firstly, water is needed to be supplemented, and the skin can perform normal metabolism only under the condition of sufficient water, so that the skin can be better recovered. In the aspects of water supplementing and moisture preserving, the product without essence and pigment is selected as far as possible, moisture is preserved fully, after the balance of the moisture and the grease is maintained, the external invasion can be effectively resisted,
because of the randomness of the sensitive muscle attacks, the need for urgent repair products that can relieve itching and relax the sensitivity for several minutes appears evident, but they have high safety requirements for the products.
The sensitive muscle group favors natural components, so natural, safe and mild natural plant extract components, especially edible natural plant raw materials are selected as core components of the sensitive muscle skin care product.
Disclosure of Invention
The invention aims to provide a multi-effect composition with the functions of moisturizing and relieving sensitive skin, an essence and a preparation method.
In order to achieve the above purpose, the invention adopts the following technical scheme:
a multi-effect composition for moisturizing and relieving sensitive skin comprises (by weight parts) panthenol 0.1-3,1-6 parts of ASIA, 0.1-3 parts of skin-nourishing medicine, 0.1-5 parts of purslane extract and 0.05-0.5 part of Xihenjing.
Preferably, the composition comprises the following components in parts by mass3 parts of ASIA, 2 parts of skin-nourishing medicine, 3 parts of purslane extract and 0.2 part of Xifensidie.
The invention also comprises a preparation method of the multi-effect composition with the functions of moisturizing and relieving sensitive skin, which comprises the following steps of:
1) Weighing the skin-nourishing and calming, the purslane extracting solution and the purslane according to the component weightASIA is mixed and then stirred to be dissolved uniformly for standby;
2) Adding panthenol and chlorpyrifos in turn, stirring rapidly, and mixing uniformly.
The invention also comprises an essence which comprises the following components in percentage by mass: 3 to 7 percent of 1,3 butanediol, 3 to 5 percent of glycerin, 0.5 to 2 percent of triolein, 0.5 to 2 percent of squalane, 0.5 to 0.9 percent of cetostearyl alcohol oleyl oleate, 0.1 to 1 percent of 0.1-tocopheryl acetate, 0.4 to 0.9 percent of sorbitan oleyl oleate, 0.1 to 0.5 percent of p-hydroxyacetophenone, 0.1 to 0.5 percent of sodium cetostearyl sulfate, 0.05 to 0.2 percent of allantoin, 0.05 to 0.3 percent of acrylic acid (ester) or C10-30 alkanol acrylate cross-linked polymer, 0.01 to 0.2 percent of xanthan gum,100 0.05-2%, chelating agent 0.01-0.05%, pH regulator 0.01-0.05%, preservative 0.4-0.9%, multi-effect composition according to claim 1 or 2 10-20%, and balance water%.
The pH regulator is sodium hydroxide; the chelating agent is EDTA-2Na.
Preferably, the composition comprises the following components in parts by mass: 6% of butanediol, 3% of glycerol, 1% of squalane, 1% of triolein, 0.72% of cetostearyl alcohol oleyl oleate, 0.5% of tocopheryl acetate, 0.48% of sorbitan oleyl oleate, 0.3% of p-hydroxyacetophenone, 0.2% of sodium cetostearyl sulfate, 0.11% of allantoin, 0.1% of acrylic acid (esters) C10-30 alkanol acrylate crosslinked polymer, 0.05% of xanthan gum,100 0.1%, 0.05% chelating agent, 0.03% pH regulator, 0.46% preservative, 6.6-9.7 parts (preferably 8.7%) of said multi-effect composition, the balance being water.
The invention also discloses a preparation method of the essence, which comprises the following steps:
(1) Dispersing xanthan gum in glycerol to obtain solution 1;
(2) Dissolving A91 and ethylhexyl glycerol in butanediol to obtain a solution 2;
(3) Accurately weighing cetostearyl alcohol olivetoate, sorbitan olivetoate, squalane, triolein, and other materials in an oil phase pretreatment tank,100. Sequentially adding tocopheryl acetate and butanediol into a tank, stirring and heating to dissolve completely, and controlling the temperature of the oil phase at 80-85deg.C to obtain oil phase.
(4) In a water phase pretreatment tank, the rest deionized water, acrylic acid (ester) C10-30 alkanol acrylate cross-linked polymer, sodium cetostearyl sulfate, solution 1, allantoin, EDTA disodium and p-hydroxyacetophenone are sequentially added into the tank, heated and stirred until the components are completely dissolved, and the water phase temperature is controlled at 86-92 ℃.
