CN112516047A - Oil-control hair washing gel and preparation method thereof - Google Patents
Oil-control hair washing gel and preparation method thereof Download PDFInfo
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- CN112516047A CN112516047A CN202011475749.3A CN202011475749A CN112516047A CN 112516047 A CN112516047 A CN 112516047A CN 202011475749 A CN202011475749 A CN 202011475749A CN 112516047 A CN112516047 A CN 112516047A
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- 210000004209 hair Anatomy 0.000 title claims abstract description 75
- 238000005406 washing Methods 0.000 title claims abstract description 57
- 238000002360 preparation method Methods 0.000 title abstract description 16
- 238000001879 gelation Methods 0.000 title description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical class [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 163
- QXNVGIXVLWOKEQ-UHFFFAOYSA-N Disodium Chemical compound [Na][Na] QXNVGIXVLWOKEQ-UHFFFAOYSA-N 0.000 claims abstract description 44
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims abstract description 31
- 229910052708 sodium Inorganic materials 0.000 claims abstract description 31
- 239000011734 sodium Substances 0.000 claims abstract description 31
- JDRSMPFHFNXQRB-CMTNHCDUSA-N Decyl beta-D-threo-hexopyranoside Chemical compound CCCCCCCCCCO[C@@H]1O[C@H](CO)C(O)[C@H](O)C1O JDRSMPFHFNXQRB-CMTNHCDUSA-N 0.000 claims abstract description 25
- MRUAUOIMASANKQ-UHFFFAOYSA-N cocamidopropyl betaine Chemical compound CCCCCCCCCCCC(=O)NCCC[N+](C)(C)CC([O-])=O MRUAUOIMASANKQ-UHFFFAOYSA-N 0.000 claims abstract description 25
- 229940073499 decyl glucoside Drugs 0.000 claims abstract description 25
- 108700004121 sarkosyl Proteins 0.000 claims abstract description 25
- 229940057950 sodium laureth sulfate Drugs 0.000 claims abstract description 25
- 229940045885 sodium lauroyl sarcosinate Drugs 0.000 claims abstract description 25
- KSAVQLQVUXSOCR-UHFFFAOYSA-M sodium lauroyl sarcosinate Chemical compound [Na+].CCCCCCCCCCCC(=O)N(C)CC([O-])=O KSAVQLQVUXSOCR-UHFFFAOYSA-M 0.000 claims abstract description 25
- SXHLENDCVBIJFO-UHFFFAOYSA-M sodium;2-[2-(2-dodecoxyethoxy)ethoxy]ethyl sulfate Chemical compound [Na+].CCCCCCCCCCCCOCCOCCOCCOS([O-])(=O)=O SXHLENDCVBIJFO-UHFFFAOYSA-M 0.000 claims abstract description 25
- 229940079988 potassium cocoyl glycinate Drugs 0.000 claims abstract description 19
- 229940065859 sodium cocoyl glycinate Drugs 0.000 claims abstract description 19
- IKGKWKGYFJBGQJ-UHFFFAOYSA-M sodium;2-(dodecanoylamino)acetate Chemical compound [Na+].CCCCCCCCCCCC(=O)NCC([O-])=O IKGKWKGYFJBGQJ-UHFFFAOYSA-M 0.000 claims abstract description 19
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims abstract description 13
- 229920002678 cellulose Polymers 0.000 claims abstract description 8
- 239000001913 cellulose Substances 0.000 claims abstract description 8
- QGZKDVFQNNGYKY-UHFFFAOYSA-O ammonium group Chemical class [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 claims abstract description 3
- 239000011259 mixed solution Substances 0.000 claims description 130
- 238000003756 stirring Methods 0.000 claims description 104
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 75
- 241000234314 Zingiber Species 0.000 claims description 69
- 235000006886 Zingiber officinale Nutrition 0.000 claims description 69
- 235000008397 ginger Nutrition 0.000 claims description 69
- 239000000843 powder Substances 0.000 claims description 46
- 235000011389 fruit/vegetable juice Nutrition 0.000 claims description 33
- 238000010411 cooking Methods 0.000 claims description 30
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 28
- 235000002639 sodium chloride Nutrition 0.000 claims description 28
- 239000011780 sodium chloride Substances 0.000 claims description 28
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 28
- 229940073507 cocamidopropyl betaine Drugs 0.000 claims description 24
- 229920002134 Carboxymethyl cellulose Polymers 0.000 claims description 22
- 102000011782 Keratins Human genes 0.000 claims description 22
- 108010076876 Keratins Proteins 0.000 claims description 22
- 239000001768 carboxy methyl cellulose Substances 0.000 claims description 22
- 235000010948 carboxy methyl cellulose Nutrition 0.000 claims description 22
- 239000008112 carboxymethyl-cellulose Substances 0.000 claims description 22
- 239000000203 mixture Substances 0.000 claims description 20
- 238000004140 cleaning Methods 0.000 claims description 15
- 238000000034 method Methods 0.000 claims description 14
- NCZPCONIKBICGS-UHFFFAOYSA-N 3-(2-ethylhexoxy)propane-1,2-diol Chemical compound CCCCC(CC)COCC(O)CO NCZPCONIKBICGS-UHFFFAOYSA-N 0.000 claims description 12
- ANZUDYZHSVGBRF-UHFFFAOYSA-N 3-ethylnonane-1,2,3-triol Chemical compound CCCCCCC(O)(CC)C(O)CO ANZUDYZHSVGBRF-UHFFFAOYSA-N 0.000 claims description 12
- VFKZECOCJCGZQK-UHFFFAOYSA-M 3-hydroxypropyl(trimethyl)azanium;chloride Chemical compound [Cl-].C[N+](C)(C)CCCO VFKZECOCJCGZQK-UHFFFAOYSA-M 0.000 claims description 12
- LXAHHHIGZXPRKQ-UHFFFAOYSA-N 5-fluoro-2-methylpyridine Chemical compound CC1=CC=C(F)C=N1 LXAHHHIGZXPRKQ-UHFFFAOYSA-N 0.000 claims description 12
- 239000003109 Disodium ethylene diamine tetraacetate Substances 0.000 claims description 12
- ZGTMUACCHSMWAC-UHFFFAOYSA-L EDTA disodium salt (anhydrous) Chemical compound [Na+].[Na+].OC(=O)CN(CC([O-])=O)CCN(CC(O)=O)CC([O-])=O ZGTMUACCHSMWAC-UHFFFAOYSA-L 0.000 claims description 12
- 238000006243 chemical reaction Methods 0.000 claims description 12
- 235000019301 disodium ethylene diamine tetraacetate Nutrition 0.000 claims description 12
- 229940100524 ethylhexylglycerin Drugs 0.000 claims description 12
- 238000010438 heat treatment Methods 0.000 claims description 12
- 238000002156 mixing Methods 0.000 claims description 12
- 230000001954 sterilising effect Effects 0.000 claims description 12
- 238000004659 sterilization and disinfection Methods 0.000 claims description 12
- 238000010009 beating Methods 0.000 claims description 11
- 238000007605 air drying Methods 0.000 claims description 10
- 238000001914 filtration Methods 0.000 claims description 10
- 238000000227 grinding Methods 0.000 claims description 10
- 239000002453 shampoo Substances 0.000 claims description 10
- 238000007873 sieving Methods 0.000 claims description 10
- 238000010981 drying operation Methods 0.000 claims description 6
- 229920002907 Guar gum Polymers 0.000 claims description 2
- -1 amido propionate Chemical compound 0.000 claims description 2
- 239000000665 guar gum Substances 0.000 claims description 2
- 229960002154 guar gum Drugs 0.000 claims description 2
- 235000010417 guar gum Nutrition 0.000 claims description 2
- 239000002245 particle Substances 0.000 claims description 2
- 239000000499 gel Substances 0.000 description 52
- 229940105329 carboxymethylcellulose Drugs 0.000 description 21
- 239000008367 deionised water Substances 0.000 description 21
- 229910021641 deionized water Inorganic materials 0.000 description 21
- 244000007835 Cyamopsis tetragonoloba Species 0.000 description 20
