CN114504530B - Skin care essence with moisturizing and relieving effects and preparation method thereof - Google Patents
Skin care essence with moisturizing and relieving effects and preparation method thereof Download PDFInfo
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- 230000003020 moisturizing effect Effects 0.000 title claims abstract description 49
- 230000000694 effects Effects 0.000 title claims abstract description 30
- 238000002360 preparation method Methods 0.000 title claims abstract description 21
- 235000013399 edible fruits Nutrition 0.000 claims abstract description 41
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 25
- 229940006364 morinda citrifolia extract Drugs 0.000 claims abstract description 20
- 239000003755 preservative agent Substances 0.000 claims abstract description 18
- 230000002335 preservative effect Effects 0.000 claims abstract description 18
- 239000002562 thickening agent Substances 0.000 claims abstract description 18
- BIVBRWYINDPWKA-VLQRKCJKSA-L Glycyrrhizinate dipotassium Chemical compound [K+].[K+].O([C@@H]1[C@@H](O)[C@H](O)[C@H](O[C@@H]1O[C@H]1CC[C@]2(C)[C@H]3C(=O)C=C4[C@@H]5C[C@](C)(CC[C@@]5(CC[C@@]4(C)[C@]3(C)CC[C@H]2C1(C)C)C)C(O)=O)C([O-])=O)[C@@H]1O[C@H](C([O-])=O)[C@@H](O)[C@H](O)[C@H]1O BIVBRWYINDPWKA-VLQRKCJKSA-L 0.000 claims abstract description 15
- 229940082500 cetostearyl alcohol Drugs 0.000 claims abstract description 15
- 229940101029 dipotassium glycyrrhizinate Drugs 0.000 claims abstract description 15
- GLDOVTGHNKAZLK-UHFFFAOYSA-N octadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCCCO GLDOVTGHNKAZLK-UHFFFAOYSA-N 0.000 claims abstract description 15
- OULAJFUGPPVRBK-UHFFFAOYSA-N tetratriacontyl alcohol Natural products CCCCCCCCCCCCCCCCCCCCCCCCCCCCCCCCCCO OULAJFUGPPVRBK-UHFFFAOYSA-N 0.000 claims abstract description 15
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- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 13
- 235000013599 spices Nutrition 0.000 claims abstract description 13
- 229940105902 mint extract Drugs 0.000 claims abstract description 8
- 239000002994 raw material Substances 0.000 claims abstract description 8
- 239000000047 product Substances 0.000 claims description 23
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 20
- 238000003756 stirring Methods 0.000 claims description 15
- 244000131360 Morinda citrifolia Species 0.000 claims description 13
- 235000008898 Morinda citrifolia Nutrition 0.000 claims description 13
- 235000017524 noni Nutrition 0.000 claims description 13
- 238000004108 freeze drying Methods 0.000 claims description 10
- 239000007788 liquid Substances 0.000 claims description 10
- 238000010298 pulverizing process Methods 0.000 claims description 9
- 238000002137 ultrasound extraction Methods 0.000 claims description 8
- 239000011259 mixed solution Substances 0.000 claims description 7
- QCDWFXQBSFUVSP-UHFFFAOYSA-N 2-phenoxyethanol Chemical compound OCCOC1=CC=CC=C1 QCDWFXQBSFUVSP-UHFFFAOYSA-N 0.000 claims description 5
- NIXOWILDQLNWCW-UHFFFAOYSA-N Acrylic acid Chemical compound OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 5
- 239000004322 Butylated hydroxytoluene Substances 0.000 claims description 5
- NLZUEZXRPGMBCV-UHFFFAOYSA-N Butylhydroxytoluene Chemical compound CC1=CC(C(C)(C)C)=C(O)C(C(C)(C)C)=C1 NLZUEZXRPGMBCV-UHFFFAOYSA-N 0.000 claims description 5
- 235000016257 Mentha pulegium Nutrition 0.000 claims description 5
- 244000246386 Mentha pulegium Species 0.000 claims description 5
- 235000004357 Mentha x piperita Nutrition 0.000 claims description 5
- 229920002125 Sokalan® Polymers 0.000 claims description 5
- 229940095259 butylated hydroxytoluene Drugs 0.000 claims description 5
- 235000010354 butylated hydroxytoluene Nutrition 0.000 claims description 5
- 229960001631 carbomer Drugs 0.000 claims description 5
- 238000001816 cooling Methods 0.000 claims description 5
- 239000000706 filtrate Substances 0.000 claims description 5
- 238000001914 filtration Methods 0.000 claims description 5
- 238000010438 heat treatment Methods 0.000 claims description 5
- 235000001050 hortel pimenta Nutrition 0.000 claims description 5
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- 238000004519 manufacturing process Methods 0.000 abstract description 2
