CN113876679A

CN113876679A - Multi-effect composition and essence with moisturizing and sensitive skin relieving functions and preparation method thereof

Info

Publication number: CN113876679A
Application number: CN202111310237.6A
Authority: CN
Inventors: 刘静; 陈萍; 马静; 葛红威
Original assignee: TIANJIN YUMEIJING GROUP CO Ltd
Current assignee: TIANJIN YUMEIJING GROUP CO Ltd
Priority date: 2021-11-04
Filing date: 2021-11-04
Publication date: 2022-01-04
Anticipated expiration: 2041-11-04
Also published as: CN113876679B

Abstract

The invention belongs to the field of cosmetics, and particularly relates to a multi-effect composition with the effects of moisturizing and soothing sensitive skin, essence and a preparation method thereof

1-6 parts of ASIA, 0.1-3 parts of Yufuning, 0.1-5 parts of purslane extract and 0.05-0.5 part of Xiyan. The invention selects a specific combination, panthenol,

ASIA, Yuexingning, purslane extract and Ximin repair, so that the composition achieves the effects of moisturizing and relieving, and has multiple-effect cooperation, natural matching, simplicity and high safety.

Description

Multi-effect composition and essence with moisturizing and sensitive skin relieving functions and preparation method thereof

Technical Field

The invention belongs to the field of cosmetics, and particularly relates to a multi-effect composition with the effects of moisturizing and soothing sensitive skin, essence and a preparation method.

Background

Sensitive muscles are the cause of this skin condition in most countries, women and nearly half of men believe themselves have, and they seriously affect quality of life.

The reason for the sensitive skin is not a single one but many factors act together. Such as personal factors and external factors. Personal factors are affected by genetics, sex, endocrine, age, disease, mental stress, etc.; external factors are mainly that skin care products are not suitable, skin care products are not used correctly and can cause damage to skin, the skin is sensitive due to sunlight, temperature, seasonal variation and air pollution, and living habits such as eating and resting habits, spicy food eating, staying up all night and alcohol action. The skin is damaged, so that the moistening degree of the skin is reduced, the immunity of the skin is reduced, and finally, the skin barrier is too weak to resist external stimulation, so that various uncomfortable symptoms such as skin redness, peeling, tightness, stabbing pain, numbness and itching, burning, persistent itching and the like are caused. Sensitive skin is the most difficult of all types to care for, so it is not easy to try for general skin care products.

Based on the special condition of sensitive muscles, water is supplemented firstly, and the skin can carry out normal metabolism only under the condition of sufficient moisture, so that the skin can be better recovered. In the aspects of water replenishing and moisture retention, products without essence and pigment are selected as far as possible, sufficient moisture retention is realized, the balance of water and grease is kept, the external invasion can be effectively resisted,

because of the randomness of sensitive muscle attacks, the demand of emergency repair products which can relieve itching and relieve sensitivity for several minutes is obvious, but the safety requirement of the products is high.

The sensitive muscle groups prefer natural components, so natural, safe and mild natural plant extract components, particularly components extracted from edible natural plant raw materials are selected as core components of the sensitive muscle skin care product.

Disclosure of Invention

The invention aims to provide a multi-effect composition and essence with the functions of moisturizing and soothing sensitive skin and a preparation method thereof.

In order to achieve the purpose, the invention adopts the technical scheme that:

a multi-effect composition with moisturizing and sensitive skin relieving effects comprises, by mass, 0.1-3 parts of panthenol,

1-6 parts of ASIA, 0.1-3 parts of Yufuning, 0.1-5 parts of purslane extract and 0.05-0.5 part of Xiyan.

Preferably, the anti-inflammatory agent comprises, by mass, 0.5 part of panthenol,

3 parts of ASIA, 2 parts of Yufuning, 3 parts of purslane extract and 0.2 part of Ximin.

The invention also comprises a preparation method of the multi-effect composition for moisturizing and soothing sensitive skin, which comprises the following steps:

1) weighing the mixture of the skin care product, the purslane extract and

ASIA, which is mixed and stirred to be dissolved uniformly for later use;

2) sequentially adding panthenol and chlorphenamine, rapidly stirring, and mixing.

