CN112826767B - Natural plant mask and preparation method thereof - Google Patents
Natural plant mask and preparation method thereof Download PDFInfo
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- CN112826767B CN112826767B CN202110357057.7A CN202110357057A CN112826767B CN 112826767 B CN112826767 B CN 112826767B CN 202110357057 A CN202110357057 A CN 202110357057A CN 112826767 B CN112826767 B CN 112826767B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9728—Fungi, e.g. yeasts
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0212—Face masks
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/42—Amides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
- A61K8/4946—Imidazoles or their condensed derivatives, e.g. benzimidazoles
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/673—Vitamin B group
- A61K8/675—Vitamin B3 or vitamin B3 active, e.g. nicotinamide, nicotinic acid, nicotinyl aldehyde
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/676—Ascorbic acid, i.e. vitamin C
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
Abstract
The invention discloses a natural plant facial mask and a preparation method thereof, wherein the natural plant facial mask comprises a facial mask liquid and facial mask cloth, and the facial mask liquid is prepared from the following raw materials: disodium ethylene diamine tetraacetate, coenzyme Q10, nicotinamide, D-panthenol, allantoin, magnesium ascorbyl phosphate, oat beta-glucan, jojoba oil, hamamelis virginiana extract, poria cocos extract, cherokee rose fruit extract, a stabilizer, a solubilizer, 1, 3-butanediol, glycerol, rose hydrosol and deionized water. The natural plant facial mask disclosed by the invention has good oxidation resistance and good stability; the poria cocos extract and the cherokee rose fruit extract with excellent oxidation resistance are prepared, and have synergistic effect in the aspect of oxidation resistance.
Description
Technical Field
The invention relates to the technical field of cosmetics, and particularly relates to a natural plant facial mask and a preparation method thereof.
Background
The action mechanism of the facial mask comprises two aspects, on one hand, the facial mask can isolate outside air and pollution, improve skin temperature, expand skin pores, promote secretion and metabolism of sweat glands, discharge products of epidermal cell metabolism and accumulated grease, and enable functional components in the facial mask to permeate into horny layers, thereby achieving the purposes of cleaning, moisturizing, whitening, resisting wrinkles, removing acnes and the like.
Skin aging has been a natural enemy of women loving beauty. Researchers have proposed many anti-aging theories, such as the genetic theory, the telomere aging theory, etc., of which the free radical theory is the most powerful. The theory considers that free radicals are normal metabolites of cells, but excessive free radicals generated by aging, medicaments, radiation, tobacco and wine and other factors attack the cells to damage the cells and further accelerate the aging of the organism, so that the key point of delaying the aging is to clear the excessive free radicals.
Disclosure of Invention
The invention provides a natural plant facial mask and a preparation method thereof.
The invention adopts the following technical scheme for solving the technical problems:
the natural plant facial mask comprises a facial mask liquid and facial mask cloth, wherein the facial mask liquid is prepared from the following raw materials in parts by weight: 0.04 to 0.08 portion of disodium ethylene diamine tetraacetate, 0.08 to 0.2 portion of coenzyme Q10, 0.2 to 0.5 portion of nicotinamide, 0.2 to 0.5 portion of D-panthenol, 0.3 to 0.5 portion of allantoin, 0.3 to 0.7 portion of magnesium ascorbyl phosphate, 0.3 to 0.7 portion of oat beta-glucan, 0.3 to 0.8 portion of jojoba oil, 0.4 to 0.8 portion of hamamelis virginiana extract, 0.4 to 0.8 portion of poria cocos extract, 0.4 to 0.8 portion of cherokee rose extract, 0.6 to 1 portion of stabilizer, 1 to 1.6 portions of solubilizer, 2 to 4 portions of 1, 3-butanediol, 3 to 6 portions of glycerin, 5 to 15 portions of rose hydrosol and 70 to 85 portions of deionized water.
