CN112980604A - 一种适用于牛仔衣物的防染洗剂及其制备方法 - Google Patents
一种适用于牛仔衣物的防染洗剂及其制备方法 Download PDFInfo
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Abstract
本发明公开了一种适用于牛仔衣物的防染洗剂及其制备方法，该洗剂主要由以下原料制成：山茶籽提取液、脂肪醇聚氧乙烯醚、山梨醇酐月桂酸酯、柠檬酸、乙二醇、偏硅酸钠、环糊精、壳聚糖、蜂胶和去离子水。本发明所制备的防染洗剂具有较高的可实用性，可充分起到防染、防褪色的作用。
Description
技术领域
本发明涉及衣物洗涤剂领域，特别是涉及一种适用于牛仔衣物的防染洗剂及其制备方法。
背景技术
牛仔服或牛仔裤是一种深受人们最喜爱的并且老少皆宜的服装，它会给人一种干练、休闲、舒适的感觉。在现今社会，无论是对青少年来说，还是对中老年人来说，牛仔基本达到了人均必备的程度。并且根据牛仔的布料、设计的款式、加工的工艺以及品牌的效应，牛仔服装的价格也各不相同，而这对于广大群众来说，也有非常多的选择空间。但是牛仔服装也会给人们带来一些困扰，诸如牛仔服装褪色的问题，其在清洗过程中会使水体染色，如果与其他衣物混洗，极易造成其他衣物被染色的风险；并且长其穿牛仔服或牛仔裤时，会发现在一段时间后，与牛仔服装密切接触的浅色衣物、鞋子以及皮肤都会被染色，且极不容易清洗处理。而带来这一系列问题的源头都是牛仔服装褪色造成的。
发明内容
本发明主要目的是解决牛仔服装易褪色的问题，提供了一种适用于牛仔衣物的防染洗剂及其制备方法，它是由如下原料制备而成的：山茶籽提取液、脂肪醇聚氧乙烯醚、山梨醇酐月桂酸酯、柠檬酸、乙二醇、偏硅酸钠、环糊精、壳聚糖、蜂胶和去离子水。
优选地，它含有如下以重量份数计的原料：0.2-1份山茶籽提取液、5-10份脂肪醇聚氧乙烯醚、5-10份山梨醇酐月桂酸酯、0.2-3份柠檬酸、2-10份乙二醇、1-3份偏硅酸钠、0.1-0.5份环糊精、0.1-0.5份壳聚糖、0.05-0.1份蜂胶和70-85份去离子水。
优选地，所述的脂肪醇聚氧乙烯醚的化学通式为RO(C2H4O)n，其中R为碳原子个数在12-18之间的烃基，n为6-8。
本发明还提供了一种适用于牛仔衣物的防染洗剂的制备方法，其具体包括如下步骤：
步骤1：将5-10份脂肪醇聚氧乙烯醚、5-10份山梨醇酐月桂酸酯和70-85份去离子水混和，并于水浴锅中加热5-20min，然后加入1-3份偏硅酸钠，搅拌均匀，将其混合液命名为L1；
步骤2：将0.1-0.5份环糊精和0.1-0.5份壳聚糖溶于2-10份乙二醇中并超声3-5次，然后进行溶剂热反应，待反应结束后，进行洗涤、离心、干燥，将产物加入L1中，再次进行超声分散，搅拌均匀后加入0.2-3份柠檬酸调节pH，然后加入0.05-0.1份蜂胶，加热搅拌5-10min，最后再加入0.2-1份山茶籽提取液，然后搅拌均匀，灭菌包装即可。
优选地，步骤1所述的加热为在42-55℃下进行。
优选地，步骤2所述的溶剂热反应为在120-200℃加热4-12h。
优选地，步骤2所述的超声为在80-120kHz频率下进行，每次超声5-10min。
优选地，步骤2所述的pH为6.5-7.5。
优选地，步骤2所述的加热为在60-70℃下进行。
与现有技术相比，本发明的技术方案具有如下有益效果：
本发明所制备的防染洗剂为具有山茶芳香的偏中性的洗涤液，较适宜人体亲肤衣物的洗涤，该洗涤液中添加的脂肪醇聚氧乙烯醚、山梨醇酐月桂酸酯可以起到乳化、清洁的作用；添加的山茶籽提取液、壳聚糖、环糊精和蜂胶可以起到抗菌作用；并且壳聚糖和蜂胶作为天然防腐剂，又可以维持该洗液的体系稳定性。
本发明所制备的防染洗剂，通过壳聚糖和和蜂胶具有的成膜性能，在牛仔衣物表面形成薄膜，同时利用环糊精的增溶、防静电的作用，对牛仔布料起到良好的固色、防染作用。
具体实施方式
为能进一步了解本发明的发明内容、特征及其优点，通过以下实施例以及对比例来进一步阐述。
实施例1
一种适用于牛仔衣物的防染洗剂，其制备方法包括如下步骤：
步骤1：将10份脂肪醇聚氧乙烯醚、5份山梨醇酐月桂酸酯和75份去离子水混和，并置于水浴锅中，在45℃加下热10min，然后加入3份偏硅酸钠，搅拌均匀，将其混合液命名为L1；
