CN112107494A - Facial mask essence - Google Patents

Facial mask essence Download PDF

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Publication number
CN112107494A
CN112107494A CN202010887579.3A CN202010887579A CN112107494A CN 112107494 A CN112107494 A CN 112107494A CN 202010887579 A CN202010887579 A CN 202010887579A CN 112107494 A CN112107494 A CN 112107494A
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parts
polysaccharide
mask essence
weight
skin
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张永梅
许兰英
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/4906—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom
    • A61K8/4913—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom having five membered rings, e.g. pyrrolidone carboxylic acid
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A61K8/26—Aluminium; Compounds thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34—Alcohols
    • A61K8/345—Alcohols containing more than one hydroxy group
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
    • A61K8/4946—Imidazoles or their condensed derivatives, e.g. benzimidazoles
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/67—Vitamins
    • A61K8/673—Vitamin B group
    • A61K8/675—Vitamin B3 or vitamin B3 active, e.g. nicotinamide, nicotinic acid, nicotinyl aldehyde
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73—Polysaccharides
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73—Polysaccharides
    • A61K8/733—Alginic acid; Salts thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73—Polysaccharides
    • A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • A—HUMAN NECESSITIES
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    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783—Angiosperms [Magnoliophyta]
    • A61K8/9794—Liliopsida [monocotyledons]
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59—Mixtures
    • A61K2800/592—Mixtures of compounds complementing their respective functions
    • A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18

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  • Oil, Petroleum & Natural Gas (AREA)
  • Emergency Medicine (AREA)
  • Cosmetics (AREA)

Abstract

The invention relates to the technical field of cosmetics, and in particular relates to a mask essence which comprises the following components in parts by weight: 0.05-0.2 part of activated carbon, 0.05-0.8 part of graphene water solution, 0.05-0.8 part of skin repair agent, 0.1-0.8 part of nicotinamide, 0.02-0.8 part of natural polysaccharide, 0.3-1.5 parts of transdermal peptide EFG, 0.2-3 parts of allantoin, 0.1-2.8 parts of sodium alginate, 0.3-2.5 parts of plant essential oil, 1-10 parts of sodium hyaluronate, 2-15 parts of modified zeolite, 1-5 parts of rice washing water fermentation liquor and 1-20 parts of glycerol. The facial mask essence provided by the invention can clean the skin, improve the absorption efficiency of the skin on active ingredients, play the role of the active ingredients to the maximum extent, reduce the volatilization of water on the surface layer of the skin and play a good moisturizing role.

