CN112641658A - Oil control shampoo and preparation method thereof - Google Patents
Oil control shampoo and preparation method thereof Download PDFInfo
- Publication number
- CN112641658A CN112641658A CN202011642308.8A CN202011642308A CN112641658A CN 112641658 A CN112641658 A CN 112641658A CN 202011642308 A CN202011642308 A CN 202011642308A CN 112641658 A CN112641658 A CN 112641658A
- Authority
- CN
- China
- Prior art keywords
- oil control
- parts
- polyquaternium
- control shampoo
- cymene
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000002453 shampoo Substances 0.000 title claims abstract description 76
- 238000002360 preparation method Methods 0.000 title abstract description 18
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims abstract description 58
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 53
- 239000011780 sodium chloride Substances 0.000 claims abstract description 39
- 235000002639 sodium chloride Nutrition 0.000 claims abstract description 39
- 229930007927 cymene Natural products 0.000 claims abstract description 38
- HFPZCAJZSCWRBC-UHFFFAOYSA-N p-cymene Chemical compound CC(C)C1=CC=C(C)C=C1 HFPZCAJZSCWRBC-UHFFFAOYSA-N 0.000 claims abstract description 38
- DTXXSJZBSTYZKE-ZDQKKZTESA-N Maxacalcitol Chemical compound C1(/[C@@H]2CC[C@@H]([C@]2(CCC1)C)[C@@H](OCCC(C)(C)O)C)=C\C=C1\C[C@@H](O)C[C@H](O)C1=C DTXXSJZBSTYZKE-ZDQKKZTESA-N 0.000 claims abstract description 32
- 239000008139 complexing agent Substances 0.000 claims abstract description 12
- 239000004094 surface-active agent Substances 0.000 claims abstract description 11
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid group Chemical group C(CC(O)(C(=O)O)CC(=O)O)(=O)O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 84
- 229940045944 sodium lauroyl glutamate Drugs 0.000 claims description 31
- IWIUXJGIDSGWDN-UQKRIMTDSA-M sodium;(2s)-2-(dodecanoylamino)pentanedioate;hydron Chemical compound [Na+].CCCCCCCCCCCC(=O)N[C@H](C([O-])=O)CCC(O)=O IWIUXJGIDSGWDN-UQKRIMTDSA-M 0.000 claims description 31
- 239000011259 mixed solution Substances 0.000 claims description 28
- 238000003756 stirring Methods 0.000 claims description 28
- QXNVGIXVLWOKEQ-UHFFFAOYSA-N Disodium Chemical compound [Na][Na] QXNVGIXVLWOKEQ-UHFFFAOYSA-N 0.000 claims description 27
- 238000001816 cooling Methods 0.000 claims description 14
- 238000010438 heat treatment Methods 0.000 claims description 14
- 239000002504 physiological saline solution Substances 0.000 claims description 14
- 229940047642 disodium cocoamphodiacetate Drugs 0.000 claims description 3
- 238000000034 method Methods 0.000 claims description 2
- 239000003002 pH adjusting agent Substances 0.000 claims description 2
- 239000004034 viscosity adjusting agent Substances 0.000 claims description 2
- 230000000694 effects Effects 0.000 abstract description 26
- 230000028327 secretion Effects 0.000 abstract description 6
- 241000894006 Bacteria Species 0.000 abstract description 5
- 238000004140 cleaning Methods 0.000 abstract description 4
- 239000002085 irritant Substances 0.000 abstract description 4
- 231100000021 irritant Toxicity 0.000 abstract description 4
- 230000002401 inhibitory effect Effects 0.000 abstract description 2
- 230000002009 allergenic effect Effects 0.000 abstract 1
- 231100000252 nontoxic Toxicity 0.000 abstract 1
- 230000003000 nontoxic effect Effects 0.000 abstract 1
- 230000000052 comparative effect Effects 0.000 description 22
- 210000004761 scalp Anatomy 0.000 description 17
- 208000001840 Dandruff Diseases 0.000 description 4
- 208000003251 Pruritus Diseases 0.000 description 4
- 206010039792 Seborrhoea Diseases 0.000 description 4
- 210000004027 cell Anatomy 0.000 description 4
- 238000013329 compounding Methods 0.000 description 4
- 239000003153 chemical reaction reagent Substances 0.000 description 3
- 230000007803 itching Effects 0.000 description 3
- 230000001954 sterilising effect Effects 0.000 description 3
- 238000004659 sterilization and disinfection Methods 0.000 description 3
- 239000002562 thickening agent Substances 0.000 description 3
- 229920000832 Cutin Polymers 0.000 description 2
- DPXJVFZANSGRMM-UHFFFAOYSA-N acetic acid;2,3,4,5,6-pentahydroxyhexanal;sodium Chemical compound [Na].CC(O)=O.OCC(O)C(O)C(O)C(O)C=O DPXJVFZANSGRMM-UHFFFAOYSA-N 0.000 description 2
- 230000004913 activation Effects 0.000 description 2
- 230000000844 anti-bacterial effect Effects 0.000 description 2
- 230000003260 anti-sepsis Effects 0.000 description 2
- 239000001768 carboxy methyl cellulose Substances 0.000 description 2
- 238000011156 evaluation Methods 0.000 description 2
- 239000004519 grease Substances 0.000 description 2
- 230000007774 longterm Effects 0.000 description 2
- 230000004060 metabolic process Effects 0.000 description 2
- 239000003755 preservative agent Substances 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 235000019812 sodium carboxymethyl cellulose Nutrition 0.000 description 2
- 229920001027 sodium carboxymethylcellulose Polymers 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- 230000000638 stimulation Effects 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 238000006467 substitution reaction Methods 0.000 description 2
