CN107184483A - High penetration camellia massage essential oil promoting blood circulation and removing obstruction in channels and preparation method thereof - Google Patents
High penetration camellia massage essential oil promoting blood circulation and removing obstruction in channels and preparation method thereof Download PDFInfo
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- CN107184483A CN107184483A CN201710517797.6A CN201710517797A CN107184483A CN 107184483 A CN107184483 A CN 107184483A CN 201710517797 A CN201710517797 A CN 201710517797A CN 107184483 A CN107184483 A CN 107184483A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4973—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom
- A61K8/498—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom having 6-membered rings or their condensed derivatives, e.g. coumarin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/06—Production of fats or fatty oils from raw materials by pressing
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0026—Essential oils; Perfumes compounds containing an alicyclic ring not condensed with another ring
- C11B9/003—Essential oils; Perfumes compounds containing an alicyclic ring not condensed with another ring the ring containing less than six carbon atoms
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/70—Biological properties of the composition as a whole
- A61K2800/72—Hypo-allergenic
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
Abstract
A kind of high penetration camellia massage essential oil promoting blood circulation and removing obstruction in channels, is uniformly mixed according to mass fraction by following component:15~25 parts of 70~80 parts of small molecule camellia oil, 2~7 parts of compound essential oil, 0.3~1 part of functional component and base oil component.Wherein compound essential oil is uniformly mixed according to mass fraction by 0.5~1 part of 0.5~1 part of Roman chamomile oil, 0.5~1 part of frankincense essential oil, 0.5~1 part of vetiver oil and Lavender；Wherein functional component is uniformly mixed according to mass fraction by vitamin E or 0.1~0.3 part of 0.1~0.3 part of its succinate, 0.1~0.3 part of Rosmarinus officinalis extract, Tea Polyphenols or its fatty acid ester；Wherein base oil is uniformly mixed according to mass fraction by 5~10 parts of jojoba oil, 3~5 parts of safflower oil, 3~5 parts of Ma Lula oil, 2~5 parts of macadimia nut oil.The camellia massages essential oil without obvious greasy feeling, and osmotic absorption is good, and Glycerin stimulates circulation, promoting blood circulation and removing obstruction in channels.
Description
Technical field
The present invention relates to a kind of essential oil, particularly a kind of high penetration camellia massage essential oil promoting blood circulation and removing obstruction in channels.
Background technology
In current Cosmetic Market, skin care item are the categories ranked the first, and accounting is close to 30%, and sales volume has nearly 160
Hundred million yuan.Skin care item are primarily referred to as the product maintained for individual's skin, typically have moist, whitening, moisturizing, anti-aging by function point
Deng product, essential oil class product therein, due to its pure plant characteristic, and obvious special efficacy, increasingly disappeared by vast
The concern and accreditation of the person of expense.
Essential oil class product, is generally divided into folk prescription essential oil and compound essential oil.
Folk prescription essential oil, be from a certain position with medication effect of medication plant, it is especially a certain with fragrance taste
Position, the single plant elite of extraction, generally with the botanical name or plant parts name nominating, typically has more strong
This plant scent, and with specific effect and characteristics of personality.
Compound essential oil, is, to reach specific using effect or curative effect, two or more folk prescription essential oils to be mixed, essential oil and essence
Can be mutually coordinated between oil, some also have the effect complemented each other, heightened the effect of a treatment, then add base oil to mix.
Essential oil can be combined into by 50-500 kind different moleculars, and be existed jointly with certain proportion so that every kind of plant is all
There is its particularity.Essential oil fragrant, when massaging and being stifling, naturally fragrance enters after brain via olfactory nerves, can pierce
Swash anterior lobe of cerebrum secretion two kinds of hormone of endorphin and enkephalins, make spirit that the state of the most comfortable is presented, releived tightly so as to reach
, bracing effect.Meanwhile, when essential oil is massaged, it can strengthen local blood microcirculation by Transdermal absorption, reach
To stimulating the circulation of the blood and cause the muscles and joints to relax, the function for the QI-blood circulation that relaxs one's muscles, promotes.
Camellia oil, also known as Wild camellia seed oil, tea-seed oil, camellia seed oil, squeeze the seed from tea oil tree.The tradition system of camellia oil
Making process includes shelling, drying, crushing, extracting oil, and filters, overall process is physical method, is fully natural green edible oil.The biography
Erucic acid, cholesterol, aflatoxins and other additives are free of in the tea oil that system technique is pressed, is beneficial to the unsaturated fat of human body
Acid content is up to more than 90%, wherein oleic acid 80-83%, linoleic acid 7-13%, and especially contained linoleic acid, leukotrienes are human bodies
Must and it can not synthesize, rich in vitamin E etc..Camellia oil contains the unrighted acid higher than olive oil and natural dimension
Raw element E, also naturally nourishes skin care ingredient and a variety of anti-oxidant, anti-inflammations, promotion containing Tea Polyphenols, squalene, Tea Saponin etc.
