CN116585206B - Shampoo and preparation method thereof - Google Patents
Shampoo and preparation method thereof Download PDFInfo
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- CN116585206B CN116585206B CN202310657924.8A CN202310657924A CN116585206B CN 116585206 B CN116585206 B CN 116585206B CN 202310657924 A CN202310657924 A CN 202310657924A CN 116585206 B CN116585206 B CN 116585206B
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- 239000002453 shampoo Substances 0.000 title claims abstract description 127
- 238000002360 preparation method Methods 0.000 title abstract description 87
- 238000001179 sorption measurement Methods 0.000 claims abstract description 122
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 119
- 239000004094 surface-active agent Substances 0.000 claims abstract description 95
- 150000002632 lipids Chemical class 0.000 claims abstract description 88
- 150000007524 organic acids Chemical class 0.000 claims abstract description 87
- MTCFGRXMJLQNBG-REOHCLBHSA-N (2S)-2-Amino-3-hydroxypropansäure Chemical compound OC[C@H](N)C(O)=O MTCFGRXMJLQNBG-REOHCLBHSA-N 0.000 claims abstract description 84
- 239000002994 raw material Substances 0.000 claims abstract description 70
- 238000003756 stirring Methods 0.000 claims abstract description 62
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- 150000004676 glycans Chemical class 0.000 claims abstract description 60
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- 239000005017 polysaccharide Substances 0.000 claims abstract description 60
- 229910021536 Zeolite Inorganic materials 0.000 claims abstract description 50
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 claims abstract description 50
- 239000000843 powder Substances 0.000 claims abstract description 50
- 239000010457 zeolite Substances 0.000 claims abstract description 50
- 238000002156 mixing Methods 0.000 claims abstract description 46
- SNPLKNRPJHDVJA-ZETCQYMHSA-N D-panthenol Chemical compound OCC(C)(C)[C@@H](O)C(=O)NCCCO SNPLKNRPJHDVJA-ZETCQYMHSA-N 0.000 claims abstract description 42
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- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 60
- GVJHHUAWPYXKBD-UHFFFAOYSA-N (±)-α-Tocopherol Chemical compound OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 claims description 42
- 238000005303 weighing Methods 0.000 claims description 32
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- URJOWNUVTORLNY-UHFFFAOYSA-N (5-hexadecanoyloxy-4-oxopyran-2-yl) hexadecanoate Chemical compound CCCCCCCCCCCCCCCC(=O)OC1=CC(=O)C(OC(=O)CCCCCCCCCCCCCCC)=CO1 URJOWNUVTORLNY-UHFFFAOYSA-N 0.000 claims description 21
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- 125000000217 alkyl group Chemical group 0.000 claims description 21
- WIGCFUFOHFEKBI-UHFFFAOYSA-N gamma-tocopherol Natural products CC(C)CCCC(C)CCCC(C)CCCC1CCC2C(C)C(O)C(C)C(C)C2O1 WIGCFUFOHFEKBI-UHFFFAOYSA-N 0.000 claims description 21
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- 240000003553 Leptospermum scoparium Species 0.000 claims description 20
- 235000015459 Lycium barbarum Nutrition 0.000 claims description 20
- MRUAUOIMASANKQ-UHFFFAOYSA-N cocamidopropyl betaine Chemical compound CCCCCCCCCCCC(=O)NCCC[N+](C)(C)CC([O-])=O MRUAUOIMASANKQ-UHFFFAOYSA-N 0.000 claims description 20
- 229940073507 cocamidopropyl betaine Drugs 0.000 claims description 20
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- BJEPYKJPYRNKOW-REOHCLBHSA-N (S)-malic acid Chemical compound OC(=O)[C@@H](O)CC(O)=O BJEPYKJPYRNKOW-REOHCLBHSA-N 0.000 claims description 4
- BJEPYKJPYRNKOW-UHFFFAOYSA-N alpha-hydroxysuccinic acid Natural products OC(=O)C(O)CC(O)=O BJEPYKJPYRNKOW-UHFFFAOYSA-N 0.000 claims description 4
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- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 2
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- 238000002386 leaching Methods 0.000 description 2
- 229940069445 licorice extract Drugs 0.000 description 2
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- 230000003647 oxidation Effects 0.000 description 2
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- DTGKSKDOIYIVQL-WEDXCCLWSA-N (+)-borneol Chemical compound C1C[C@@]2(C)[C@@H](O)C[C@@H]1C2(C)C DTGKSKDOIYIVQL-WEDXCCLWSA-N 0.000 description 1
- REPVLJRCJUVQFA-UHFFFAOYSA-N (-)-isopinocampheol Natural products C1C(O)C(C)C2C(C)(C)C1C2 REPVLJRCJUVQFA-UHFFFAOYSA-N 0.000 description 1
- FJKROLUGYXJWQN-UHFFFAOYSA-M 4-hydroxybenzoate Chemical compound OC1=CC=C(C([O-])=O)C=C1 FJKROLUGYXJWQN-UHFFFAOYSA-M 0.000 description 1
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- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
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- 238000010521 absorption reaction Methods 0.000 description 1
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- 238000000861 blow drying Methods 0.000 description 1
- 229940116229 borneol Drugs 0.000 description 1
- CKDOCTFBFTVPSN-UHFFFAOYSA-N borneol Natural products C1CC2(C)C(C)CC1C2(C)C CKDOCTFBFTVPSN-UHFFFAOYSA-N 0.000 description 1
- 239000004359 castor oil Substances 0.000 description 1
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- 239000012153 distilled water Substances 0.000 description 1
- DTGKSKDOIYIVQL-UHFFFAOYSA-N dl-isoborneol Natural products C1CC2(C)C(O)CC1C2(C)C DTGKSKDOIYIVQL-UHFFFAOYSA-N 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
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- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 description 1
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- 239000011780 sodium chloride Substances 0.000 description 1
- 229940057950 sodium laureth sulfate Drugs 0.000 description 1
- SXHLENDCVBIJFO-UHFFFAOYSA-M sodium;2-[2-(2-dodecoxyethoxy)ethoxy]ethyl sulfate Chemical group [Na+].CCCCCCCCCCCCOCCOCCOCCOS([O-])(=O)=O SXHLENDCVBIJFO-UHFFFAOYSA-M 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
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- 210000004243 sweat Anatomy 0.000 description 1
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Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/26—Aluminium; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/42—Amides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/736—Chitin; Chitosan; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/002—Preparations for repairing the hair, e.g. hair cure
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/596—Mixtures of surface active compounds
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Abstract
The application relates to the technical field of washing and caring products, and particularly discloses shampoo and a preparation method thereof, wherein the shampoo comprises raw material adsorption type active components, a surfactant, a lipid component, organic acid and water; the adsorption type active component consists of the following raw materials: zeolite powder, chitosan, algal polysaccharide, L-serine, panthenol and water; the shampoo preparation method comprises the steps of adding a surfactant and a lipid component into water, and stirring and mixing uniformly to obtain a premix; adding the adsorption type active components and the organic acid into the premix, stirring and mixing uniformly, and sub-packaging to obtain the required shampoo; the shampoo has the advantages of simple formula, strict proportion, simple preparation method, mild preparation conditions, suitability for industrial production, excellent foaming performance, rich, fine and stable foam, and can be used for hair washing and caring, effectively clean hair, nourish and repair scalp and hair, and avoid excessive cleaning of scalp and hair.