As a preferable scheme, the mask liquid is prepared from the following raw materials in parts by weight: 0.04 to 0.07 portion of disodium ethylene diamine tetraacetate, 0.08 to 0.15 portion of coenzyme Q10, 0.2 to 0.4 portion of nicotinamide, 0.2 to 0.4 portion of D-panthenol, 0.35 to 0.5 portion of allantoin, 0.3 to 0.6 portion of magnesium ascorbyl phosphate, 0.3 to 0.6 portion of oat beta-glucan, 0.3 to 0.7 portion of jojoba oil, 0.5 to 0.8 portion of hamamelis virginiana extract, 0.5 to 0.8 portion of poria cocos extract, 0.5 to 0.8 portion of cherokee rose extract, 0.6 to 0.9 portion of stabilizer, 1 to 1.4 portions of solubilizer, 2.5 to 4 portions of 1, 3-butanediol, 3 to 5 portions of glycerin, 8 to 15 portions of rose hydrosol and 70 to 80 portions of deionized water.
As a preferable scheme, the mask liquid is prepared from the following raw materials in parts by weight: 0.06 part of disodium ethylene diamine tetraacetate, 0.1 part of coenzyme Q10, 0.25 part of nicotinamide, 0.3 part of D-panthenol, 0.4 part of allantoin, 0.5 part of magnesium ascorbyl phosphate, 0.5 part of oat beta-glucan, 0.5 part of jojoba oil, 0.6 part of witch hazel extract, 0.7 part of tuckahoe extract, 0.7 part of cherokee rose fruit extract, 0.8 part of stabilizer, 1.2 parts of solubilizer, 3 parts of 1, 3-butanediol, 4 parts of glycerin, 10 parts of rose hydrosol and 76.39 parts of deionized water.
As a preferred scheme, the preparation method of the poria cocos extract comprises the following steps:
s1, cleaning, drying and crushing poria cocos to 60-100 meshes to obtain poria cocos powder;
s2, adding 8-15 parts by weight of poria cocos powder into 85-92 parts by weight of enzymolysis liquid, and carrying out enzymolysis for 4-10 hours at the temperature of 60-75 ℃ to obtain a mixed solution;
s3, distilling the mixed solution with water vapor to obtain an oil-water mixture, and collecting an oil phase to obtain the poria cocos extract.
The inventor of the present invention has surprisingly found in a great deal of research that a component with excellent antioxidant performance is obtained by extracting a volatile oil component of poria cocos through enzyme-assisted steam distillation, and the poria cocos is sufficiently crushed by using saccharifying enzyme, CTAB and trypsin so as to facilitate dissolution of the antioxidant active component.
Preferably, the enzymolysis solution in the S2 is prepared from 0.4 to 1.2 weight parts of saccharifying enzyme, 0.5 to 1.5 weight parts of CTAB, 0.5 to 1.5 weight parts of trypsin and 90 to 98 weight parts of deionized water.
As a preferable scheme, the preparation method of the cherokee rose fruit extract comprises the following steps:
s11, cleaning, drying and crushing the cherokee rose fruit to 60-100 meshes to obtain cherokee rose fruit powder;
s12, adding 10-20 parts by weight of fructus rosae laevigatae powder into 85-92 parts by weight of enzymolysis liquid, and carrying out enzymolysis for 4-10 hours at 60-75 ℃ to obtain a mixed solution;
s13, distilling the mixed solution with water vapor to obtain an oil-water mixture, and collecting an oil phase to obtain the cherokee rose fruit extract.
The invention extracts the volatile oil component of the cherokee rose fruit by enzyme-assisted steam distillation to obtain the component with excellent oxidation resistance, and further discovers that the volatile oil component of the cherokee rose fruit extracted by enzyme-assisted steam distillation has more excellent oxidation resistance than the water-soluble component of the cherokee rose fruit extracted by enzyme-assisted steam distillation.
Preferably, the S12 enzymolysis solution is prepared from 0.4-1 part by weight of pectinase, 0.5-1.5 parts by weight of CTAB, 0.5-1.5 parts by weight of cellulase and 90-98 parts by weight of deionized water.
As a preferable scheme, the solubilizer is tween 80, and the mask cloth is spunlace non-woven cloth.
As a preferable scheme, the stabilizer is prepared from hydrolyzed sclerotium rolfsii gum, chitosan and sodium gluconate according to the weight ratio of (0.1-0.5): (0.2-0.8): 1.
The inventor of the invention surprisingly discovers in research that the poria cocos extract and the cherokee rose fruit extract prepared by the invention have synergistic effect on oxidation resistance.
