CN112516026A - Shampoo cream and preparation method thereof - Google Patents
Shampoo cream and preparation method thereof Download PDFInfo
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- CN112516026A CN112516026A CN202011475761.4A CN202011475761A CN112516026A CN 112516026 A CN112516026 A CN 112516026A CN 202011475761 A CN202011475761 A CN 202011475761A CN 112516026 A CN112516026 A CN 112516026A
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- shampoo
- mixed solution
- activated carbon
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- 239000002453 shampoo Substances 0.000 title claims abstract description 74
- 238000002360 preparation method Methods 0.000 title abstract description 16
- 239000006071 cream Substances 0.000 title description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical class [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 96
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims abstract description 78
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 75
- 239000000843 powder Substances 0.000 claims abstract description 65
- -1 alkyl glycoside Chemical class 0.000 claims abstract description 35
- 229940105847 calamine Drugs 0.000 claims abstract description 27
- 229910052864 hemimorphite Inorganic materials 0.000 claims abstract description 27
- 235000014692 zinc oxide Nutrition 0.000 claims abstract description 27
- 239000011787 zinc oxide Substances 0.000 claims abstract description 27
- CPYIZQLXMGRKSW-UHFFFAOYSA-N zinc;iron(3+);oxygen(2-) Chemical compound [O-2].[O-2].[O-2].[O-2].[Fe+3].[Fe+3].[Zn+2] CPYIZQLXMGRKSW-UHFFFAOYSA-N 0.000 claims abstract description 27
- MRUAUOIMASANKQ-UHFFFAOYSA-N cocamidopropyl betaine Chemical compound CCCCCCCCCCCC(=O)NCCC[N+](C)(C)CC([O-])=O MRUAUOIMASANKQ-UHFFFAOYSA-N 0.000 claims abstract description 26
- 229940073507 cocamidopropyl betaine Drugs 0.000 claims abstract description 26
- QXNVGIXVLWOKEQ-UHFFFAOYSA-N Disodium Chemical compound [Na][Na] QXNVGIXVLWOKEQ-UHFFFAOYSA-N 0.000 claims abstract description 25
- 239000004094 surface-active agent Substances 0.000 claims abstract description 21
- 150000001413 amino acids Chemical class 0.000 claims abstract description 20
- 239000000022 bacteriostatic agent Substances 0.000 claims abstract description 18
- 229930182470 glycoside Natural products 0.000 claims abstract description 18
- 239000003109 Disodium ethylene diamine tetraacetate Substances 0.000 claims abstract description 13
- ZGTMUACCHSMWAC-UHFFFAOYSA-L EDTA disodium salt (anhydrous) Chemical compound [Na+].[Na+].OC(=O)CN(CC([O-])=O)CCN(CC(O)=O)CC([O-])=O ZGTMUACCHSMWAC-UHFFFAOYSA-L 0.000 claims abstract description 13
- 235000019301 disodium ethylene diamine tetraacetate Nutrition 0.000 claims abstract description 13
- QGZKDVFQNNGYKY-UHFFFAOYSA-O ammonium group Chemical class [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 claims abstract description 10
- 239000011259 mixed solution Substances 0.000 claims description 72
- 239000002002 slurry Substances 0.000 claims description 55
- 238000003756 stirring Methods 0.000 claims description 36
- 238000010411 cooking Methods 0.000 claims description 32
- 238000000227 grinding Methods 0.000 claims description 30
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 29
- 235000001855 Portulaca oleracea Nutrition 0.000 claims description 26
- 241000219304 Portulacaceae Species 0.000 claims description 26
- 235000011389 fruit/vegetable juice Nutrition 0.000 claims description 25
- 239000000243 solution Substances 0.000 claims description 25
- HSEMFIZWXHQJAE-UHFFFAOYSA-N hexadecanamide Chemical compound CCCCCCCCCCCCCCCC(N)=O HSEMFIZWXHQJAE-UHFFFAOYSA-N 0.000 claims description 24
- 239000011268 mixed slurry Substances 0.000 claims description 23
- 238000002156 mixing Methods 0.000 claims description 23
- 239000008367 deionised water Substances 0.000 claims description 22
- 229910021641 deionized water Inorganic materials 0.000 claims description 22
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 14
- 238000000034 method Methods 0.000 claims description 14
- 229940079988 potassium cocoyl glycinate Drugs 0.000 claims description 14
- 229910052708 sodium Inorganic materials 0.000 claims description 14
- 239000011734 sodium Substances 0.000 claims description 14
- 229940065859 sodium cocoyl glycinate Drugs 0.000 claims description 14
- IKGKWKGYFJBGQJ-UHFFFAOYSA-M sodium;2-(dodecanoylamino)acetate Chemical compound [Na+].CCCCCCCCCCCC(=O)NCC([O-])=O IKGKWKGYFJBGQJ-UHFFFAOYSA-M 0.000 claims description 14
- 229940104261 taurate Drugs 0.000 claims description 14
- QCDWFXQBSFUVSP-UHFFFAOYSA-N 2-phenoxyethanol Chemical group OCCOC1=CC=CC=C1 QCDWFXQBSFUVSP-UHFFFAOYSA-N 0.000 claims description 12
- LXAHHHIGZXPRKQ-UHFFFAOYSA-N 5-fluoro-2-methylpyridine Chemical compound CC1=CC=C(F)C=N1 LXAHHHIGZXPRKQ-UHFFFAOYSA-N 0.000 claims description 12
- JDRSMPFHFNXQRB-CMTNHCDUSA-N Decyl beta-D-threo-hexopyranoside Chemical group CCCCCCCCCCO[C@@H]1O[C@H](CO)C(O)[C@H](O)C1O JDRSMPFHFNXQRB-CMTNHCDUSA-N 0.000 claims description 12
- 238000006243 chemical reaction Methods 0.000 claims description 12
- 229940073499 decyl glucoside Drugs 0.000 claims description 12
- 238000010438 heat treatment Methods 0.000 claims description 12
- 229960005323 phenoxyethanol Drugs 0.000 claims description 12
- NRWCNEBHECBWRJ-UHFFFAOYSA-M trimethyl(propyl)azanium;chloride Chemical compound [Cl-].CCC[N+](C)(C)C NRWCNEBHECBWRJ-UHFFFAOYSA-M 0.000 claims description 12
- 238000007873 sieving Methods 0.000 claims description 11
- 238000007605 air drying Methods 0.000 claims description 10
- 238000001914 filtration Methods 0.000 claims description 10
- 238000010981 drying operation Methods 0.000 claims description 6
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 2
- 229910052799 carbon Inorganic materials 0.000 description 38
- 210000004761 scalp Anatomy 0.000 description 26
- 206010015150 Erythema Diseases 0.000 description 19