Blood microcirculation composition is beauty treatment moisturizing, clearing and activating the channels and collaterals holy product.
Camellia oil, although with above-mentioned advantage, but because main component is fatty glyceride, viscosity is larger, molecule compared with
When greatly, for skin care item, often show that percutaneous absorption is slow, assimilation effect is poor, skin greasy feeling substantially, the shortcomings of be easily sticky with.
The content of the invention
The purpose of the present invention, is to overcome the deficiencies in the prior art to be massaged there is provided a kind of high penetration camellia promoting blood circulation and removing obstruction in channels
Essential oil, the camellia massages essential oil without obvious greasy feeling, and osmotic absorption is good, and Glycerin stimulates circulation, promoting blood circulation and removing obstruction in channels.
The technical scheme is that：
A kind of high penetration camellia massage essential oil promoting blood circulation and removing obstruction in channels, is uniformly mixed according to mass fraction by following component:It is high
70~80 parts of penetration small molecule camellia oil, 2~7 parts of compound essential oil, 0.3~1 part of functional component and base oil component 15~25
Part.
Described compound essential oil according to mass fraction by 0.5~1 part of silk Roman chamomile oil, 0.5~1 part of frankincense essential oil,
0.5~1 part of 0.5~1 part of vetiver oil and Lavender are uniformly mixed.
Described functional component is extracted according to mass fraction by vitamin E or 0.1~0.3 part of its succinate, rosemary
0.1~0.3 part of 0.1~0.3 part of thing, Tea Polyphenols or its fatty acid ester are uniformly mixed.
Described base oil is according to mass fraction by 5~10 parts of jojoba oil, 3~5 parts of safflower oil, Ma Lula oil 3~5
Part, 2~5 parts of macadimia nut oil are uniformly mixed.
Described small molecule camellia oil, is go glycerine reaction of the camellia oil with ethanol under highly basic existence condition, then through dividing
From, purification, obtain small molecule camellia oil, remain the oleic acid for being beneficial to human body in camellia oil, linoleic acid, leukotrienes, also retain
It is beneficial to vitamin E, Tea Polyphenols, sterol, squalene, Tea Saponin of human body etc. in camellia oil and naturally nourishes skin care ingredient and many
Plant anti-oxidant, anti-inflammation composition, it is preferable that can be made up of following processing step：
Step 1: producing small molecule camellia oil crude product
Raw material is weighed by following proportion by weight：75~85 parts of camellia oil, 15~25 parts of food-grade ethanol, highly basic 0.2~1.0
Part；By the camellia oil weighed, 40~60 DEG C are heated to；Load weighted highly basic is added in food-grade ethanol, makes it fully molten
Solution, is made into alcohol aqueous slkali；Alcohol aqueous slkali is slowly added in camellia oil, 40~70 DEG C, constant temperature stirring at low speed 30~60 are heated to
Minute；It is heated to 80~100 DEG C, constant temperature high-speed stirred 1~2 hour；Cooling, stands 3~4 hours, takes edible vegetable oil liquid thereon；Will be upper
Edible vegetable oil liquid is cooled to -5~5 DEG C, stands 3~4 hours, rapid vacuum suction filtration obtains filtrate；In filtrate add proper amount of active carbon and
Atlapulgite, is heated to 80~100 DEG C, constant temperature is stirred 1-3 hours, filters to obtain high penetration small molecule camellia oil crude product；
Step 2: producing cosmetics-stage high penetration small molecule camellia oil
Step one is made into small molecule camellia oil crude product to be separated in short-range molecular distillation device, plate temperature 130~150 is scraped
DEG C, scraper velocity 200-250r/min, 0.04~0.06MPa of vacuum, condensate liquid are collected as small molecule camellia oil, and heavy phase is given up
Liquid is separately collected.
Contained fatty-acid ethyl ester molecule in the small molecule camellia oil is smaller very than contained fatty glyceride in camellia oil
It is many, where this is the reason for its penetration original is higher than camellia oil, in addition, small molecule camellia oil remain camellia oil it is contained beneficial to
Most contents of the unrighted acids such as oleic acid, linoleic acid, the leukotrienes of human body, remain camellia oil contained vitamin E,
The major part that Tea Polyphenols, squalene, Tea Saponin etc. are naturally nourished in skin care ingredient and a variety of anti-oxidant, anti-inflammation compositions contains
Amount, thus, not only percutaneous absorption speed is fast, and maintenance effect is good, and skin does not have greasy feeling substantially, is not easy to be sticky with, and solves mountain
Percutaneous absorption effect that tea oil has is poor, skin greasy feeling is strong, the shortcomings of be easily sticky with.It is harmful on being typically considered to
Alcohol problems, after tested, detection ethanol in end in the small molecule camellia oil, and ethanol Permissible limit is in cosmetics
2000mg/Kg（《Cosmetics health specification》Version in 2007）.