The poria cocos extract and the cherokee rose fruit extract are volatile oil, so that the stability is insufficient, namely volatilization occurs, the quality loss is caused, and the antioxidant performance of the natural plant mask is influenced, so that a stabilizer is required for preventing the volatilization of the poria cocos extract and the cherokee rose fruit extract. The inventor adopts xanthan gum and carbomer commonly used in the field of cosmetics in the selection of the stabilizer, finds that the xanthan gum and the carbomer can achieve a stable effect to a certain extent, but can still cause large volatilization, and therefore, the inventor adopts the stabilizer consisting of hydrolyzed sclerotium rolfsii gum, chitosan and sodium gluconate in a large amount of research, finds that the stabilizer consisting of hydrolyzed sclerotium rolfsii gum, chitosan and sodium gluconate can effectively prevent volatilization, and avoids causing quality loss.
The invention also provides a preparation method of the natural plant facial mask, which comprises the following steps:
s21, premixing the poria cocos extract, the cherokee rose fruit extract and the solubilizer, adding rose hydrosol, and uniformly mixing to obtain a first mixed solution;
s22, uniformly mixing disodium ethylene diamine tetraacetate, nicotinamide, D-panthenol, oat beta-glucan, jojoba oil, a Hamamelis virginiana extract, 1, 3-butanediol, glycerol and deionized water to obtain a second mixed solution;
s23, uniformly mixing the first mixed solution, the second mixed solution, coenzyme Q10, allantoin, magnesium ascorbyl phosphate and a stabilizer to obtain a facial mask solution;
s24, packaging 20-30 ml of the facial mask liquid and 1 piece of facial mask cloth to obtain the natural plant facial mask.
The invention has the beneficial effects that: (1) The natural plant facial mask disclosed by the invention has good oxidation resistance and good stability, and is natural and non-irritating due to the adoption of the plant extract; (2) The poria cocos extract and the cherokee rose fruit extract with excellent oxidation resistance are prepared, and have a synergistic effect in the aspect of oxidation resistance; (3) The invention extracts the volatile oil component of the tuckahoe by adopting enzyme-assisted steam distillation to obtain the component with excellent oxidation resistance, adopts saccharifying enzyme, CTAB and trypsin to fully crush the tuckahoe and is convenient for dissolving out the antioxidant active component.
Detailed Description
In order to make the objects, technical solutions and advantages of the embodiments of the present invention clearer, the technical solutions in the embodiments of the present invention will be clearly and completely described below, and it is obvious that the described embodiments are a part of the embodiments of the present invention, but not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
In the present invention, the parts are all parts by weight unless otherwise specified. In the invention, the poria cocos extract and the cherokee rose fruit extract are self-made and the rest are commercially available.
Example 1
The natural plant facial mask is prepared from the following raw materials in parts by weight: 0.06 part of disodium ethylene diamine tetraacetate, 0.1 part of coenzyme Q10, 0.25 part of nicotinamide, 0.3 part of D-panthenol, 0.4 part of allantoin, 0.5 part of magnesium ascorbyl phosphate, 0.5 part of oat beta-glucan, 0.5 part of jojoba oil, 0.6 part of witch hazel extract, 0.7 part of tuckahoe extract, 0.7 part of cherokee rose fruit extract, 0.8 part of stabilizer, 1.2 parts of solubilizer, 3 parts of 1, 3-butanediol, 4 parts of glycerin, 10 parts of rose hydrosol and 76.39 parts of deionized water.
The preparation method of the tuckahoe extract comprises the following steps:
s1, cleaning, drying and crushing poria cocos to 90 meshes to obtain poria cocos powder;
s2, adding 12 parts by weight of poria cocos powder into 88 parts by weight of enzymolysis liquid, and carrying out enzymolysis for 5 hours at 72 ℃ to obtain a mixed solution;
s3, distilling the mixed solution with water vapor to obtain an oil-water mixture, and collecting an oil phase to obtain the poria cocos extract.
The enzymolysis solution in the S2 is prepared from 0.8 weight part of saccharifying enzyme, 1 weight part of CTAB, 1.2 weight parts of trypsin and 97 weight parts of deionized water.