- 230000000694 effects Effects 0.000 description 14
- 208000002874 Acne Vulgaris Diseases 0.000 description 13
- 206010000496 acne Diseases 0.000 description 13
- 208000003251 Pruritus Diseases 0.000 description 12
- MPNXSZJPSVBLHP-UHFFFAOYSA-N 2-chloro-n-phenylpyridine-3-carboxamide Chemical compound ClC1=NC=CC=C1C(=O)NC1=CC=CC=C1 MPNXSZJPSVBLHP-UHFFFAOYSA-N 0.000 description 10
- 230000000052 comparative effect Effects 0.000 description 8
- 231100000321 erythema Toxicity 0.000 description 7
- 238000004140 cleaning Methods 0.000 description 5
- 230000036541 health Effects 0.000 description 5
- 230000007803 itching Effects 0.000 description 5
- 238000012360 testing method Methods 0.000 description 5
- 230000002378 acidificating effect Effects 0.000 description 4
- 241000894006 Bacteria Species 0.000 description 3
- 208000010201 Exanthema Diseases 0.000 description 3
- 206010061218 Inflammation Diseases 0.000 description 3
- 238000011156 evaluation Methods 0.000 description 3
- 201000005884 exanthem Diseases 0.000 description 3
- 230000004054 inflammatory process Effects 0.000 description 3
- 206010037844 rash Diseases 0.000 description 3
- 239000004480 active ingredient Substances 0.000 description 2
- 230000003266 anti-allergic effect Effects 0.000 description 2
- 230000003110 anti-inflammatory effect Effects 0.000 description 2
- 238000009835 boiling Methods 0.000 description 2
- 239000003153 chemical reaction reagent Substances 0.000 description 2
- 230000003467 diminishing effect Effects 0.000 description 2
- 230000002401 inhibitory effect Effects 0.000 description 2
- 239000002085 irritant Substances 0.000 description 2
- 231100000021 irritant Toxicity 0.000 description 2
- 229940064064 purslane extract Drugs 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 238000010025 steaming Methods 0.000 description 2
- 238000006467 substitution reaction Methods 0.000 description 2
- 230000002195 synergetic effect Effects 0.000 description 2
- 206010020751 Hypersensitivity Diseases 0.000 description 1
- 208000026935 allergic disease Diseases 0.000 description 1
- 230000007815 allergy Effects 0.000 description 1
- 230000007012 clinical effect Effects 0.000 description 1
- 238000013329 compounding Methods 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000006260 foam Substances 0.000 description 1
- 239000004519 grease Substances 0.000 description 1
- 230000003648 hair appearance Effects 0.000 description 1
- 230000003779 hair growth Effects 0.000 description 1
- 210000003128 head Anatomy 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 230000000622 irritating effect Effects 0.000 description 1
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- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 231100000344 non-irritating Toxicity 0.000 description 1
- 230000000474 nursing effect Effects 0.000 description 1
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- 238000001179 sorption measurement Methods 0.000 description 1
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Images
Classifications
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
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- A61K8/27—Zinc; Compounds thereof
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
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Abstract
The invention belongs to the technical field of shampoo and discloses a shampoo and a preparation method thereof. The shampoo provided by the invention comprises the following components in parts by mass: 11-35 parts of amino acid type surfactant, 20-60 parts of disodium cocoamido MIPA-sulfosuccinate, 5-15 parts of cocamidopropyl betaine, 1-5 parts of alkyl glycoside, 0.05-0.2 part of disodium EDTA, 6-30 parts of calamine powder, 3-15 parts of glycerol, 0.5-5 parts of modified activated carbon powder, 0.03-1 part of polyquaternary ammonium salt-10, 0.05-1 part of polyquaternary ammonium salt-7, 0.5-2 parts of palmitoyl propyl trimethyl ammonium chloride, 0.3-1 part of bacteriostatic agent and 0.05-0.5 part of citric acid.
Description
Technical Field
The invention relates to the technical field of shampoo, in particular to a shampoo and a preparation method thereof.
Background
The shampoo paste is a daily use cosmetic specially used for washing hair, generally is prepared by taking a surfactant as a main component, is in a paste shape, can achieve the effect of cleaning scalp and hair, is a common cleanser in daily life of people, has the basic function of cleaning, can remove oil stains on the hair and the scalp of people, is convenient to use, can be used for hair only by taking the shampoo paste and adding water to beat foam, can make the hair light and cool after being used, and makes people feel comfortable and pleasant.
However, with the development of industrialization, the pollution of our living environment and working environment is more and more serious, various harmful bacteria exist in our living environment and working environment, and people are easy to be dirty in the process of contacting with the surrounding environment, and the scalp of people is easy to be itchy due to the grease secreted by the scalp, even the scalp is red, acne, red rash and the like, which causes discomfort, and the health and balance of the ecological environment of the scalp as the soil for hair growth are the root of the healthy growth of hair, so that the problem to be solved by researchers in the field is to provide a shampoo for effectively and healthily caring the scalp.
Disclosure of Invention
In order to overcome the defects of the prior art, the invention mainly aims to provide the shampoo paste which can be used for deeply cleaning and has the functions of astringing, relieving itching, diminishing inflammation and inhibiting bacteria to the scalp, thereby achieving the aim of health care of the scalp.
The invention also aims to provide a preparation method of the shampoo.