Preferably, in the step one, camellia oil does not add using obtained by camellia seed physical squeezing by further
Work, it is to avoid the unreasonable refining losses of the contained mentioned component beneficial to human body.
Preferably, in the step one, this kind of camellia oil sorting is good, and processing technology is rationally, contained above-mentioned to be beneficial to human body
Composition content it is high.
In the step one, highly basic can be the one or more in sodium hydroxide, potassium hydroxide, caustic alcohol, potassium ethoxide,
It is preferred that sodium hydroxide cheap and easy to get.
Preferably, in the step one, the esterification conversion ratio of contained fatty glyceride is more than 90% in camellia oil.
Preferably, in the step 2, the distillation yield 55~70% of high penetration small molecule camellia oil is controlled, now, is steamed
Distillation unit operating is more steady, and the quality of gained small molecule camellia oil is preferable.
Preferably, the distillation heavy phase waste liquid in the step 2 is reclaimed, and replaces camellia oil raw material, by being similar to step
One method prepares small molecule camellia oil crude product again, then is separated by the method for step 2, and condensate liquid is used as small molecule mountain
Tea oil is collected, and what distillation heavy phase waste liquid was abandoned no longer uses.
Preferably, Rosmarinus officinalis extract is fat-soluble Rosmarinus officinalis extract, the liposoluble in the compound essential oil functional component
Property Rosmarinus officinalis extract the functional component, high penetration of the present invention it is promoting blood circulation and removing obstruction in channels camellia massage essential oil in dissolubility
More preferably, disperse more preferable, more stable, be more beneficial for playing its effect.
High penetration camellia promoting blood circulation and removing obstruction in channels of the present invention massages the preparation method of essential oil：Each component is uniformly mixed.
High penetration of the present invention camellia promoting blood circulation and removing obstruction in channels massages the use of essential oil, generally with semar technique, such as appropriate to smear
In skin, then the uniform pressing of appropriateness, moderately rub until fully absorbing.
High penetration of the present invention camellia massage essential oil promoting blood circulation and removing obstruction in channels, its preparation technology is simple and reliable, small molecule mountain
Tea oil remains the oleic acid for being beneficial to human body in camellia oil, linoleic acid, leukotrienes, is compounded with other raw materials, can effectively cooperate with each
Active factors penetrates into skin, promotes skin metabolism, and product is naturally grown rich in vitamin E, Tea Polyphenols, squalene, Tea Saponin etc.
Skin care ingredient and a variety of anti-oxidant, anti-inflammation compositions are supported, percutaneous absorption speed is fast, effect is good, and skin does not have greasy feeling substantially,
It is not easy to be sticky with, the shortcomings of solving that the percutaneous absorption effect that camellia oil has is poor, skin greasy feeling is strong, be easily sticky with.It is described
High penetration camellia massage essential oil promoting blood circulation and removing obstruction in channels, stability is good, and penetrating power is strong, good absorbing effect, no greasy feeling, safety temperature
With, it is non-toxic, nonirritant, without anaphylaxis, stimulate circulation, it is promoting blood circulation and removing obstruction in channels, the preferable day of the daily skin care of people can be used as
Right skin care item.
Primary raw material used in the present invention is described as follows：
Camellia oil：Camellia seed kernel is through cleaning, air-drying（Temperature is less than 100 DEG C）, shelling, seed selection sterilization after, at 20-50 DEG C carry out
Squeezing gained, active material enriches, generally about containing vitamin E 90mg/Kg, sterol 30mg/Kg, squalene 20mg/Kg.