步骤2：将0.5份环糊精和0.5份壳聚糖溶于5份乙二醇中，在100kHz频率下超声3次，每次超声10min，然后在150℃下进行6h的溶剂热反应，待反应结束后，进行洗涤、离心、干燥，将产物加入L1中，再次进行超声分散，搅拌均匀后加入柠檬酸调节pH至7.5，然后加入0.1份蜂胶，加热搅拌5min，最后再加入1份山茶籽提取液，然后搅拌均匀，灭菌包装即可。
实施例2
一种适用于牛仔衣物的防染洗剂，其制备方法包括如下步骤：
步骤1：将5份脂肪醇聚氧乙烯醚、10份山梨醇酐月桂酸酯和适量去离子水混和，并置于水浴锅中，在45℃加下热10min，然后加入3份偏硅酸钠，搅拌均匀，将其混合液命名为L1；
步骤2：将0.2份环糊精和0.2份壳聚糖溶于2份乙二醇中，在100kHz频率下超声3次，每次超声10min，然后在150℃下进行6h的溶剂热反应，待反应结束后，进行洗涤、离心、干燥，将产物加入L1中，再次进行超声分散，搅拌均匀后加入柠檬酸调节pH至7.5，然后加入0.05份蜂胶，加热搅拌5min，最后再加入1份山茶籽提取液，然后搅拌均匀，灭菌包装即可。
对比例1
本发明对比例1与实施例2的区别在于未添加环糊精。
对比例2
本发明对比例2与实施例2的区别在于未添加环糊精、壳聚糖和蜂胶。
选取12件仅洗过一水且连续穿过1个月的蓝色牛仔裤(以上牛仔裤均存在不同程度的褪色问题)，并采用实施例1-2和对比例1-2的技术方案(每组技术方案设有3组平行试验)制得的洗剂进行清洗、晾晒，然后将清洗干净的蓝色牛裤的内外两面对白色毛巾进行轻柔的摩擦，维持30min，观察白色毛巾是否会被染蓝，其具体评价如下表所示。
由上表评价可知，本发明实施例1-2所制备的洗剂不仅具有良好的去污能力，还可以对牛仔起到防褪色、防染色的保护作用。
以上所述是本发明的优选实施方式而已，当然不能以此来限定本发明之权利范围，应当指出，对于本技术领域的普通技术人员来说，在不脱离本发明原理的前提下，还可以做出若干改进和变动，这些都属于本发明的保护范围。这些改进和变动也视为本发明的保护范围。
Claims (9)
1.一种适用于牛仔衣物的防染洗剂，其特征在于，所述防染洗剂含有如下原料：山茶籽提取液、脂肪醇聚氧乙烯醚、山梨醇酐月桂酸酯、柠檬酸、乙二醇、偏硅酸钠、环糊精、壳聚糖、蜂胶和去离子水。
2.根据权利要求1所述的一种适用于牛仔衣物的防染洗剂，其特征在于，所述防染洗剂含有如下以重量份数计的原料：0.2-1份山茶籽提取液、5-10份脂肪醇聚氧乙烯醚、5-10份山梨醇酐月桂酸酯、0.2-3份柠檬酸、2-10份乙二醇、1-3份偏硅酸钠、0.1-0.5份环糊精、0.1-0.5份壳聚糖、0.05-0.1份蜂胶和70-85份去离子水。
3.根据权利要求1所述的一种适用于牛仔衣物的防染洗剂，其特征在于，所述的脂肪醇聚氧乙烯醚的化学通式为RO(C2H4O)n，其中R为碳原子个数在12-18之间的烃基，n为6-8。
4.如权利要求2所述的一种适用于牛仔衣物的防染洗剂的制备方法，其特征在于，包括如下步骤：
步骤1：将5-10份脂肪醇聚氧乙烯醚、5-10份山梨醇酐月桂酸酯和70-85份去离子水混和，并于水浴锅中加热5-20min，然后加入1-3份偏硅酸钠，搅拌均匀，将其混合液命名为L1；
步骤2：将0.1-0.5份环糊精和0.1-0.5份壳聚糖溶于2-10份乙二醇中并超声3-5次，然后进行溶剂热反应，待反应结束后，进行洗涤、离心、干燥，将产物加入L1中，再次进行超声分散，搅拌均匀后加入0.2-3份柠檬酸调节pH，然后加入0.05-0.1份蜂胶，加热搅拌5-10min，最后再加入0.2-1份山茶籽提取液，然后搅拌均匀，灭菌包装即可。
5.根据权利要求4所述的一种适用于牛仔衣物的防染洗剂的制备方法，其特征在于，步骤1所述的加热为在42-55℃下进行。
6.根据权利要求4所述的一种适用于牛仔衣物的防染洗剂的制备方法，其特征在于，步骤2所述的溶剂热反应为在120-200℃加热4-12h。
7.根据权利要求4所述的一种适用于牛仔衣物的防染洗剂的制备方法，其特征在于，步骤2所述的超声为在80-120kHz频率下进行，每次超声5-10min。
8.根据权利要求4所述的一种适用于牛仔衣物的防染洗剂的制备方法，其特征在于，步骤2所述的pH为6.5-7.5。
9.根据权利要求4所述的一种适用于牛仔衣物的防染洗剂的制备方法，其特征在于，步骤2所述的加热为在60-70℃下进行。
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