The preparation method of the cherokee rose fruit extract comprises the following steps:
s11, cleaning, drying and crushing the cherokee rose fruit to 80 meshes to obtain cherokee rose fruit powder;
s12, adding 14 parts by weight of fructus rosae laevigatae powder into 86 parts by weight of enzymolysis liquid, and carrying out enzymolysis for 6 hours at 68 ℃ to obtain a mixed solution;
s13, distilling the mixed solution with water vapor to obtain an oil-water mixture, and collecting an oil phase to obtain the cherokee rose fruit extract.
The enzymolysis liquid in the S12 is prepared from 0.6 weight part of pectinase, 1.2 weight parts of CTAB, 1.4 weight parts of cellulase and 96.8 weight parts of deionized water.
The solubilizer is Tween 80, and the mask cloth is spunlace non-woven cloth.
The stabilizer is prepared from hydrolyzed sclerotium rolfsii gum, chitosan and sodium gluconate according to the weight ratio of 0.2:0.5: 1.
The preparation method of the natural plant facial mask comprises the following steps:
s21, premixing the poria cocos extract, the cherokee rose fruit extract and the solubilizer, adding rose hydrosol, and uniformly mixing to obtain a first mixed solution;
s22, uniformly mixing disodium ethylene diamine tetraacetate, nicotinamide, D-panthenol, oat beta-glucan, jojoba oil, a Hamamelis virginiana extract, 1, 3-butanediol, glycerol and deionized water to obtain a second mixed solution;
s23, uniformly mixing the first mixed solution, the second mixed solution, coenzyme Q10, allantoin, magnesium ascorbyl phosphate and a stabilizer to obtain a mask solution;
s24, packaging 25ml of facial mask liquid and 1 piece of facial mask cloth to obtain the natural plant facial mask.
Example 2
The natural plant facial mask is prepared from the following raw materials in parts by weight: the mask liquid is prepared from the following raw materials in parts by weight: 0.04 part of disodium ethylene diamine tetraacetate, 0.08 part of coenzyme Q10, 0.2 part of nicotinamide, 0.2 part of D-panthenol, 0.3 part of allantoin, 0.3 part of magnesium ascorbyl phosphate, 0.3 part of oat beta-glucan, 0.3 part of jojoba oil, 0.4 part of witch hazel extract, 0.5 part of poria extract, 0.5 part of cherokee rose fruit extract, 0.6 part of stabilizer, 1 part of solubilizer, 2 parts of 1, 3-butanediol, 3 parts of glycerol, 5 parts of rose hydrosol and 70 parts of deionized water.
The preparation method of the tuckahoe extract comprises the following steps:
s1, cleaning, drying and crushing poria cocos to 90 meshes to obtain poria cocos powder;
s2, adding 12 parts by weight of poria cocos powder into 88 parts by weight of enzymolysis liquid, and carrying out enzymolysis for 5 hours at 72 ℃ to obtain a mixed solution;
and S3, distilling the mixed solution with water vapor to obtain an oil-water mixture, and collecting an oil phase to obtain the poria cocos extract.
The enzymolysis solution in the S2 is prepared from 0.8 weight part of saccharifying enzyme, 1 weight part of CTAB, 1.2 weight parts of trypsin and 97 weight parts of deionized water.
The preparation method of the cherokee rose fruit extract comprises the following steps:
s11, cleaning, drying and crushing the cherokee rose fruit to 80 meshes to obtain cherokee rose fruit powder;
s12, adding 14 parts by weight of fructus rosae laevigatae powder into 86 parts by weight of enzymolysis liquid, and carrying out enzymolysis for 6 hours at 68 ℃ to obtain a mixed solution;
s13, distilling the mixed solution with water vapor to obtain an oil-water mixture, and collecting an oil phase to obtain the cherokee rose fruit extract.
The S12 enzymolysis solution is prepared from 0.6 weight part of pectinase, 1.2 weight parts of CTAB, 1.4 weight parts of cellulase and 96.8 weight parts of deionized water.
The solubilizer is Tween 80, and the mask cloth is spunlace non-woven cloth.
The stabilizer is prepared from hydrolyzed sclerotium rolfsii gum, chitosan and sodium gluconate according to the weight ratio of 0.2:0.5: 1.