Jojoba oil：Also known as jojoba seed oil, SIMMONDSIA CHINENSIS SEED OIL（SIMMONDSIA CHINENSIS, No. CAS:61789-91-
1, INCI：SIMMONDSIA CHINENSIS (JOJOBA) SEED OIL）, it is the monounsaturated fatty acids and straight chain of straight chain
Monounsaturated fatty acid alcohol composition fat.Jojoba, is to be grown in South West USA and Mexico northwest one with Arid desert region
A kind of wild plant, the king of Ren Cheng worlds oil plant.Jojoba oil, is to refine and obtain after flash crotons are squeezed through cold pressing, in gold
Yellow, cured containing abundant mineral matter, vitamin, protein, collagen, plant, moisturizing effect is good, tasteless, and oil is relatively light to be slided seemingly
The grease of adipose gland secretion, permeability is good, extremely stablizes, resistance to strong light, high temperature resistant, and holding structure is constant, can hide long.He Heba
The chemical molecular structure of oil is very similar with the sebum of the mankind, is easy to by skin and absorption, is adapted to all skin quality, especially
It is adapted to dry, coarse, dark and gloomy, oiliness, whelk skin quality, there are very significant beauty functions to skin, it is important natural containing skin
Vitamin and collagenic protein, mineral matter containing high nourishing degree, can massage and protect skin, it is to avoid water loss, nourish deep layer
Skin is takeed good care of, makes skin gloss flexible, and relaxes the injury to skin of exposing to the weather；Skin pH balances can be recovered, wrinkle is gone
Line, is effectively improved Oily, nurses one's health smegma function, pore refining, while being also optimal skin moisture-keeping oil.It institute
The oil film of formation is different from mineral oil, can pass through the moisture of evaporation, can also control the loss of moisture, and improves the skin of inflammation,
Eczema, chronic eczema, pimples etc., it has suitable curative effect to allergic skin with releiving, will not produce acne and antigen, is various skins
The base oil that skin property can be used；Absorption and maintenance that hair moistens material to external world can be promoted, and can be impaired to scalp
Keratan cell rise maintenance effect, its gloss that rejuvenates can be made to Dry Hair and dryness wrinkle skin.Substantial amounts of safety
Property and toxicological test confirm, Jojoba Oil be used as cosmetics be foolproof.
Safflower oil：It is called safflower seed oil, English name Safflowerseed Oil, Classification system Carthamus
Tinctorius L, No. CAS:8001-23-8, INCI：Safflower（carthamus tinctorius) Oil.Safflower
Belong to annual herb plant for composite family safflower.Its Main Ingredients and Appearance is insatiable hunger that is needed by human but can not voluntarily synthesizing in vivo
And aliphatic acid --- linoleic acid, the linoleic content within safflower oil belongs to content highest within current plant, so
Safflower oil is also called as " king of linoleic acid ".It has reducing blood lipid, softening blood vessel, reduces blood pressure and promote microcirculation
Effect；In addition, the vitamin E being rich in safflower oil is a kind of natural, it divides to human body cell, anti-aging has
Important function.Meanwhile, also there is extraordinary effect to the microcirculation of human skin superficial vessels, with promoting blood circulation and removing obstruction in channels, medicine powder for relaxing muscle
The effect of trembling with fear, stimulate circulation.
Ma Lula oil：English name Marula oil, are the Ma Lula trees (Sclerocarya birrea) from Anacardiaceae
Benevolence (nut) is extracted, with it is faint yellow, have nut fragrant, as clear as crystal, Ma Lula oil also include vitamin E, sterol, flavones
Class compound and antioxidant content such as OPC, gallic acid tannin and catechin.The Tsonga people of South Africa Mozambique, uses
This oil is as body moistening oil, and local women uses it as the massage oil of baby.Past, local women using Ma Lula oil rather than
Water cleans oneself.Ma Lula fatty acid oils composition is rich in the oleic acid of omega 9, linoleic acid and palmitoleic acid, can lift guarantor's Wet effects,
Tighten skin moisture and then grow Run skin.Fu Han Victoria life element C (more than orange four times), are described as free radical jinx, can prevent
With the water loss for slowing down skin, the elasticity and flexibility of skin can be kept, helps to rebuild the skin of damage, repairs and compact
Skin.
Macadimia nut oil：It is called Hawaii macadamia nut oil, English name Macadamia nut oil, INCI：
Macadamia ternifolia nut oil,CAS:128497-20-1.Queensland nut is the original evergreen tree in Australia, but is led
The place of production is Hawaii.The oil that the fruit of Hawaii nut is squeezed into is exactly macadimia nut oil.One big feature of macadimia nut oil
It is to contain palmitoleic acid more than 20%.Palmitoleic acid is played an important role in the regeneration of Skin Cell because with age and
Gradually decreasing, therefore whether there is this material is considered as having close relationship with aging.Also contribute to repair wound or eczema is injured
Skin.The composition contained in oil be similar to skin because the age increase and the protection grease of reduction.Oiliness is gentle, and penetration is good,
Skin blood circulation, toxin expelling are helped, moistening effect is good.