- 210000004761 scalp Anatomy 0.000 description 17
- 230000001276 controlling effect Effects 0.000 description 10
- 230000000694 effects Effects 0.000 description 10
- OYINQIKIQCNQOX-UHFFFAOYSA-M 2-hydroxybutyl(trimethyl)azanium;chloride Chemical compound [Cl-].CCC(O)C[N+](C)(C)C OYINQIKIQCNQOX-UHFFFAOYSA-M 0.000 description 9
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 6
- 229910052799 carbon Inorganic materials 0.000 description 6
- 230000000052 comparative effect Effects 0.000 description 6
- 229940047642 disodium cocoamphodiacetate Drugs 0.000 description 6
- 229910052700 potassium Inorganic materials 0.000 description 6
- 239000011591 potassium Substances 0.000 description 6
- 206010039792 Seborrhoea Diseases 0.000 description 5
- 239000002085 irritant Substances 0.000 description 4
- 231100000021 irritant Toxicity 0.000 description 4
- 230000028327 secretion Effects 0.000 description 4
- 125000003368 amide group Chemical group 0.000 description 3
- 239000004519 grease Substances 0.000 description 3
- 230000036541 health Effects 0.000 description 3
- 206010019049 Hair texture abnormal Diseases 0.000 description 2
- 210000004027 cell Anatomy 0.000 description 2
- 239000003153 chemical reaction reagent Substances 0.000 description 2
- 239000012459 cleaning agent Substances 0.000 description 2
- 238000011156 evaluation Methods 0.000 description 2
- 210000003780 hair follicle Anatomy 0.000 description 2
- 238000004898 kneading Methods 0.000 description 2
- 230000007774 longterm Effects 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 238000006467 substitution reaction Methods 0.000 description 2
- 239000004094 surface-active agent Substances 0.000 description 2
- RIAJTMUAPNIDSS-UHFFFAOYSA-N 3-aminopropan-1-ol;hydron;chloride Chemical compound Cl.NCCCO RIAJTMUAPNIDSS-UHFFFAOYSA-N 0.000 description 1
- 241000894006 Bacteria Species 0.000 description 1
- 229920000832 Cutin Polymers 0.000 description 1
- 208000001840 Dandruff Diseases 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 230000004913 activation Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000017531 blood circulation Effects 0.000 description 1
- 239000013043 chemical agent Substances 0.000 description 1
- 230000007012 clinical effect Effects 0.000 description 1
- 230000000875 corresponding effect Effects 0.000 description 1
- 238000005536 corrosion prevention Methods 0.000 description 1
- 230000002354 daily effect Effects 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 230000002542 deteriorative effect Effects 0.000 description 1
- 230000003203 everyday effect Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000006260 foam Substances 0.000 description 1
- 230000007794 irritation Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 230000004060 metabolic process Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
- 238000003672 processing method Methods 0.000 description 1
- 210000004927 skin cell Anatomy 0.000 description 1
- 238000002791 soaking Methods 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 210000000106 sweat gland Anatomy 0.000 description 1
- 230000002195 synergetic effect Effects 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 239000002562 thickening agent Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/20—Halogens; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/731—Cellulose; Quaternized cellulose derivatives
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/008—Preparations for oily hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/48—Thickener, Thickening system
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/52—Stabilizers
- A61K2800/524—Preservatives
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
Abstract
The invention belongs to the technical field of hair washing gel, and discloses oil-control hair washing gel and a preparation method thereof. The oil-control hair washing gel provided by the invention comprises the following components in parts by mass: 10-30 parts of sodium laureth sulfate, 1-5 parts of cocoamidomethyl MEA (methyl MEA), 5-15 parts of cocoamidopropyl betaine, 0.1-3 parts of polyquaternary ammonium salt-7, 1-5 parts of disodium cocoyl amphodiacetate, 1-10 parts of sodium cocoamidopropionate, 1-5 parts of sodium lauroyl sarcosinate, 1-10 parts of disodium cocoamidoMIPA-sulfosuccinate, 1-10 parts of potassium cocoyl glycinate, 1-10 parts of sodium cocoyl glycinate, 1-6 parts of decyl glucoside, 0.1-2 parts of cellulose and 11-35 parts of modified activated carbon.
Description
Technical Field
The invention relates to the technical field of shampoos, in particular to oil-control hair washing gel and a preparation method thereof.
Background
The hair washing gel is a daily cleaning agent for cleaning hair, is usually prepared by taking a surfactant as a main component, is in the shape of gel, can be used for cleaning hair and scalp by adding water into a proper amount of hair washing gel in hands, kneading the hair and scalp to obtain foam, and washing the hair and scalp after kneading for a proper time, so that dirt on the hair and grease on the scalp are taken away.
However, since the scalp secretes oil, in order to achieve a high oil removal effect, a chemical agent with a corresponding effect is usually added to the conventional hair gel, so as to achieve a strong oil removal effect, but the hair gel can damage the scalp of a user, the user usually feels tight after washing the hair, the hair is dry, knotted and dry, and the scalp and the hair of the user can be seriously damaged after long-term use, in particular, for the user of oily hair with abundant oil secretion, the user of oily hair usually needs to wash the hair everyday to remove the oil, the hair is more easily damaged, and the health of the user is not good.
Disclosure of Invention
In order to overcome the defects of the prior art, the invention firstly aims to provide the oil-control hair washing gel which can control oil efficiently and is mild and non-irritant to the scalp, thereby achieving the purposes of deep cleaning and health care of the hair.
The invention also aims to provide a preparation method of the oil-control hair washing gel.
In order to achieve the purpose, the invention adopts the following technical scheme:
the oil-control hair washing gel comprises the following components in parts by mass: 10-30 parts of sodium laureth sulfate, 1-5 parts of cocamidomethyl MEA, 5-15 parts of cocamidopropyl betaine, 0.1-3 parts of polyquaternary ammonium salt-7, 1-5 parts of disodium cocoyl amphodiacetate, 1-10 parts of sodium cocoyl amido propionate, 1-5 parts of sodium lauroyl sarcosinate, 1-10 parts of disodium cocoyl MIPA-sulfosuccinate, 1-10 parts of potassium cocoyl glycinate, 1-10 parts of sodium cocoyl glycinate, 1-6 parts of decyl glucoside, 0.05-0.5 part of disodium EDTA, 0.1-2 parts of cellulose, 0.001-2 parts of citric acid, 11-35 parts of modified activated carbon powder, 50-100 parts of water and 0.1-0.5 part of ethylhexyl glycerol.