Description

Facial mask essence
Technical Field
The invention relates to the technical field of cosmetics, and particularly relates to a facial mask essence.
Background
In modern society, the temperature change and pressure caused by air conditioning, environmental pollution and season change, skin aging, metabolism slowing and other factors can cause skin moisture loss, so that the skin is rough, dull, dry and wrinkled, and various skin problems are caused. Skin problems caused by water deficit are by no means as simple as dryness, and almost every skin problem is associated with moisture replenishment and maintenance. Moisture is the first essential factor for beautifying skin, and whitening, sun protection, oil control and the like are all completed on the basis of moisturizing. Skin problems of any season, age, skin type are perfect in water soothing and moisturizing. Therefore, the moisturizing work of the skin is very important.
The facial mask is a special cosmetic, and is applied on facial skin to form a film to isolate skin from the outside, and the effective components in the facial mask can permeate into skin to moisten skin, increase nutrition, and promote skin skill and metabolism, so that the facial skin is white, soft, comfortable, and youthful. The mask has the functions of nourishing and cleaning skin, is considered as a first aid expert of the skin, and can provide the most sufficient nutrients for the skin in the shortest time to recover the vitality of the skin. The skin care mask is periodically adhered to make the skin more delicate and smooth, and can effectively reduce wrinkles and slow down aging.
However, most of the existing moisturizing masks adopt synthetic/semisynthetic moisturizers, but in an environment with low humidity, the moisturizers can absorb moisture from the surface of the skin, so that the phenomenon of skin water shortage is more serious.
Disclosure of Invention
The invention aims to overcome the problems in the prior art and provide the mask essence with good moisturizing effect.
In order to achieve the above objects, the present invention provides, in one aspect, a mask essence comprising: 0.05-0.2 part of activated carbon, 0.05-0.8 part of graphene water solution, 0.05-0.8 part of skin repair agent, 0.1-0.8 part of nicotinamide, 0.02-0.8 part of natural polysaccharide, 0.3-1.5 parts of transdermal peptide EFG, 0.2-3 parts of allantoin, 0.1-2.8 parts of sodium alginate, 0.3-2.5 parts of plant essential oil, 1-10 parts of sodium hyaluronate, 2-15 parts of modified zeolite, 1-5 parts of rice washing water fermentation liquor and 1-20 parts of glycerol.
According to the facial mask essence, the natural polysaccharide has a dynamic moisturizing effect, the hyaluronic acid has an excellent moisturizing effect, the active substances can be fully absorbed by the skin, the skin repairing agent can repair damaged skin, the graphene can form a film layer on the surface of the skin and plays a role in isolating air oxidation for the skin, so that the active ingredients in the facial mask essence can be absorbed by the skin to the maximum extent, the absorption efficiency of the skin on the active ingredients is improved, the effect of the active ingredients is exerted to the maximum extent, the volatilization of water on the surface layer of the skin can be reduced, and a good moisturizing effect is achieved.
In order to further optimize the moisturizing effect of the mask essence, the mask essence comprises the following components under the optimal conditions: 0.1-0.15 part of activated carbon, 0.1-0.5 part of graphene water solution, 0.1-0.6 part of skin repair agent, 0.2-0.5 part of nicotinamide, 0.1-0.5 part of natural polysaccharide, 0.8-1.2 parts of transdermal peptide EFG, 0.6-2.2 parts of allantoin, 0.2-2.3 parts of sodium alginate, 0.5-2 parts of plant essential oil, 3-8 parts of sodium hyaluronate, 3-10 parts of modified zeolite, 1-5 parts of rice washing water fermentation liquor and 3-18 parts of glycerol.
In a preferred embodiment of the present invention, the method for preparing the rice-washing water fermentation broth comprises: washing 1kg of rice with water, soaking in 5L of water, adding 30-50g of pericarpium Citri Tangerinae, fermenting at 30-50 deg.C for 10-30 days, and collecting supernatant.
According to the invention, the zeolite in the mask liquid is mixed with water after adsorbing a large amount of alcohol solvent to release heat, and the released heat can heat the mask essence, so that skin pores can be opened while the mask is applied, the absorption of skin to active substances is promoted, and the efficacy of the mask is improved. In order to control the heat release speed of the zeolite, avoid too slow heat release to play a role in heating or too fast heat release, which results in short heating time and damage to skin, the zeolite is preferably modified, and the modification method of the zeolite comprises the following steps:
performing first acid treatment on zeolite powder in a first acid solution to obtain an acidified product, performing ultrasonic dispersion on the acidified product and a crown ether reagent for 30-60min, performing microwave reaction for 1-3min, and performing second acid treatment on the acidified product in a second acid solution to obtain modified zeolite.
Preferably, the crown ether reagent is at least one selected from aminobenzo-15-crown ether-5, aminobenzo-18-crown ether-6, aminobenzo-21-crown ether-7, aminobenzo-24-crown ether-8, aminoholothia-15-crown ether-5, aminoholothia-18-crown ether-6 and aminobenzothiacrown ether.