Vetiver oil：It is called cus-cus essential oil, English name WETIVER, Classification system Vetiveria zizanioides,
CNIC：Vetiveria zizanioides oil.This product is grass family Vetiveria plant, in amber to olive green or depth
Brown, it is very sticky, it is very deep careful with native fragrance , Yan Smoked tastes.Main component is sesquiterpenoid 60%, sequiterpene ketone
15%.Purifying skin, convergence is anti-infective；Nurse one's health greasy unclean skin；Cell is waken up, improves impaired skin；Strengthen red blood
Ball, therefore there is promoting blood circulation, can treatment of arthritis, rheumatism and myalgia.
Frankincense essential oil：Also known as jasmine caul-fat, INCI JASMINE（JASMINUM OFFICINALE) OIL, CAS:8022-
96-6.The extraction of frankincense essential oil distributes warm pure wooden fragrance, light fruity is appeared again, can be made us from olibanum resin
What impression was had no precedent loosens and releives.Originate in the Lebanon and Iran in the Middle East, the tropical desert of Somalia's most area category
Weather, the west and south is savanna climate, and whole high temperature and little rainfall throughout the year, river is rare, and its special geographical environment makes
The optimal place of production of frankincense essential oil.There is opsonic action for dry, aging, obscure skin, vouchsafe aging skin new life, desalinate scar
Trace, smooth out wrinkles, convergence balance inflammation skin, to for relieving pain, stagnation resolvation, promoting blood circulation effect it is remarkable.
Roman chamomile oil：Also known as blue camomile essential oil, INCI CNAMOMILE (ANTHEMIS NOBILIS) OIL, CAS:
8015-92-7.German foreign chrysanthemum is grown in, a kind of " blue camomile spit of fland " is produced, is a kind of efficient antiallergy material, occur rare
Blueness, be referred to as blue camomile.Potent antibacterial anti-inflammatory, is effective against scytitis, extremely effective in cure to dryness and sensitive skin.Have
Calming nerves are helped, relieving insomnia is helped.Distinctive fragrance can make one to feel happy and auspicious and calmness, have to mood and very big pacify effect
Really, there is reinforcing tissue for skin, eliminate red and swollen and improvement allergy.
Rosmarinus officinalis extract:INCI ROSEMARY (ROSMARINUS OFFICINALIS) EXTRACT, CAS:
84604-14-8.Rosemary, Labiatae Rosmarinus, shrub is high up to 2 meters.Active ingredient includes carnosic acid, Salvia japonica
Phenol, rosmanol, ursolic acid, Rosmarinic acid, major function is anti-oxidant, can improve activities of antioxidant enzymes in human body, suppresses
Lipid peroxidation, the effect with anti-aging, contained Rosmarinic acid and carnosic acid and skin epidermis compatibility are good, are difficult
Be flush with water loss, so good absorbing effect, antioxidation is strong, can also effective stimulus scalp blood circulation, sterilizing and itch-relieving, extensively
It is general to be used for hair products.
Tea Polyphenols：Also known as tea tannin, tannin, English name Tea Polyphenols, CAS:84650-60-2.With extremely strong
Harmful free radicals Scavenging activity, block lipid peroxidation process, improve the activity of human enzymes, thus play anti-mutation, it is anti-
Effect of cancer；Important role is metabolized to body fat, it is possible to decrease the content of cholesterol, triglycerides etc., removes blood vessel
Inwall fat deposition and atheromatous plaque；LOX and lipid peroxidation in skin mitochondria can be suppressed, so that
With anti-aging effect.Antioxidant is substantially better than vitamin E, and has synergy with injection Vitamin B_6；It is water-soluble substances, energy
The greasy of face is removed, pore is restrained, with sterilization, sterilizing, resisting age of skin, the ultraviolet radiation in daylight is reduced to skin
Damage the effects such as, can stop ultraviolet and remove ultraviolet induction free radical, so as to protect the normal of melanocyte
Function, suppresses the formation of melanin, suppresses lipid oxidation, mitigates pigmentation.
Embodiment
Embodiment 1
The high penetration small molecule camellia oil of embodiment 1, is made up of following processing step：
Step 1: producing high penetration small molecule camellia oil crude product
Camellia oil 7500g, food-grade ethanol 2000g, sodium hydroxide 20g are weighed by mass fraction；Camellia oil is heated to 60 DEG C；
Sodium hydroxide is added in food-grade ethanol, it is fully dissolved, is made into alcohol aqueous slkali；Alcohol aqueous slkali is slowly added to camellia oil
In, it is heated to 70 DEG C, constant temperature stirring at low speed 0.5 hour；It is heated to 80 DEG C, constant temperature high-speed stirred 2 hours；It is quickly cooled to often
Temperature, stands 4 hours, takes edible vegetable oil liquid thereon；Supernatant fluid is cooled fast to -5 DEG C（The temperature stood after the cooling of supernatant fluid）,
Stand 3 hours（The time stood after the cooling of supernatant fluid）, fast vacuum suction filtration obtains filtrate 7434ml（Amount of filtrate）；In filtrate
Middle addition 100g activated carbons（Activated carbon addition in filtrate）With 300g atlapulgites（Atlapulgite addition in filtrate）, heating
To 100 DEG C（Filtrate extraction temperature）, constant temperature stirring 1 hour（Filtrate Refining times）, filter to obtain high penetration small molecule camellia oil
Crude product 6528ml；
Step 2: producing cosmetics-stage high penetration small molecule camellia oil
Step one is made into high penetration small molecule camellia oil crude product to be separated in short-range molecular distillation device, plate temperature is scraped
130 DEG C, scraper velocity 200r/min, vacuum 0.06MPa, condensate liquid are collected as small molecule camellia oil, obtain 4047ml, heavy phase
Waste collection, obtains 2481ml.