Description
Technical Field
The application relates to the technical field of washing and caring products, in particular to shampoo and a preparation method thereof.
Background
Shampoo, also known as shampoo, is the most widely used shampoo for cleaning the body which adheres to the scalp and hair to excrete grease and sweat scale, the cells which fall off the scalp, foreign dust, microorganisms, residues and bad smell of styling products, and the like, and keeping the scalp and hair clean and beautiful. The components contained in the shampoo commonly used in the market at present are mainly surfactants, and the addition of the surfactants can effectively clean grease and dirt on hair, but can also cause the problems of dry hair, dysphoria, easy breakage, even scalp sensitivity, itching, alopecia and the like; in addition, the sulfate, parahydroxybenzoate and other components contained in the shampoo may cause damage to scalp and hair, and may even have negative effects on human health.
With the increasing importance of hair health, more and more consumers are looking for shampoo with nourishing and repairing effects. In the prior art, a shampoo with nourishing and repairing effects is manufactured by adding natural plant components, and the shampoo is disclosed in Chinese patent application number 202210312814.3, and is characterized by comprising the following components in mass: 30-40 parts of rice washing water fermentation product, 0.05-0.08 part of licorice extract, 0.03-0.05 part of clove extract, 0.04-0.06 part of ice R, 0.3-1.2 part of phellodendron extract, 0.3-0.8 part of radix scutellariae extract, 0.8-1.2 parts of tea bran extract, 0.4-0.8 part of oil seed extract, 1-2 parts of polygonum multiflorum extract, 0.6-1.2 parts of poria cocos extract, 0.6-1.2 parts of semen cuscutae extract, 0.2-0.6 part of rabbit hair keratin, 3-7 parts of surfactant, 0.1-0.3 part of hydrogenated castor oil and 0.6-15 parts of thickening agent; wherein the surfactant is sodium laureth sulfate, cocamidopropyl betaine and coconut diethanolamide, which are mixed according to the mass ratio of 12-18:2-4:4-8; the thickener is compounded by sodium chloride and Versathix according to the mass ratio of 1:1, and the Versathix is produced by Heda; the preparation method of the shampoo comprises the following steps: mixing cortex Phellodendri, scutellariae radix, and Glycyrrhrizae radix in 4-6 times of water by mass ratio, soaking for 2 hr, inoculating 5-8% Aspergillus niger, fermenting at 28-30deg.C and 180-220rpm for 40-60 hr, sterilizing, filtering to obtain fermentation liquid, and concentrating to 1-2 times of the medicinal herbs by mass ratio to obtain extract mixed solution; adding yeast strain with mass of 2-5% into rice washing water, fermenting at 25-32deg.C for 50-70 hr, sterilizing, and filtering to obtain rice washing water fermented product; leaching the tea bran subjected to pressure treatment under 0.8-1.0MPa with water, filtering, separating to obtain leaching solution, and concentrating to 0.5-0.8 times of the weight of the tea bran to obtain tea bran extract; pulverizing Polygoni Multiflori radix into granule, mixing with distilled water to obtain 3-8% mixed solution, sterilizing under high pressure, inoculating Rhizopus oryzae strain, fermenting at 25-28deg.C at 100-150rpm for 40-50 hr, sterilizing, filtering, and concentrating to 1-2 times of the medicine mass to obtain Polygoni Multiflori radix extract; mixing semen Cuscutae, semen Sapindi Mukouossi, flos Caryophylli and Poria at a mass ratio, soaking in 5 times of water for 4 hr, decocting, concentrating to 2.5 times of the weight of the medicine, filtering, and concentrating the filtrate under heating to 0.6-0.8 times of the weight of the medicine to obtain semen Cuscutae, semen Sapindi Mukouossi, flos Caryophylli and Poria extract. The shampoo product uses rice washing water fermentation product and traditional Chinese medicine extract as main active ingredients, and the traditional Chinese medicine extract comprises ten kinds of licorice extract, clove extract, borneol, phellodendron extract, baical skullcap root extract, tea bran extract, oil seed extract, polygonum multiflorum extract, poria cocos extract and semen cuscutae extract; although the prepared shampoo has certain softening and nourishing effects, the shampoo has the defect of insufficient cleaning force, and for users with more oil, the shampoo can cause the problems of hair root dirt accumulation, scalp inflammation induction and the like after long-term use; in addition, the shampoo product has the defects of complex formula, complex preparation process, high preparation cost and the like. Based on the statement, the application provides the shampoo and the preparation method thereof, and aims to ensure the effects of cleaning, nourishing, repairing and the like of the shampoo, simplify the formula and the preparation process, reduce the preparation cost and promote the healthy development of the shampoo industry.
Disclosure of Invention
The application provides a shampoo and a preparation method thereof, aiming at solving the problems of poor cleaning, nourishing, repairing and other effects of the traditional shampoo, complex formula of the shampoo, complex preparation process, preparation cost and the like.
In a first aspect, the application provides a shampoo, which adopts the following technical scheme:
the shampoo comprises the following raw materials in parts by weight: 27-43 parts of adsorption type active components, 10-16 parts of surfactants, 3-8 parts of lipid components, 1-1.5 parts of organic acids and 40-50 parts of water;
the adsorption type active component consists of the following raw materials in parts by weight: 1-3 parts of zeolite powder, 5-12 parts of chitosan, 3-6 parts of algal polysaccharide, 1-3 parts of L-serine, 0.8-1.2 parts of panthenol and 30-50 parts of water.
Preferably, the shampoo comprises the following raw materials in parts by weight: 30-40 parts of adsorption type active component, 12-14 parts of surfactant, 4-6 parts of lipid component, 1.2-1.4 parts of organic acid and 42-48 parts of water.
Preferably, the shampoo comprises the following raw materials in parts by weight: 35 parts of adsorption type active component, 13 parts of surfactant, 5 parts of lipid component, 1.3 parts of organic acid and 45 parts of water.
By adopting the technical scheme, the hair-cleaning agent disclosed by the application is simple in formula and strict in proportion, and can be used for effectively cleaning hair and simultaneously nourishing and repairing scalp and hair through the combined action of the adsorption type active components and the surfactant; the addition of the lipid component in the formula can endow the shampoo with excellent sterilization, corrosion resistance, oxidation resistance and other functions, and further enhance the nourishing and repairing functions of the shampoo; the addition of the organic acid component can regulate the pH value of the shampoo, help restore the acid-base balance of the scalp, relieve the problems of dandruff, itching and the like, and further lead the hair to be more flexible and glossy.
The application adopts zeolite powder, chitosan, algal polysaccharide, L-serine, panthenol and water to prepare adsorption type active components together; in the hair washing process, the chitosan loaded with the active substances L-serine and panthenol can be coated on the surface of the hair to form a layer of protective film, so that the hair is sufficiently nourished and repaired, the hair is softer and smoother, the hair is easy to comb, and the phenomena of frizziness and bifurcation of the hair are reduced; the zeolite powder can not be directly adsorbed on the surface of hair, can effectively adsorb dirt and grease on the hair, is easy to wash by water, and does not need to use other hair care products again after the shampoo of the application is used for washing hair.