Preferably, the oil-control hair washing gel further comprises 0.05-1 part of guar gum hydroxypropyl trimethyl ammonium chloride.
Preferably, the oil-control hair washing gel also comprises 0.05-1 part of hydrolyzed keratin.
Preferably, the oil-control hair washing gel further comprises 0.1-3 parts of essence.
Preferably, the modified activated carbon powder is treated by the following method: providing activated carbon, sea salt and ginger, cleaning and performing irradiation sterilization operation on the ginger, beating the ginger into ginger juice through a wall breaking machine, adding the activated carbon into the ginger juice, uniformly stirring, performing cooking operation, filtering to obtain an activated carbon mixture, adding the sea salt into the activated carbon mixture, uniformly stirring, performing drying operation to obtain dried modified activated carbon, performing grinding operation on the dried modified activated carbon, and sieving to obtain the modified activated carbon powder.
Preferably, the dried modified activated carbon may be ground by a grinder and then sieved through a 400-mesh screen to obtain the modified activated carbon powder.
Preferably, in the cooking operation, the cooking temperature is controlled to be 75-85 ℃, and the cooking time is 1.5-2.5 h.
Preferably, in the drying operation, the drying operation is an air drying operation.
Preferably, the particle size of the sea salt is 0.1mm to 0.2 mm.
Preferably, the cellulose is carboxymethyl cellulose.
Preferably, the water may be deionized water.
The invention also provides a preparation method of the oil-control hair washing gel, which comprises the following steps:
(1) adding water and EDTA disodium into a reaction kettle according to a certain proportion, stirring and heating to 75-80 ℃ to obtain a mixed solution A;
(2) adding sodium laureth sulfate and cocamide methyl MEA into the mixed solution A according to a proportion at the temperature of 65 ℃, and uniformly stirring to obtain a mixed solution B;
(3) adding modified activated carbon powder into the mixed solution B in proportion at the temperature of 60 ℃, and uniformly stirring to obtain mixed solution C;
(4) under the condition of normal temperature, evenly mixing and stirring the cocamidopropyl betaine and the polyquaternium-7 in proportion to obtain a mixed solution D;
(5) adding the mixed solution D into the mixed solution C at the temperature of 55 ℃, and uniformly stirring to obtain a mixed solution E;
(6) adding disodium cocoyl amphodiacetate, sodium cocoyl amidopropionate, sodium lauroyl sarcosinate, disodium cocoyl amidoMIPA-sulfosuccinate, potassium cocoyl glycinate, sodium cocoyl glycinate, decyl glucoside and cellulose into the mixed solution E in proportion at the temperature of 45 ℃, and uniformly stirring to obtain a mixed solution F;
(7) and adding citric acid and ethylhexyl glycerin according to a proportion at the temperature of 35 ℃, and uniformly stirring to obtain the oil-control hair washing gel.
Compared with the prior art, the invention has the following advantages and technical effects:
(1) the oil-control hair washing gel provided by the invention adopts a mild surfactant, is matched with cellulose as a thickening agent, is added with the modified activated carbon powder, has mild and non-irritant components, can generate the optimal synergistic effect, can achieve the obvious oil-control effect, simultaneously has no irritation to scalp temperature, does not have the conditions of tight scalp, dry hair, knotting and dryness after being used, greatly improves the comfort of a user, is especially suitable for the user with oily hair, and is beneficial to caring the health of the scalp.
(2) The citric acid is added, so that the pH value of the oil-control hair washing gel can be adjusted, the oil-control hair washing gel is adjusted to be weakly acidic, and can be attached to the weak acidity of the scalp of a normal person.
(3) The oil-control hair washing gel adopts modified activated carbon powder, the ginger is sterilized by a cleaning agent, and then is subjected to wall breaking by a wall breaking machine to obtain the juice, so that the homogenized ginger juice can be obtained, the components are natural and pollution-free, the price is low, then the activated carbon is added into the ginger juice and is uniformly stirred, the activated carbon has an excellent adsorption function, so that the active components in the ginger juice can be adsorbed, further, the activated carbon can be expanded and loosened at high temperature through cooking operation, the molecular motion in the ginger juice is accelerated, the active components in the ginger juice can be further promoted to be adsorbed by the activated carbon, the production efficiency can be improved, meanwhile, the active components in the ginger juice can be better adsorbed by the activated carbon, the filtered sea salt can be adsorbed and locked in the activated carbon, and the ginger and the sea salt can be adsorbed and locked in the activated carbon through the activated carbon, The ginger is filtered, dried and ground into powder, the obtained modified activated carbon powder stimulates the hair follicles to open by accelerating blood circulation, the sea salt is adsorbed on hair follicles of the scalp, sweat glands, grease dirt with positive charges on the surface, dead skin cells and bacteria, and after deep cleaning, the released nutrient components are absorbed, so that the cell activity is increased, the activation and metabolism of superficial cells of the scalp are promoted, the scalp is deeply purified, the problems of scalp cutin and grease are solved, the sea salt can play a sterilization and corrosion prevention effect, the ginger components can be effectively prevented from deteriorating, the stability of the prepared oil-control hair gel is greatly improved, the quality of the oil-control hair gel is improved, the obvious oil-removing and oil-control effects are achieved by adding the modified activated carbon powder, the components are natural and non-irritant, no pollution is caused to the environment, and the environment is protected.
Detailed Description
The present invention will be described in further detail with reference to specific examples, but the embodiments of the present invention are not limited thereto. All the raw materials and reagents used in the present invention are commercially available raw materials and reagents, unless otherwise specified. In the examples, the components are used in g and mL in parts by mass.