The invention also comprises an essence which comprises the following components in percentage by mass: 3 to 7 percent of 1, 3-butanediol, 3 to 5 percent of glycerol, 0.5 to 2 percent of triolein, 0.5 to 2 percent of squalane, 0.5 to 0.9 percent of cetearyl olive oleate, 0.1 to 1 percent of 0.1-tocopheryl acetate, 0.4 to 0.9 percent of sorbitan olive oleate, 0.1 to 0.5 percent of p-hydroxyacetophenone, 0.1 to 0.5 percent of sodium cetearyl sulfate, 0.05 to 0.2 percent of allantoin, 0.05 to 0.3 percent of acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, 0.01 to 0.2 percent of xanthan gum,

1000.05-2%, a chelating agent 0.01-0.05%, a pH regulator 0.01-0.05%, a preservative 0.4-0.9%, a multi-effect composition of claim 1 or 2 10-20%, and the balance water.

The pH regulator is sodium hydroxide; the chelating agent is EDTA-2 Na.

Preferably, the composition comprises the following components in percentage by mass: 6 percent of butanediol, 3 percent of glycerol, 1 percent of squalane, 1 percent of triolein, 0.72 percent of cetearyl olive oleate, 0.5 percent of tocopherol acetate, 0.48 percent of sorbitan olive oleate, 0.3 percent of p-hydroxyacetophenone, 0.2 percent of cetearyl sulfate sodium, 0.11 percent of allantoin, 0.1 percent of acrylic acid (ester)/C10-30 percent of alkanol acrylate cross-linked polymer, 0.05 percent of xanthan gum,

1000.1 percent, 0.05 percent of chelating agent, 0.03 percent of pH regulator, 0.46 percent of preservative, 6.6 to 9.7 parts (preferably, 8.7 percent) of the multi-effect composition and the balance of water.

The invention also comprises a preparation method of the essence, which comprises the following steps:

(1) dispersing xanthan gum in glycerol to obtain a solution 1;

(2) dissolving A91 and ethylhexyl glycerol in butanediol to obtain solution 2;

(3) accurately weighing cetearyl alcohol olive oleate, sorbitan olive oleate, squalane, triolein, vitamin C and vitamin C in an oil phase pretreatment tank,

100. And (3) sequentially putting the tocopherol acetate and the butanediol into a tank, stirring and heating until the tocopherol acetate and the butanediol are completely dissolved, and controlling the temperature of an oil phase at 80-85 ℃ to obtain an oil phase substance.

(4) In a water phase pretreatment tank, the rest deionized water, acrylic acid (acrylate)/C10-30 alkanol acrylate cross-linked polymer, cetearyl alcohol sodium sulfate, solution 1, allantoin, EDTA disodium and p-hydroxyacetophenone are sequentially put into the tank, heated and stirred until the mixture is completely dissolved, and the temperature of the water phase is controlled to be 86-92 ℃.

(5) And (3) sealing the vacuum kettle, starting heating, starting a vacuum pump when the temperature reaches over 50 ℃, sucking the filtered oil phase substances into a preheated emulsification tank after the vacuum degree reaches-0.04 Mpa, then sucking the water phase substances through filtering, starting a scraper for stirring, homogenizing for 25-30 minutes, and carrying out vacuum emulsification. When the temperature in the emulsifying kettle reaches 85 ℃, stopping heating, keeping the temperature, stirring for 15-20 minutes, and beginning to cool.

(6) When the temperature of the paste is reduced to 70-75 ℃, adding a sodium hydroxide solution from a hopper, fully and uniformly stirring, stopping stirring when the temperature of the paste is reduced to 52-55 ℃, putting into vacuum, adding a multi-effect composition of the neutralizing solution 2 from a pot cover, starting vacuum, keeping the temperature, uniformly stirring, and then continuously cooling.

(7) When the temperature is reduced to below 38 ℃, discharging.

Compared with the prior art, the invention has the beneficial effects that:

the invention selects a specific combination, panthenol,

The invention also provides an essence of the multi-effect composition, which provides high-efficiency moisturizing effect by selecting proper oil phase such as squalane, triolein and the like, and the water phase such as allantoin and other functional components are proportioned to achieve the effects of moisturizing and relieving,

the skin care composition with moisturizing and soothing functions comprises the following components by analysis:

panthenol is supplied by basf, germany and is a synthetic precursor of vitamin B5, and D-pantothenic acid plays a key role in the metabolism of the human body. It is a component of coenzyme A. The deficiency of vitamin B5 can cause many skin nerve disorders with deep moistening, epithelial cell growth stimulating, wound healing, and anti-inflammatory effects.