- 230000002195 synergetic effect Effects 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- 201000004384 Alopecia Diseases 0.000 description 1
- 206010061218 Inflammation Diseases 0.000 description 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- 206010070834 Sensitisation Diseases 0.000 description 1
- 230000001133 acceleration Effects 0.000 description 1
- 230000003064 anti-oxidating effect Effects 0.000 description 1
- 230000002421 anti-septic effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000002738 chelating agent Substances 0.000 description 1
- 239000012459 cleaning agent Substances 0.000 description 1
- 230000007012 clinical effect Effects 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000018109 developmental process Effects 0.000 description 1
- 235000005911 diet Nutrition 0.000 description 1
- 230000037213 diet Effects 0.000 description 1
- 239000003974 emollient agent Substances 0.000 description 1
- 210000001339 epidermal cell Anatomy 0.000 description 1
- 230000003203 everyday effect Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 239000006260 foam Substances 0.000 description 1
- 230000006870 function Effects 0.000 description 1
- 230000003648 hair appearance Effects 0.000 description 1
- 208000024963 hair loss Diseases 0.000 description 1
- 230000003676 hair loss Effects 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 208000015181 infectious disease Diseases 0.000 description 1
- 230000004054 inflammatory process Effects 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 230000007794 irritation Effects 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000011777 magnesium Substances 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 235000010755 mineral Nutrition 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 231100000956 nontoxicity Toxicity 0.000 description 1
- BTSZTGGZJQFALU-UHFFFAOYSA-N piroctone olamine Chemical compound NCCO.CC(C)(C)CC(C)CC1=CC(C)=CC(=O)N1O BTSZTGGZJQFALU-UHFFFAOYSA-N 0.000 description 1
- 229940081510 piroctone olamine Drugs 0.000 description 1
- 230000002335 preservative effect Effects 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 230000033764 rhythmic process Effects 0.000 description 1
- 210000002374 sebum Anatomy 0.000 description 1
- 230000008313 sensitization Effects 0.000 description 1
- -1 skin conditioner Substances 0.000 description 1
- 230000036560 skin regeneration Effects 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 230000008719 thickening Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4906—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom
- A61K8/4926—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom having six membered rings
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/20—Halogens; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/31—Hydrocarbons
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/006—Antidandruff preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/008—Preparations for oily hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/48—Thickener, Thickening system
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/52—Stabilizers
- A61K2800/524—Preservatives
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
Abstract
The invention belongs to the technical field of cleaning supplies, and discloses oil control shampoo and a preparation method thereof. The oil control shampoo comprises the following components: the hair conditioner comprises a surfactant, a hair conditioner, a pH regulator, a viscosity regulator, an oil control complexing agent and water, wherein the oil control complexing agent comprises cymene, OCT and sea salt. The cymene, the OCT and the sea salt are compounded to be used as the oil control complexing agent, the components are mild and non-irritant, the oil control complexing agent is capable of deeply nourishing and replenishing water while achieving the obvious oil control effect, the situations of tightness, dryness, knotting and the like are avoided, the comfort level of a user is improved, the cymene, the OCT and the sea salt are very reliable in safety to eyes and skin, absolutely non-toxic, irritant and allergenic, the cymene, the OCT and the sea salt are compounded to be used for resisting and inhibiting bacteria, the effect of obviously reducing oil secretion is achieved, the oil control effect is fundamentally achieved, and the efficient oil control effect is synergistically exerted.
Description
Technical Field
The invention relates to the technical field of cleaning supplies, in particular to oil control shampoo and a preparation method thereof.
Background
The shampoo is a hair care product with the functions of removing dandruff, relieving itching, treating hair oil, nourishing hair and the like, is a daily-use cleaning agent, contains a plurality of components in shampoo, has the comprehensive effects of mainly cleaning scalp and hair, can be used for rubbing a period of time by removing a proper amount of shampoo from palms and adding a proper amount of water to generate foam after mixing, and can be used for cleaning hair by being used for washing the hair for a period of time and then being washed clean by clear water.