The preparation method of the natural plant facial mask comprises the following steps:
s21, premixing the poria cocos extract, the cherokee rose fruit extract and the solubilizer, adding rose hydrosol, and uniformly mixing to obtain a first mixed solution;
s22, uniformly mixing disodium ethylene diamine tetraacetate, nicotinamide, D-panthenol, oat beta-glucan, jojoba oil, a Hamamelis virginiana extract, 1, 3-butanediol, glycerol and deionized water to obtain a second mixed solution;
s23, uniformly mixing the first mixed solution, the second mixed solution, coenzyme Q10, allantoin, magnesium ascorbyl phosphate and a stabilizer to obtain a facial mask solution;
s24, packaging 25ml of facial mask liquid and 1 piece of facial mask cloth to obtain the natural plant facial mask.
Example 3
The natural plant facial mask is prepared from the following raw materials in parts by weight: the mask liquid is prepared from the following raw materials in parts by weight: 0.08 part of disodium ethylene diamine tetraacetate, 0.2 part of coenzyme Q10, 0.5 part of nicotinamide, 0.5 part of D-panthenol, 0.5 part of allantoin, 0.7 part of magnesium ascorbyl phosphate, 0.7 part of oat beta-glucan, 0.8 part of jojoba oil, 0.8 part of witch hazel extract, 0.8 part of tuckahoe extract, 0.8 part of cherokee rose fruit extract, 1 part of stabilizer, 1.6 parts of solubilizer, 4 parts of 1, 3-butanediol, 6 parts of glycerol, 15 parts of rose hydrosol and 85 parts of deionized water.
The preparation method of the poria cocos extract comprises the following steps:
s1, cleaning, drying and crushing poria cocos to 90 meshes to obtain poria cocos powder;
s2, adding 12 parts by weight of poria cocos powder into 88 parts by weight of enzymolysis liquid, and carrying out enzymolysis for 5 hours at 72 ℃ to obtain a mixed solution;
and S3, distilling the mixed solution with water vapor to obtain an oil-water mixture, and collecting an oil phase to obtain the poria cocos extract.
The enzymolysis liquid in the S2 is prepared from 0.8 part by weight of saccharifying enzyme, 1 part by weight of CTAB, 1.2 parts by weight of trypsin and 97 parts by weight of deionized water.
The preparation method of the cherokee rose fruit extract comprises the following steps:
s11, cleaning, drying and crushing the cherokee rose fruit to 80 meshes to obtain cherokee rose fruit powder;
s12, adding 14 parts by weight of fructus rosae laevigatae powder into 86 parts by weight of enzymolysis liquid, and carrying out enzymolysis for 6 hours at 68 ℃ to obtain a mixed solution;
s13, distilling the mixed solution with water vapor to obtain an oil-water mixture, and collecting an oil phase to obtain the cherokee rose fruit extract.
The enzymolysis liquid in the S12 is prepared from 0.6 weight part of pectinase, 1.2 weight parts of CTAB, 1.4 weight parts of cellulase and 96.8 weight parts of deionized water.
The solubilizer is Tween 80, and the mask cloth is spunlace non-woven cloth.
The stabilizer is prepared from hydrolytic sclerotium rolfsii gum, chitosan and sodium gluconate according to the weight ratio of 0.2:0.5: 1.
The preparation method of the natural plant facial mask comprises the following steps:
s21, premixing the poria cocos extract, the cherokee rose fruit extract and the solubilizer, adding rose hydrosol, and uniformly mixing to obtain a first mixed solution;
s22, uniformly mixing disodium ethylene diamine tetraacetate, nicotinamide, D-panthenol, oat beta-glucan, jojoba oil, a Hamamelis virginiana extract, 1, 3-butanediol, glycerol and deionized water to obtain a second mixed solution;
s23, uniformly mixing the first mixed solution, the second mixed solution, coenzyme Q10, allantoin, magnesium ascorbyl phosphate and a stabilizer to obtain a mask solution;
s24, packaging 25ml of facial mask liquid and 1 piece of facial mask cloth to obtain the natural plant facial mask.