ASIA is provided by lucasmeyer, and mainly comprises bamboo shoot extract of Bombarus domestica (BAMBUSA VULARIS), flos Nelumbinis (Nelumbo NUCIFERA) extract, and radix Nymphaeae (Nymphaea ALBA) extract. The extract of the phyllostachys praecox can supplement skin moisture and eliminate skin inflammation; the lotus extract contains various mineral substances and has strong free radical scavenging capacity and anti-aging effect; the extract of the root of water lily can relieve the skin discomfort caused by neurogenic inflammation. The compound of three Asian moisturizing plants has the advantages of activation, long-acting maintenance of skin hydration and promotion of cell renewal.

The skin-caring medicine adopts green tangerine peels harvested in 5-6 months, the most effective active ingredients in the green tangerine peels are reserved by a biological activity tracking method, the proportion of flavone and alkaloid in the green tangerine peels is controlled to be about 1:1 so as to achieve the optimal effect, and the skin-caring medicine is provided by Shanghai Gaojia Kai biotechnology limited company, can be used for targeted regulation and control of TRPV1 receptors, regulation of the response of skin nerves to stimulation, resetting of skin balance and rapid suppression of skin discomfort response.

The purslane extracting solution is colorless or yellowish clear liquid obtained by squeezing and precipitating whole purslane and then distilling the purslane by steam, has special raw material smell and pH of 4.0-6.0, is provided by Shanghai Luya biotechnology limited company, can hydrate the skin, can relieve inflammation, increases the oxidation resistance of skin cells so as to reduce the damage of free radicals to the skin, and simultaneously has certain help to enhance the barrier function of the skin by conditioning horny layer and maintaining stable skin. Is safe for children's skin and sensitive skin.

The high-activity micromolecule hyaluronic acid is obtained by carrying out natural mild patent enzyme digestion on hyaluronic acid from fermentation sources. Supplied by Huaxi Biotech Ltd. The allergy repairing agent can effectively inhibit the release of inflammatory factors, relieve the skin sensitivity state caused by various factors, and simultaneously can effectively remove free radicals and repair skin damage caused by ultraviolet or chemical substance stimulation.

Drawings

FIG. 1 shows the average water content increase rate of the skin of the examples and the comparative examples.

Detailed Description

In order to make the technical solutions of the present invention better understood by those skilled in the art, the present invention will be further described in detail with reference to the accompanying drawings and preferred embodiments.

Example 1: the raw materials of this example are shown in table 1, and the preparation process of the composition is as follows:

1. weighing 2g of Yufuning, 3g of purslane extract and

3g of ASIA, and stirring and dissolving the ASIA uniformly for later use.

2. Sequentially adding 0.5g of panthenol and 0.2g of chlorphenamine maleate, quickly stirring, and uniformly mixing to obtain the multi-effect composition.

The preparation process of the essence comprises the following steps:

1. firstly, dispersing xanthan gum in glycerin to obtain a solution 1,

2. dissolving A91 and ethylhexylglycerin in butanediol to obtain solution 2,

3. in an oil phase pretreatment tank, the cetearyl alcohol olive oleate, the sorbitan olive oleate, the squalane, the triolein and the water soluble polymer of the component A are weighed,

100. And (3) sequentially putting the tocopherol acetate and the residual butanediol into a tank, stirring and heating until the tocopherol acetate and the residual butanediol are completely dissolved, and controlling the temperature of an oil phase at 80-85 ℃ to obtain an oil phase substance.

4. Weighing the component B, putting deionized water, acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, cetearyl alcohol sodium sulfate, solution 1, allantoin, EDTA disodium and p-hydroxyacetophenone into a water phase pretreatment tank in sequence, heating and stirring until the components are completely dissolved, and controlling the temperature of the water phase at 86-92 ℃.

5. Starting a vacuum pump, sucking the filtered oil phase substances into a preheated emulsifying tank when the temperature reaches above 50 ℃ and the vacuum degree reaches-0.04 Mpa, sucking the filtered water phase substances, starting a scraper to stir (rotating speed is 30Hz), homogenizing for 25-30 minutes (rotating speed is 50Hz) at the same time, and carrying out vacuum emulsification. When the temperature in the emulsifying kettle reaches 85 ℃, stopping heating, keeping the temperature, stirring for 15-20 minutes (the rotating speed is 30Hz), and beginning to cool.