Under the preferable conditions, the power of the ultrasonic dispersion is 300-500W, and the power of the microwave reaction is 400-600W.
The second acid treatment step is as follows: dispersing the microwave reaction product in a second acidic solution, and activating at 80-100 ℃ for 3-8h, wherein the second acidic solution is at least two of salicylic acid, lauric acid, myristic acid and palmitic acid.
The zeolite powder is subjected to first acidification, so that impurities in gaps of the zeolite can be removed, the pore diameter and the specific surface area of the zeolite are increased, the zeolite is reacted with a crown ether reagent and subjected to microwave reaction, active groups are introduced into the gaps of the zeolite, the active groups can have good affinity with water, alcohol substances in the gaps can be replaced by water when the active groups are contacted with the water, the zeolite can release heat for a long time, in addition, the zeolite is subjected to secondary acid treatment, small molecular acid can be introduced into the surface of the zeolite, when the mask is applied to a face, the skin can be sufficiently cleaned, and at the moment, active carbon in mask essence can adsorb generated dirt.
More preferably, the zeolite powder has a particle size of 20 to 100 μm, and more preferably 30 to 60 μm.
According to the invention, the graphene can kill bacteria on the surface of the skin, accelerate metabolism of the skin and promote absorption of active ingredients by the skin, if the concentration of the graphene is too low, the graphene cannot achieve an ideal effect, and if the concentration of the graphene is too high, on one hand, the graphene self generates a agglomeration phenomenon, on the other hand, the graphene can adsorb other active ingredients in the mask, so that the efficacy of the mask is reduced, and under the preferable condition, the concentration of the graphene is 5-16 mg/L.
According to the invention, the natural polysaccharide has good biological activity and can play a role in repairing, replenishing water and brightening skin, and under the preferable condition, the natural polysaccharide is selected from at least one of tremella polysaccharide, ganoderma lucidum polysaccharide, pachyman, angelica polysaccharide, ginseng polysaccharide, cactus polysaccharide, mannan, flammulina velutipes polysaccharide, coix seed polysaccharide, cactus polysaccharide, aloe polysaccharide, glossy privet fruit polysaccharide, chromocene polysaccharide, white mustard seed polysaccharide, barbat skullcap polysaccharide and rhizoma anemarrhenae polysaccharide.
In a preferred embodiment of the invention, the natural polysaccharide is prepared from tremella polysaccharide, ganoderma lucidum polysaccharide, flammulina velutipes polysaccharide, coix seed polysaccharide and glossy privet fruit polysaccharide according to a weight ratio of 1:0.2-0.5: 1-2: 2-3: 3-5.
In a preferred embodiment of the invention, the natural polysaccharide is composed of cactus polysaccharide, mannan, chromocene polysaccharide and white mustard seed polysaccharide according to the weight ratio of 1:2-5:0.2-0.5: 1-3.
In a preferred embodiment of the invention, the natural polysaccharide is selected from pachyman, angelica polysaccharide, ginseng polysaccharide, ligustrum lucidum polysaccharide, sculellaria barbata polysaccharide and rhizoma anemarrhenae polysaccharide according to the weight ratio of 1:3-6:0.05-0.2:0.5-2: 0.1-0.8: 0.5-1.2.
According to the present invention, preferably, the plant essential oil is at least one selected from the group consisting of rose essential oil, camellia essential oil, lemon essential oil, lavender essential oil, calendula oil and geranium essential oil, and the addition of the plant essential oil can be adjusted according to the fragrance of the essential oil and the efficacy of the essential oil, which is not described herein again.
According to the present invention, in order to improve the repair ability of the mask essence, it is preferable that the skin repair agent is at least one selected from the group consisting of glycine, alanine, valine, isoleucine, leucine, proline, arginine, aspartic acid, glutamic acid, L-threonine, citric acid, and betaine.
According to the present invention, the mask essence further comprises an auxiliary agent commonly known to those skilled in the art, such as at least one of a preservative, a thickener, a pH adjuster and a humectant, and further, the preservative is at least one selected from diazolidinyl urea, methylparaben and phenoxyethanol; the pH regulator is triethanolamine; the thickener can be xanthan gum and carbomer; the humectant may be at least one of polyethylene glycol, polypropylene glycol, butylene glycol, propylene glycol, hexylene glycol, xylitol, sorbitol, and the like.
According to the technical scheme, the natural polysaccharide has a dynamic moisturizing effect, the hyaluronic acid has an excellent moisturizing effect, the active substances can be fully absorbed by the skin, the skin repairing agent can repair damaged skin, the graphene can form a film layer on the surface of the skin and plays a role in isolating air oxidation for the skin, so that the active ingredients in the mask essence can be absorbed by the skin to the maximum extent, the absorption efficiency of the skin on the active ingredients is improved, the effect of the active ingredients is exerted to the maximum extent, the volatilization of the moisture on the surface layer of the skin can be reduced, and a good moisturizing effect is achieved.