In order to achieve the purpose, the invention adopts the following technical scheme:
a shampoo paste comprises the following components in parts by mass: 11-35 parts of amino acid type surfactant, 20-60 parts of disodium cocoamido MIPA-sulfosuccinate, 5-15 parts of cocamidopropyl betaine, 1-5 parts of alkyl glycoside, 0.05-0.2 part of disodium EDTA, 6-30 parts of calamine powder, 3-15 parts of glycerol, 0.5-5 parts of modified activated carbon powder, 0.03-1 part of polyquaternary ammonium salt-10, 0.05-1 part of polyquaternary ammonium salt-7, 0.5-2 parts of palmitoyl propyl trimethyl ammonium chloride, 0.3-1 part of bacteriostatic agent, 0.05-0.5 part of citric acid and 3-6 parts of water.
Preferably, the amino acid type surfactant includes sodium cocoyl methyl taurate, potassium cocoyl glycinate and sodium cocoyl glycinate.
Preferably, the amino acid type surfactant comprises, by mass, 5-15 parts of sodium cocoyl methyl taurate, 3-10 parts of potassium cocoyl glycinate and 3-10 parts of sodium cocoyl glycinate.
Preferably, the water is deionized water.
Preferably, the alkyl glycoside is decyl glucoside.
Preferably, the modified activated carbon powder is treated by the following method: providing purslane juice and activated carbon, adding the activated carbon into the purslane juice, performing cooking operation, then filtering, performing drying operation to obtain dried modified activated carbon, and performing grinding operation on the dried modified activated carbon to obtain the modified activated carbon powder.
Preferably, in the cooking operation, the cooking temperature is controlled to be 55-65 ℃, and the cooking time is controlled to be 0.5-1.5 h.
Preferably, in the drying operation, the drying operation is an air drying operation.
Preferably, the bacteriostatic agent is phenoxyethanol.
The invention also provides a preparation method of the shampoo, which comprises the following steps:
(1) adding polyquaternium-10, EDTA disodium, palmitamide propyl trimethyl ammonium chloride and water into a reaction kettle according to a certain proportion, heating to 75-80 ℃, and preserving heat for 5min to obtain a mixed solution A;
(2) adding disodium cocoamido MIPA-sulfosuccinate into the mixed solution A in proportion at the temperature of 60 ℃, and uniformly stirring to obtain mixed solution B;
(3) under the condition of normal temperature, evenly mixing the cocamidopropyl betaine and the polyquaternium-7 in proportion to obtain a mixed solution C;
(4) under the condition of normal temperature, uniformly mixing calamine powder, glycerol and modified activated carbon powder in proportion to obtain premixed slurry, adding the premixed slurry into a three-roller grinder, grinding to obtain premixed slurry, vacuumizing the premixed slurry to remove air bubbles, and sieving the vacuumized premixed slurry through a 400-mesh screen to obtain mixed slurry;
(5) and adding the mixed solution C into the mixed solution B, adding the amino acid type surfactant and the alkyl glycoside, uniformly stirring to obtain a blended solution, adding the mixed slurry, the bacteriostatic agent and the citric acid into the blended solution, and uniformly stirring to obtain the shampoo.
Preferably, in the step (4), the pre-mixed slurry is added into a three-roll grinder to perform a grinding operation, wherein the gap between a front roll and a middle roll is adjusted to be 0.3 mm-0.5 mm, and the gap between the middle roll and a rear roll is adjusted to be 0.03 mm-0.06 mm.
Compared with the prior art, the invention has the following advantages and technical effects:
(1) the shampoo provided by the invention adopts mild amino acid type surfactant, and is matched with cocamido MIPA-disodium sulfosuccinate, cocamido propyl betaine and alkyl glycoside, each component is mild and non-irritant, the optimal synergistic effect can be generated, the good cleaning effect can be achieved, the shampoo has mild and non-irritant effects on the scalp, the comfort of users is improved, and the shampoo can be safely used by pregnant women and children.
(2) According to the invention, by adding effective contents of calamine powder, modified activated carbon powder and bacteriostatic agent, the effects of astringing, relieving itching, diminishing inflammation, inhibiting bacteria, resisting inflammation, resisting irritation and resisting allergy can be achieved while deep cleaning is carried out, the problems of scalp redness, acne growth, erythema and the like can be effectively solved, and the aim of health care of scalp is achieved by combining a mild system shampoo formula.
(3) The shampoo can be adjusted to be weakly acidic by adding the citric acid, and as the scalp of a normal person is weakly acidic and the pH value is 4.5-5.5, the weakly acidic property of the shampoo disclosed by the invention is attached to the acidic property of the human body, the effect of nourishing the skin of the head can be further achieved, and the scalp can be better nursed.
(4) The shampoo paste of the invention is prepared by adding the active carbon into the purslane juice, steaming and boiling, wherein the purslane is low in price and easy to obtain, the purslane juice can be obtained by squeezing and crushing, the active carbon has excellent adsorption function, the active carbon can be bulked more through the steaming and boiling, the molecular motion in the purslane juice is accelerated, and the active carbon can be further promoted to adsorb active ingredients in the purslane juice, so that the active ingredients in the purslane juice can be better locked in the active carbon, and then the active carbon is filtered, dried and ground into powder to obtain modified active carbon powder which is natural and non-irritant in components, is suitable for various hair qualities and can not pollute the environment, and is green and environment-friendly. Effectively care the scalp health.
Drawings
In order to more clearly illustrate the technical solutions of the embodiments of the present invention, the drawings needed to be used in the embodiments will be briefly described below, it should be understood that the following drawings only illustrate some embodiments of the present invention and therefore should not be considered as limiting the scope, and for those skilled in the art, other related drawings can be obtained according to the drawings without inventive efforts.
FIG. 1 is a photograph showing the evaluation results of the improvement effect of acne and redness of scalp of the subject of Experimental example 7.
Detailed Description
The present invention will be described in further detail with reference to specific examples, but the embodiments of the present invention are not limited thereto. All the raw materials and reagents used in the present invention are commercially available raw materials and reagents, unless otherwise specified. In the examples, the components are used in g and mL in parts by mass.