Example 1
In the embodiment, the oil-control hair washing gel comprises the following components in parts by mass: 30 parts of sodium laureth sulfate, 5 parts of cocamidomethyl MEA, 15 parts of cocamidopropyl betaine, 3 parts of polyquaternium-7, 5 parts of disodium cocoyl amphodiacetate, 10 parts of sodium cocoyl amidopropionate, 5 parts of sodium lauroyl sarcosinate, 10 parts of disodium cocoyl amido MIPA-sulfosuccinate, 10 parts of potassium cocoyl glycinate, 10 parts of sodium cocoyl glycinate, 6 parts of decyl glucoside, 0.5 part of disodium EDTA, 2 parts of carboxymethyl cellulose, 2 parts of citric acid, 11 parts of modified activated carbon powder, 100 parts of deionized water, 0.5 part of ethylhexyl glycerol, 1 part of guar hydroxypropyltrimonium chloride, 1 part of hydrolyzed keratin and 3 parts of essence;
in this embodiment, the method for treating the modified activated carbon powder comprises: providing activated carbon, sea salt and ginger, performing cleaning and irradiation sterilization operations on the ginger, beating the ginger into ginger juice by using a wall breaking machine, adding the activated carbon into the ginger juice, uniformly stirring, performing cooking operation, controlling the cooking temperature to be 80 ℃, cooking time to be 2 hours, then filtering to obtain an activated carbon mixture, adding the sea salt into the activated carbon mixture, uniformly stirring, performing air drying operation to obtain dried modified activated carbon, performing grinding operation on the dried modified activated carbon by using a grinder, and sieving by using a 400-mesh sieve to obtain modified activated carbon powder;
the preparation method of the oil-control hair washing gel provided by the embodiment comprises the following steps:
(1) adding deionized water, guar hydroxypropyl trimethyl ammonium chloride, EDTA disodium and hydrolyzed keratin into a reaction kettle according to a certain proportion, stirring and heating to 78 ℃ to obtain a mixed solution A;
(2) adding sodium laureth sulfate and cocamide methyl MEA into the mixed solution A according to a proportion at the temperature of 65 ℃, and uniformly stirring to obtain a mixed solution B;
(3) adding modified activated carbon powder into the mixed solution B in proportion at the temperature of 60 ℃, and uniformly stirring to obtain mixed solution C;
(4) under the condition of normal temperature, evenly mixing and stirring the cocamidopropyl betaine and the polyquaternium-7 in proportion to obtain a mixed solution D;
(5) adding the mixed solution D into the mixed solution C at the temperature of 55 ℃, and uniformly stirring to obtain a mixed solution E;
(6) adding disodium cocoyl amphodiacetate, sodium cocoyl amidopropionate, sodium lauroyl sarcosinate, disodium cocoyl amidoMIPA-sulfosuccinate, potassium cocoyl glycinate, sodium cocoyl glycinate, decyl glucoside and carboxymethyl cellulose into the mixed solution E in proportion at the temperature of 45 ℃, and uniformly stirring to obtain a mixed solution F;
(7) and adding citric acid, ethylhexyl glycerin and essence in proportion at 35 ℃, and uniformly stirring to obtain the oil-control hair washing gel.
Example 2
In the embodiment, the oil-control hair washing gel comprises the following components in parts by mass: 25 parts of sodium laureth sulfate, 4 parts of cocamidomethyl MEA, 12 parts of cocamidopropyl betaine, 2 parts of polyquaternium-7, 4 parts of disodium cocoamphodiacetate, 8 parts of sodium cocoamidopropionate, 4 parts of sodium lauroyl sarcosinate, 8 parts of disodium cocoamidoMIPA-sulfosuccinate, 8 parts of potassium cocoamidoglycinate, 8 parts of sodium cocoamidoglycinate, 5 parts of decyl glucoside, 0.4 part of disodium EDTA, 1 part of carboxymethyl cellulose, 1 part of citric acid, 18 parts of modified activated carbon powder, 80 parts of deionized water, 0.4 part of ethylhexyl glycerol, 0.5 part of guar hydroxypropyltrimonium chloride, 0.6 part of hydrolyzed keratin and 2 parts of essence;
in this embodiment, the method for treating the modified activated carbon powder comprises: providing activated carbon, sea salt and ginger, performing cleaning and irradiation sterilization operations on the ginger, beating the ginger into ginger juice by using a wall breaking machine, adding the activated carbon into the ginger juice, uniformly stirring, performing cooking operation, controlling the cooking temperature to be 80 ℃, cooking time to be 2 hours, then filtering to obtain an activated carbon mixture, adding the sea salt into the activated carbon mixture, uniformly stirring, performing air drying operation to obtain dried modified activated carbon, performing grinding operation on the dried modified activated carbon by using a grinder, and sieving by using a 400-mesh sieve to obtain modified activated carbon powder;
the preparation method of the oil-control hair washing gel provided by the embodiment comprises the following steps:
(1) adding deionized water, guar hydroxypropyl trimethyl ammonium chloride, EDTA disodium and hydrolyzed keratin into a reaction kettle according to a certain proportion, stirring and heating to 78 ℃ to obtain a mixed solution A;
(2) adding sodium laureth sulfate and cocamide methyl MEA into the mixed solution A according to a proportion at the temperature of 65 ℃, and uniformly stirring to obtain a mixed solution B;
(3) adding modified activated carbon powder into the mixed solution B in proportion at the temperature of 60 ℃, and uniformly stirring to obtain mixed solution C;
(4) under the condition of normal temperature, evenly mixing and stirring the cocamidopropyl betaine and the polyquaternium-7 in proportion to obtain a mixed solution D;
(5) adding the mixed solution D into the mixed solution C at the temperature of 55 ℃, and uniformly stirring to obtain a mixed solution E;
(6) adding disodium cocoyl amphodiacetate, sodium cocoyl amidopropionate, sodium lauroyl sarcosinate, disodium cocoyl amidoMIPA-sulfosuccinate, potassium cocoyl glycinate, sodium cocoyl glycinate, decyl glucoside and carboxymethyl cellulose into the mixed solution E in proportion at the temperature of 45 ℃, and uniformly stirring to obtain a mixed solution F;
(7) and adding citric acid, ethylhexyl glycerin and essence in proportion at 35 ℃, and uniformly stirring to obtain the oil-control hair washing gel.
Example 3
In the embodiment, the oil-control hair washing gel comprises the following components in parts by mass: 15 parts of sodium laureth sulfate, 3 parts of cocamidomethyl MEA, 8 parts of cocamidopropyl betaine, 1 part of polyquaternium-7, 3 parts of disodium cocoamphodiacetate, 5 parts of sodium cocoamidopropionate, 3 parts of sodium lauroyl sarcosinate, 5 parts of disodium cocoamidoMIPA-sulfosuccinate, 5 parts of potassium cocoamidoglycinate, 5 parts of sodium cocoamidoglycinate, 3 parts of decyl glucoside, 0.3 part of disodium EDTA, 0.5 part of carboxymethyl cellulose, 0.5 part of citric acid, 25 parts of modified activated carbon powder, 70 parts of deionized water, 0.3 part of ethylhexyl glycerol, 0.2 part of guar hydroxypropyltrimonium chloride, 0.2 part of hydrolyzed keratin and 1 part of essence;
in this embodiment, the method for treating the modified activated carbon powder comprises: providing activated carbon, sea salt and ginger, performing cleaning and irradiation sterilization operations on the ginger, beating the ginger into ginger juice by using a wall breaking machine, adding the activated carbon into the ginger juice, uniformly stirring, performing cooking operation, controlling the cooking temperature to be 80 ℃, cooking time to be 2 hours, then filtering to obtain an activated carbon mixture, adding the sea salt into the activated carbon mixture, uniformly stirring, performing air drying operation to obtain dried modified activated carbon, performing grinding operation on the dried modified activated carbon by using a grinder, and sieving by using a 400-mesh sieve to obtain modified activated carbon powder;
the preparation method of the oil-control hair washing gel provided by the embodiment comprises the following steps:
(1) adding deionized water, guar hydroxypropyl trimethyl ammonium chloride, EDTA disodium and hydrolyzed keratin into a reaction kettle according to a certain proportion, stirring and heating to 78 ℃ to obtain a mixed solution A;
(2) adding sodium laureth sulfate and cocamide methyl MEA into the mixed solution A according to a proportion at the temperature of 65 ℃, and uniformly stirring to obtain a mixed solution B;
(3) adding modified activated carbon powder into the mixed solution B in proportion at the temperature of 60 ℃, and uniformly stirring to obtain mixed solution C;
(4) under the condition of normal temperature, evenly mixing and stirring the cocamidopropyl betaine and the polyquaternium-7 in proportion to obtain a mixed solution D;
(5) adding the mixed solution D into the mixed solution C at the temperature of 55 ℃, and uniformly stirring to obtain a mixed solution E;
(6) adding disodium cocoyl amphodiacetate, sodium cocoyl amidopropionate, sodium lauroyl sarcosinate, disodium cocoyl amidoMIPA-sulfosuccinate, potassium cocoyl glycinate, sodium cocoyl glycinate, decyl glucoside and carboxymethyl cellulose into the mixed solution E in proportion at the temperature of 45 ℃, and uniformly stirring to obtain a mixed solution F;
(7) and adding citric acid, ethylhexyl glycerin and essence in proportion at 35 ℃, and uniformly stirring to obtain the oil-control hair washing gel.