Comparative example 1
Comparative example 1 is different from example 1 in that comparative example 1 replaces the cherokee rose fruit extract with the same amount of poria cocos extract, and the others are the same.
Comparative example 2
Comparative example 1 is different from example 1 in that comparative example 1 uses the same amount of cherokee rose-hip extract instead of poria cocos extract, and the others are the same.
Comparative example 3
Comparative example 3 is different from example 1 in that the poria cocos extract as described in comparative example 3 is prepared differently from example 1, and in this comparative example, an aqueous phase is collected, and the others are the same.
The preparation method of the tuckahoe extract comprises the following steps:
s1, cleaning, drying and crushing poria cocos to 90 meshes to obtain poria cocos powder;
s2, adding 12 parts by weight of poria cocos powder into 88 parts by weight of enzymolysis liquid, and carrying out enzymolysis for 5 hours at 72 ℃ to obtain a mixed solution;
and S3, distilling the mixed solution with water vapor to obtain an oil-water mixture, and collecting a water phase to obtain the poria cocos extract.
The enzymolysis liquid in the S2 is prepared from 0.8 part by weight of saccharifying enzyme, 1 part by weight of CTAB, 1.2 parts by weight of trypsin and 97 parts by weight of deionized water.
Comparative example 4
Comparative example 4 is different from example 1 in that the poria cocos extract as described in comparative example 4 is prepared differently from example 1, and in this comparative example, microwave assistance is used instead of enzyme-assisted extraction, and the rest is the same.
The preparation method of the tuckahoe extract comprises the following steps:
s1, cleaning, drying and crushing poria cocos to 90 meshes to obtain poria cocos powder;
s2, adding 12 parts by weight of poria cocos powder into 88 parts of deionized water, uniformly dispersing, placing in a microwave extraction instrument, and treating for 50min under 400W power to obtain a mixed solution;
and S3, distilling the mixed solution with water vapor to obtain an oil-water mixture, and collecting an oil phase to obtain the poria cocos extract.
The enzymolysis liquid in the S2 is prepared from 0.8 part by weight of saccharifying enzyme, 1 part by weight of CTAB, 1.2 parts by weight of trypsin and 97 parts by weight of deionized water.
Comparative example 5
Comparative example 5 is different from example 1 in that the preparation method of the cherokee rose fruit extract described in comparative example 5 is different from example 1, and in this comparative example, an aqueous phase is collected, and the others are the same.
The preparation method of the cherokee rose fruit extract comprises the following steps:
s11, cleaning, drying and crushing the cherokee rose fruit to 80 meshes to obtain cherokee rose fruit powder;
s12, adding 14 parts by weight of fructus rosae laevigatae powder into 86 parts by weight of enzymolysis liquid, and carrying out enzymolysis for 6 hours at 68 ℃ to obtain a mixed solution;
s13, distilling the mixed solution with steam to obtain an oil-water mixture, and collecting a water phase to obtain the cherokee rose fruit extract.
The enzymolysis liquid in the S12 is prepared from 0.6 weight part of pectinase, 1.2 weight parts of CTAB, 1.4 weight parts of cellulase and 96.8 weight parts of deionized water.
Comparative example 6
Comparative example 6 is different from example 1 in that the stabilizer described in comparative example 6 is different from example 1 and the others are the same.
The stabilizer is xanthan gum.
Comparative example 7
Comparative example 7 is different from example 1 in that the stabilizer described in comparative example 7 is different from example 1 and the others are the same.
The stabilizer is carbomer 980.
To further demonstrate the effect of the present invention, the following test methods were provided:
DPPH.clear Capacity measurement: preparing 1X 10 by using absolute ethyl alcohol -4 And (4) storing the DPPH solution in mol/L in dark for later use. Respectively taking 2mL of sample liquid (the mask liquid described in examples 1-3 and comparative examples 1-5, and the sample liquid is tested in preparation 1 d), adding 2mL of prepared DPPH solution into a test tube, uniformly mixing, pouring into a cuvette with an optical diameter of 1cm at room temperature for 30min, measuring the absorbance at 517nm, and measuring the absorbance of a blank sample and a blank sample without the addition of the enzymolysis liquid. The radical clearance to DPPH & is calculated as follows: clearance (%) = (1- (Ai-Aj)/A0) × 100% wherein: ai =2mL DPPH solution + absorbance of 2mL sample solution; aj = absorbance of 2mL sample solution +2mL ethanol; a0=2mL DPPH · solution + absorbance of 2mL sample solvent, the test results are given in table 1.