Example 1
In the embodiment, the shampoo comprises the following components in parts by mass: 15 parts of sodium cocoyl methyl taurate, 10 parts of potassium cocoyl glycinate, 10 parts of sodium cocoyl glycinate, 60 parts of disodium cocoamido MIPA-sulfosuccinate, 15 parts of cocamidopropyl betaine, 5 parts of decyl glucoside, 0.2 part of disodium EDTA, 6 parts of calamine powder, 3 parts of glycerol, 0.5 part of modified activated carbon powder, 1 part of polyquaternium-10, 1 part of polyquaternium-7, 2 parts of palmitoylamidopropyl trimethyl ammonium chloride, 1 part of phenoxyethanol, 0.5 part of citric acid and 6 parts of deionized water;
in this embodiment, the method for treating the modified activated carbon powder comprises: providing purslane juice and active carbon, adding the active carbon into the purslane juice, performing cooking operation, controlling the cooking temperature to be 60 ℃, cooking time to be 1h, then filtering, performing air drying operation to obtain dried modified active carbon, and performing grinding operation on the dried modified active carbon to obtain modified active carbon powder;
the preparation method of the shampoo provided by the embodiment comprises the following steps:
(1) adding polyquaternium-10, EDTA disodium, palmitamide propyl trimethyl ammonium chloride and deionized water into a reaction kettle according to a certain proportion, heating to 78 ℃, and preserving heat for 5min to obtain a mixed solution A;
(2) adding disodium cocoamido MIPA-sulfosuccinate into the mixed solution A in proportion at the temperature of 60 ℃, and uniformly stirring to obtain mixed solution B;
(3) under the condition of normal temperature, evenly mixing the cocamidopropyl betaine and the polyquaternium-7 in proportion to obtain a mixed solution C;
(4) under the condition of normal temperature, uniformly mixing calamine powder, glycerol and modified activated carbon powder in proportion to obtain premixed slurry, adding the premixed slurry into a three-roller grinding machine, grinding, adjusting the gap between a front roller and a middle roller to be 0.4mm, and adjusting the gap between the middle roller and a rear roller to be 0.04mm to obtain premixed slurry, vacuumizing the premixed slurry to remove air bubbles, and sieving the vacuumized premixed slurry through a 400-mesh screen to obtain mixed slurry;
(5) and adding the mixed solution C into the mixed solution B, adding the amino acid type surfactant and the alkyl glycoside, uniformly stirring to obtain a blended solution, adding the mixed slurry, the bacteriostatic agent and the citric acid into the blended solution, and uniformly stirring to obtain the shampoo.
Example 2
In the embodiment, the shampoo comprises the following components in parts by mass: 12 parts of sodium cocoyl methyl taurate, 8 parts of potassium cocoyl glycinate, 8 parts of sodium cocoyl glycinate, 50 parts of disodium cocoamido MIPA-sulfosuccinate, 12 parts of cocamidopropyl betaine, 4 parts of decyl glucoside, 0.15 part of disodium EDTA, 15 parts of calamine powder, 7 parts of glycerol, 2 parts of modified activated carbon powder, 0.7 part of polyquaternium-10, 0.7 part of polyquaternium-7, 1.5 parts of palmitoylamidopropyl trimethyl ammonium chloride, 0.8 part of phenoxyethanol, 0.4 part of citric acid and 5 parts of deionized water;
in this embodiment, the method for treating the modified activated carbon powder comprises: providing purslane juice and active carbon, adding the active carbon into the purslane juice, performing cooking operation, controlling the cooking temperature to be 60 ℃, cooking time to be 1h, then filtering, performing air drying operation to obtain dried modified active carbon, and performing grinding operation on the dried modified active carbon to obtain modified active carbon powder;
the preparation method of the shampoo provided by the embodiment comprises the following steps:
(1) adding polyquaternium-10, EDTA disodium, palmitamide propyl trimethyl ammonium chloride and deionized water into a reaction kettle according to a certain proportion, heating to 78 ℃, and preserving heat for 5min to obtain a mixed solution A;
(2) adding disodium cocoamido MIPA-sulfosuccinate into the mixed solution A in proportion at the temperature of 60 ℃, and uniformly stirring to obtain mixed solution B;
(3) under the condition of normal temperature, evenly mixing the cocamidopropyl betaine and the polyquaternium-7 in proportion to obtain a mixed solution C;
(4) under the condition of normal temperature, uniformly mixing calamine powder, glycerol and modified activated carbon powder in proportion to obtain premixed slurry, adding the premixed slurry into a three-roller grinding machine, grinding, adjusting the gap between a front roller and a middle roller to be 0.4mm, and adjusting the gap between the middle roller and a rear roller to be 0.04mm to obtain premixed slurry, vacuumizing the premixed slurry to remove air bubbles, and sieving the vacuumized premixed slurry through a 400-mesh screen to obtain mixed slurry;
(5) and adding the mixed solution C into the mixed solution B, adding the amino acid type surfactant and the alkyl glycoside, uniformly stirring to obtain a blended solution, adding the mixed slurry, the bacteriostatic agent and the citric acid into the blended solution, and uniformly stirring to obtain the shampoo.
Example 3
In the embodiment, the shampoo comprises the following components in parts by mass: 8 parts of sodium cocoyl methyl taurate, 5 parts of potassium cocoyl glycinate, 5 parts of sodium cocoyl glycinate, 30 parts of disodium cocoamido MIPA-sulfosuccinate, 8 parts of cocamidopropyl betaine, 2 parts of decyl glucoside, 0.1 part of disodium EDTA, 20 parts of calamine powder, 10 parts of glycerol, 4 parts of modified activated carbon powder, 0.4 part of polyquaternium-10, 0.4 part of polyquaternium-7, 1 part of palmitylamidopropyl trimethyl ammonium chloride, 0.5 part of phenoxyethanol, 0.2 part of citric acid and 4 parts of deionized water;
in this embodiment, the method for treating the modified activated carbon powder comprises: providing purslane juice and active carbon, adding the active carbon into the purslane juice, performing cooking operation, controlling the cooking temperature to be 60 ℃, cooking time to be 1h, then filtering, performing air drying operation to obtain dried modified active carbon, and performing grinding operation on the dried modified active carbon to obtain modified active carbon powder;
the preparation method of the shampoo provided by the embodiment comprises the following steps:
(1) adding polyquaternium-10, EDTA disodium, palmitamide propyl trimethyl ammonium chloride and deionized water into a reaction kettle according to a certain proportion, heating to 78 ℃, and preserving heat for 5min to obtain a mixed solution A;
(2) adding disodium cocoamido MIPA-sulfosuccinate into the mixed solution A in proportion at the temperature of 60 ℃, and uniformly stirring to obtain mixed solution B;
(3) under the condition of normal temperature, evenly mixing the cocamidopropyl betaine and the polyquaternium-7 in proportion to obtain a mixed solution C;
(4) under the condition of normal temperature, uniformly mixing calamine powder, glycerol and modified activated carbon powder in proportion to obtain premixed slurry, adding the premixed slurry into a three-roller grinding machine, grinding, adjusting the gap between a front roller and a middle roller to be 0.4mm, and adjusting the gap between the middle roller and a rear roller to be 0.04mm to obtain premixed slurry, vacuumizing the premixed slurry to remove air bubbles, and sieving the vacuumized premixed slurry through a 400-mesh screen to obtain mixed slurry;
(5) and adding the mixed solution C into the mixed solution B, adding the amino acid type surfactant and the alkyl glycoside, uniformly stirring to obtain a blended solution, adding the mixed slurry, the bacteriostatic agent and the citric acid into the blended solution, and uniformly stirring to obtain the shampoo.