Embodiment 2-6
Embodiment 2-6 high penetration small molecule camellia oil, the basic be the same as Example 1 of its preparation process condition, simply reaction raw materials
And the condition such as proportion scale, temperature, time is slightly different, specifically as listed in table 1.
Embodiment 7
Gained heavy phase waste liquid will be separated and collected in embodiment 1-6 medium or short range molecular distillation apparatus, it is every kind of respectively to take 1300g, altogether
7800g, substitution camellia oil adds food-grade ethanol 1000g, other basic be the same as Examples of step of preparation process as reaction raw materials
1, simply the condition such as proportion scale, temperature, time be slightly different, specifically as listed in table 1.
The embodiment 1-7 of table 1 high penetration small molecule camellia oil preparation process condition
Embodiment 8-14
Respectively with embodiment 1-7 high penetration small molecule camellia oil, other raw materials are equipped with, through uniform mixing, reality is obtained successively
The high penetration of 8-14 camellia massage essential oil promoting blood circulation and removing obstruction in channels is applied, specific dispensing situation is as listed in table 2.
Comparative example 1
With the raw materials used camellia oil of embodiment 3, replace the high penetration small molecule camellia oil in embodiment 11, other dispensings and ratio
Example be the same as Example 11, is well mixed, and high penetration camellia massage essential oil promoting blood circulation and removing obstruction in channels is made, as a comparison case, is specifically listed in
Table 2.
Comparative example 2
Comparative example 2 eliminates Tea Polyphenols fatty acid ester on the basis of embodiment 11, and other are identical with embodiment 11.
Comparative example 3
Comparative example 3 eliminates Ma Lula oil on the basis of embodiment 11, and other are identical with embodiment 11.
The embodiment 8-14 of table 2 and comparative example compound camellia oil dispensing situation, gram
The behavior pattern of embodiment 8-14 high penetrations camellia massage essential oil promoting blood circulation and removing obstruction in channels and comparative example 1-3 compound camellia oils,
Including viscosity, osmotic absorption speed, promoting blood circulation and removing obstruction in channels, antioxidative stabilizer, table 3 is specifically listed in.
The behavior pattern of the embodiment of table 3 and comparative example
Used method of testing is as follows in table 3:
(1) viscosity of high penetration camellia massage essential oil promoting blood circulation and removing obstruction in channels and compound camellia oil, is determined using capillary tube method.
(2) osmotic absorption speed and performance of keeping humidity one are the impressions after human hand back use；
(3) method of testing promoting blood circulation and removing obstruction in channels:
It is promoting blood circulation and removing obstruction in channels, with dispelling wind and eliminating dampness, the promoting flow of qi and blood circulation, refresh the mind the effect of.Using this product massage skin 20-30 minutes,
Human skin is fully absorbed the active ingredient in this product, QI-blood circulation will be made unobstructed, adjustment human body is caused by stagnation of the circulation of vital energy blood hinders
Sense of discomfort.After the present invention, it will feel that spirit and QI cleaning, pain mitigate, sense of heaviness is eliminated, joint pain sense reduction.
Specific method of testing is as follows:
Choose 80 patients and clinical verification is carried out using embodiment 8-14, its Chinese men and women half and half, the age is in 30-70 Sui, readme
Symptom, is generally experienced as：Four limbs are calm, and arthralgia, knee is ached, and trick has paralysis to feel, and body is tired, listless.Pin
To above-mentioned symptom, appropriateness massage 20-30 minutes is carried out to uncomfortable position or skin in right amount with of the invention, once a day, continuously
Massage 15 days, patient generally reacts state of mind improvement, and joint pain mitigates, body sense of heaviness is eliminated.So as to judge the present invention
The grain that has promoting blood circulation and removing obstruction in channels, relaxing muscles and tendons cold dispelling, qi depression to blood stasis or wind-cold damp pathogen to cause to human body is unfavorable obvious mitigation.