TABLE 1 Oxidation resistance test results
| DPPH.Rate of removal (%) | |
| Example 1 | 97.5 |
| Example 2 | 92.7 |
| Example 3 | 93.9 |
| Comparative example 1 | 75.8 |
| Comparative example 2 | 76.3 |
| Comparative example 3 | 80.6 |
| Comparative example 4 | 84.3 |
| Comparative example 5 | 82.4 |
As can be seen from Table 1, the natural plant facial mask of the present invention has good antioxidant properties.
As can be seen from the comparison of examples 1-3, the raw material ratios of different natural plant facial masks can affect the antioxidant performance, wherein example 1 has the best antioxidant performance.
As can be seen from the comparison between example 1 and comparative examples 1 and 2, the poria cocos extract and the cherokee rose fruit extract prepared by the invention have synergistic effect on oxidation resistance.
As can be seen from the comparison of example 1 with comparative examples 3 and 4, the poria cocos extract obtained by the enzyme-assisted steam distillation extraction of the present invention has better antioxidant properties than the poria cocos extract obtained by the microwave-assisted steam distillation extraction; and compared with the water phase, the oil phase extracted by the enzyme-assisted steam distillation has better antioxidant property.
As can be seen from the comparison of example 1 with comparative example 5, in the preparation method of the Cherokee rose fruit extract, the oil phase extracted by the enzyme-assisted steam distillation of the present invention has better antioxidant properties than the water phase.
2. And (3) stability investigation: the antioxidant performance of the mask liquid of the examples 1, 6 and 7 is tested to be T0 within 1d after the preparation according to the method 1, the mask liquid of the examples 1, 6 and 7 is placed at 40 ℃ for 60d, the antioxidant performance of the mask liquid is tested to be T60 according to the method 1 again, and the test results are shown in Table 2.
TABLE 2 test results
As can be seen from table 2, the stabilizer described in example 1 can stabilize the formulation system and prevent volatilization of the poria extract and the rosa laevigata extract. If the stabilizer is replaced by conventional xanthan gum or carbomer, the stability will be reduced, and the Poria extract and fructus Rosae Laevigatae extract will volatilize more.
In light of the foregoing description of preferred embodiments according to the invention, it is clear that many changes and modifications can be made by the person skilled in the art without departing from the scope of the invention. The technical scope of the present invention is not limited to the content of the specification, and must be determined according to the scope of the claims.
Claims (5)
1. The natural plant facial mask is characterized by comprising a facial mask liquid and facial mask cloth, wherein the facial mask liquid is prepared from the following raw materials in parts by weight: 0.04 to 0.08 portion of disodium ethylene diamine tetraacetate, 0.08 to 0.2 portion of coenzyme Q10, 0.2 to 0.5 portion of nicotinamide, 0.2 to 0.5 portion of D-panthenol, 0.3 to 0.5 portion of allantoin, 0.3 to 0.7 portion of magnesium ascorbyl phosphate, 0.3 to 0.7 portion of oat beta-glucan, 0.3 to 0.8 portion of jojoba oil, 0.4 to 0.8 portion of hamamelis virginiana extract, 0.4 to 0.8 portion of poria cocos extract, 0.4 to 0.8 portion of cherokee rose extract, 0.6 to 1 portion of stabilizer, 1 to 1.6 portions of solubilizer, 2 to 4 portions of 1, 3-butanediol, 3 to 6 portions of glycerin, 5 to 15 portions of rose hydrosol, and 70 to 85 portions of deionized water;
the preparation method of the tuckahoe extract comprises the following steps:
s1, cleaning, drying and crushing poria cocos to 60-100 meshes to obtain poria cocos powder;
s2, adding 8-15 parts by weight of poria cocos powder into 85-92 parts by weight of enzymolysis liquid, and carrying out enzymolysis for 4-10 hours at the temperature of 60-75 ℃ to obtain a mixed solution;