- 235000020737 peppermint extract Nutrition 0.000 abstract description 2
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- 230000005923 long-lasting effect Effects 0.000 description 2
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- 239000002904 solvent Substances 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 206010067484 Adverse reaction Diseases 0.000 description 1
- 206010013786 Dry skin Diseases 0.000 description 1
- XQFRJNBWHJMXHO-RRKCRQDMSA-N IDUR Chemical compound C1[C@H](O)[C@@H](CO)O[C@H]1N1C(=O)NC(=O)C(I)=C1 XQFRJNBWHJMXHO-RRKCRQDMSA-N 0.000 description 1
- 206010033733 Papule Diseases 0.000 description 1
- 206010000496 acne Diseases 0.000 description 1
- 230000006838 adverse reaction Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 235000015115 caffè latte Nutrition 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
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Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/342—Alcohols having more than seven atoms in an unbroken chain
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/63—Steroids; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Dermatology (AREA)
- Mycology (AREA)
- Microbiology (AREA)
- Botany (AREA)
- Biotechnology (AREA)
- Engineering & Computer Science (AREA)
- Emergency Medicine (AREA)
- Gerontology & Geriatric Medicine (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a skin care essence with moisturizing and relieving effects, which comprises the following raw materials in parts by weight: 3-5 parts of a vine fruit extract, 4-6 parts of a morinda citrifolia extract, 1-5 parts of a mint extract, 0.5-1 part of dipotassium glycyrrhizinate, 0.3-0.5 part of cetostearyl alcohol, 0.1-0.5 part of a thickening agent, 0.3-0.6 part of a preservative, 0.001-0.005 part of a spice and 40-50 parts of deionized water. The invention adds the vine fruit extract and the morinda citrifolia extract, and the two components play roles in instant moisturizing and long-acting moisturizing under the synergistic effect, so that the invention has better water locking capability, reduces the evaporation of water in skin, improves the water content in skin, and further slows down skin aging. The components such as peppermint extract, dipotassium glycyrrhizinate, cetostearyl alcohol and the like are also added in the skin care essence, so that on one hand, the irritation to skin is reduced; on the other hand, the absorption of the active ingredients is promoted, and the long-acting moisturizing effect is improved. The invention also provides a preparation method of the skin care essence with the moisturizing and soothing effects, the preparation process is simple and convenient and easy to operate, and the commercial production of the product is facilitated.
Description
Technical Field
The invention relates to the field of skin care products, in particular to a skin care essence with moisturizing and relieving effects and a preparation method thereof.
Background
With the improvement of the living standard of substances of people, people pay more and more attention to daily maintenance of skin, wherein cleaning and moisturizing are basic steps in daily maintenance, dirt on the surface of the skin is removed through cleaning products such as facial cleanser, facial cleanser and the like, and after excessive moisture is wiped, skin care products such as skin care water emulsion and the like are utilized to moisturize the skin, so that discomfort to the skin of a human body caused by the skin in a tight state is avoided.
Moisture is the basis of skin metabolism, and skin needs to be nourished by water, and various skin problems such as dryness, roughness, fine lines and the like can occur when the skin is lack of water. Skin dryness is also one of the causative factors for accelerating skin aging, and because dry skin has a thin stratum corneum, it is unfavorable for absorption of active ingredients in skin care products, and the skin condition is hardly improved. The skin moisture is physiologically reduced due to the increase of the age, and external environmental factors such as switching of autumn and winter have great influence on the skin, so that the skin has great crowd demands for moisturizing.