Example 4
In the embodiment, the shampoo comprises the following components in parts by mass: 5 parts of sodium cocoyl methyl taurate, 3 parts of potassium cocoyl glycinate, 3 parts of sodium cocoyl glycinate, 20 parts of disodium cocoamido MIPA-sulfosuccinate, 5 parts of cocamidopropyl betaine, 1 part of decyl glucoside, 0.05 part of disodium EDTA, 30 parts of calamine powder, 15 parts of glycerol, 5 parts of modified activated carbon powder, 0.03 part of polyquaternary ammonium salt-10, 0.05 part of polyquaternary ammonium salt-7, 0.5 part of palmitoylamidopropyl trimethyl ammonium chloride, 0.3 part of phenoxyethanol, 0.05 part of citric acid and 3 parts of deionized water;
in this embodiment, the method for treating the modified activated carbon powder comprises: providing purslane juice and active carbon, adding the active carbon into the purslane juice, performing cooking operation, controlling the cooking temperature to be 60 ℃, cooking time to be 1h, then filtering, performing air drying operation to obtain dried modified active carbon, and performing grinding operation on the dried modified active carbon to obtain modified active carbon powder;
the preparation method of the shampoo provided by the embodiment comprises the following steps:
(1) adding polyquaternium-10, EDTA disodium, palmitamide propyl trimethyl ammonium chloride and deionized water into a reaction kettle according to a certain proportion, heating to 78 ℃, and preserving heat for 5min to obtain a mixed solution A;
(2) adding disodium cocoamido MIPA-sulfosuccinate into the mixed solution A in proportion at the temperature of 60 ℃, and uniformly stirring to obtain mixed solution B;
(3) under the condition of normal temperature, evenly mixing the cocamidopropyl betaine and the polyquaternium-7 in proportion to obtain a mixed solution C;
(4) under the condition of normal temperature, uniformly mixing calamine powder, glycerol and modified activated carbon powder in proportion to obtain premixed slurry, adding the premixed slurry into a three-roller grinding machine, grinding, adjusting the gap between a front roller and a middle roller to be 0.4mm, and adjusting the gap between the middle roller and a rear roller to be 0.04mm to obtain premixed slurry, vacuumizing the premixed slurry to remove air bubbles, and sieving the vacuumized premixed slurry through a 400-mesh screen to obtain mixed slurry;
(5) and adding the mixed solution C into the mixed solution B, adding the amino acid type surfactant and the alkyl glycoside, uniformly stirring to obtain a blended solution, adding the mixed slurry, the bacteriostatic agent and the citric acid into the blended solution, and uniformly stirring to obtain the shampoo.
Example 5
In the embodiment, the shampoo comprises the following components in parts by mass: 8 parts of sodium cocoyl methyl taurate, 5 parts of potassium cocoyl glycinate, 5 parts of sodium cocoyl glycinate, 30 parts of disodium cocoamido MIPA-sulfosuccinate, 8 parts of cocamidopropyl betaine, 2 parts of decyl glucoside, 0.1 part of disodium EDTA, 20 parts of calamine powder, 10 parts of glycerol, 4 parts of modified activated carbon powder, 0.4 part of polyquaternium-10, 0.4 part of polyquaternium-7, 1 part of palmitylamidopropyl trimethyl ammonium chloride, 0.5 part of phenoxyethanol, 0.2 part of citric acid and 4 parts of deionized water;
in this embodiment, the method for treating the modified activated carbon powder comprises: providing purslane juice and active carbon, adding the active carbon into the purslane juice, performing cooking operation, controlling the cooking temperature to be 55 ℃, and the cooking time to be 0.5h, then filtering, performing air drying operation to obtain dry modified active carbon, and performing grinding operation on the dry modified active carbon to obtain modified active carbon powder;
the preparation method of the shampoo provided by the embodiment comprises the following steps:
(1) adding polyquaternium-10, EDTA disodium, palmitamide propyl trimethyl ammonium chloride and deionized water into a reaction kettle according to a certain proportion, heating to 75 ℃, and preserving heat for 5min to obtain a mixed solution A;
(2) adding disodium cocoamido MIPA-sulfosuccinate into the mixed solution A in proportion at the temperature of 60 ℃, and uniformly stirring to obtain mixed solution B;
(3) under the condition of normal temperature, evenly mixing the cocamidopropyl betaine and the polyquaternium-7 in proportion to obtain a mixed solution C;
(4) under the condition of normal temperature, uniformly mixing calamine powder, glycerol and modified activated carbon powder in proportion to obtain premixed slurry, adding the premixed slurry into a three-roller grinding machine, grinding, adjusting the gap between a front roller and a middle roller to be 0.4mm, and adjusting the gap between the middle roller and a rear roller to be 0.04mm to obtain premixed slurry, vacuumizing the premixed slurry to remove air bubbles, and sieving the vacuumized premixed slurry through a 400-mesh screen to obtain mixed slurry;
(5) and adding the mixed solution C into the mixed solution B, adding the amino acid type surfactant and the alkyl glycoside, uniformly stirring to obtain a blended solution, adding the mixed slurry, the bacteriostatic agent and the citric acid into the blended solution, and uniformly stirring to obtain the shampoo.