s3, distilling the mixed solution with water vapor to obtain an oil-water mixture, and collecting an oil phase to obtain a poria cocos extract;
the enzymolysis liquid in the S2 is prepared by 0.4 to 1.2 weight parts of saccharifying enzyme, 0.5 to 1.5 weight parts of CTAB, 0.5 to 1.5 weight parts of trypsin and 90 to 98 weight parts of deionized water;
the preparation method of the cherokee rose fruit extract comprises the following steps:
s11, cleaning, drying and crushing the cherokee rose fruit to 60-100 meshes to obtain cherokee rose fruit powder;
s12, adding 10-20 parts by weight of fructus rosae laevigatae powder into 85-92 parts by weight of enzymolysis liquid, and carrying out enzymolysis for 4-10 hours at 60-75 ℃ to obtain a mixed solution;
s13, distilling the mixed solution with water vapor to obtain an oil-water mixture, and collecting an oil phase to obtain a cherokee rose fruit extract;
the enzymolysis liquid in the S12 is prepared by 0.4 to 1 weight part of pectinase, 0.5 to 1.5 weight parts of CTAB, 0.5 to 1.5 weight parts of cellulase and 90 to 98 weight parts of deionized water;
the stabilizer is prepared from hydrolyzed sclerotium rolfsii gum, chitosan and sodium gluconate according to the weight ratio of (0.1-0.5): (0.2-0.8): 1.
2. The natural plant facial mask according to claim 1, wherein the facial mask solution is prepared from the following raw materials in parts by weight: 0.04 to 0.07 portion of disodium ethylene diamine tetraacetate, 0.08 to 0.15 portion of coenzyme Q10, 0.2 to 0.4 portion of nicotinamide, 0.2 to 0.4 portion of D-panthenol, 0.35 to 0.5 portion of allantoin, 0.3 to 0.6 portion of magnesium ascorbyl phosphate, 0.3 to 0.6 portion of oat beta-glucan, 0.3 to 0.7 portion of jojoba oil, 0.5 to 0.8 portion of hamamelis virginiana extract, 0.5 to 0.8 portion of poria cocos extract, 0.5 to 0.8 portion of cherokee rose extract, 0.6 to 0.9 portion of stabilizer, 1 to 1.4 portions of solubilizer, 2.5 to 4 portions of 1, 3-butanediol, 3 to 5 portions of glycerin, 8 to 15 portions of rose hydrosol and 70 to 80 portions of deionized water.
3. The natural plant mask solution as claimed in claim 1, wherein the mask solution is prepared from the following raw materials in parts by weight: 0.06 part of disodium ethylene diamine tetraacetate, 0.1 part of coenzyme Q10, 0.25 part of nicotinamide, 0.3 part of D-panthenol, 0.4 part of allantoin, 0.5 part of magnesium ascorbyl phosphate, 0.5 part of oat beta-glucan, 0.5 part of jojoba oil, 0.6 part of witch hazel extract, 0.7 part of tuckahoe extract, 0.7 part of cherokee rose fruit extract, 0.8 part of stabilizer, 1.2 parts of solubilizer, 3 parts of 1, 3-butanediol, 4 parts of glycerin, 10 parts of rose hydrosol and 76.39 parts of deionized water.
4. The natural plant facial mask as claimed in claim 1, wherein the solubilizer is tween 80 and the facial mask cloth is spunlace nonwoven fabric.
5. A method for preparing a natural plant facial mask, which is used for preparing the natural plant facial mask as claimed in any one of claims 1 to 4, comprising the following steps:
s21, premixing the poria cocos extract, the cherokee rose fruit extract and the solubilizer, adding rose hydrosol, and uniformly mixing to obtain a first mixed solution;
s22, uniformly mixing disodium ethylene diamine tetraacetate, nicotinamide, D-panthenol, oat beta-glucan, jojoba oil, a Hamamelis virginiana extract, 1, 3-butanediol, glycerol and deionized water to obtain a second mixed solution;
s23, uniformly mixing the first mixed solution, the second mixed solution, coenzyme Q10, allantoin, magnesium ascorbyl phosphate and a stabilizer to obtain a facial mask solution;
and S24, packaging 20-30 ml of facial mask liquid and 1 piece of facial mask cloth to obtain the natural plant facial mask.
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