When the skin care product is used, moisture retention components enter the skin along with a solvent at the initial stage of smearing the skin surface, but along with the evaporation of the solvent, a plurality of moisture retention components cannot effectively permeate into the skin cuticle to exert the actual effect, the deep moisture retention requirement of the skin cannot be met, the moisture retention time is short, even the phenomenon of unbalanced skin grease secretion is caused, a plurality of functional components are wasted, and the ideal moisture retention effect cannot be achieved. Meanwhile, some moisturizing functional components are easy to be inactivated due to instability of the moisturizing functional components in an external environment. Therefore, it is necessary to provide a skin care product with stable and deep moisturizing effect.
Disclosure of Invention
In order to overcome the defects of the prior art, one of the purposes of the invention is to provide skin care essence with moisturizing and relieving effects, which has good effects of instant moisturizing and long-acting moisturizing, and is safe in product and free of irritation to skin.
The second purpose of the invention is to provide a preparation method of skin care essence with moisturizing and relieving effects.
One of the purposes of the invention is realized by adopting the following technical scheme:
a skin care essence with moisturizing and relieving effects comprises the following raw materials in parts by weight: 3-5 parts of a vine fruit extract, 4-6 parts of a morinda citrifolia extract, 1-5 parts of a mint extract, 0.5-1 part of dipotassium glycyrrhizinate, 0.3-0.5 part of cetostearyl alcohol, 0.1-0.5 part of a thickening agent, 0.3-0.6 part of a preservative, 0.001-0.005 part of a spice and 40-50 parts of deionized water.
Further, the skin care essence with the moisturizing and soothing effects comprises the following raw materials in parts by weight: 4 parts of a vine fruit extract, 5 parts of a morinda citrifolia extract, 3 parts of a mint extract, 0.8 part of dipotassium glycyrrhizinate, 0.4 part of cetostearyl alcohol, 0.3 part of a thickening agent, 0.4 part of a preservative, 0.003 part of a spice and 45 parts of deionized water.
Further, the preparation process of the vine fruit extract is as follows: peeling ripe vine fruits and pulp, separating to obtain vine fruit seeds, washing the vine fruit seeds, pulverizing to 100 meshes, adding 80-85% ethanol according to a feed-liquid ratio of 1:5-10, performing ultrasonic extraction at 60-70deg.C and power of 100-150W for 20-25min, maintaining at 60deg.C for 30min, filtering with 0.22 μm filter membrane, collecting filtrate, distilling under reduced pressure, and freeze drying.
Further, the Morinda citrifolia extract is prepared by the following steps: pulverizing dried Morinda citrifolia stems and leaves to 80 mesh, adding 80-85% ethanol according to a feed liquid ratio of 1:10-20, performing ultrasonic extraction at 70-80deg.C and power of 300-350W for 10-15min for 2-3 times, collecting extractive solution, distilling under reduced pressure, and freeze drying.
Further, the thickener is composed of carbomer and gamma-polyglutamic acid in a weight ratio of 1:0.05-0.1.
Further, the preservative is composed of phenoxyethanol and butylated hydroxytoluene in a weight ratio of 1:0.5-1.
The second purpose of the invention is realized by adopting the following technical scheme:
the preparation method of the skin care essence with the moisturizing and soothing effects comprises the following steps of:
(1) Adding the extract of the vine fruit, the extract of the morinda citrifolia and the extract of the peppermint into deionized water according to the formula amount, and uniformly stirring and mixing;
(2) Heating the mixed solution obtained in the step (1) to 50-60 ℃, adding dipotassium glycyrrhizinate, cetostearyl alcohol and a thickening agent, and continuously stirring until the mixed solution is uniformly mixed;
(3) Cooling the mixed material in the step (2) to room temperature, adding the preservative and the spice, and uniformly stirring to obtain the product.