Example 6
In the embodiment, the shampoo comprises the following components in parts by mass: 8 parts of sodium cocoyl methyl taurate, 5 parts of potassium cocoyl glycinate, 5 parts of sodium cocoyl glycinate, 30 parts of disodium cocoamido MIPA-sulfosuccinate, 8 parts of cocamidopropyl betaine, 2 parts of decyl glucoside, 0.1 part of disodium EDTA, 20 parts of calamine powder, 10 parts of glycerol, 4 parts of modified activated carbon powder, 0.4 part of polyquaternium-10, 0.4 part of polyquaternium-7, 1 part of palmitylamidopropyl trimethyl ammonium chloride, 0.5 part of phenoxyethanol, 0.2 part of citric acid and 4 parts of deionized water;
in this embodiment, the method for treating the modified activated carbon powder comprises: providing purslane juice and active carbon, adding the active carbon into the purslane juice, performing cooking operation, controlling the cooking temperature to be 65 ℃ and the cooking time to be 1.5h, then filtering, performing air drying operation to obtain dried modified active carbon, and performing grinding operation on the dried modified active carbon to obtain modified active carbon powder;
the preparation method of the shampoo provided by the embodiment comprises the following steps:
(1) adding polyquaternium-10, EDTA disodium, palmitamide propyl trimethyl ammonium chloride and deionized water into a reaction kettle according to a certain proportion, heating to 80 ℃, and preserving heat for 5min to obtain a mixed solution A;
(2) adding disodium cocoamido MIPA-sulfosuccinate into the mixed solution A in proportion at the temperature of 60 ℃, and uniformly stirring to obtain mixed solution B;
(3) under the condition of normal temperature, evenly mixing the cocamidopropyl betaine and the polyquaternium-7 in proportion to obtain a mixed solution C;
(4) under the condition of normal temperature, uniformly mixing calamine powder, glycerol and modified activated carbon powder in proportion to obtain premixed slurry, adding the premixed slurry into a three-roller grinding machine, grinding, adjusting the gap between a front roller and a middle roller to be 0.4mm, and adjusting the gap between the middle roller and a rear roller to be 0.04mm to obtain premixed slurry, vacuumizing the premixed slurry to remove air bubbles, and sieving the vacuumized premixed slurry through a 400-mesh screen to obtain mixed slurry;
(5) and adding the mixed solution C into the mixed solution B, adding the amino acid type surfactant and the alkyl glycoside, uniformly stirring to obtain a blended solution, adding the mixed slurry, the bacteriostatic agent and the citric acid into the blended solution, and uniformly stirring to obtain the shampoo.
Example 7
In the embodiment, the shampoo comprises the following components in parts by mass: 10 parts of sodium cocoyl methyl taurate, 7 parts of potassium cocoyl glycinate, 7 parts of sodium cocoyl glycinate, 42 parts of disodium cocoamido MIPA-sulfosuccinate, 10 parts of cocamidopropyl betaine, 2 parts of decyl glucoside, 0.1 part of disodium EDTA, 28 parts of calamine powder, 12 parts of glycerol, 4.5 parts of modified activated carbon powder, 0.35 part of polyquaternary ammonium salt-10, 0.35 part of polyquaternary ammonium salt-7, 0.12 part of palmitoylamidopropyl trimethyl ammonium chloride, 0.4 part of phenoxyethanol, 0.2 part of citric acid and 4 parts of deionized water;
in this embodiment, the method for treating the modified activated carbon powder comprises: providing purslane juice and active carbon, adding the active carbon into the purslane juice, performing cooking operation, controlling the cooking temperature to be 65 ℃ and the cooking time to be 1.5h, then filtering, performing air drying operation to obtain dried modified active carbon, and performing grinding operation on the dried modified active carbon to obtain modified active carbon powder;
the preparation method of the shampoo provided by the embodiment comprises the following steps:
(1) adding polyquaternium-10, EDTA disodium, palmitamide propyl trimethyl ammonium chloride and deionized water into a reaction kettle according to a certain proportion, heating to 80 ℃, and preserving heat for 5min to obtain a mixed solution A;
(2) adding disodium cocoamido MIPA-sulfosuccinate into the mixed solution A in proportion at the temperature of 60 ℃, and uniformly stirring to obtain mixed solution B;
(3) under the condition of normal temperature, evenly mixing the cocamidopropyl betaine and the polyquaternium-7 in proportion to obtain a mixed solution C;
(4) under the condition of normal temperature, uniformly mixing calamine powder, glycerol and modified activated carbon powder in proportion to obtain premixed slurry, adding the premixed slurry into a three-roller grinding machine, grinding, adjusting the gap between a front roller and a middle roller to be 0.4mm, and adjusting the gap between the middle roller and a rear roller to be 0.04mm to obtain premixed slurry, vacuumizing the premixed slurry to remove air bubbles, and sieving the vacuumized premixed slurry through a 400-mesh screen to obtain mixed slurry;
(5) and adding the mixed solution C into the mixed solution B, adding the amino acid type surfactant and the alkyl glycoside, uniformly stirring to obtain a blended solution, adding the mixed slurry, the bacteriostatic agent and the citric acid into the blended solution, and uniformly stirring to obtain the shampoo.