Detailed Description
The endpoints of the ranges and any values disclosed herein are not limited to the precise range or value, and such ranges or values should be understood to encompass values close to those ranges or values. For ranges of values, between the endpoints of each of the ranges and the individual points, and between the individual points may be combined with each other to give one or more new ranges of values, and these ranges of values should be considered as specifically disclosed herein.
The present invention will be described in detail below by way of examples.
In the following examples, the preparation method of the rice washing water comprises: washing 1kg of rice with water, soaking in 5L of water, adding 40g of pericarpium Citri Tangerinae, fermenting at 45 deg.C for 30 days, and collecting supernatant.
The natural polysaccharide A is as follows: the tremella polysaccharide-containing tea is composed of tremella polysaccharide, ganoderma lucidum polysaccharide, flammulina velutipes polysaccharide, coix seed polysaccharide and glossy privet fruit polysaccharide according to the weight ratio of 1:0.3:1.2:2.5: 3.2.
The natural polysaccharide B is: the cactus polysaccharide-mannan composite material is composed of cactus polysaccharide, mannan, chromocene polysaccharide and brassica alba polysaccharide according to a weight ratio of 1:3:0.3: 2.
The natural polysaccharide C is: the polysaccharide is prepared from pachyman, angelica polysaccharide, ginseng polysaccharide, glossy privet fruit polysaccharide, barbat skullcap polysaccharide and rhizoma anemarrhenae polysaccharide according to the weight ratio of 1:5:0.1:1.3: 0.6: 0.8.
The concentration of the graphene aqueous solution is 10 mg/L.
Example 1
The mask essence comprises the following components in parts by weight: 0.12 part by weight of activated carbon, 0.2 part by weight of graphene aqueous solution, 0.5 part by weight of glycine, 0.3 part by weight of nicotinamide, 0.1 part by weight of natural polysaccharide A, 0.2 part by weight of natural polysaccharide B, 1 part by weight of transdermal peptide EFG, 1.5 parts by weight of allantoin, 2.1 parts by weight of sodium alginate, 1.5 parts by weight of rose essential oil, 5 parts by weight of sodium hyaluronate, 8 parts by weight of modified zeolite, 12 parts by weight of rice washing water fermentation liquor, 15 parts by weight of glycerol, 0.05 part by weight of methylparaben, 0.3 part by weight of polyethylene glycol, 0.5 part by weight of polypropylene glycol and 5 parts by weight of carbomer.
The preparation method of the facial mask essence comprises the following steps:
(1) soaking zeolite powder (with particle size of 30-50 μm) in 1mol/L hydrochloric acid solution for 60min, centrifuging, washing, and drying to obtain an acidified product, ultrasonically dispersing the acidified product and aminobenzo-21-crown ether-7 at 80 ℃ for 45min, performing microwave reaction in an XH-300UP type microwave reactor at the ultrasonic power of 400W for 2min and the power of 500W, dispersing the microwave reaction product in a second acidic solution (1mol/L salicylic acid and 3mol/L myristic acid), and performing activation treatment at 90 ℃ for 4h to obtain modified zeolite powder;
(2) uniformly dispersing activated carbon, a graphene water solution, glycine, nicotinamide, natural polysaccharide A, natural polysaccharide B, transdermal peptide EFG, allantoin, sodium alginate, rose essential oil, sodium hyaluronate, modified zeolite, rice washing water fermentation liquor, glycerol, methyl hydroxybenzoate, polyethylene glycol, polypropylene glycol and carbomer by ultrasonic, and then adjusting the pH to 6.5-7 to obtain the mask essence.
Example 2
The mask essence comprises the following components in parts by weight: 0.1 part by weight of activated carbon, 0.1 part by weight of graphene water solution, 0.6 part by weight of isoleucine, 0.5 part by weight of nicotinamide, 0.1 part by weight of natural polysaccharide A, 0.8 part by weight of transdermal peptide EFG, 2.2 parts by weight of allantoin, 0.2 part by weight of sodium alginate, 2 parts by weight of calendula oil, 3 parts by weight of sodium hyaluronate, 10 parts by weight of modified zeolite, 5 parts by weight of rice washing water fermentation liquor, 3 parts by weight of glycerol, 0.05 part by weight of methylparaben, 0.3 part by weight of polyethylene glycol, 0.5 part by weight of polypropylene glycol and 5 parts by weight of carbomer.
The preparation method of the mask essence is the same as that of example 1.
Example 3
The mask essence comprises the following components in parts by weight: 0.15 part by weight of activated carbon, 0.5 part by weight of graphene aqueous solution, 0.1 part by weight of valine, 0.2 part by weight of nicotinamide, 0.5 part by weight of natural polysaccharide B, 01.2 parts by weight of transdermal peptide EFG, 0.6 part by weight of allantoin, 2.3 parts by weight of sodium alginate, 0.5 part by weight of calendula oil, 8 parts by weight of sodium hyaluronate, 3 parts by weight of modified zeolite, 1 part by weight of rice washing water fermentation broth, 18 parts by weight of glycerol, 0.05 part by weight of methylparaben, 0.3 part by weight of polyethylene glycol, 0.5 part by weight of polypropylene glycol and 5 parts by weight of carbomer.