Compared with the prior art, the invention has the beneficial effects that: the skin care essence with the moisturizing and soothing effects provided by the invention has the advantages that the latte vine fruit extract and the morinda citrifolia extract are added, the synergistic effect of the two components plays a role in instant moisturizing and long-acting moisturizing, the moisture-retaining capacity is better, the evaporation of moisture in skin is reduced, the moisture content in skin is improved, the skin elasticity is further improved, and the skin aging is slowed down. The components such as peppermint extract, dipotassium glycyrrhizinate, cetostearyl alcohol and the like are also added in the skin care essence, so that on one hand, the irritation to skin is reduced; on the other hand, the absorption of the active ingredients is promoted, and the long-acting moisturizing effect is improved.
The invention also provides a preparation method of the skin care essence with the moisturizing and soothing effects, the preparation process is simple and convenient and easy to operate, and the commercial production of the product is facilitated.
Detailed Description
The present invention will be further described with reference to the following specific embodiments, and it should be noted that, on the premise of no conflict, new embodiments may be formed by any combination of the embodiments or technical features described below.
Example 1
A skin care essence with moisturizing and relieving effects comprises the following raw materials in parts by weight: 4 parts of a vine fruit extract, 5 parts of a morinda citrifolia extract, 3 parts of a mint extract, 0.8 part of dipotassium glycyrrhizinate, 0.4 part of cetostearyl alcohol, 0.3 part of a thickening agent, 0.4 part of a preservative, 0.003 part of a spice and 45 parts of deionized water; the thickener is composed of carbomer and gamma-polyglutamic acid according to the weight ratio of 1:0.08; the preservative consists of phenoxyethanol and butylated hydroxytoluene in a weight ratio of 1:0.7.
The preparation process of the vine fruit extract comprises the following steps: peeling mature vine fruit and pulp, separating to obtain vine fruit seed, washing vine fruit seed, pulverizing to 100 mesh, adding 85% ethanol at a feed-liquid ratio of 1:5, ultrasonic extracting at 60deg.C under power of 150W for 25min, maintaining at 60deg.C for 30min, filtering with 0.22 μm filter membrane, collecting filtrate, distilling under reduced pressure, and freeze drying.
The preparation process of the morinda citrifolia extract comprises the following steps: pulverizing dried Morinda citrifolia stems and leaves to 80 meshes, adding 85% ethanol according to a feed-liquid ratio of 1:10, performing ultrasonic extraction at 70deg.C and power of 350W for 15min for 3 times, collecting extractive solution, distilling under reduced pressure, and freeze drying.
The preparation method of the skin care essence with the moisturizing and soothing effects comprises the following steps of:
(1) Adding the extract of the vine fruit, the extract of the morinda citrifolia and the extract of the peppermint into deionized water according to the formula amount, and uniformly stirring and mixing;
(2) Heating the mixed solution obtained in the step (1) to 50 ℃, adding dipotassium glycyrrhizinate, cetostearyl alcohol and a thickening agent, and continuously stirring until the mixture is uniformly mixed;
(3) Cooling the mixed material in the step (2) to room temperature, adding the preservative and the spice, and uniformly stirring to obtain the product.
Example 2
A skin care essence with moisturizing and relieving effects comprises the following raw materials in parts by weight: 3 parts of a vine fruit extract, 4 parts of a morinda citrifolia extract, 1 part of a mint extract, 0.5 part of dipotassium glycyrrhizinate, 0.3 part of cetostearyl alcohol, 0.1 part of a thickening agent, 0.3 part of a preservative, 0.001 part of a spice and 40 parts of deionized water; the thickener is composed of carbomer and gamma-polyglutamic acid according to the weight ratio of 1:0.05; the preservative consists of phenoxyethanol and butylated hydroxytoluene in a weight ratio of 1:0.5.
The preparation process of the vine fruit extract comprises the following steps: peeling mature vine fruit, separating to obtain vine fruit seed, washing vine fruit seed, pulverizing to 100 mesh, adding 88% ethanol at a feed-liquid ratio of 1:8, ultrasonic extracting at 65deg.C and power of 120W for 22min, maintaining at 60deg.C for 30min, filtering with 0.22 μm filter membrane, collecting filtrate, distilling under reduced pressure, and freeze drying.