Comparative example 1
In the embodiment, the shampoo comprises the following components in parts by mass: 8 parts of sodium cocoyl methyl taurate, 5 parts of potassium cocoyl glycinate, 5 parts of sodium cocoyl glycinate, 30 parts of disodium cocoamido MIPA-sulfosuccinate, 8 parts of cocamidopropyl betaine, 2 parts of decyl glucoside, 0.1 part of disodium EDTA, 20 parts of calamine powder, 10 parts of glycerol, 0.4 part of polyquaternium-10, 0.4 part of polyquaternium-7, 1 part of palmitoylamidopropyl trimethyl ammonium chloride, 0.5 part of phenoxyethanol, 0.2 part of citric acid and 4 parts of deionized water;
the preparation method of the shampoo provided by the embodiment comprises the following steps:
(1) adding polyquaternium-10, EDTA disodium, palmitamide propyl trimethyl ammonium chloride and deionized water into a reaction kettle according to a certain proportion, heating to 78 ℃, and preserving heat for 5min to obtain a mixed solution A;
(2) adding disodium cocoamido MIPA-sulfosuccinate into the mixed solution A in proportion at the temperature of 60 ℃, and uniformly stirring to obtain mixed solution B;
(3) under the condition of normal temperature, evenly mixing the cocamidopropyl betaine and the polyquaternium-7 in proportion to obtain a mixed solution C;
(4) under the condition of normal temperature, uniformly mixing calamine powder and glycerol in proportion to obtain premixed slurry, adding the premixed slurry into a three-roller grinding machine, grinding, adjusting the gap between a front roller and a middle roller to be 0.4mm, and adjusting the gap between the middle roller and a rear roller to be 0.04mm to obtain premixed slurry, vacuumizing the premixed slurry to remove air bubbles, and sieving the vacuumized premixed slurry through a 400-mesh screen to obtain mixed slurry;
(5) and adding the mixed solution C into the mixed solution B, adding the amino acid type surfactant and the alkyl glycoside, uniformly stirring to obtain a blended solution, adding the mixed slurry, the bacteriostatic agent and the citric acid into the blended solution, and uniformly stirring to obtain the shampoo.
Comparative example 2
In the embodiment, the shampoo comprises the following components in parts by mass: 8 parts of sodium cocoyl methyl taurate, 5 parts of potassium cocoyl glycinate, 5 parts of sodium cocoyl glycinate, 30 parts of disodium cocoamido MIPA-sulfosuccinate, 8 parts of cocamidopropyl betaine, 2 parts of decyl glucoside, 0.1 part of disodium EDTA, 20 parts of calamine powder, 10 parts of glycerol, 4 parts of purslane extract, 0.4 part of polyquaternium-10, 0.4 part of polyquaternium-7, 1 part of palmitoylamidopropyl trimethyl ammonium chloride, 0.5 part of phenoxyethanol, 0.2 part of citric acid and 4 parts of deionized water;
the preparation method of the shampoo provided by the embodiment comprises the following steps:
(1) adding polyquaternium-10, EDTA disodium, palmitamide propyl trimethyl ammonium chloride and deionized water into a reaction kettle according to a certain proportion, heating to 78 ℃, and preserving heat for 5min to obtain a mixed solution A;
(2) adding disodium cocoamido MIPA-sulfosuccinate into the mixed solution A in proportion at the temperature of 60 ℃, and uniformly stirring to obtain mixed solution B;
(3) under the condition of normal temperature, evenly mixing the cocamidopropyl betaine and the polyquaternium-7 in proportion to obtain a mixed solution C;
(4) under the condition of normal temperature, uniformly mixing calamine powder, glycerol and purslane extract according to a proportion to obtain premixed slurry, adding the premixed slurry into a three-roller grinder, grinding, adjusting the gap between a front roller and a middle roller to be 0.4mm, and adjusting the gap between a middle roller and a rear roller to be 0.04mm to obtain premixed slurry, vacuumizing the premixed slurry to remove air bubbles, and sieving the vacuumized premixed slurry through a 400-mesh screen to obtain mixed slurry;
(5) and adding the mixed solution C into the mixed solution B, adding the amino acid type surfactant and the alkyl glycoside, uniformly stirring to obtain a blended solution, adding the mixed slurry, the bacteriostatic agent and the citric acid into the blended solution, and uniformly stirring to obtain the shampoo.
Comparative example 3
In the embodiment, the shampoo comprises the following components in parts by mass: 8 parts of sodium cocoyl methyl taurate, 5 parts of potassium cocoyl glycinate, 5 parts of sodium cocoyl glycinate, 30 parts of disodium cocoamido MIPA-sulfosuccinate, 8 parts of cocamidopropyl betaine, 2 parts of decyl glucoside, 0.1 part of disodium EDTA, 20 parts of calamine powder, 10 parts of glycerol, 4 parts of modified activated carbon powder, 0.4 part of polyquaternium-10, 0.4 part of polyquaternium-7, 1 part of palmitylamidopropyl trimethyl ammonium chloride, 0.5 part of phenoxyethanol, 0.2 part of citric acid and 4 parts of deionized water;
in this embodiment, the method for treating the modified activated carbon powder comprises: providing purslane juice and active carbon, adding the active carbon into the purslane juice, performing cooking operation, controlling the cooking temperature to be 60 ℃, cooking time to be 1h, then filtering, performing air drying operation to obtain dried modified active carbon, and performing grinding operation on the dried modified active carbon to obtain modified active carbon powder;
the preparation method of the shampoo provided by the embodiment comprises the following steps:
(1) adding polyquaternium-10, EDTA disodium, palmitamide propyl trimethyl ammonium chloride and deionized water into a reaction kettle according to a certain proportion, heating to 78 ℃, and preserving heat for 5min to obtain a mixed solution A;
(2) adding disodium cocoamido MIPA-sulfosuccinate into the mixed solution A in proportion at the temperature of 60 ℃, and uniformly stirring to obtain mixed solution B;
(3) under the condition of normal temperature, evenly mixing the cocamidopropyl betaine and the polyquaternium-7 in proportion to obtain a mixed solution C;
(4) adding the mixed solution C into the mixed solution B, adding an amino acid type surfactant and alkyl glycoside, uniformly stirring to obtain a blended solution, adding the calamine powder, the glycerol, the modified activated carbon powder, the bacteriostatic agent and the citric acid into the blended solution according to the proportion, and uniformly stirring to obtain the shampoo.
Clinical effect experiment:
test subjects: by 200 (men and women account for half of the population): patients with scalp itching, redness, acne and erythema are tried out, 200 (half of men and women) patients with scalp itching, redness, acne and erythema are randomly divided into 10 groups, and each group comprises 20 patients;
the using method comprises the following steps: the shampoo prepared in examples 1 to 7 and comparative examples 1 to 3 was used for each group, and the hair was washed once every two days, each time, the shampoo was used for 200 seconds of rubbing and 100 seconds of rinsing, and the shampoo was used continuously for 1 month.