Choose 30 patients and clinical verification carried out using comparative example 1-3, its Chinese men and women half and half, the age at 30-70 Sui, oneself
Symptom is stated, is generally experienced as：Four limbs are calm, and arthralgia, knee is ached, and trick has paralysis to feel, and body is tired, listless.
For above-mentioned symptom, massaged 20-30 minutes, once a day, connected with the appropriate appropriateness that carried out to uncomfortable position or skin of the invention
Continuous massage 15 days, 30 patient's mitigations of comparative example are not obvious, continue to massage 15 days, there is promoting blood circulation and removing obstruction in channels, medicine powder for relaxing muscle to human body
Grain that cold, qi depression to blood stasis or wind-cold damp pathogen are caused is unfavorable just obvious mitigation.
(4) antioxidative stabilizer method of testing：
Test objective：When oxidation of the camellia compound essential oil of Observe and measure embodiments of the invention under different high-temperature conditions is induced
Between calculate that oxidation stability is fixed and shelf life, be that the Thief zone of embodiments of the invention resists the camellia compound essential oil of skin aging strenuously
Product stability foundation is provided.
Test apparatus：Oil oxidative stability analyzer（743 types are led in Switzerland ten thousand）
Experimental procedure：Randomly select the 8-11 embodiments of the present invention camellia compound essential oil weigh respectively it is appropriate in 100,110,
120th, oxidation induction time is determined at 130 DEG C, pass through system plug-in and export shelf life.
Result of the test is shown in Table 4.
Table 4
.
Conclusion (of pressure testing)：The camellia massage essential oil that the high penetration of various embodiments of the present invention is promoting blood circulation and removing obstruction in channels has significant oxidation steady
It is qualitative.
Result listed by table 3,4 illustrates that high penetration of the present invention camellia massage essential oil promoting blood circulation and removing obstruction in channels, viscosity is low, penetration
By force, easily absorb, promoting blood circulation and removing obstruction in channels, relaxing muscles and tendons cold dispelling, antioxidative stabilizer is good, performance is better than compound camellia oil.
In addition, the camellia promoting blood circulation and removing obstruction in channels of the high penetration obtained by embodiment 8-14 is massaged into essential oil, by examining microorganism
Index, sanitary index《Cosmetics health specification》（Version in 2007）, obtain the testing result shown in table 5 below：
Table 5
High penetration of the present invention camellia massage essential oil toxicology test promoting blood circulation and removing obstruction in channels：Skin irritation test（Multiple skin thorn
Swash property experiment）
Test objective：Observe rabbit intact skin long-time multiple-contact tested material（The camellia compound essence of embodiments of the invention
Oil）Produced skin irritation reaction afterwards, is the high penetration of embodiments of the invention camellia massage essential oil promoting blood circulation and removing obstruction in channels
Security foundation is provided.
Test basis：《Cosmetics health specification》Version in 2007
Test method：From white New Zealand rabbits 8,2 groups, every group 4 are randomly divided into.A groups:Intact skin group, B groups:Olive
Sunflower oil control group.24h cuts family's rabbit back backbone both sides hair before experiment, not injured skin surface, unhairing model in cropping
Enclose for 3cm × 3cm, application area is 2.5cm × 2.5cm., tested material group resists flesh strenuously to the Thief zone of various embodiments of the present invention
The camellia compound essential oil of skin aging, takes tested material 0.5ml to be coated directly on the side of back backbone, and opposite side applies 0.5ml control groups
Olive sunflower oil, smears 1 time, continuously smears 14d daily.Since second day, cropping when smearing every time was clear with olive sunflower oil
Except residual tested material.Result is observed after one hour, according to《Cosmetics health specification》The skin irritation test of version in 2007
Table is scored, and check plot and trial zone are equally handled.
Evaluation of result：Every rabbit average integral daily is calculated according to the following formula, is pierced by specification list deciding rabbit skin
Swash intensity, and observe other toxic actions in addition to excitant.
Result of the test：Tested material was carried out in the multiple skin irritation test observation period, gave various embodiments of the present invention
High penetration it is promoting blood circulation and removing obstruction in channels camellia massage essential oil after, rabbit has no erythema, oedema.Have no systemic toxicity profiles performance and dead feelings
Condition, the weight of animals increase, on breathing, circulation, central nervous system, four limbs activity etc. without influence.
Conclusion (of pressure testing)：The camellia that the high penetration of various embodiments of the present invention is promoting blood circulation and removing obstruction in channels massages essential oil to white New Zealand
Rabbit intact skin is nonirritant.