The preparation process of the morinda citrifolia extract comprises the following steps: pulverizing dried Morinda citrifolia stems and leaves to 80 meshes, adding 805% ethanol according to a feed-liquid ratio of 1:15, performing ultrasonic extraction at 75deg.C and power of 330W for 12min, performing ultrasonic extraction for 2 times, collecting extractive solution, distilling under reduced pressure, and freeze drying.
The preparation method of the skin care essence with the moisturizing and soothing effects comprises the following steps of:
(1) Adding the extract of the vine fruit, the extract of the morinda citrifolia and the extract of the peppermint into deionized water according to the formula amount, and uniformly stirring and mixing;
(2) Heating the mixed solution obtained in the step (1) to 55 ℃, adding dipotassium glycyrrhizinate, cetostearyl alcohol and a thickening agent, and continuously stirring until the mixture is uniformly mixed;
(3) Cooling the mixed material in the step (2) to room temperature, adding the preservative and the spice, and uniformly stirring to obtain the product.
Example 3
A skin care essence with moisturizing and relieving effects comprises the following raw materials in parts by weight: 5 parts of a vine fruit extract, 6 parts of a morinda citrifolia extract, 5 parts of a mint extract, 1 part of dipotassium glycyrrhizinate, 0.5 part of cetostearyl alcohol, 0.5 part of a thickening agent, 0.6 part of a preservative, 0.005 part of a spice and 50 parts of deionized water; the thickener is composed of carbomer and gamma-polyglutamic acid according to the weight ratio of 1:0.1; the preservative consists of phenoxyethanol and butylated hydroxytoluene in a weight ratio of 1:1.
The preparation process of the vine fruit extract comprises the following steps: peeling ripe vine fruit and pulp, separating to obtain vine fruit seed, washing vine fruit seed, pulverizing to 100 mesh, adding 80% ethanol according to a feed-liquid ratio of 1:10, ultrasonic extracting at 70deg.C under power of 100W for 20min, maintaining at 60deg.C for 30min, filtering with 0.22 μm filter membrane, collecting filtrate, distilling under reduced pressure, and freeze drying.
The preparation process of the morinda citrifolia extract comprises the following steps: pulverizing dried Morinda citrifolia stems and leaves to 80 mesh, adding 80% ethanol according to a feed-liquid ratio of 1:20, performing ultrasonic extraction at 80deg.C under power of 300W for 10min for 2 times, collecting extractive solution, distilling under reduced pressure, and freeze drying.
The preparation method of the skin care essence with the moisturizing and soothing effects comprises the following steps of:
(1) Adding the extract of the vine fruit, the extract of the morinda citrifolia and the extract of the peppermint into deionized water according to the formula amount, and uniformly stirring and mixing;
(2) Heating the mixed solution obtained in the step (1) to 60 ℃, adding dipotassium glycyrrhizinate, cetostearyl alcohol and a thickening agent, and continuously stirring until the mixture is uniformly mixed;
(3) Cooling the mixed material in the step (2) to room temperature, adding the preservative and the spice, and uniformly stirring to obtain the product.
Comparative example 1
Comparative example 1 provides a skin care essence with moisturizing and soothing effects, which differs from example 1 in that: the extract of the vine fruit was omitted and the rest was the same as in example 1.
Comparative example 2
Comparative example 2 provides a skin care essence with moisturizing and soothing effects, which differs from example 1 in that: the Morinda citrifolia extract was omitted and the remainder was the same as in example 1.
Comparative example 3
Comparative example 3 provides a skin care essence with moisturizing and soothing effects, which differs from example 1 in that: the extract of the vine fruit was omitted and the amount of the Morinda citrifolia extract was adjusted to 9 parts, the remainder being the same as in example 1.
Comparative example 4
Comparative example 4 provides a skin care essence with moisturizing and soothing effects, which differs from example 1 in that: the Morinda citrifolia extract was omitted and the amount of the extract was adjusted to 9 parts, the remainder being the same as in example 1.