Preferably, the surfactant is a compound of alkyl polyglucoside, potassium cocoyl glycinate and cocamidopropyl betaine with the mass ratio of 3:0.5-0.7:0.1-0.3.
By adopting the technical scheme, the surfactant is prepared by mixing and compounding alkyl polyglucoside, potassium cocoyl glycinate and cocamidopropyl betaine, so that the surfactant can be used for preparing shampoo, the addition amount is reduced, and meanwhile, the strong cleaning capability is ensured, and the compound surfactant has mild performance, good biodegradability, good thickening performance and good compatibility with components in a shampoo formula; the finally prepared shampoo has excellent foaming performance, rich, fine and stable foam, is used for hair washing and caring, has good cleaning, foaming and conditioning effects, and can not cause excessive cleaning of scalp and hair.
Preferably, the lipid component comprises vitamin E, tea tree essential oil and kojic dipalmitate in a mass ratio of 10:3-5:1-2.
By adopting the technical scheme, the vitamin E has excellent oxidation resistance, can promote the regeneration of epithelial cells at scalp parts, quickly enter into hair cores, strengthen the elasticity of hair, improve the problems of fragile hair breakage and the like while improving the stability of shampoo; the tea tree essential oil has excellent sterilization and corrosion prevention effects, and can effectively remove dandruff, moisten cutin, dredge hair follicles, nourish hair roots, thereby achieving the effects of protecting and nourishing hair; kojic dipalmitate has the effects of antistatic, moisturizing, softening and the like, and can help stabilize the shampoo formula and prevent layering and deterioration; the three components are compounded and added as lipid components, so that the shampoo has good synergistic effect, the finally prepared shampoo has good stability, long shelf life, strong cleaning capability, high absorption and utilization rate of active ingredients and remarkable nourishing and repairing effects.
Preferably, the organic acid is citric acid and/or malic acid.
Preferably, the adsorption type active component consists of the following raw materials in parts by weight: 2 parts of zeolite powder, 8 parts of chitosan, 5 parts of algal polysaccharide, 2 parts of L-serine, 1 part of panthenol and 40 parts of water.
Preferably, the adsorbed active component is prepared by the following method:
(1) Weighing raw materials including zeolite powder, chitosan, algal polysaccharide, L-serine, panthenol and water in parts by weight for later use;
(2) Adding water into chitosan and algal polysaccharide, stirring and dissolving, and then adding L-serine and panthenol for continuous full dissolution to obtain a mixed solution A;
(3) Adding zeolite powder into the mixed solution A, and uniformly dispersing by ultrasonic vibration to obtain the required adsorption type active component.
By adopting the technical scheme, the adsorption type active component is prepared by zeolite powder, chitosan, algal polysaccharide, L-serine, panthenol and water together; wherein, the chitosan and the seaweed polysaccharide are natural polysaccharide substances, have the effects of moisturizing and nourishing hair, and the chitosan molecules have positive charges, and can be adsorbed on the hair surface to form a layer of protective film because the hair surface has negative charges, so that the effects of protecting hair, preventing dehydration and static electricity are achieved, and the chitosan also has the effects of mildly cleaning and softening hair, and the like; the seaweed polysaccharide is used as natural polysaccharide substance, has effects of moisturizing, nourishing and repairing hair, and can penetrate into hair, enhance hair elasticity and luster, and prevent hair from drying up and breaking; the chitosan and the seaweed polysaccharide have good antibacterial, antioxidant and biocompatibility, and the composite use of the chitosan and the seaweed polysaccharide has good synergistic effect, so that the nourishing and repairing effects of the shampoo can be improved, and the stability of active substances in the formula can be enhanced.
The L-serine has the effects of moisturizing, nourishing, repairing and the like, can enhance the nourishing effect of the shampoo, and improves the elasticity and glossiness of hair; the panthenol can balance the grease secretion of scalp, reduce dandruff and inflammation, help to improve hair health, strengthen hair strength and elasticity, and protect scalp and hair from dryness and damage; the chitosan and the seaweed polysaccharide are utilized to absorb the L-serine and the panthenol together, so that the moistening and repairing effects of the L-serine and the panthenol can be prolonged and enhanced, and the water content, the glossiness, the softness and the like of the hair are improved.
The zeolite powder is used as a natural adsorbent, has a large number of micropore structures and strong adsorption capacity, and can enhance the adsorptivity of chitosan and algal polysaccharide and improve the stability of chitosan and algal polysaccharide in water by adding the zeolite powder; in the hair washing process, the zeolite powder can release active components to act on hair, nourish and repair, and can adsorb dirt and grease washed out by the surfactant.
In a second aspect, the application provides a method for preparing shampoo, which adopts the following technical scheme:
the preparation method of the shampoo comprises the following preparation steps:
s1, weighing raw material adsorption type active components, a surfactant, a lipid component, organic acid and water according to parts by weight for later use;
s2, adding the surfactant and the lipid component into water, and uniformly stirring and mixing to obtain a premix;
s3, adding the adsorption type active components and the organic acid into the premix, stirring and mixing uniformly, and sub-packaging to obtain the required shampoo.
In summary, the application has the following beneficial effects:
the shampoo provided by the application has the advantages of simple formula design, simple preparation method and low preparation cost, and is suitable for industrial production; the shampoo disclosed by the application is used for washing and protecting hair, can effectively remove dirt and grease on the hair, is easy to rinse cleanly, and cannot cause excessive cleaning; meanwhile, the shampoo provided by the application has remarkable nourishing and repairing effects, can effectively improve hair quality, reduce hair damage, increase hair luster, promote hair growth and the like, ensures safe use and no side effect, is beneficial to meeting the needs of people on hair health and beauty, and promotes the healthy development of the hair washing and caring product industry.
Detailed Description
The present application will be described in further detail with reference to examples.
Preparation examples 1 to 3 and comparative preparation examples 1 to 6 provide a preparation method of the adsorption type active ingredient, and are specifically described below.
Preparation example 1
The adsorption type active component consists of the following raw materials: 1Kg of natural zeolite powder, 5Kg of chitosan, 3Kg of algal polysaccharide, 1Kg of L-serine, 0.8Kg of panthenol and 30Kg of water;
the adsorption type active component is prepared by the following method:
(1) Weighing raw materials of natural zeolite powder, chitosan, algal polysaccharide, L-serine, panthenol and water according to parts by weight for standby;
(2) Adding chitosan and algal polysaccharide into water at 50 ℃, stirring and dissolving for 20min at a rotating speed of 450r/min, cooling to 20 ℃, adding L-serine and panthenol, and continuously stirring for 20min until the mixture is fully dissolved to obtain a mixed solution A;
(3) Adding natural zeolite powder into the mixed solution A, controlling the ultrasonic vibration power to be 100W, and dispersing for 40min by ultrasonic vibration to obtain the required adsorption type active component;
the natural zeolite powder has a particle size of 500 meshes, the chitosan is carboxymethyl chitosan, and the seaweed polysaccharide (polysaccharide content is 30%).