(5) Heating after the vacuum kettle is closed, starting a vacuum pump when the temperature reaches more than 50 ℃, sucking the filtered oil phase into a preheated emulsifying tank after the vacuum degree reaches-0.04 Mpa, then sucking the water phase through filtration, starting a scraper for stirring, homogenizing for 25-30 minutes, and performing vacuum emulsification. When the temperature in the emulsifying kettle reaches 85 ℃, stopping heating, preserving heat and stirring for 15-20 minutes, and starting to cool.
(6) When the temperature of the paste drops to 70-75 ℃, adding sodium hydroxide solution from a hopper, fully and uniformly stirring, stopping stirring when the temperature of the paste drops to 52-55 ℃, placing in vacuum, adding the multi-effect composition of the solution 2 from a pot cover, opening the vacuum, keeping the temperature, uniformly stirring, and continuously cooling.
(7) And discharging when the temperature is reduced to below 38 ℃.
Compared with the prior art, the invention has the beneficial effects that:
the invention selects a specific combination, panthenol,ASIA, yufuning, herba Portulacae extract and Ximanpu can make the composition achieve the effects of keeping moisture and relieving, and has the advantages of multiple effects, cooperation, natural and simple collocation, and high safety.
The invention also provides the essence of the multi-effect composition, which provides high-efficiency moisturizing effect by selecting proper oil phases such as squalane, triolein and the like, and the proportion of the functional components such as allantoin and the like in the water phase so as to achieve the dual effects of moisturizing and relieving,
the above skin care composition with moisturizing and soothing functions is analyzed as follows:
panthenol is provided by basf in germany, is a synthetic precursor of vitamin B5, and D-pantothenic acid plays a key role in metabolism in humans. It is a constituent of coenzyme A. The deficiency of vitamin B5 results in many cutaneous neurological disorders with deep moisturization, stimulation of epithelial cell growth, wound healing, and anti-inflammatory effects.
ASIA is provided by lucanseyer and mainly comprises bamboo shoot extract of Sasa veitchii (Bambusa vulgare) and lotus flower extract (Nelumbo NUCIFERA) and white water lily (Nymphaea album) root extract. The extract of the phyllostachys praecox shoot can supplement skin moisture and simultaneously eliminate skin inflammation; the lotus flower extract contains various mineral substances, and has strong free radical scavenging ability and anti-aging effect; the white water lily root extract relieves the skin discomfort caused by neurogenic inflammation. The composition of three asian moisturizing plants has the functions of activating and long-acting keeping skin hydrated, and can promote cell renewal.
Skin-nourishing tannin adopts green tangerine peel harvested for 5-6 months, the most effective active ingredients in the green tangerine peel are reserved through a biological activity tracking method, and then the ratio of flavone to alkaloid in the green tangerine peel is controlled at about 1:1 to realize the optimal effect, and the skin-nourishing tannin can be provided by Shanghai Jia Kai biotechnology Co Ltd, can target and regulate TRPV1 receptor, regulate the response of skin nerves to stimulus, reset skin balance and quickly compress skin discomfort response.
The purslane extract is colorless or yellowish clear liquid obtained by steam distillation after the whole purslane is squeezed and precipitated, has specific raw material smell and pH of 4.0-6.0, is provided by Shanghai Luya biotechnology limited company, can hydrate skin, can relieve inflammation, increase the antioxidant capacity of skin cells so as to reduce the damage of free radicals to the skin, and has certain help for enhancing the barrier function of the skin by conditioning the stratum corneum and maintaining the skin. Is safe for both child skin and sensitive type skin.
The Ximanzhi is high activity micro molecule hyaluronic acid obtained from fermentation source hyaluronic acid by natural mild patent enzyme digestion technology. Provided by Hua Xi biotechnology, inc. The sensitization repair can effectively inhibit the release of inflammatory factors, relieve the sensitization state of the skin caused by various factors, and simultaneously can effectively remove free radicals and repair skin injury caused by ultraviolet or chemical stimulation.
Drawings
FIG. 1 shows the average water content increase rate of the skin of examples and comparative examples.
Detailed Description
The present invention will be described in further detail below with reference to the drawings and preferred embodiments, so that those skilled in the art can better understand the technical solutions of the present invention.