50 volunteers aged 30-40 years were selected, of which 15 men and 35 women were randomly divided into 5 groups of 10 persons each, using the products of example 1, comparative examples 1 to 4, respectively. The subjects evenly spread the corresponding products on the face, and the water content in the skin was measured by using German CK Corneometer CM825 for 0h, 4h, 8h and 12h after the use of the products before the use of the products, respectively, and the change of the skin water content was counted as compared with the water content before the use of the products, as shown in Table 1.
TABLE 1
| Sample of | 0h | 4h | 8h | 12h |
| Example 1 | +41.79% | +36.36% | +30.73% | +23.51% |
| Comparative example 1 | +31.24% | +25.91% | +18.14% | +10.31% |
| Comparative example 2 | +36.50% | +28.42% | +18.09% | +7.33% |
| Comparative example 3 | +33.62% | +26.04% | +19.42% | +10.75% |
| Comparative example 4 | +34.01% | +25.17% | +15.61% | +4.83% |
It can be seen from table 1 that the product of example 1 has both the instant moisturizing effect and the long-lasting moisturizing effect superior to those of comparative examples 1 to 4. The instant moisturizing effect of the product was significantly reduced by omitting the extract of the vine fruit in comparative example 1, the moisture content in the skin was reduced with the lapse of time, and the moisture content in the skin was lower than in example 1 at 12 h. The elimination of the Morinda citrifolia extract in comparative example 2, the moisture content in the skin at 0h was lower than in example 1 and higher than in comparative example 1, indicating that the product of comparative example 2 showed superior instant moisturizing effect to the product of comparative example 1 after elimination of the Morinda citrifolia extract, but the moisture content in the skin was significantly reduced over time, with less long-lasting moisturizing effect than in comparative example 1. In comparative examples 3 and 4, the use amount of the remaining components is increased after one of the extract of the vine fruit and the extract of the morinda citrifolia is omitted, so that the instant moisturizing effect and the long-acting moisturizing effect of the extract of the vine fruit and the extract of the morinda citrifolia are lower than those of example 1, and further the synergistic effect of the two components of the extract of the vine fruit and the extract of the morinda citrifolia added in the skin care essence provided by the invention plays the roles of instant moisturizing and long-acting moisturizing, so that the skin care essence has better water locking capability, reduces the evaporation of water in the skin, improves the water content in the skin, further improves the skin elasticity and slows down the skin aging.
Subjects were selected for patch testing in 30 subjects, between 30 and 40 years of age, and half of each male and female, randomly divided into 3 groups of 10 subjects each. About 0.02-0.03g of the products of examples 1-3 were placed in a plaque tester, respectively, and applied to the back of a subject with a medical tape, removed after 24 hours, and skin reactions were observed at 0.5h,24h and 48h, respectively, and the results were recorded according to the skin reactions in the cosmetic safety technical Specification, and the standard is shown in Table 1.
TABLE 1
| Grade | Skin reaction |
| 0 | Negative reaction |
| 1 | Suspicious reaction: weak erythema |
| 2 | Weak positive reaction: skin erythema, pimple |
| 3 | Strong positive reaction: skin erythema, edema, papule, herpes, and reactions beyond the test area |
| 4 | Very strong positive reaction: obvious erythema, severe edema and reaction beyond the tested area of the skin |
Through observation, the participating subjects do not have adverse reactions (all are negative), which indicates that the skin care essence provided by the invention has mild efficacy and no stimulation to skin.
The above embodiments are only preferred embodiments of the present invention, and the scope of the present invention is not limited thereto, but any insubstantial changes and substitutions made by those skilled in the art on the basis of the present invention are intended to be within the scope of the present invention as claimed.