The preparation method of the mask essence is the same as that of example 1.
Example 4
The mask essence comprises the following components in parts by weight: 0.05 part of activated carbon, 0.05 part of graphene aqueous solution, 0.05 part of proline, 0.1 part of nicotinamide, 0.8 part of natural polysaccharide C, 0.3 part of transdermal peptide EFG, 0.2 part of allantoin, 2.8 parts of sodium alginate, 0.3 part of camellia essential oil, 10 parts of sodium hyaluronate, 2 parts of modified zeolite, 5 parts of rice washing water fermentation liquor, 1 part of glycerol, 0.05 part of methylparaben, 0.3 part of polyethylene glycol, 0.5 part of polypropylene glycol and 5 parts of carbomer.
The preparation method of the mask essence is the same as that of example 1.
Example 5
The mask essence comprises the following components in parts by weight: 0.2 part by weight of activated carbon, 0.8 part by weight of graphene water solution, 0.8 part by weight of aspartic acid, 0.8 part by weight of nicotinamide, 0.02 part by weight of natural polysaccharide A, 1.5 parts by weight of transdermal peptide EFG, 3 parts by weight of allantoin, 0.1 part by weight of sodium alginate, 2.5 parts by weight of camellia essential oil, 1 part by weight of sodium hyaluronate, 15 parts by weight of modified zeolite, 1 part by weight of rice washing water fermentation broth, 20 parts by weight of glycerol, 0.05 part by weight of methylparaben, 0.3 part by weight of polyethylene glycol, 0.5 part by weight of polypropylene glycol and 5 parts by weight of carbomer.
The preparation method of the mask essence is the same as that of example 1.
Example 6
The process of example 1 was followed except that: the modification method of the zeolite comprises the following steps: soaking zeolite powder (with particle size of 30-50 μm) in 1mol/L hydrochloric acid solution for 60min, centrifuging, washing, and drying to obtain acidified product, ultrasonically dispersing the acidified product and aminobenzo-21-crown ether-7 at 80 deg.C for 45min, performing microwave reaction with ultrasonic power of 400W in XH-300UP type microwave reactor for 2min, and power of 500W to obtain modified zeolite powder.
Example 7
The process of example 1 was followed except that: soaking zeolite powder (with particle size of 30-50 μm) in 1mol/L hydrochloric acid solution for 60min, centrifuging, washing, drying to obtain acidified product, dispersing the acidified product in second acidic solution (1mol/L salicylic acid and 3mol/L myristic acid), and activating at 90 deg.C for 4 hr to obtain modified zeolite powder.
Example 8
The process of example 1 was followed except that the second acid solution was hydrochloric acid.
Example 9
The procedure of example 1 was followed except that the zeolite was not modified.
Example 10
The process of example 1 was followed except that no zeolite was added.
Example 11
The procedure of example 1 was followed except that no natural polysaccharide was included.
Example 12
The procedure of example 1 was followed except that no activated carbon was added.
Test example
120 healthy female volunteers with no history of allergy aged 20-35 were selected and divided into 12 groups of 10 persons each, and the facial mask essences prepared in examples 1-12 were tested, respectively. All subjects had signed an informed consent.
The use of the mask essence comprises the following steps: firstly, soaking a compressed facial mask in facial mask essence for 2-3min, then spraying a small amount of cosmetic water on the face to keep the face moist, then applying the soaked facial mask on the skin, and removing the facial mask after 10-20 min.
In the test, the left forearm of the subject was used as the test site, the mask sample was applied 1 time a day, gently massaged with a finger until complete absorption, and the skin reaction after 24 hours was observed using the right forearm itself as a blank control.
As a result: after detection, the product has good smell and stability, all subjects have no abnormal phenomena such as erythema and the like, and the result is still free of any reaction after continuous observation for 3-4 days, which indicates that the moisturizing mask prepared by the technical scheme is safe.
During testing, the inner area of the left forearm of a subject is used as a tested part, the tested part is cleaned by clean water before testing and is stabilized for 30min before testing, the testing temperature is 20-25 ℃, the relative humidity is 50-60%, after the inner sides of the left forearm and the right forearm are respectively coated with a mask sample for 15min, the mask is taken down, the percentage contents of moisture of the tested part at 0min, 60min and 120min are measured by an intelligent moisture tester, the testing is repeated for 5 times each time, the average value is obtained, and the experimental result is shown in table 1.
TABLE 1
Figure BDA0002656017120000091
Figure BDA0002656017120000101
The preferred embodiments of the present invention have been described above in detail, but the present invention is not limited thereto. Within the scope of the technical idea of the invention, many simple modifications can be made to the technical solution of the invention, including combinations of various technical features in any other suitable way, and these simple modifications and combinations should also be regarded as the disclosure of the invention, and all fall within the scope of the invention.