Preparation example 2
The adsorption type active component consists of the following raw materials: 2Kg of natural zeolite powder, 8Kg of chitosan, 5Kg of algal polysaccharide, 2Kg of L-serine, 1Kg of panthenol and 40Kg of water;
the adsorption type active component is prepared by the following method:
(1) Weighing raw materials of natural zeolite powder, chitosan, algal polysaccharide, L-serine, panthenol and water according to parts by weight for standby;
(2) Adding chitosan and algal polysaccharide into water at 60 ℃, stirring and dissolving for 15min at a rotating speed of 500r/min, cooling to 27 ℃, adding L-serine and panthenol, and continuously stirring for 15min until the mixture is fully dissolved to obtain a mixed solution A;
(3) Adding natural zeolite powder into the mixed solution A, controlling the ultrasonic vibration power to be 110W, and dispersing for 30min by ultrasonic vibration to obtain the required adsorption type active component;
the natural zeolite powder has a particle size of 650 meshes, the chitosan is carboxymethyl chitosan, and the seaweed polysaccharide (the polysaccharide content is 30%).
Preparation example 3
The adsorption type active component consists of the following raw materials: 3Kg of natural zeolite powder, 12Kg of chitosan, 6Kg of algal polysaccharide, 3Kg of L-serine, 1.2Kg of panthenol and 50Kg of water;
the adsorption type active component is prepared by the following method:
(1) Weighing raw materials of natural zeolite powder, chitosan, algal polysaccharide, L-serine, panthenol and water according to parts by weight for standby;
(2) Adding chitosan and algal polysaccharide into 70 ℃ water, stirring and dissolving for 10min at a rotating speed of 550r/min, cooling to 34 ℃, adding L-serine and panthenol, and continuously stirring for 10min until the mixture is fully dissolved to obtain a mixed solution A;
(3) Adding natural zeolite powder into the mixed solution A, controlling the ultrasonic vibration power to be 120W, and dispersing for 20min by ultrasonic vibration to obtain the required adsorption type active component;
the natural zeolite powder has a particle size of 800 meshes, the chitosan is carboxymethyl chitosan, and the seaweed polysaccharide (polysaccharide content is 30%).
Comparative preparation example 1
The adsorption type active component consists of the following raw materials: 5Kg of chitosan, 3Kg of algal polysaccharide, 1Kg of L-serine, 0.8Kg of panthenol and 30Kg of water;
the adsorption type active component is prepared by the following method:
(1) Weighing raw materials of chitosan, algal polysaccharide, L-serine, panthenol and water according to parts by weight for standby;
(2) Adding chitosan and algal polysaccharide into water at 50 ℃, stirring and dissolving for 20min at a rotating speed of 450r/min, cooling to 20 ℃, adding L-serine and panthenol, and continuously stirring for 20min until the mixture is fully dissolved to obtain a mixed solution A;
(3) Controlling the ultrasonic vibration power to be 100W, and dispersing the mixed solution A for 40min by ultrasonic vibration to obtain the required adsorption type active component;
the chitosan is carboxymethyl chitosan, and algal polysaccharide (polysaccharide content is 30%).
Comparative preparation example 2
The adsorption type active component consists of the following raw materials: 4Kg of natural zeolite powder, 5Kg of chitosan, 3Kg of algal polysaccharide, 1Kg of L-serine, 0.8Kg of panthenol and 30Kg of water;
the adsorption type active component is prepared by the following method:
(1) Weighing raw materials of natural zeolite powder, chitosan, algal polysaccharide, L-serine, panthenol and water according to parts by weight for standby;
(2) Adding chitosan and algal polysaccharide into water at 50 ℃, stirring and dissolving for 20min at a rotating speed of 450r/min, cooling to 20 ℃, adding L-serine and panthenol, and continuously stirring for 20min until the mixture is fully dissolved to obtain a mixed solution A;
(3) Adding natural zeolite powder into the mixed solution A, controlling the ultrasonic vibration power to be 100W, and dispersing for 40min by ultrasonic vibration to obtain the required adsorption type active component;
the natural zeolite powder has a particle size of 500 meshes, the chitosan is carboxymethyl chitosan, and the seaweed polysaccharide (polysaccharide content is 30%).
Comparative preparation example 3
The adsorption type active component consists of the following raw materials: 1Kg of natural zeolite powder, 5Kg of chitosan, 3Kg of algal polysaccharide, 1Kg of L-serine, 0.8Kg of panthenol and 30Kg of water;
the adsorption type active component is prepared by the following method:
(1) Weighing raw materials of natural zeolite powder, chitosan, algal polysaccharide, L-serine, panthenol and water according to parts by weight for standby;
(2) Adding chitosan and algal polysaccharide into water at 50 ℃, stirring and dissolving for 20min at a rotating speed of 450r/min, cooling to 20 ℃, adding L-serine and panthenol, and continuously stirring for 20min until the mixture is fully dissolved to obtain a mixed solution A;
(3) Adding natural zeolite powder into the mixed solution A, controlling the ultrasonic vibration power to be 100W, and dispersing for 40min by ultrasonic vibration to obtain the required adsorption type active component;
the natural zeolite powder has a particle size of 1000 meshes, the chitosan is carboxymethyl chitosan, and the seaweed polysaccharide (polysaccharide content is 30%).
Comparative preparation example 4
The adsorption type active component consists of the following raw materials: 1Kg of natural zeolite powder, 5Kg of chitosan, 3Kg of algal polysaccharide, 1Kg of L-serine, 0.8Kg of panthenol and 30Kg of water;
the adsorption type active component is prepared by the following method:
(1) Weighing raw materials of natural zeolite powder, chitosan, algal polysaccharide, L-serine, panthenol and water according to parts by weight for standby;
(2) Adding chitosan and algal polysaccharide into water at 50 ℃, stirring and dissolving for 20min at a rotating speed of 450r/min, cooling to 20 ℃, adding L-serine and panthenol, and continuously stirring for 20min until the mixture is fully dissolved to obtain a mixed solution A;
(3) Adding natural zeolite powder into the mixed solution A, controlling the ultrasonic vibration power to be 100W, and dispersing for 40min by ultrasonic vibration to obtain the required adsorption type active component;
the particle size of the natural zeolite powder is 100 meshes, the chitosan is carboxymethyl chitosan, and the seaweed polysaccharide (the polysaccharide content is 30%).
Comparative preparation example 5
The adsorption type active component consists of the following raw materials: 1Kg of natural zeolite powder, 8Kg of chitosan, 1Kg of L-serine, 0.8Kg of panthenol and 30Kg of water;
the adsorption type active component is prepared by the following method:
(1) Weighing raw materials of natural zeolite powder, chitosan, L-serine, panthenol and water in parts by weight for later use;
(2) Adding chitosan into water at 50deg.C, stirring at 450r/min for dissolving for 20min, cooling to 20deg.C, adding L-serine and panthenol, and stirring for 20min to obtain mixed solution A;
(3) Adding natural zeolite powder into the mixed solution A, controlling the ultrasonic vibration power to be 100W, and dispersing for 40min by ultrasonic vibration to obtain the required adsorption type active component;
the particle size of the natural zeolite powder is 500 meshes, and the chitosan is carboxymethyl chitosan.