Example 4
In the embodiment, the oil-control hair washing gel comprises the following components in parts by mass: 10 parts of sodium laureth sulfate, 1 part of cocamidomethyl MEA, 5 parts of cocamidopropyl betaine, 0.1 part of polyquaternium-7, 1 part of disodium cocoyl amphodiacetate, 1 part of sodium cocoyl amidopropionate, 1 part of sodium lauroyl sarcosinate, 1 part of disodium cocoyl amidoMIPA-sulfosuccinate, 1 part of potassium cocoyl glycinate, 1 part of sodium cocoyl glycinate, 1 part of decyl glucoside, 0.05 part of disodium EDTA, 0.1 part of carboxymethyl cellulose, 0.001 part of citric acid, 35 parts of modified activated carbon powder, 50 parts of deionized water, 0.1 part of ethylhexyl glycerol, 0.05 part of guar hydroxypropyl ammonium chloride, 0.05 part of hydrolyzed keratin and 0.1 part of essence;
in this embodiment, the method for treating the modified activated carbon powder comprises: providing activated carbon, sea salt and ginger, performing cleaning and irradiation sterilization operations on the ginger, beating the ginger into ginger juice by using a wall breaking machine, adding the activated carbon into the ginger juice, uniformly stirring, performing cooking operation, controlling the cooking temperature to be 80 ℃, cooking time to be 2 hours, then filtering to obtain an activated carbon mixture, adding the sea salt into the activated carbon mixture, uniformly stirring, performing air drying operation to obtain dried modified activated carbon, performing grinding operation on the dried modified activated carbon by using a grinder, and sieving by using a 400-mesh sieve to obtain modified activated carbon powder;
the preparation method of the oil-control hair washing gel provided by the embodiment comprises the following steps:
(1) adding deionized water, guar hydroxypropyl trimethyl ammonium chloride, EDTA disodium and hydrolyzed keratin into a reaction kettle according to a certain proportion, stirring and heating to 78 ℃ to obtain a mixed solution A;
(2) adding sodium laureth sulfate and cocamide methyl MEA into the mixed solution A according to a proportion at the temperature of 65 ℃, and uniformly stirring to obtain a mixed solution B;
(3) adding modified activated carbon powder into the mixed solution B in proportion at the temperature of 60 ℃, and uniformly stirring to obtain mixed solution C;
(4) under the condition of normal temperature, evenly mixing and stirring the cocamidopropyl betaine and the polyquaternium-7 in proportion to obtain a mixed solution D;
(5) adding the mixed solution D into the mixed solution C at the temperature of 55 ℃, and uniformly stirring to obtain a mixed solution E;
(6) adding disodium cocoyl amphodiacetate, sodium cocoyl amidopropionate, sodium lauroyl sarcosinate, disodium cocoyl amidoMIPA-sulfosuccinate, potassium cocoyl glycinate, sodium cocoyl glycinate, decyl glucoside and carboxymethyl cellulose into the mixed solution E in proportion at the temperature of 45 ℃, and uniformly stirring to obtain a mixed solution F;
(7) and adding citric acid, ethylhexyl glycerin and essence in proportion at 35 ℃, and uniformly stirring to obtain the oil-control hair washing gel.
Example 5
In the embodiment, the oil-control hair washing gel comprises the following components in parts by mass: 15 parts of sodium laureth sulfate, 3 parts of cocamidomethyl MEA, 8 parts of cocamidopropyl betaine, 1 part of polyquaternium-7, 3 parts of disodium cocoamphodiacetate, 5 parts of sodium cocoamidopropionate, 3 parts of sodium lauroyl sarcosinate, 5 parts of disodium cocoamidoMIPA-sulfosuccinate, 5 parts of potassium cocoamidoglycinate, 5 parts of sodium cocoamidoglycinate, 3 parts of decyl glucoside, 0.3 part of disodium EDTA, 0.5 part of carboxymethyl cellulose, 0.5 part of citric acid, 25 parts of modified activated carbon powder, 70 parts of deionized water, 0.3 part of ethylhexyl glycerol, 0.2 part of guar hydroxypropyltrimonium chloride, 0.2 part of hydrolyzed keratin and 1 part of essence;
in this embodiment, the method for treating the modified activated carbon powder comprises: providing active carbon, sea salt and ginger, performing cleaning and irradiation sterilization operations on the ginger, beating the ginger into ginger juice by using a wall breaking machine, adding the active carbon into the ginger juice, uniformly stirring, performing cooking operation, controlling the cooking temperature to be 75 ℃ and the cooking time to be 1.5h, then filtering to obtain an active carbon mixture, adding the sea salt into the active carbon mixture, uniformly stirring, performing air drying operation to obtain dried modified active carbon, performing grinding operation on the dried modified active carbon by using a grinder, and sieving by using a 400-mesh sieve to obtain modified active carbon powder;
the preparation method of the oil-control hair washing gel provided by the embodiment comprises the following steps:
(1) adding deionized water, guar hydroxypropyl trimethyl ammonium chloride, EDTA disodium and hydrolyzed keratin into a reaction kettle according to a certain proportion, stirring and heating to 75 ℃ to obtain a mixed solution A;
(2) adding sodium laureth sulfate and cocamide methyl MEA into the mixed solution A according to a proportion at the temperature of 65 ℃, and uniformly stirring to obtain a mixed solution B;
(3) adding modified activated carbon powder into the mixed solution B in proportion at the temperature of 60 ℃, and uniformly stirring to obtain mixed solution C;
(4) under the condition of normal temperature, evenly mixing and stirring the cocamidopropyl betaine and the polyquaternium-7 in proportion to obtain a mixed solution D;
(5) adding the mixed solution D into the mixed solution C at the temperature of 55 ℃, and uniformly stirring to obtain a mixed solution E;
(6) adding disodium cocoyl amphodiacetate, sodium cocoyl amidopropionate, sodium lauroyl sarcosinate, disodium cocoyl amidoMIPA-sulfosuccinate, potassium cocoyl glycinate, sodium cocoyl glycinate, decyl glucoside and carboxymethyl cellulose into the mixed solution E in proportion at the temperature of 45 ℃, and uniformly stirring to obtain a mixed solution F;
(7) and adding citric acid, ethylhexyl glycerin and essence in proportion at 35 ℃, and uniformly stirring to obtain the oil-control hair washing gel.