Claims (10)

1. The mask essence is characterized by comprising the following components in parts by weight: 0.05-0.2 part of activated carbon, 0.05-0.8 part of graphene water solution, 0.05-0.8 part of skin repair agent, 0.1-0.8 part of nicotinamide, 0.02-0.8 part of natural polysaccharide, 0.3-1.5 parts of transdermal peptide EFG, 0.2-3 parts of allantoin, 0.1-2.8 parts of sodium alginate, 0.3-2.5 parts of plant essential oil, 1-10 parts of sodium hyaluronate, 2-15 parts of modified zeolite, 1-5 parts of rice washing water fermentation liquor and 1-20 parts of glycerol.
2. The mask essence of claim 1, wherein the mask essence comprises: 0.1-0.15 part of activated carbon, 0.1-0.5 part of graphene water solution, 0.1-0.6 part of skin repair agent, 0.2-0.5 part of nicotinamide, 0.1-0.5 part of natural polysaccharide, 0.8-1.2 parts of transdermal peptide EFG, 0.6-2.2 parts of allantoin, 0.2-2.3 parts of sodium alginate, 0.5-2 parts of plant essential oil, 3-8 parts of sodium hyaluronate, 3-10 parts of modified zeolite, 1-5 parts of rice washing water fermentation liquor and 3-18 parts of glycerol.
3. The mask essence according to claim 1 or 2, wherein the modification method of the zeolite comprises:
performing first acid treatment on zeolite powder in a first acid solution to obtain an acidified product, performing ultrasonic dispersion on the acidified product and a crown ether reagent for 30-60min, performing microwave reaction for 1-3min, and performing second acid treatment on the acidified product in a second acid solution to obtain modified zeolite.
4. The mask essence of claim 3, wherein the crown ether agent is at least one selected from aminobenzo-15-crown ether-5, aminobenzo-18-crown ether-6, aminobenzo-21-crown ether-7, aminobenzo-24-crown ether-8, aminoholothia-15-crown ether-5, aminoholothia-18-crown ether-6, and aminobenzothiacrown ether.
5. The mask essence of claim 3 or 4, wherein the power of the ultrasonic dispersion is 300-500W, and the power of the microwave reaction is 400-600W.
6. The mask essence according to any one of claims 1 to 5, wherein the natural polysaccharide is at least one selected from tremella polysaccharide, ganoderan, pachyman, angelicae gigantis polysaccharide, ginseng polysaccharide, cactus polysaccharide, mannan, flammulina velutipes polysaccharide, coix seed polysaccharide, cactus polysaccharide, aloe polysaccharide, ligustrum lucidum polysaccharide, chromocene polysaccharide, brassica alba polysaccharide, barbat skullcap polysaccharide, and anemarrhena asphodeloides polysaccharide.
7. The mask essence according to claim 6, wherein the natural polysaccharides comprise tremella polysaccharides, ganoderan, flammulina velutipes polysaccharides, coix seed polysaccharides and glossy privet fruit polysaccharides according to a weight ratio of 1:0.2-0.5: 1-2: 2-3: 3-5.
8. The mask essence of claim 6, wherein the natural polysaccharides comprise cactus polysaccharide, mannan, chromocene polysaccharide and mustard seed polysaccharide in a weight ratio of 1:2-5:0.2-0.5: 1-3.
9. The mask essence of claim 6, wherein the natural polysaccharides comprise pachyman, angelica sinensis polysaccharide, ginseng polysaccharide, ligustrum lucidum polysaccharide, barbat skullcap polysaccharide and rhizoma anemarrhenae polysaccharide in a weight ratio of 1:3-6:0.05-0.2:0.5-2: 0.1-0.8: 0.5-1.2.
10. The mask essence according to any one of claims 1 to 9, further comprising at least one of a preservative, a thickener, a pH adjuster and a humectant.
CN202010887579.3A 2020-08-28 2020-08-28 Facial mask essence Withdrawn CN112107494A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115300445A (en) * 2022-08-29 2022-11-08 凯里学院 Skin care product based on rice sour soup as raw material and preparation method thereof

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115300445A (en) * 2022-08-29 2022-11-08 凯里学院 Skin care product based on rice sour soup as raw material and preparation method thereof

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Application publication date: 20201222