Comparative preparation example 6
The adsorption type active component consists of the following raw materials: 1Kg of natural zeolite powder, 8Kg of seaweed polysaccharide, 1Kg of L-serine, 0.8Kg of panthenol and 30Kg of water;
the adsorption type active component is prepared by the following method:
(1) Weighing raw materials of natural zeolite powder, algal polysaccharide, L-serine, panthenol and water in parts by weight for later use;
(2) Adding algal polysaccharide into water at 50 ℃, stirring and dissolving for 20min at a rotating speed of 450r/min, cooling to 20 ℃, adding L-serine and panthenol, and continuously stirring for 20min until the mixture is fully dissolved to obtain a mixed solution A;
(3) Adding natural zeolite powder into the mixed solution A, controlling the ultrasonic vibration power to be 100W, and dispersing for 40min by ultrasonic vibration to obtain the required adsorption type active component;
the particle size of the natural zeolite powder is 500 meshes, and the seaweed polysaccharide (polysaccharide content is 30%).
Examples 1-7 provide a shampoo and a preparation method thereof, and the following description is given.
Example 1
A shampoo comprises the following raw materials: 27Kg of adsorption type active component, 10Kg of surfactant, 3Kg of lipid component, 1Kg of organic acid and 40Kg of water;
wherein, the adsorption type active component is prepared in preparation example 1;
the surfactant is a compound of alkyl polyglucoside, potassium cocoyl glycinate and cocamidopropyl betaine with the mass ratio of 3:0.5:0.1;
the lipid component comprises vitamin E, tea tree essential oil and kojic dipalmitate in a mass ratio of 10:3:1;
the organic acid is citric acid.
The preparation method of the shampoo comprises the following preparation steps:
s1, weighing raw material adsorption type active components, a surfactant, a lipid component, organic acid and water according to parts by weight for later use;
s2, adding the surfactant and the lipid component into 65 ℃ water, and stirring and mixing for 50min at a rotating speed of 100r/min to obtain a premix;
and S3, cooling the premix to 20 ℃, adding the adsorption type active component and the organic acid, continuously stirring and mixing for 40min until the mixture is uniform, and sub-packaging to obtain the required shampoo.
Example 2
A shampoo comprises the following raw materials: 35Kg of adsorption type active component, 13Kg of surfactant, 5Kg of lipid component, 1.3Kg of organic acid and 45Kg of water;
wherein the adsorption type active component is prepared in preparation example 2;
the surfactant is a compound of alkyl polyglucoside, potassium cocoyl glycinate and cocamidopropyl betaine with the mass ratio of 3:0.6:0.2;
the lipid component comprises vitamin E, tea tree essential oil and kojic dipalmitate in a mass ratio of 10:4:1.5;
the organic acid is mixed acid of citric acid and malic acid in the mass ratio of 1:1.
The preparation method of the shampoo comprises the following preparation steps:
s1, weighing raw material adsorption type active components, a surfactant, a lipid component, organic acid and water according to parts by weight for later use;
s2, adding the surfactant and the lipid component into water at 72 ℃, and stirring and mixing for 40min at the rotating speed of 130r/min to obtain a premix;
s3, cooling the premix to 30 ℃, adding the adsorption type active component and the organic acid, continuously stirring and mixing for 30min until the mixture is uniform, and sub-packaging to obtain the required shampoo.
Example 3
A shampoo comprises the following raw materials: 43Kg of adsorption type active component, 16Kg of surfactant, 8Kg of lipid component, 1.5Kg of organic acid and 50Kg of water;
wherein the adsorption type active component is prepared in preparation example 3;
the surfactant is a compound of alkyl polyglucoside, potassium cocoyl glycinate and cocamidopropyl betaine with the mass ratio of 3:0.7:0.3;
the lipid component comprises vitamin E, tea tree essential oil and kojic dipalmitate in a mass ratio of 10:5:2;
the organic acid is citric acid and/or malic acid.
The preparation method of the shampoo comprises the following preparation steps:
s1, weighing raw material adsorption type active components, a surfactant, a lipid component, organic acid and water according to parts by weight for later use;
s2, adding the surfactant and the lipid component into water at 80 ℃, and stirring and mixing for 30min at a rotating speed of 150r/min to obtain a premix;
and S3, cooling the premix to 40 ℃, adding the adsorption type active component and the organic acid, continuously stirring and mixing for 20min until the mixture is uniform, and sub-packaging to obtain the required shampoo.
Example 4
A shampoo comprises the following raw materials: 27Kg of adsorption type active component, 10Kg of surfactant, 3Kg of lipid component, 1Kg of organic acid and 40Kg of water;
wherein the adsorption type active component is prepared in preparation example 2;
the surfactant is a compound of alkyl polyglucoside, potassium cocoyl glycinate and cocamidopropyl betaine with the mass ratio of 3:0.5:0.1;
the lipid component comprises vitamin E, tea tree essential oil and kojic dipalmitate in a mass ratio of 10:3:1;
the organic acid is citric acid.
The preparation method of the shampoo comprises the following preparation steps:
s1, weighing raw material adsorption type active components, a surfactant, a lipid component, organic acid and water according to parts by weight for later use;
s2, adding the surfactant and the lipid component into 65 ℃ water, and stirring and mixing for 50min at a rotating speed of 100r/min to obtain a premix;
and S3, cooling the premix to 20 ℃, adding the adsorption type active component and the organic acid, continuously stirring and mixing for 40min until the mixture is uniform, and sub-packaging to obtain the required shampoo.
Example 5
A shampoo comprises the following raw materials: 27Kg of adsorption type active component, 10Kg of surfactant, 3Kg of lipid component, 1Kg of organic acid and 40Kg of water;
wherein the adsorption type active component is prepared in preparation example 3;
the surfactant is a compound of alkyl polyglucoside, potassium cocoyl glycinate and cocamidopropyl betaine with the mass ratio of 3:0.5:0.1;
the lipid component comprises vitamin E, tea tree essential oil and kojic dipalmitate in a mass ratio of 10:3:1;
the organic acid is citric acid.
The preparation method of the shampoo comprises the following preparation steps:
s1, weighing raw material adsorption type active components, a surfactant, a lipid component, organic acid and water according to parts by weight for later use;
s2, adding the surfactant and the lipid component into 65 ℃ water, and stirring and mixing for 50min at a rotating speed of 100r/min to obtain a premix;
and S3, cooling the premix to 20 ℃, adding the adsorption type active component and the organic acid, continuously stirring and mixing for 40min until the mixture is uniform, and sub-packaging to obtain the required shampoo.
Example 6
A shampoo comprises the following raw materials: 27Kg of adsorption type active component, 10Kg of surfactant, 3Kg of lipid component, 1Kg of organic acid and 40Kg of water;
wherein, the adsorption type active component is prepared in preparation example 1;
the surfactant is a compound of alkyl polyglucoside, potassium cocoyl glycinate and cocamidopropyl betaine with the mass ratio of 3:0.6:0.2;
the lipid component comprises vitamin E, tea tree essential oil and kojic dipalmitate in a mass ratio of 10:3:1;
the organic acid is citric acid.