Example 1: the raw materials of this embodiment are shown in table 1, and the preparation process of the composition is as follows:
1. weighing skin-nourishing 2g, purslane extract 3g andASIA 3g, and after mixing, stirring and dissolving uniformly for standby.
2. Adding 0.5g of panthenol and 0.2g of Xifensine in turn, rapidly stirring, and uniformly mixing to obtain the multi-effect composition.
The preparation process of the essence comprises the following steps:
1. firstly, dispersing xanthan gum in glycerin to obtain solution 1,
2. a91 and ethylhexyl glycerol are dissolved in butanediol to give solution 2,
3. in an oil phase pretreatment tank, weighing cetyl stearyl oleate, sorbitan oleate, squalane, triolein, alpha-olein and alpha-olein of the component A,100. Sequentially adding tocopheryl acetate and residual butanediol into a tank, stirring and heating to dissolve completely, and controlling the temperature of the oil phase at 80-85deg.C to obtain oil phase.
4. In a water phase pretreatment tank, weighing the component B, sequentially adding deionized water, acrylic acid (esters)/C10-30 alkanol acrylate crosslinked polymer, sodium cetostearyl sulfate, solution 1, allantoin, EDTA disodium and p-hydroxyacetophenone into the tank, heating and stirring until the components B are completely dissolved, and controlling the temperature of the water phase at 86-92 ℃.
5. Starting a vacuum pump, sucking the filtered oil phase into a preheated emulsifying tank after the temperature reaches more than 50 ℃ and the vacuum degree reaches-0.04 Mpa, then sucking the filtered water phase, starting a scraper for stirring (the rotating speed is 30 Hz), homogenizing for 25-30 minutes (the rotating speed is 50 Hz), and performing vacuum emulsification. When the temperature in the emulsifying kettle reaches 85 ℃, stopping heating, preserving heat and stirring for 15-20 minutes (the rotating speed is 30 Hz), and starting to cool.
6. When the temperature of the paste drops to 70-75 ℃, adding sodium hydroxide solution from a hopper, fully and uniformly stirring, stopping stirring when the temperature of the paste drops to 52-55 ℃, placing the paste in vacuum, adding the solution 2 and the multi-effect composition from a pot cover, opening the vacuum, keeping the temperature and uniformly stirring (the rotating speed is 15-50 Hz), and continuously cooling.
7. And when the temperature is reduced to below 38 ℃, taking materials, checking, detecting physical and chemical indexes, and discharging after the detection is qualified.
Table 1 shows the ratios of the raw materials used for the essences prepared in examples 1 to 4 and comparative examples 1 to 5.
TABLE 1
Example 2:
the raw materials of this embodiment are shown in table 1, and the preparation process of the composition is as follows:
1. weighing 3g of Yufuning, 0.1g of purslane extract andASIA 6g, and after mixing, stirring and dissolving uniformly for standby.
2. Adding 0.1g of panthenol and 0.5g of Xifensine in turn, rapidly stirring, and uniformly mixing to obtain the multi-effect composition.
The preparation process of the essence comprises the following steps:
1. firstly, dispersing xanthan gum in glycerin to obtain solution 1,
2. dissolving A91 and ethylhexyl glycerol in butanediol to obtain a solution 2;
3. in an oil phase pretreatment tank, weighing cetyl stearyl oleate, sorbitan oleate, squalane, triolein, alpha-olein and alpha-olein of the component A,100. Sequentially adding tocopheryl acetate and residual butanediol into a tank, stirring and heating to dissolve completely, and controlling the temperature of the oil phase at 80-85deg.C.
4. In a water phase pretreatment tank, weighing the component B, sequentially adding deionized water, acrylic acid (esters)/C10-30 alkanol acrylate crosslinked polymer, sodium cetostearyl sulfate, solution 1, allantoin, EDTA disodium and p-hydroxyacetophenone into the tank, heating and stirring until the components B are completely dissolved, and controlling the temperature of the water phase at 86-92 ℃.
5. Starting a vacuum pump, sucking the filtered oil phase into a preheated emulsifying tank after the temperature reaches more than 50 ℃ and the vacuum degree reaches-0.04 Mpa, then sucking the filtered water phase, starting a scraper for stirring (the rotating speed is 30 Hz), homogenizing for 25-30 minutes (the rotating speed is 50 Hz), and performing vacuum emulsification. When the temperature in the emulsifying kettle reaches 85 ℃, stopping heating, preserving heat and stirring for 15-20 minutes (the rotating speed is 30 Hz), and starting to cool.