Example 6
In the embodiment, the oil-control hair washing gel comprises the following components in parts by mass: 15 parts of sodium laureth sulfate, 3 parts of cocamidomethyl MEA, 8 parts of cocamidopropyl betaine, 1 part of polyquaternium-7, 3 parts of disodium cocoamphodiacetate, 5 parts of sodium cocoamidopropionate, 3 parts of sodium lauroyl sarcosinate, 5 parts of disodium cocoamidoMIPA-sulfosuccinate, 5 parts of potassium cocoamidoglycinate, 5 parts of sodium cocoamidoglycinate, 3 parts of decyl glucoside, 0.3 part of disodium EDTA, 0.5 part of carboxymethyl cellulose, 0.5 part of citric acid, 25 parts of modified activated carbon powder, 70 parts of deionized water, 0.3 part of ethylhexyl glycerol, 0.2 part of guar hydroxypropyltrimonium chloride, 0.2 part of hydrolyzed keratin and 1 part of essence;
in this embodiment, the method for treating the modified activated carbon powder comprises: providing activated carbon, sea salt and ginger, performing cleaning and irradiation sterilization operations on the ginger, beating the ginger into ginger juice by using a wall breaking machine, adding the activated carbon into the ginger juice, uniformly stirring, performing cooking operation, controlling the cooking temperature to be 85 ℃, cooking time to be 2.5 hours, then filtering to obtain an activated carbon mixture, adding the sea salt into the activated carbon mixture, uniformly stirring, performing air drying operation to obtain dried modified activated carbon, performing grinding operation on the dried modified activated carbon by using a grinder, and sieving by using a 400-mesh sieve to obtain modified activated carbon powder;
the preparation method of the oil-control hair washing gel provided by the embodiment comprises the following steps:
(1) adding deionized water, guar hydroxypropyl trimethyl ammonium chloride, EDTA disodium and hydrolyzed keratin into a reaction kettle according to a certain proportion, stirring and heating to 80 ℃ to obtain a mixed solution A;
(2) adding sodium laureth sulfate and cocamide methyl MEA into the mixed solution A according to a proportion at the temperature of 65 ℃, and uniformly stirring to obtain a mixed solution B;
(3) adding modified activated carbon powder into the mixed solution B in proportion at the temperature of 60 ℃, and uniformly stirring to obtain mixed solution C;
(4) under the condition of normal temperature, evenly mixing and stirring the cocamidopropyl betaine and the polyquaternium-7 in proportion to obtain a mixed solution D;
(5) adding the mixed solution D into the mixed solution C at the temperature of 55 ℃, and uniformly stirring to obtain a mixed solution E;
(6) adding disodium cocoyl amphodiacetate, sodium cocoyl amidopropionate, sodium lauroyl sarcosinate, disodium cocoyl amidoMIPA-sulfosuccinate, potassium cocoyl glycinate, sodium cocoyl glycinate, decyl glucoside and carboxymethyl cellulose into the mixed solution E in proportion at the temperature of 45 ℃, and uniformly stirring to obtain a mixed solution F;
(7) and adding citric acid, ethylhexyl glycerin and essence in proportion at 35 ℃, and uniformly stirring to obtain the oil-control hair washing gel.
Example 7
In the embodiment, the oil-control hair washing gel comprises the following components in parts by mass: 20 parts of sodium laureth sulfate, 4 parts of cocamidomethyl MEA, 6 parts of cocamidopropyl betaine, 2 parts of polyquaternium-7, 2 parts of disodium cocoamphodiacetate, 7 parts of sodium cocoamidopropionate, 3 parts of sodium lauroyl sarcosinate, 7 parts of disodium cocoamidoMIPA-sulfosuccinate, 7 parts of potassium cocoamidoglycinate, 7 parts of sodium cocoamidoglycinate, 3 parts of decyl glucoside, 0.3 part of disodium EDTA, 1.2 parts of carboxymethyl cellulose, 1.2 parts of citric acid, 28 parts of modified activated carbon powder, 60 parts of deionized water, 0.35 part of ethylhexyl glycerol, 0.6 part of guar hydroxypropyltrimonium chloride, 0.5 part of hydrolyzed keratin and 1.2 parts of essence;
in this embodiment, the method for treating the modified activated carbon powder comprises: providing activated carbon, sea salt and ginger, performing cleaning and irradiation sterilization operations on the ginger, beating the ginger into ginger juice by using a wall breaking machine, adding the activated carbon into the ginger juice, uniformly stirring, performing cooking operation, controlling the cooking temperature to be 85 ℃, cooking time to be 2.5 hours, then filtering to obtain an activated carbon mixture, adding the sea salt into the activated carbon mixture, uniformly stirring, performing air drying operation to obtain dried modified activated carbon, performing grinding operation on the dried modified activated carbon by using a grinder, and sieving by using a 400-mesh sieve to obtain modified activated carbon powder;
the preparation method of the oil-control hair washing gel provided by the embodiment comprises the following steps:
(1) adding deionized water, guar hydroxypropyl trimethyl ammonium chloride, EDTA disodium and hydrolyzed keratin into a reaction kettle according to a certain proportion, stirring and heating to 80 ℃ to obtain a mixed solution A;
(2) adding sodium laureth sulfate and cocamide methyl MEA into the mixed solution A according to a proportion at the temperature of 65 ℃, and uniformly stirring to obtain a mixed solution B;
(3) adding modified activated carbon powder into the mixed solution B in proportion at the temperature of 60 ℃, and uniformly stirring to obtain mixed solution C;
(4) under the condition of normal temperature, evenly mixing and stirring the cocamidopropyl betaine and the polyquaternium-7 in proportion to obtain a mixed solution D;
(5) adding the mixed solution D into the mixed solution C at the temperature of 55 ℃, and uniformly stirring to obtain a mixed solution E;
(6) adding disodium cocoyl amphodiacetate, sodium cocoyl amidopropionate, sodium lauroyl sarcosinate, disodium cocoyl amidoMIPA-sulfosuccinate, potassium cocoyl glycinate, sodium cocoyl glycinate, decyl glucoside and carboxymethyl cellulose into the mixed solution E in proportion at the temperature of 45 ℃, and uniformly stirring to obtain a mixed solution F;
(7) and adding citric acid, ethylhexyl glycerin and essence in proportion at 35 ℃, and uniformly stirring to obtain the oil-control hair washing gel.