The preparation method of the shampoo comprises the following preparation steps:
s1, weighing raw material adsorption type active components, a surfactant, a lipid component, organic acid and water according to parts by weight for later use;
s2, adding the surfactant and the lipid component into 65 ℃ water, and stirring and mixing for 50min at a rotating speed of 100r/min to obtain a premix;
and S3, cooling the premix to 20 ℃, adding the adsorption type active component and the organic acid, continuously stirring and mixing for 40min until the mixture is uniform, and sub-packaging to obtain the required shampoo.
Example 7
A shampoo comprises the following raw materials: 27Kg of adsorption type active component, 10Kg of surfactant, 3Kg of lipid component, 1Kg of organic acid and 40Kg of water;
wherein, the adsorption type active component is prepared in preparation example 1;
the surfactant is a compound of alkyl polyglucoside, potassium cocoyl glycinate and cocamidopropyl betaine with the mass ratio of 3:0.7:0.3;
the lipid component comprises vitamin E, tea tree essential oil and kojic dipalmitate in a mass ratio of 10:3:1;
the organic acid is citric acid.
The preparation method of the shampoo comprises the following preparation steps:
s1, weighing raw material adsorption type active components, a surfactant, a lipid component, organic acid and water according to parts by weight for later use;
s2, adding the surfactant and the lipid component into 65 ℃ water, and stirring and mixing for 50min at a rotating speed of 100r/min to obtain a premix;
and S3, cooling the premix to 20 ℃, adding the adsorption type active component and the organic acid, continuously stirring and mixing for 40min until the mixture is uniform, and sub-packaging to obtain the required shampoo.
To verify the cleaning, nourishing and repairing properties of the shampoos prepared in examples 1-7 of the present application, the applicant set comparative examples 1-11, in particular as follows:
comparative example 1
A shampoo comprises the following raw materials: 27Kg of adsorption type active component, 10Kg of surfactant, 3Kg of lipid component, 1Kg of organic acid and 40Kg of water;
wherein the adsorption type active component is prepared in comparative preparation example 1;
the surfactant is a compound of alkyl polyglucoside, potassium cocoyl glycinate and cocamidopropyl betaine with the mass ratio of 3:0.5:0.1;
the lipid component comprises vitamin E, tea tree essential oil and kojic dipalmitate in a mass ratio of 10:3:1;
the organic acid is citric acid.
The preparation method of the shampoo comprises the following preparation steps:
s1, weighing raw material adsorption type active components, a surfactant, a lipid component, organic acid and water according to parts by weight for later use;
s2, adding the surfactant and the lipid component into 65 ℃ water, and stirring and mixing for 50min at a rotating speed of 100r/min to obtain a premix;
and S3, cooling the premix to 20 ℃, adding the adsorption type active component and the organic acid, continuously stirring and mixing for 40min until the mixture is uniform, and sub-packaging to obtain the required shampoo.
Comparative example 2
A shampoo comprises the following raw materials: 27Kg of adsorption type active component, 10Kg of surfactant, 3Kg of lipid component, 1Kg of organic acid and 40Kg of water;
wherein the adsorption type active component is prepared in comparative preparation example 2;
the surfactant is a compound of alkyl polyglucoside, potassium cocoyl glycinate and cocamidopropyl betaine with the mass ratio of 3:0.5:0.1;
the lipid component comprises vitamin E, tea tree essential oil and kojic dipalmitate in a mass ratio of 10:3:1;
the organic acid is citric acid.
The preparation method of the shampoo comprises the following preparation steps:
s1, weighing raw material adsorption type active components, a surfactant, a lipid component, organic acid and water according to parts by weight for later use;
s2, adding the surfactant and the lipid component into 65 ℃ water, and stirring and mixing for 50min at a rotating speed of 100r/min to obtain a premix;
and S3, cooling the premix to 20 ℃, adding the adsorption type active component and the organic acid, continuously stirring and mixing for 40min until the mixture is uniform, and sub-packaging to obtain the required shampoo.
Comparative example 3
A shampoo comprises the following raw materials: 27Kg of adsorption type active component, 10Kg of surfactant, 3Kg of lipid component, 1Kg of organic acid and 40Kg of water;
wherein the adsorption type active ingredient is prepared in comparative preparation example 3;
the surfactant is a compound of alkyl polyglucoside, potassium cocoyl glycinate and cocamidopropyl betaine with the mass ratio of 3:0.5:0.1;
the lipid component comprises vitamin E, tea tree essential oil and kojic dipalmitate in a mass ratio of 10:3:1;
the organic acid is citric acid.
The preparation method of the shampoo comprises the following preparation steps:
s1, weighing raw material adsorption type active components, a surfactant, a lipid component, organic acid and water according to parts by weight for later use;
s2, adding the surfactant and the lipid component into 65 ℃ water, and stirring and mixing for 50min at a rotating speed of 100r/min to obtain a premix;
and S3, cooling the premix to 20 ℃, adding the adsorption type active component and the organic acid, continuously stirring and mixing for 40min until the mixture is uniform, and sub-packaging to obtain the required shampoo.
Comparative example 4
A shampoo comprises the following raw materials: 27Kg of adsorption type active component, 10Kg of surfactant, 3Kg of lipid component, 1Kg of organic acid and 40Kg of water;
wherein the adsorption type active ingredient is prepared in comparative preparation example 4;
the surfactant is a compound of alkyl polyglucoside, potassium cocoyl glycinate and cocamidopropyl betaine with the mass ratio of 3:0.5:0.1;
the lipid component comprises vitamin E, tea tree essential oil and kojic dipalmitate in a mass ratio of 10:3:1;
the organic acid is citric acid.
The preparation method of the shampoo comprises the following preparation steps:
s1, weighing raw material adsorption type active components, a surfactant, a lipid component, organic acid and water according to parts by weight for later use;
s2, adding the surfactant and the lipid component into 65 ℃ water, and stirring and mixing for 50min at a rotating speed of 100r/min to obtain a premix;
and S3, cooling the premix to 20 ℃, adding the adsorption type active component and the organic acid, continuously stirring and mixing for 40min until the mixture is uniform, and sub-packaging to obtain the required shampoo.
Comparative example 5
A shampoo comprises the following raw materials: 27Kg of adsorption type active component, 10Kg of surfactant, 3Kg of lipid component, 1Kg of organic acid and 40Kg of water;
wherein the adsorption type active component is prepared in comparative preparation example 5;
the surfactant is a compound of alkyl polyglucoside, potassium cocoyl glycinate and cocamidopropyl betaine with the mass ratio of 3:0.5:0.1;
the lipid component comprises vitamin E, tea tree essential oil and kojic dipalmitate in a mass ratio of 10:3:1;
the organic acid is citric acid.
The preparation method of the shampoo comprises the following preparation steps:
s1, weighing raw material adsorption type active components, a surfactant, a lipid component, organic acid and water according to parts by weight for later use;
s2, adding the surfactant and the lipid component into 65 ℃ water, and stirring and mixing for 50min at a rotating speed of 100r/min to obtain a premix;
and S3, cooling the premix to 20 ℃, adding the adsorption type active component and the organic acid, continuously stirring and mixing for 40min until the mixture is uniform, and sub-packaging to obtain the required shampoo.