6. When the temperature of the paste is reduced to 70-75 ℃, adding a sodium hydroxide solution from a hopper, fully and uniformly stirring, reducing the temperature of the paste to 52-55 ℃, stopping stirring, vacuumizing, adding the solution 2 and the multi-effect composition from a pot cover, keeping the vacuum, uniformly stirring at a constant temperature (the rotating speed is 15-50Hz), and continuously reducing the temperature.

7. When the temperature is reduced to below 38 ℃, the materials are taken and inspected, the physical and chemical indexes are detected, and the materials can be discharged after the detection is qualified.

Table 1 shows the raw material ratios of the essences prepared in examples 1 to 4 and comparative examples 1 to 5.

TABLE 1

Example 2:

the raw materials of this example are shown in table 1, and the preparation process of the composition is as follows:

1. weighing 3g of Yufuning, 0.1g of purslane extract and

and 6g of ASIA, and stirring and dissolving the ASIA uniformly for later use.

2. Sequentially adding 0.1g of panthenol and 0.5g of chlorphenamine maleate, quickly stirring, and uniformly mixing to obtain the multi-effect composition.

The preparation process of the essence comprises the following steps:

1. firstly, dispersing xanthan gum in glycerin to obtain a solution 1,

2. dissolving A91 and ethylhexyl glycerol in butanediol to obtain solution 2;

100. And (3) sequentially putting the tocopherol acetate and the residual butanediol into a tank, stirring and heating until the tocopherol acetate and the residual butanediol are completely dissolved, and controlling the temperature of an oil phase at 80-85 ℃.

Example 3:

1. weighing 0.1g of Yufuning, 5g of purslane extract and

and 1g of ASIA, and stirring and dissolving the ASIA uniformly for later use.

2. Sequentially adding 3g of panthenol and 0.05g of Xiyanthes, quickly stirring, and uniformly mixing to obtain the multi-effect composition.

The preparation process of the essence comprises the following steps:

1. firstly, dispersing xanthan gum in glycerin to obtain a solution 1,

2. dissolving A91 and ethylhexylglycerin in butanediol to obtain solution 2,

Example 4:

1. weighing 1.5g of Yuexingning, 1g of purslane extract and

2g of ASIA, and stirring and dissolving the ASIA uniformly for later use.

2. Sequentially adding 2g of panthenol and 0.1g of Xiyanthes, quickly stirring, and uniformly mixing to obtain the multi-effect composition.

The preparation process of the essence comprises the following steps:

1. firstly, dispersing xanthan gum in glycerin to obtain a solution 1,

2. dissolving A91 and ethylhexylglycerin in butanediol to obtain solution 2,

ControlExample 1 this comparative example 1 differs from example 1 only in that panthenol is not contained,

ASIA 3.5g, the remainder being in accordance with example 1.

Comparative example 2 this comparative example 2 differs from example 1 only in that it does not contain yuexingnin, 4g of purslane extract,

ASIA 4g, otherwise in accordance with example 1.

Comparative example 3 this comparative example 3 differs from example 1 only in that it does not contain a purslane extract, 3g of yuenheing,

ASIA 5g, otherwise consistent with example 1.

Comparative example 4 this comparative example 4 differs from example 1 only in that it does not contain susceptibility modification,

ASIA 3.2g, the remainder being in accordance with example 1.

Comparative example 5 this comparative example 5 differs from example 1 only in not containing

ASIA, 3g of Yuexingning, 5g of purslane extract, the rest of which is consistent with example 1.

Product effect test 1

A certain amount of 10% lactic acid was applied to the cheek and nasolabial folds, 54 sensitive subjects were screened, randomly divided into 6 groups, and the test results were arithmetically averaged.

Measurement parameters are as follows: pricking discomfort (subjective feeling of subject)

The test method comprises the following steps:

selecting sensitive subject cheek and nasolabial sulcus as test region, respectively performing spot test with 10% lactic acid, and after 5min, the skin has stabbing pain and discomfort feeling, using example (2.0 + -0.1) mg/cm²Comparison of the twoExample product (2.0. + -. 0.1) mg/cm²And no product (blank) was used, and the test site was measured for tingling and discomfort after 0 min, 5min, 15 min, 30 min, 60 min, 120 min, and the results of the specific tests are shown in table 2.

TABLE 2

Table 2 the evaluation results show that: panthenol in the moisturizing and soothing compositions of examples 1-4,

The five compositions of ASIA, Yuexingning, purslane extract and Xianmei have synergistic effect, have certain effect on relieving skin irritation instantly and for a long time, effectively relieve the skin irritation from the outside and calm the skin. The synergistic effect is obviously better than that of other combinations of the control groups 1-5. This indicates that the moisturizing and soothing essence of examples 1 to 4 of the present invention has superior efficacy to the essence of control group 1 to 5.