Claims (5)
1. The skin care essence with the moisturizing and soothing effects is characterized by comprising the following raw materials in parts by weight: 3-5 parts of a vine fruit extract, 4-6 parts of a morinda citrifolia extract, 1-5 parts of a mint extract, 0.5-1 part of dipotassium glycyrrhizinate, 0.3-0.5 part of cetostearyl alcohol, 0.1-0.5 part of a thickening agent, 0.3-0.6 part of a preservative, 0.001-0.005 part of a spice and 40-50 parts of deionized water;
the preparation process of the vine fruit extract comprises the following steps: peeling ripe vine fruits and pulp, separating to obtain vine fruit seeds, washing the vine fruit seeds, crushing to 100 meshes, adding 80-85% ethanol according to a feed-liquid ratio of 1:5-10, performing ultrasonic extraction for 20-25min at a temperature of 60-70 ℃ and a power of 100-150W, preserving heat for 30min at 60 ℃, filtering with a 0.22 mu m filter membrane, collecting filtrate, performing reduced pressure distillation, and performing freeze drying to obtain the Chinese medicinal composition;
the preparation process of the morinda citrifolia extract comprises the following steps: pulverizing dried Morinda citrifolia stems and leaves to 80 mesh, adding 80-85% ethanol according to a feed liquid ratio of 1:10-20, performing ultrasonic extraction at 70-80deg.C and power of 300-350W for 10-15min for 2-3 times, collecting extractive solution, distilling under reduced pressure, and freeze drying.
2. The skin care essence with moisturizing and soothing effects as claimed in claim 1, which is characterized by comprising the following raw materials in parts by weight: 4 parts of a vine fruit extract, 5 parts of a morinda citrifolia extract, 3 parts of a mint extract, 0.8 part of dipotassium glycyrrhizinate, 0.4 part of cetostearyl alcohol, 0.3 part of a thickening agent, 0.4 part of a preservative, 0.003 part of a spice and 45 parts of deionized water.
3. The skin care essence with moisturizing and soothing effects according to claim 1, wherein the thickener is composed of carbomer and gamma-polyglutamic acid in a weight ratio of 1:0.05-0.1.
4. The skin care essence with moisturizing and soothing effects as claimed in claim 1, wherein the preservative is composed of phenoxyethanol and butylated hydroxytoluene in a weight ratio of 1:0.5-1.
5. The method for preparing skin care essence with moisturizing and soothing effects according to any one of claims 1 to 4, comprising the steps of:
(1) Adding the extract of the vine fruit, the extract of the morinda citrifolia and the extract of the peppermint into deionized water according to the formula amount, and uniformly stirring and mixing;
(2) Heating the mixed solution obtained in the step (1) to 50-60 ℃, adding dipotassium glycyrrhizinate, cetostearyl alcohol and a thickening agent, and continuously stirring until the mixed solution is uniformly mixed;
(3) Cooling the mixed material in the step (2) to room temperature, adding the preservative and the spice, and uniformly stirring to obtain the product.
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Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108653140A (en) * | 2018-06-28 | 2018-10-16 | 广西浙缘农业科技有限公司 | A kind of camellia seed oil cosmetic composition and preparation method thereof |
| CN111803413A (en) * | 2020-07-08 | 2020-10-23 | 爱诗欧迪生物科技(海南)有限公司 | Noni SOD skin care product and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108653140A (en) * | 2018-06-28 | 2018-10-16 | 广西浙缘农业科技有限公司 | A kind of camellia seed oil cosmetic composition and preparation method thereof |
| CN111803413A (en) * | 2020-07-08 | 2020-10-23 | 爱诗欧迪生物科技(海南)有限公司 | Noni SOD skin care product and preparation method thereof |
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| Title |
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| 李黎仙 等.舒缓修复面膜制备及效果观察.香料香精化妆品.2020,(第03期),33-37. * |
| 梅全喜.广东地产药材研究.广东科技出版社,2011,572-574. * |
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Effective date of registration: 20231010 Address after: Room 701A, Block B, Building 9, No. 2679 Hechuan Road, Minhang District, Shanghai, 201100 Applicant after: Shanghai feike'er Cosmetics Co.,Ltd. Address before: 210000 School of Bioscience and medical engineering, Southeast University, No. 2 Sipailou, Xinjiekou Street, Xuanwu District, Nanjing, Jiangsu Province Applicant before: Cui Yanting |
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