Comparative example 6
A shampoo comprises the following raw materials: 27Kg of adsorption type active component, 10Kg of surfactant, 3Kg of lipid component, 1Kg of organic acid and 40Kg of water;
wherein the adsorption type active ingredient is prepared in comparative preparation example 6;
the surfactant is a compound of alkyl polyglucoside, potassium cocoyl glycinate and cocamidopropyl betaine with the mass ratio of 3:0.5:0.1;
the lipid component comprises vitamin E, tea tree essential oil and kojic dipalmitate in a mass ratio of 10:3:1;
the organic acid is citric acid.
The preparation method of the shampoo comprises the following preparation steps:
s1, weighing raw material adsorption type active components, a surfactant, a lipid component, organic acid and water according to parts by weight for later use;
s2, adding the surfactant and the lipid component into 65 ℃ water, and stirring and mixing for 50min at a rotating speed of 100r/min to obtain a premix;
and S3, cooling the premix to 20 ℃, adding the adsorption type active component and the organic acid, continuously stirring and mixing for 40min until the mixture is uniform, and sub-packaging to obtain the required shampoo.
Comparative example 7
A shampoo comprises the following raw materials: 27Kg of adsorption type active component, 10Kg of surfactant, 3Kg of lipid component, 1Kg of organic acid and 40Kg of water;
wherein, the adsorption type active component is prepared in preparation example 1;
the surfactant is a compound of alkyl polyglucoside and potassium cocoyl glycinate with the mass ratio of 3:0.6;
the lipid component comprises vitamin E, tea tree essential oil and kojic dipalmitate in a mass ratio of 10:3:1;
the organic acid is citric acid.
The preparation method of the shampoo comprises the following preparation steps:
s1, weighing raw material adsorption type active components, a surfactant, a lipid component, organic acid and water according to parts by weight for later use;
s2, adding the surfactant and the lipid component into 65 ℃ water, and stirring and mixing for 50min at a rotating speed of 100r/min to obtain a premix;
and S3, cooling the premix to 20 ℃, adding the adsorption type active component and the organic acid, continuously stirring and mixing for 40min until the mixture is uniform, and sub-packaging to obtain the required shampoo.
Comparative example 8
A shampoo comprises the following raw materials: 27Kg of adsorption type active component, 10Kg of surfactant, 3Kg of lipid component, 1Kg of organic acid and 40Kg of water;
wherein, the adsorption type active component is prepared in preparation example 1;
the surfactant is a compound of alkyl polyglucoside and cocamidopropyl betaine with the mass ratio of 3:0.6;
the lipid component comprises vitamin E, tea tree essential oil and kojic dipalmitate in a mass ratio of 10:3:1;
the organic acid is citric acid.
The preparation method of the shampoo comprises the following preparation steps:
s1, weighing raw material adsorption type active components, a surfactant, a lipid component, organic acid and water according to parts by weight for later use;
s2, adding the surfactant and the lipid component into 65 ℃ water, and stirring and mixing for 50min at a rotating speed of 100r/min to obtain a premix;
and S3, cooling the premix to 20 ℃, adding the adsorption type active component and the organic acid, continuously stirring and mixing for 40min until the mixture is uniform, and sub-packaging to obtain the required shampoo.
Comparative example 9
A shampoo comprises the following raw materials: 27Kg of adsorption type active component, 10Kg of surfactant, 3Kg of lipid component, 1Kg of organic acid and 40Kg of water;
wherein, the adsorption type active component is prepared in preparation example 1;
the surfactant is alkyl polyglucoside;
the lipid component comprises vitamin E, tea tree essential oil and kojic dipalmitate in a mass ratio of 10:3:1;
the organic acid is citric acid.
The preparation method of the shampoo comprises the following preparation steps:
s1, weighing raw material adsorption type active components, a surfactant, a lipid component, organic acid and water according to parts by weight for later use;
s2, adding the surfactant and the lipid component into 65 ℃ water, and stirring and mixing for 50min at a rotating speed of 100r/min to obtain a premix;
and S3, cooling the premix to 20 ℃, adding the adsorption type active component and the organic acid, continuously stirring and mixing for 40min until the mixture is uniform, and sub-packaging to obtain the required shampoo.
Comparative example 10
A shampoo comprises the following raw materials: 27Kg of adsorption type active component, 10Kg of surfactant, 3Kg of lipid component, 1Kg of organic acid and 40Kg of water;
wherein, the adsorption type active component is prepared in preparation example 1;
the surfactant is a compound of alkyl polyglucoside, potassium cocoyl glycinate and cocamidopropyl betaine with the mass ratio of 3:0.5:0.1;
the lipid component comprises vitamin E and tea tree essential oil in a mass ratio of 10:4;
the organic acid is citric acid.
The preparation method of the shampoo comprises the following preparation steps:
s1, weighing raw material adsorption type active components, a surfactant, a lipid component, organic acid and water according to parts by weight for later use;
s2, adding the surfactant and the lipid component into 65 ℃ water, and stirring and mixing for 50min at a rotating speed of 100r/min to obtain a premix;
and S3, cooling the premix to 20 ℃, adding the adsorption type active component and the organic acid, continuously stirring and mixing for 40min until the mixture is uniform, and sub-packaging to obtain the required shampoo.
Comparative example 11
A shampoo comprises the following raw materials: 27Kg of adsorption type active component, 10Kg of surfactant, 3Kg of lipid component, 1Kg of organic acid and 40Kg of water;
wherein, the adsorption type active component is prepared in preparation example 1;
the surfactant is a compound of alkyl polyglucoside, potassium cocoyl glycinate and cocamidopropyl betaine with the mass ratio of 3:0.5:0.1;
the lipid component comprises vitamin E and kojic dipalmitate in a mass ratio of 10:4;
the organic acid is citric acid.
The preparation method of the shampoo comprises the following preparation steps:
s1, weighing raw material adsorption type active components, a surfactant, a lipid component, organic acid and water according to parts by weight for later use;
s2, adding the surfactant and the lipid component into 65 ℃ water, and stirring and mixing for 50min at a rotating speed of 100r/min to obtain a premix;
and S3, cooling the premix to 20 ℃, adding the adsorption type active component and the organic acid, continuously stirring and mixing for 40min until the mixture is uniform, and sub-packaging to obtain the required shampoo.
Performance testing
Shampoo compositions of examples 1-7 and comparative examples 1-11 of the present application were tested for cleaning and conditioning efficacy, respectively, as follows:
1. safety evaluation
The shampoos prepared in examples 1-7 and comparative examples 1-11 of the present application were subjected to a plurality of acute skin irritation tests and a plurality of eye irritation tests, respectively, and the results showed no irritation reaction, indicating that the shampoo formulation of the present application is safe and has no irritation and no side effects.