6. When the temperature of the paste drops to 70-75 ℃, adding sodium hydroxide solution from a hopper, fully and uniformly stirring, stopping stirring when the temperature of the paste drops to 52-55 ℃, placing the paste in vacuum, adding the solution 2 and the multi-effect composition from a pot cover, opening the vacuum, keeping the temperature and uniformly stirring (the rotating speed is 15-50 Hz), and continuously cooling.
7. And when the temperature is reduced to below 38 ℃, taking materials, checking, detecting physical and chemical indexes, and discharging after the detection is qualified.
Example 3:
the raw materials of this embodiment are shown in table 1, and the preparation process of the composition is as follows:
1. weighing 0.1g of Yufuning, 5g of purslane extract andASIA 1g, and after mixing, stirring and dissolving uniformly for standby.
2. 3g of panthenol and 0.05g of Xifensine are added in sequence, and the mixture is rapidly stirred and uniformly mixed to obtain the multi-effect composition.
The preparation process of the essence comprises the following steps:
1. firstly, dispersing xanthan gum in glycerin to obtain solution 1,
2. a91 and ethylhexyl glycerol are dissolved in butanediol to give solution 2,
3. in an oil phase pretreatment tank, weighing cetyl stearyl oleate, sorbitan oleate, squalane, triolein, alpha-olein and alpha-olein of the component A,100. Sequentially adding tocopheryl acetate and residual butanediol into a tank, stirring and heating to dissolve completely, and controlling the temperature of the oil phase at 80-85deg.C.
4. In a water phase pretreatment tank, weighing the component B, sequentially adding deionized water, acrylic acid (esters)/C10-30 alkanol acrylate crosslinked polymer, sodium cetostearyl sulfate, solution 1, allantoin, EDTA disodium and p-hydroxyacetophenone into the tank, heating and stirring until the components B are completely dissolved, and controlling the temperature of the water phase at 86-92 ℃.
5. Starting a vacuum pump, sucking the filtered oil phase into a preheated emulsifying tank after the temperature reaches more than 50 ℃ and the vacuum degree reaches-0.04 Mpa, then sucking the filtered water phase, starting a scraper for stirring (the rotating speed is 30 Hz), homogenizing for 25-30 minutes (the rotating speed is 50 Hz), and performing vacuum emulsification. When the temperature in the emulsifying kettle reaches 85 ℃, stopping heating, preserving heat and stirring for 15-20 minutes (the rotating speed is 30 Hz), and starting to cool.
6. When the temperature of the paste drops to 70-75 ℃, adding sodium hydroxide solution from a hopper, fully and uniformly stirring, stopping stirring when the temperature of the paste drops to 52-55 ℃, placing the paste in vacuum, adding the solution 2 and the multi-effect composition from a pot cover, opening the vacuum, keeping the temperature and uniformly stirring (the rotating speed is 15-50 Hz), and continuously cooling.
7. And when the temperature is reduced to below 38 ℃, taking materials, checking, detecting physical and chemical indexes, and discharging after the detection is qualified.
Example 4:
the raw materials of this embodiment are shown in table 1, and the preparation process of the composition is as follows:
1. weighing 1.5g of Yufuning, 1g of purslane extract andASIA 2g, and after mixing, stirring and dissolving uniformly for standby.
2. 2g of panthenol and 0.1g of Xifensine are added in sequence, and the mixture is rapidly stirred and uniformly mixed to obtain the multi-effect composition.
The preparation process of the essence comprises the following steps:
1. firstly, dispersing xanthan gum in glycerin to obtain solution 1,
2. a91 and ethylhexyl glycerol are dissolved in butanediol to give solution 2,
3. in an oil phase pretreatment tank, weighing cetyl stearyl oleate, sorbitan oleate, squalane, triolein, alpha-olein and alpha-olein of the component A,100、Sequentially adding tocopheryl acetate and residual butanediol into a tank, stirring and heating to dissolve completely, and controlling the temperature of the oil phase at 80-85deg.C.
4. In a water phase pretreatment tank, weighing the component B, sequentially adding deionized water, acrylic acid (esters)/C10-30 alkanol acrylate crosslinked polymer, sodium cetostearyl sulfate, solution 1, allantoin, EDTA disodium and p-hydroxyacetophenone into the tank, heating and stirring until the components B are completely dissolved, and controlling the temperature of the water phase at 86-92 ℃.