Comparative example 1
In the embodiment, the oil-control hair washing gel comprises the following components in parts by mass: 15 parts of sodium laureth sulfate, 3 parts of cocamidomethyl MEA, 8 parts of cocamidopropyl betaine, 1 part of polyquaternium-7, 3 parts of disodium cocoyl amphodiacetate, 5 parts of sodium cocoyl amidopropionate, 3 parts of sodium lauroyl sarcosinate, 5 parts of disodium cocoyl amido MIPA-sulfosuccinate, 5 parts of potassium cocoyl glycinate, 5 parts of sodium cocoyl glycinate, 3 parts of decyl glucoside, 0.3 part of disodium EDTA, 0.5 part of carboxymethyl cellulose, 0.5 part of citric acid, 70 parts of deionized water, 0.3 part of ethylhexyl glycerol, 0.2 part of guar hydroxypropyl trimonium chloride, 0.2 part of hydrolyzed keratin and 1 part of essence;
the preparation method of the oil-control hair washing gel provided by the embodiment comprises the following steps:
(1) adding deionized water, guar hydroxypropyl trimethyl ammonium chloride, EDTA disodium and hydrolyzed keratin into a reaction kettle according to a certain proportion, stirring and heating to 78 ℃ to obtain a mixed solution A;
(2) adding sodium laureth sulfate and cocamide methyl MEA into the mixed solution A according to a proportion at the temperature of 65 ℃, and uniformly stirring to obtain a mixed solution B;
(3) under the condition of normal temperature, evenly mixing and stirring the cocamidopropyl betaine and the polyquaternium-7 in proportion to obtain a mixed solution D;
(4) adding the mixed solution D into the mixed solution B at the temperature of 55 ℃, and uniformly stirring to obtain a mixed solution E;
(5) adding disodium cocoyl amphodiacetate, sodium cocoyl amidopropionate, sodium lauroyl sarcosinate, disodium cocoyl amidoMIPA-sulfosuccinate, potassium cocoyl glycinate, sodium cocoyl glycinate, decyl glucoside and carboxymethyl cellulose into the mixed solution E in proportion at the temperature of 45 ℃, and uniformly stirring to obtain a mixed solution F;
(6) and adding citric acid, ethylhexyl glycerin and essence in proportion at 35 ℃, and uniformly stirring to obtain the oil-control hair washing gel.
Comparative example 2
In the embodiment, the oil-control hair washing gel comprises the following components in parts by mass: 15 parts of sodium laureth sulfate, 3 parts of cocamidomethyl MEA, 8 parts of cocamidopropyl betaine, 1 part of polyquaternium-7, 3 parts of disodium cocoyl amphodiacetate, 5 parts of sodium cocoyl amidopropionate, 3 parts of sodium lauroyl sarcosinate, 5 parts of disodium cocoyl amido MIPA-sulfosuccinate, 5 parts of potassium cocoyl glycinate, 5 parts of sodium cocoyl glycinate, 3 parts of decyl glucoside, 0.3 part of disodium EDTA, 0.5 part of carboxymethyl cellulose, 0.5 part of citric acid, 25 parts of ginger juice, 70 parts of deionized water, 1 part of ethylhexyl glycerol, 0.2 part of guar hydroxypropyl trimonium chloride, 0.2 part of hydrolyzed keratin and 1 part of essence;
in this embodiment, the processing method of the ginger juice comprises: providing ginger and sea salt, cleaning the ginger, performing irradiation sterilization, beating the ginger into ginger juice by using a wall breaking machine, adding the sea salt into the ginger juice, and uniformly stirring to obtain the ginger juice;
the preparation method of the oil-control hair washing gel provided by the embodiment comprises the following steps:
(1) adding deionized water, guar hydroxypropyl trimethyl ammonium chloride, EDTA disodium and hydrolyzed keratin into a reaction kettle according to a certain proportion, stirring and heating to 78 ℃ to obtain a mixed solution A;
(2) adding sodium laureth sulfate and cocamide methyl MEA into the mixed solution A according to a proportion at the temperature of 65 ℃, and uniformly stirring to obtain a mixed solution B;
(3) adding the ginger juice into the mixed solution B in proportion at the temperature of 60 ℃, and uniformly stirring to obtain a mixed solution C;
(4) under the condition of normal temperature, evenly mixing and stirring the cocamidopropyl betaine and the polyquaternium-7 in proportion to obtain a mixed solution D;
(5) adding the mixed solution D into the mixed solution C at the temperature of 55 ℃, and uniformly stirring to obtain a mixed solution E;
(6) adding disodium cocoyl amphodiacetate, sodium cocoyl amidopropionate, sodium lauroyl sarcosinate, disodium cocoyl amidoMIPA-sulfosuccinate, potassium cocoyl glycinate, sodium cocoyl glycinate, decyl glucoside and carboxymethyl cellulose into the mixed solution E in proportion at the temperature of 45 ℃, and uniformly stirring to obtain a mixed solution F;
(7) and adding citric acid, ethylhexyl glycerin and essence in proportion at 35 ℃, and uniformly stirring to obtain the oil-control hair washing gel.
Comparative example 3
In the embodiment, the oil-control hair washing gel comprises the following components in parts by mass: 15 parts of sodium laureth sulfate, 3 parts of cocamidomethyl MEA, 8 parts of cocamidopropyl betaine, 1 part of polyquaternium-7, 3 parts of disodium cocoamphodiacetate, 5 parts of sodium cocoamidopropionate, 3 parts of sodium lauroyl sarcosinate, 5 parts of disodium cocoamidoMIPA-sulfosuccinate, 5 parts of potassium cocoamidoglycinate, 5 parts of sodium cocoamidoglycinate, 3 parts of decyl glucoside, 0.3 part of disodium EDTA, 0.5 part of carboxymethyl cellulose, 0.5 part of citric acid, 25 parts of modified activated carbon powder, 70 parts of deionized water, 0.3 part of ethylhexyl glycerol, 0.2 part of guar hydroxypropyltrimonium chloride, 0.2 part of hydrolyzed keratin and 1 part of essence;
in this embodiment, the method for treating the modified activated carbon powder comprises: providing activated carbon, sea salt and ginger, cleaning and performing irradiation sterilization on the ginger, beating the ginger into ginger juice by using a wall breaking machine, adding the activated carbon into the ginger juice, uniformly stirring, soaking for 2 hours, then filtering to obtain an activated carbon mixture, adding the sea salt into the activated carbon mixture, uniformly stirring, performing air drying operation to obtain dried modified activated carbon, performing grinding operation on the dried modified activated carbon by using a grinder, and sieving by using a 400-mesh sieve to obtain modified activated carbon powder;
the preparation method of the oil-control hair washing gel provided by the embodiment comprises the following steps:
(1) adding deionized water, guar hydroxypropyl trimethyl ammonium chloride, EDTA disodium and hydrolyzed keratin into a reaction kettle according to a certain proportion, stirring and heating to 78 ℃ to obtain a mixed solution A;
(2) adding sodium laureth sulfate and cocamide methyl MEA into the mixed solution A according to a proportion at the temperature of 65 ℃, and uniformly stirring to obtain a mixed solution B;
(3) adding modified activated carbon powder into the mixed solution B in proportion at the temperature of 60 ℃, and uniformly stirring to obtain mixed solution C;
(4) under the condition of normal temperature, evenly mixing and stirring the cocamidopropyl betaine and the polyquaternium-7 in proportion to obtain a mixed solution D;
(5) adding the mixed solution D into the mixed solution C at the temperature of 55 ℃, and uniformly stirring to obtain a mixed solution E;
(6) adding disodium cocoyl amphodiacetate, sodium cocoyl amidopropionate, sodium lauroyl sarcosinate, disodium cocoyl amidoMIPA-sulfosuccinate, potassium cocoyl glycinate, sodium cocoyl glycinate, decyl glucoside and carboxymethyl cellulose into the mixed solution E in proportion at the temperature of 45 ℃, and uniformly stirring to obtain a mixed solution F;
(7) and adding citric acid, ethylhexyl glycerin and essence in proportion at 35 ℃, and uniformly stirring to obtain the oil-control hair washing gel.