Claims (10)
1. a kind of high penetration camellia massage essential oil promoting blood circulation and removing obstruction in channels, is made up according to mass fraction of following component:High penetration
15~25 parts of 70~80 parts of small molecule camellia oil, 2~7 parts of compound essential oil, 0.3~1 part of functional component and base oil component.
2. high penetration camellia promoting blood circulation and removing obstruction in channels massages essential oil according to claim 1, it is characterised in that：Described compound essence
Oil is according to mass fraction is by 0.5~1 part of Roman chamomile oil, 0.5~1 part of frankincense essential oil, 0.5~1 part of vetiver oil and smokes clothing
Careless 0.5~1 part of essential oil is uniformly mixed.
3. high penetration camellia promoting blood circulation and removing obstruction in channels massages essential oil according to claim 1, it is characterised in that：Described function into
Point according to mass fraction by 0.1~0.3 part of vitamin E or its succinate, 0.1~0.3 part of Rosmarinus officinalis extract, Tea Polyphenols or
0.1~0.3 part of its fatty acid ester is uniformly mixed.
4. essential oil is massaged according to any high penetrations of claim 1-3 camellia promoting blood circulation and removing obstruction in channels, it is characterised in that：Described
Base oil according to mass fraction by 5~10 parts of jojoba oil, 3~5 parts of safflower oil, 3~5 parts of Ma Lula oil, macadimia nut oil 2~
5 parts are uniformly mixed.
5. high penetration camellia promoting blood circulation and removing obstruction in channels massages essential oil according to claim 1, it is characterised in that：Described is hypertonic
Saturating power small molecule camellia oil, is made via following processing step：
Step 1: producing high penetration small molecule camellia oil crude product
Raw material is weighed by following proportion by weight：75~85 parts of camellia oil, 15~25 parts of food-grade ethanol, highly basic 0.2~1.0
Part；By the camellia oil weighed, 50~60 DEG C are heated to；Load weighted highly basic is added in food-grade ethanol, makes it fully molten
Solution, is made into alcohol aqueous slkali；Alcohol aqueous slkali is slowly added in camellia oil, 60~70 DEG C, constant temperature stirring at low speed 30~60 are heated to
Minute；It is then heated to 80~100 DEG C, constant temperature high-speed stirred 1~2 hour；Cooling, stands 3~4 hours, takes edible vegetable oil liquid thereon；
Supernatant fluid is cooled to -5~5 DEG C, 3~4 hours are stood, rapid vacuum suction filtration obtains filtrate；Appropriate activity is added in filtrate
Charcoal and atlapulgite, are heated to 80~100 DEG C, constant temperature is stirred 1-3 hours, filters to obtain high penetration small molecule camellia oil crude product；
Step 2: producing cosmetics-stage high penetration small molecule camellia oil
Step one is made into high penetration small molecule camellia oil crude product to be separated in short-range molecular distillation device, plate temperature is scraped
130~150 DEG C, scraper velocity 200-250r/min, 0.04~0.06MPa of vacuum, condensate liquid is used as high penetration small molecule
Camellia oil is collected, and heavy phase waste liquid is separately collected.
6. high penetration camellia promoting blood circulation and removing obstruction in channels massages essential oil according to claim 5, it is characterised in that：The step one
In, camellia oil is using obtained by physical squeezing.
7. high penetration camellia promoting blood circulation and removing obstruction in channels massages essential oil according to claim 5, it is characterised in that：The step one
In, highly basic is the one or more in sodium hydroxide, potassium hydroxide, caustic alcohol, potassium ethoxide.
8. high penetration camellia promoting blood circulation and removing obstruction in channels massages essential oil according to claim 5, it is characterised in that：In the step 2
Heavy phase waste liquid reclaimed, replace camellia oil raw material, prepare high penetration small molecule again by the method for being similar to step one
Camellia oil crude product, then separated by the method for step 2, condensate liquid is high penetration small molecule camellia oil, distills heavy phase waste liquid
Abandon it.
9. high penetration camellia promoting blood circulation and removing obstruction in channels massages essential oil according to claim 3, it is characterised in that：The rosemary is carried
It is fat-soluble Rosmarinus officinalis extract to take thing.
10. high penetration camellia promoting blood circulation and removing obstruction in channels massages the preparation method of essential oil according to claim 1, it is characterised in that：Will
Each component is uniformly mixed.
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| CN108938828A (en) * | 2018-08-28 | 2018-12-07 | 赖琼玮 | Camellia massage oil of anti-inflammatory invigorates blood circulation stagnation resolvation and preparation method thereof |
| CN111437220A (en) * | 2020-04-29 | 2020-07-24 | 广东聚石化学股份有限公司 | Camellia oil fatty acid ester composition and preparation method and application thereof |
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