5. Starting a vacuum pump, sucking the filtered oil phase into a preheated emulsifying tank after the temperature reaches more than 50 ℃ and the vacuum degree reaches-0.04 Mpa, then sucking the filtered water phase, starting a scraper for stirring (the rotating speed is 30 Hz), homogenizing for 25-30 minutes (the rotating speed is 50 Hz), and performing vacuum emulsification. When the temperature in the emulsifying kettle reaches 85 ℃, stopping heating, preserving heat and stirring for 15-20 minutes (the rotating speed is 30 Hz), and starting to cool.
6. When the temperature of the paste drops to 70-75 ℃, adding sodium hydroxide solution from a hopper, fully and uniformly stirring, stopping stirring when the temperature of the paste drops to 52-55 ℃, placing the paste in vacuum, adding the solution 2 and the multi-effect composition from a pot cover, opening the vacuum, keeping the temperature and uniformly stirring (the rotating speed is 15-50 Hz), and continuously cooling.
Comparative example 1 this comparative example 1 differs from example 1 only in that no panthenol is contained,ASIA 3.5g, the remainder remained the same as in example 1.
Comparative example 2 this comparative example 2 differs from example 1 only in that it does not contain yufuning, 4g of purslane extract,ASIA 4g, the remainder remained the same as in example 1.
Comparative example 3 this comparative example 3 differs from example 1 only in that the purslane extract, 3g of yufuning,ASIA 5g, the rest andexample 1 remained the same.
Comparative example 4 this comparative example 4 differs from example 1 only in that it does not contain the Xiximab,ASIA 3.2g, the remainder remained the same as in example 1.
Comparative example 5 this comparative example 5 differs from example 1 only in that it does not containASIA, yufuning 3g, portulaca oleracea extract 5g, the remainder were identical to example 1.
1. Product effect test 1
A quantity of 10% lactic acid was applied to the cheek and nasolabial folds, 54 sensitive subjects were screened, randomized into 6 groups and the test results were arithmetically averaged.
Measurement parameters: tingling discomfort (subjective feeling of the subject)
The testing method comprises the following steps:
sensitive subjects were selected for the test area for cheek and nasolabial folds, each with 10% lactic acid for patch test, and after 5min, skin was stingy and uncomfortable, using the example (2.0.+ -. 0.1) mg/cm 2 Control product (2.0.+ -. 0.1) mg/cm 2 And without using the product (blank), the stinging discomfort of the test site was measured after 0 minutes, 5 minutes, 15 minutes, 30 minutes, 60 minutes, 120 minutes, and the specific detection results are shown in table 2.
TABLE 2
Table 2 the evaluation results show that: panthenol in the moisturizing relief compositions of examples 1-4,The five compositions of ASIA, yufuning, purslane extract and Ximangxijing have synergistic effect, have a certain effect on instantly and long-acting relieving skin irritation, effectively relieve external skin irritation and calm skin. The synergistic effect is obviously better than other combinations of the control groups 1-5. This demonstrates that the efficacy of the moisturizing relief essence of examples 1-4 of the present invention is superior to the control 1-5.
2. Skin moisture moisturization test
50 volunteers with healthy body were selected, and the test samples were tested at a ratio of (2.0.+ -. 0.1) mg/cm 2 The amount was applied in a single pass, and the test was uniformly applied to the test area using a latex fingerstall, and then the moisture of the skin was evaluated after 5 hours. The moisturizing effect of each group of samples was tested in table 3 and fig. 1.
TABLE 3 Table 3
The test results in table 3 show that the skin moisture content of the subjects was significantly increased after 5 hours using the extracts of examples 1-4, demonstrating that the skin moisture content of the extracts was increased by 28.5% using example 1, and that the skin moisture content of the subjects was less than the moisture content of examples 1-4 after 5 hours using the extracts of control groups 1-5, demonstrating that the multi-effect composition lacks one, the synergy was reduced, and the moisturizing effect was affected.
The foregoing is merely a preferred embodiment of the present invention and it should be noted that modifications and adaptations to those skilled in the art may be made without departing from the principles of the present invention, which are intended to be comprehended within the scope of the present invention.