Second, skin moisture test

50 healthy volunteers are selected, and the test samples are (2.0 +/-0.1) mg/cm²The amount was applied in a single application, the test was evenly spread in the test area using a latex finger cot and the moisture of the skin was assessed after 5 hours. The moisturizing effect of each group of samples was tested in table 3 and fig. 1.

TABLE 3

The test results in table 3 show that the skin moisture content of the subjects is obviously increased after 5 hours of using the essences of examples 1-4, which indicates that the essences have good moisturizing effect, the skin moisture content of the subjects is increased by 28.5% when the subjects use the essences of examples 1-5, and the skin moisture content of the subjects is not increased by more than that of examples 1-4 after 5 hours of using the essences of control groups 1-5, which indicates that one of the multiple-effect compositions is lacked, the synergistic effect of the multiple-effect compositions is reduced, and the moisturizing effect is affected.

The foregoing is only a preferred embodiment of the present invention, and it should be noted that, for those skilled in the art, various modifications and decorations can be made without departing from the principle of the present invention, and these modifications and decorations should also be regarded as the protection scope of the present invention.

Claims

1. A multi-effect composition with the functions of moisturizing and soothing sensitive skin is characterized by comprising, by mass, 0.1-3 parts of panthenol,

2. The multi-effect composition for moisturizing and soothing sensitive skin according to claim 1, comprising, by mass, 0.5 parts of panthenol,

3. A method of preparing a multi-effect composition for moisturizing and soothing sensitive skin according to any one of claims 1-2, comprising the steps of:

1) weighing the mixture of the skin care product, the purslane extract and

ASIA，mixing, stirring and dissolving uniformly for later use;

4. The essence is characterized by comprising the following components in parts by mass: 3 to 7 percent of 1, 3-butanediol, 3 to 5 percent of glycerol, 0.5 to 2 percent of triolein, 0.5 to 2 percent of squalane, 0.5 to 0.9 percent of cetearyl alcohol olive oleate, 0.1 to 1 percent of tocopherol acetate, 0.4 to 0.9 percent of sorbitan olive oleate, 0.1 to 0.5 percent of p-hydroxyacetophenone, 0.1 to 0.5 percent of cetearyl alcohol sodium sulfate, 0.05 to 0.2 percent of allantoin, 0.05 to 0.3 percent of acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, 0.01 to 0.2 percent of xanthan gum,

5. The essence of claim 4, wherein the pH regulator is sodium hydroxide; the chelating agent is EDTA-2 Na.

6. The essence of claim 4, which consists of the following components in percentage by mass: 6 percent of butanediol, 3 percent of glycerol, 1 percent of triolein, 1 percent of squalane, 0.72 percent of cetearyl olive oleate, 0.5 percent of tocopherol acetate, 0.48 percent of sorbitan olive oleate, 0.3 percent of p-hydroxyacetophenone, 0.2 percent of cetearyl sulfate sodium, 0.11 percent of allantoin, 0.1 percent of acrylic acid (ester)/C10-30 percent of alkanol acrylate cross-linked polymer, 0.05 percent of xanthan gum,

1000.1%, chelating agent 0.05%, pH adjusting agent 0.03%, preservative 0.46%, multi-effect composition of claim 1 or 2 6.6-9.7%, balance water.

7. A method for preparing the essence of any one of claims 4 to 6, comprising the steps of:

(1) dispersing xanthan gum in glycerol to obtain a solution 1;

(2) dissolving A91 and ethylhexyl glycerol in butanediol to obtain solution 2;

100. Sequentially putting the tocopherol acetate and the residual butanediol into a tank, stirring and heating until the tocopherol acetate and the residual butanediol are completely dissolved, and controlling the temperature of an oil phase at 80-85 ℃ to obtain an oil phase substance;

(6) When the temperature of the paste is reduced to 70-75 ℃, adding a sodium hydroxide solution from a hopper, fully and uniformly stirring, reducing the temperature of the paste to 52-55 ℃, stopping stirring, vacuumizing, adding the solution 2 and the multi-effect composition from a pot cover, vacuumizing, keeping the temperature, uniformly stirring, and continuously reducing the temperature.

(7) When the temperature is reduced to below 38 ℃, discharging.