2. Cleaning effect detection
1. Test design
Randomly selecting 180 long-hair female volunteers with similar hair length (shoulder alignment) and similar hair quality, wherein the ages of the volunteers are 25-50 years, and each volunteer has the phenomena of dry hair, easy breakage, excessive dandruff, alopecia and the like; randomly dividing 180 volunteers into 18 groups, and respectively using 10 persons in each group, wherein the shampoo in the examples 1-7 and the comparative examples 1-11 is used for cleaning every three days, specifically, the shampoo is squeezed to dry the hair, the shampoo is squeezed out, 2 pumps are used for kneading foam, the foam is uniformly coated on the wet hair for 5 minutes, meanwhile, the scalp is massaged, then the shampoo is washed for 3 minutes by running water, and the hair drier is used for drying after the water is squeezed; (in order to ensure the authenticity of the test effect of the shampoo as much as possible, in the test process, the water temperature and the shampoo time in the shampoo process are ensured to be the same, and meanwhile, the blowing temperature and the blowing time of the blower are ensured to be the same).
2. Cleaning and repairing effect detection
Before hair is cleaned for the first time and hair is cleaned for the 10 th time, the face oil absorbing paper with the size of 3cm multiplied by 3cm is lightly pressed on the hair for 3 times, the oil absorbing area ratio (%) of oil stains on the oil absorbing paper is observed and recorded, and the average value of the oil absorbing area ratio obtained by detection of 10 persons of the same group of volunteers is calculated;
before hair is cleaned for the first time and hair is cleaned for the 10 th time, combing from the top of the hair to the tail of the hair by using a comb for 5 times at different positions, observing and recording the smooth condition (knotting times) of the hair and the hair dropping condition (root), and calculating 10 persons of the same group of volunteers;
after the hair is cleaned for the first time and the hair is cleaned for the 10 th time respectively, observing whether residual dandruff or other pollutants exist on the hair and the scalp after blow-drying, taking down and collecting the residual dandruff or the pollutants if the residual dandruff or the pollutants exist, weighing, and calculating the average value of the residual dandruff and the residual pollutant quantity (mg) of 10 persons of the same group of volunteers;
the specific test results are shown in table 1 below:
table 1:
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as can be seen from the data shown in table 1: compared with comparative examples 1-11, the shampoo prepared in examples 1-7 has more remarkable cleaning effect, and the scalp and hair after washing are fresh and clean without residues, and also has the effects of moistening and softening hair, and the hair after washing is knotted and has obviously reduced hair loss, and the nourishing and repairing effects are more remarkable.
Comparative example 2 compared with example 1, the use amount of zeolite powder is increased, and comparative example 4 compared with example 1, the particle size of zeolite powder is increased, and although the effect of the shampoo obtained by the formula is not obvious, the shampoo is easy to precipitate, delaminate and the like in the storage process; comparative example 10 compared with example 1, the addition of kojic dipalmitate is reduced, and the shampoo performance is reduced, and meanwhile, the phenomena of precipitation, delamination and the like are easy to occur in the storage process of the shampoo.
The present embodiment is only for explanation of the present application and is not to be construed as limiting the present application, and modifications to the present embodiment, which may not creatively contribute to the present application as required by those skilled in the art after reading the present specification, are all protected by patent laws within the scope of claims of the present application.
Claims (6)
1. The shampoo is characterized by comprising the following raw materials in parts by weight: 27-43 parts of adsorption type active components, 10-16 parts of surfactants, 3-8 parts of lipid components, 1-1.5 parts of organic acids and 40-50 parts of water;
the adsorption type active component consists of the following raw materials in parts by weight: 1-3 parts of zeolite powder, 5-12 parts of chitosan, 3-6 parts of algal polysaccharide, 1-3 parts of L-serine, 0.8-1.2 parts of panthenol and 30-50 parts of water;
the surfactant is a compound of alkyl polyglucoside, potassium cocoyl glycinate and cocamidopropyl betaine with the mass ratio of 3:0.5-0.7:0.1-0.3;
the lipid component comprises vitamin E, tea tree essential oil and kojic dipalmitate in a mass ratio of 10:3-5:1-2;
the organic acid is citric acid and/or malic acid;
the zeolite powder particle size is 500 meshes, 650 meshes or 800 meshes.
2. The shampoo according to claim 1, which is characterized by comprising the following raw materials in parts by weight: 30-40 parts of adsorption type active component, 12-14 parts of surfactant, 4-6 parts of lipid component, 1.2-1.4 parts of organic acid and 42-48 parts of water.
3. The shampoo according to claim 1, which is characterized by comprising the following raw materials in parts by weight: 35 parts of adsorption type active component, 13 parts of surfactant, 5 parts of lipid component, 1.3 parts of organic acid and 45 parts of water.
4. The shampoo according to claim 1, wherein the adsorption-type active component comprises the following raw materials in parts by weight: 2 parts of zeolite powder, 8 parts of chitosan, 5 parts of algal polysaccharide, 2 parts of L-serine, 1 part of panthenol and 40 parts of water.
5. The shampoo of claim 1, wherein the adsorptive active component is prepared by the following method:
(1) Weighing the raw materials of zeolite powder, chitosan, algal polysaccharide, and the like according to parts by weight,
L-serine, panthenol and water for standby;
(2) Adding water into chitosan and algal polysaccharide, stirring and dissolving, and then adding L-serine and panthenol for continuous full dissolution to obtain a mixed solution A;
(3) Adding zeolite powder into the mixed solution A, and uniformly dispersing by ultrasonic vibration to obtain the required adsorption type active component.
6. A method for preparing a shampoo according to any one of claims 1-5, comprising the following steps:
s1, weighing raw material adsorption type active components, a surfactant, a lipid component, organic acid and water according to parts by weight for later use;
s2, adding the surfactant and the lipid component into water, and uniformly stirring and mixing to obtain a premix;
s3, adding the adsorption type active components and the organic acid into the premix, stirring and mixing uniformly, and sub-packaging to obtain the required shampoo.
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1665916A (en) * | 2002-06-25 | 2005-09-07 | 株式会社资生堂 | Detergent composition |
| KR102231747B1 (en) * | 2019-10-16 | 2021-03-24 | 대경대학교 산학협력단 | Complementary Color Shampoo Composition and Manufacturing Method thereof |
| CN113398037A (en) * | 2021-07-23 | 2021-09-17 | 广州澳乐健康产业有限公司 | Wash-free mousse capable of improving hair refreshing feeling and fluffy feeling |
| CN115737492A (en) * | 2022-08-08 | 2023-03-07 | 上海若梵生物科技有限公司 | Anti-hair loss hair-fixing product and preparation method thereof |
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Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1665916A (en) * | 2002-06-25 | 2005-09-07 | 株式会社资生堂 | Detergent composition |
| KR102231747B1 (en) * | 2019-10-16 | 2021-03-24 | 대경대학교 산학협력단 | Complementary Color Shampoo Composition and Manufacturing Method thereof |
| CN113398037A (en) * | 2021-07-23 | 2021-09-17 | 广州澳乐健康产业有限公司 | Wash-free mousse capable of improving hair refreshing feeling and fluffy feeling |
| CN115737492A (en) * | 2022-08-08 | 2023-03-07 | 上海若梵生物科技有限公司 | Anti-hair loss hair-fixing product and preparation method thereof |
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