Claims (1)
1. The essence is characterized by comprising the following preparation processes:
s1, dispersing xanthan gum in glycerol to obtain a solution 1;
s2, dissolving A91 and ethylhexyl glycerol in 1, 3-butanediol to obtain a solution 2;
s3, in an oil phase pretreatment tank, weighing cetyl stearyl oleate, sorbitan oleate, squalane, triolein, symRelief 100, tocopheryl acetate and the rest 1, 3-butanediol which are components A, sequentially putting into the tank, stirring and heating until the components A are completely dissolved, and controlling the temperature of the oil phase at 80-85 ℃ to obtain an oil phase substance;
s4, weighing the component B, sequentially adding deionized water, acrylic acid (esters)/C10-30 alkanol acrylate crosslinked polymer, sodium cetostearyl sulfate, solution 1, allantoin, disodium EDTA and p-hydroxyacetophenone into a water phase pretreatment tank, heating and stirring until the components B are completely dissolved, and controlling the water phase temperature to be 86-92 ℃;
s5, starting a vacuum pump, sucking the filtered oil phase into a preheated emulsifying tank after the temperature reaches more than 50 ℃ and the vacuum degree reaches-0.04 Mpa, then sucking the filtered water phase, starting a scraper for stirring at the rotating speed of 30Hz, homogenizing for 25-30 minutes at the same time and at the rotating speed of 50Hz, and performing vacuum emulsification; stopping heating when the temperature in the emulsifying kettle reaches 85 ℃, preserving heat and stirring for 15-20 minutes, and starting to cool at the rotating speed of 30 Hz;
s6, when the temperature of the paste drops to 70-75 ℃, adding sodium hydroxide solution from a hopper, fully and uniformly stirring, stopping stirring when the temperature of the paste drops to 52-55 ℃, placing vacuum, adding solution 2 and a multi-effect composition from a pot cover, opening vacuum, keeping the temperature and uniformly stirring, and continuously cooling at the rotating speed of 15-50 Hz;
the preparation process of the multi-effect composition comprises the following steps:
6.1 2g of Yufuning, 3g of purslane extract and HYDRALPHATINE g of ASIA 3g are weighed, mixed, stirred and dissolved uniformly for later use;
6.2 0.5g of panthenol and 0.2g of Xifensine are added in sequence, and the mixture is rapidly stirred and uniformly mixed to obtain a multi-effect composition;
s7, when the temperature is reduced to be lower than 38 ℃, taking materials, checking, detecting physical and chemical indexes, and discharging after the detection is qualified;
wherein the contents of the components are as follows:
phase A: cetylstearyl olive oleate 0.72%, sorbitan olive oleate 0.48%, glycerin 3.00%, squalane 1.00%, triolein 1.00%, symRelief 100.10%, 1,3 butylene glycol 6.00%, tocopheryl acetate 0.50%;
and B phase: acrylic acid (esters)/C10-30 alkanol acrylate cross-linked polymer 0.10%, sodium cetostearyl sulfate 0.20%, xanthan gum 0.05%, allantoin 0.10%, disodium EDTA 0.05%, p-hydroxyacetophenone 0.30%;
and C phase: sodium hydroxide 0.03%;
and D phase: a91 0.40% and 0.06% of ethylhexyl glycerol; panthenol 0.50%, skin-nourishing tannin 2.00%, herba Portulacae extract 3.00%, xijin 0.20%, HYDRALPHATINE% ASIA 3.00%;
and the balance of water.
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| KR101891951B1 (en) * | 2017-12-29 | 2018-08-27 | 유서연 | Mask pack comprising emulsion composition containing peach-extract |
| CN108635328A (en) * | 2018-07-16 | 2018-10-12 | 徐杨 | Plant extraction lifts the facial mask that compacts |
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| CN110974775A (en) * | 2019-12-30 | 2020-04-10 | 湖南炎帝生物工程有限公司 | Allergy-relieving composition containing nostoc sphaeroides and preparation method and application thereof |
| CN111265431A (en) * | 2020-02-25 | 2020-06-12 | 合肥君梓堂生物科技有限公司 | Moisturizing and repairing composition |
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| KR101891951B1 (en) * | 2017-12-29 | 2018-08-27 | 유서연 | Mask pack comprising emulsion composition containing peach-extract |
| CN108635328A (en) * | 2018-07-16 | 2018-10-12 | 徐杨 | Plant extraction lifts the facial mask that compacts |
| CN109044909A (en) * | 2018-09-12 | 2018-12-21 | 广西古瑶方药妆研发科技有限公司 | A kind of natural sponge gourd bleeding water whitening foster skin Essence |
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