Clinical effect experiment:
test subjects: the hair is prepared by 200 oily hair (half of men and women): the patients with the excessive oil secretion are tried out, 200 (half of men and women respectively) patients with the excessive oil secretion are randomly divided into 10 groups, and each group comprises 20 patients;
the using method comprises the following steps: after each group is wetted, an appropriate amount of the product is applied to the hair, rubbed and foamed, massaged for 3-5 minutes and then washed with warm water, and the hair is washed once every two days for 2 weeks.
Grading standard: the testers grade the evaluation items according to the use feelings of the testers, and the grade standard adopts a 10-point system.
The results, tested after 2 weeks of use by the subjects, were as follows:
TABLE 1 evaluation results of subjects after 2 weeks of use
As can be seen from Table 1, the oil-controlling hair gels of examples 1-7 have oil removing, dandruff removing, hair softening and softening degrees and oil-controlling effects which are all superior to those of comparative examples 1-3, and can achieve excellent oil-controlling effect after long-term use, compared with the comparative examples 1 to 2, the modified activated carbon powder component is added in the examples 1 to 7, can achieve the effects of effectively removing and controlling oil, effectively relieve the condition of vigorous secretion of oily hair oil, and the components are mild and non-irritant, the situations of tight scalp, dry hair, knotting and dryness can not be caused, the comfort of a user is greatly improved, compared with the comparative example 3, the modified activated carbon obtained by the modified activated carbon treatment method disclosed by the invention has the advantages that the better oil removing and controlling effect can be achieved, the oil removing and controlling effect is remarkable, the use comfort level is better, and the modified activated carbon treatment method is suitable for various crowds.
The above embodiments are the best mode for carrying out the present invention, but the embodiments of the present invention are not limited to the above embodiments, and any other changes, modifications, substitutions, combinations, and simplifications which do not depart from the spirit and principle of the present invention should be regarded as equivalent substitutions and are included in the scope of the present invention.
Claims (10)
1. The oil-control hair washing gel is characterized by comprising the following components in parts by mass: 10-30 parts of sodium laureth sulfate, 1-5 parts of cocamidomethyl MEA, 5-15 parts of cocamidopropyl betaine, 0.1-3 parts of polyquaternary ammonium salt-7, 1-5 parts of disodium cocoyl amphodiacetate, 1-10 parts of sodium cocoyl amido propionate, 1-5 parts of sodium lauroyl sarcosinate, 1-10 parts of disodium cocoyl MIPA-sulfosuccinate, 1-10 parts of potassium cocoyl glycinate, 1-10 parts of sodium cocoyl glycinate, 1-6 parts of decyl glucoside, 0.05-0.5 part of disodium EDTA, 0.1-2 parts of cellulose, 0.001-2 parts of citric acid, 11-35 parts of modified activated carbon powder, 50-100 parts of water and 0.1-0.5 part of ethylhexyl glycerol.
2. The oil control shampoo gel according to claim 1 wherein: the oil-control hair washing gel also comprises 0.05-1 part of guar gum hydroxypropyl trimethyl ammonium chloride.
3. The oil control shampoo gel according to claim 2 wherein: the oil-control hair washing gel also comprises 0.05-1 part of hydrolyzed keratin.
4. The oil control shampoo gel according to claim 1 wherein: the oil-control hair washing gel further comprises 0.1-3 parts of essence.
5. The oil control shampoo gel according to claim 1 wherein: the treatment method of the modified activated carbon powder comprises the following steps: providing activated carbon, sea salt and ginger, cleaning and performing irradiation sterilization operation on the ginger, beating the ginger into ginger juice through a wall breaking machine, adding the activated carbon into the ginger juice, uniformly stirring, performing cooking operation, filtering to obtain an activated carbon mixture, adding the sea salt into the activated carbon mixture, uniformly stirring, performing drying operation to obtain dried modified activated carbon, performing grinding operation on the dried modified activated carbon, and sieving to obtain the modified activated carbon powder.
6. The oil control shampoo gel according to claim 5 wherein: in the cooking operation, the cooking temperature is controlled to be 75-85 ℃, and the cooking time is 1.5-2.5 h.
7. The oil control shampoo gel according to claim 5 wherein: in the drying operation, an air drying operation is adopted as the drying operation.
8. The oil control shampoo gel according to claim 5 wherein: the particle size of the sea salt is 0.1 mm-0.2 mm.
9. The oil control shampoo gel according to claim 1 wherein: the cellulose is carboxymethyl cellulose.
10. The method of preparing an oil control shampoo gel according to any of claims 1 to 9, comprising the steps of:
(1) adding water and EDTA disodium into a reaction kettle according to a certain proportion, stirring and heating to 75-80 ℃ to obtain a mixed solution A;
(2) adding sodium laureth sulfate and cocamide methyl MEA into the mixed solution A according to a proportion at the temperature of 65 ℃, and uniformly stirring to obtain a mixed solution B;
(3) adding modified activated carbon powder into the mixed solution B in proportion at the temperature of 60 ℃, and uniformly stirring to obtain mixed solution C;
(4) under the condition of normal temperature, evenly mixing and stirring the cocamidopropyl betaine and the polyquaternium-7 in proportion to obtain a mixed solution D;
(5) adding the mixed solution D into the mixed solution C at the temperature of 55 ℃, and uniformly stirring to obtain a mixed solution E;
(6) adding disodium cocoyl amphodiacetate, sodium cocoyl amidopropionate, sodium lauroyl sarcosinate, disodium cocoyl amidoMIPA-sulfosuccinate, potassium cocoyl glycinate, sodium cocoyl glycinate, decyl glucoside and cellulose into the mixed solution E in proportion at the temperature of 45 ℃, and uniformly stirring to obtain a mixed solution F;
(7) and adding citric acid and ethylhexyl glycerin according to a proportion at the temperature of 35 ℃, and uniformly stirring to obtain the oil-control hair washing gel.
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| CN105748376A (en) * | 2016-04-26 | 2016-07-13 | 成都彦宁科技有限公司 | Oil-control anti-hair-loss liquid shampoo |
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| CN107536749A (en) * | 2017-08-23 | 2018-01-05 | 杭州兰茜化妆品有限公司 | Chinese medicine shampoo and its preparation technology |
| CN108186439A (en) * | 2018-02-09 | 2018-06-22 | 广州御延堂生物科技有限公司 | A kind of sea salt nourishes hair cream and preparation method thereof |
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| CN103877552A (en) * | 2014-04-01 | 2014-06-25 | 邓林生 | Application of powdered activated carbon in treating alopecia and hair growth liquid |
| CN105853256A (en) * | 2016-04-07 | 2016-08-17 | 广东珍宝健康日用品科技有限公司 | Oil-control and moisturizing low-irritation shampoo composition |
| CN105748376A (en) * | 2016-04-26 | 2016-07-13 | 成都彦宁科技有限公司 | Oil-control anti-hair-loss liquid shampoo |
| CN107233271A (en) * | 2017-06-29 | 2017-10-10 | 广州科玛生物科技股份有限公司 | A kind of true ginger shampoo of amino acid and preparation method thereof |
| CN107536749A (en) * | 2017-08-23 | 2018-01-05 | 杭州兰茜化妆品有限公司 | Chinese medicine shampoo and its preparation technology |
| CN108186439A (en) * | 2018-02-09 | 2018-06-22 | 广州御延堂生物科技有限公司 | A kind of sea salt nourishes hair cream and preparation method thereof |
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