Grading standard: the testers score each evaluation item according to their own use feeling, the full score is 10 points, 10 points are that the scalp is not itchy, redness, acne and red rash are obviously reduced, the effect is obvious, the effect is the worst at 1 point, the scalp is itchy, and redness, acne and red rash are easy to occur.
The results, which were examined after 1 month of use by the subjects, were as follows:
TABLE 1 evaluation results of subjects 1 month after use
As can be seen from Table 1, the shampoo pastes of examples 1 to 7 have overall better effects on relieving scalp itch, redness, acne and erythema than comparative examples 1 to 3, compared with comparative example 1, the modified activated carbon powder component is added in the shampoo pastes of examples 1 to 7, the shampoo pastes and the calamine powder have good compounding synergistic effect, can have effective itching relieving, anti-inflammatory, anti-irritation and anti-allergy effects, effectively relieve itch, acne, redness and erythema, and effectively care for scalp health, compared with comparative example 2, the modified activated carbon powder obtained by the treatment method of the modified activated carbon powder has better effects on relieving scalp itch, redness, acne and erythema, compared with comparative example 3, the shampoo pastes of examples 1 to 7 have better effects on relieving scalp itch, redness, acne and erythema, the shampoo of the embodiments of the invention can achieve good anti-inflammatory, anti-irritation and anti-allergy effects, is mild and non-irritating to the scalp, and is suitable for various crowds. Wherein, the photo before and after the shampoo nursing of one test subject of the test subject in the example 7 is shown in figure 1, and the photo shows that the scalp has the problems of acne growing and redness before the test subject uses the shampoo provided by the invention, and the acne is dispelled and the redness disappears after the test subject uses the shampoo provided by the invention, and the effect is obvious.
The above embodiments are the best mode for carrying out the present invention, but the embodiments of the present invention are not limited to the above embodiments, and any other changes, modifications, substitutions, combinations, and simplifications which do not depart from the spirit and principle of the present invention should be regarded as equivalent substitutions and are included in the scope of the present invention.
Claims (10)
1. The shampoo is characterized by comprising the following components in parts by mass: 11-35 parts of amino acid type surfactant, 20-60 parts of disodium cocoamido MIPA-sulfosuccinate, 5-15 parts of cocamidopropyl betaine, 1-5 parts of alkyl glycoside, 0.05-0.2 part of disodium EDTA, 6-30 parts of calamine powder, 3-15 parts of glycerol, 0.5-5 parts of modified activated carbon powder, 0.03-1 part of polyquaternary ammonium salt-10, 0.05-1 part of polyquaternary ammonium salt-7, 0.5-2 parts of palmitoyl propyl trimethyl ammonium chloride, 0.3-1 part of bacteriostatic agent, 0.05-0.5 part of citric acid and 3-6 parts of water.
2. The shampoo according to claim 1, wherein: the amino acid type surfactant comprises sodium cocoyl methyl taurate, potassium cocoyl glycinate and sodium cocoyl glycinate.
3. The shampoo according to claim 2, wherein: the amino acid type surfactant comprises, by mass, 5-15 parts of sodium cocoyl methyl taurate, 3-10 parts of potassium cocoyl glycinate and 3-10 parts of sodium cocoyl glycinate.
4. The shampoo according to claim 1, wherein: the water is deionized water.
5. The shampoo according to claim 1, wherein: the alkyl glycoside is decyl glucoside.
6. The shampoo according to claim 1, wherein: the treatment method of the modified activated carbon powder comprises the following steps: providing purslane juice and activated carbon, adding the activated carbon into the purslane juice, performing cooking operation, then filtering, performing drying operation to obtain dried modified activated carbon, and performing grinding operation on the dried modified activated carbon to obtain the modified activated carbon powder.
7. The shampoo according to claim 6, wherein: in the cooking operation, the cooking temperature is controlled to be 55-65 ℃, and the cooking time is 0.5-1.5 h.
8. The shampoo according to claim 6, wherein: in the drying operation, an air drying operation is adopted as the drying operation.
9. The shampoo according to claim 1, wherein: the bacteriostatic agent is phenoxyethanol.
10. The method for preparing the shampoo paste according to any one of claims 1 to 9, characterized by comprising the steps of:
(1) adding polyquaternium-10, EDTA disodium, palmitamide propyl trimethyl ammonium chloride and water into a reaction kettle according to a certain proportion, heating to 75-80 ℃, and preserving heat for 5min to obtain a mixed solution A;
(2) adding disodium cocoamido MIPA-sulfosuccinate into the mixed solution A in proportion at the temperature of 60 ℃, and uniformly stirring to obtain mixed solution B;
(3) under the condition of normal temperature, evenly mixing the cocamidopropyl betaine and the polyquaternium-7 in proportion to obtain a mixed solution C;
(4) under the condition of normal temperature, uniformly mixing calamine powder, glycerol and modified activated carbon powder in proportion to obtain premixed slurry, adding the premixed slurry into a three-roller grinder, grinding to obtain premixed slurry, vacuumizing the premixed slurry to remove air bubbles, and sieving the vacuumized premixed slurry through a 400-mesh screen to obtain mixed slurry;
(5) and adding the mixed solution C into the mixed solution B, adding the amino acid type surfactant and the alkyl glycoside, uniformly stirring to obtain a blended solution, adding the mixed slurry, the bacteriostatic agent and the citric acid into the blended solution, and uniformly stirring to obtain the shampoo.
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| CN103877552A (en) * | 2014-04-01 | 2014-06-25 | 邓林生 | Application of powdered activated carbon in treating alopecia and hair growth liquid |
| CN105232404A (en) * | 2015-11-11 | 2016-01-13 | 曹涛 | Liquid shampoo for repairing damaged scalp after hair dyeing and hair perming and removing scrap and resisting to allergy |
| CN109381363A (en) * | 2018-12-20 | 2019-02-26 | 广州艾蓓生物科技有限公司 | A kind of amino acid shampoo and preparation method thereof |
| CN109498494A (en) * | 2018-12-26 | 2019-03-22 | 广州蜜妆生物科技有限公司 | A kind of salubrious oil-control is without silicone oil shampoo and preparation method thereof |
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