However, with the development of modern society and the acceleration of life rhythm, the pressure of people is increased, and diet is unbalanced, which easily causes excessive sebum secretion, and the hair is easily greasy, especially for people with oily hair, even the second day after shampooing, the hair roots will immediately become greasy, the scalp will be accumulated on the hair roots as thick scales, and the hair is easily itchy, and many people are troubled by oily hair.
Disclosure of Invention
In order to overcome the defects of the prior art, the invention mainly aims to provide mild and efficient oil control shampoo.
The invention also aims to provide a preparation method of the oil control shampoo.
In order to achieve the purpose, the invention adopts the following technical scheme:
an oil control shampoo comprises the following components: surfactant, hair conditioner, pH regulator, viscosity regulator, oil control complexing agent and water;
wherein, the oil control complexing agent comprises cymene, OCT and sea salt.
Preferably, the coating comprises the following components in parts by mass: 19-30 parts of surfactant, 0.7-2.1 parts of conditioner for hair, 0.1-0.5 part of pH regulator, 2-10 parts of viscosity regulator, 0.06-0.08 part of cymene, 0.2-0.3 part of OCT, 0.1-0.3 part of sea salt and 70-80 parts of water.
Preferably, the surfactant comprises AES, sodium lauroyl glutamate and disodium cocoamphodiacetate.
Preferably, the surfactant comprises, by mass, 10-15 parts of AES, 6-10 parts of sodium lauroyl glutamate and 3-5 parts of disodium cocoyl amphodiacetate.
Preferably, the hair conditioner comprises at least one of polyquaternium-7, polyquaternium-10 and polyquaternium-22.
Preferably, the pH adjusting agent is citric acid.
Preferably, the viscosity modifier is physiological saline.
Preferably, the concentration of the physiological saline is 0.9%.
Preferably, the oil control shampoo comprises the following components in parts by mass: 10-15 parts of AES, 6-10 parts of sodium lauroyl glutamate, 3-5 parts of disodium cocoyl amphodiacetate, 0.5-1.5 parts of polyquaternium-7, 0.1-0.3 part of polyquaternium-10, 0.1-0.3 part of polyquaternium-22, 0.1-0.5 part of citric acid, 2-10 parts of normal saline, 0.06-0.08 part of cymene, 0.2-0.3 part of OCT, 0.1-0.3 part of sea salt and 70-80 parts of water.
Preferably, the oil control shampoo can also be added with proper components such as chelating agent, emollient, skin conditioner, essence, preservative and the like.
The invention also provides a preparation method of the oil control shampoo, which comprises the following steps:
(1) adding a surfactant and a pH regulator into a part of water according to a proportion, heating to 70-80 ℃, and uniformly stirring to obtain a mixed solution A;
(2) and cooling to 40-45 ℃, adding the hair conditioner, the oil control complexing agent, the viscosity regulator and the rest amount of water into the mixed solution A in proportion, and uniformly stirring to obtain the oil control shampoo.
Compared with the prior art, the invention has the following advantages and technical effects:
(1) the shampoo provided by the invention adopts the compounding of cymene, OCT and sea salt as an oil control complexing agent, the components are mild and non-irritant, specifically, OCT is the abbreviation of piroctone olamine, OCT blocks the external channel generated by scurf fundamentally through the sterilization and antioxidation effects, thereby effectively and fundamentally removing the scurf and achieving the itching relieving effect, cymene also has the antibacterial, sterilization and antisepsis effects, and the sea salt contains mineral substances, can be absorbed by scalp epidermal cells, increases the cell vitality, promotes the activation and metabolism of scalp superficial layer cells, deeply purifies scalp, improves the problems of scalp cutin and grease, simultaneously, the sea salt also can play the sterilization and antisepsis effects, can prevent the inflammation and the infection of skin in time by matching with the cymene, thereby being beneficial to helping the skin regeneration, promoting the activation and the metabolism of skin superficial layer cells, purifying scalp deeply, and improving the problems of scalp cutin and grease, the hair loss is reduced, the hair fiber, especially magnesium element contained in sea salt is strengthened, a layer of water film can be formed in the scalp after hair washing, moisture can be kept continuously, the moisture of the scalp which is lack of water can be improved in time, the moisture can be deeply nourished and supplemented while the obvious oil control effect is achieved, the situations of tightness, dryness, knotting and the like are avoided, the comfort level of a user is improved, the safety of cymene, OCT and sea salt to eyes and skin is very reliable, absolute non-toxicity, irritation and sensitization are achieved, the effects of resisting bacteria and inhibiting bacteria can be achieved through the compound use of the cymene, the OCT and the sea salt, the effect of obviously reducing oil secretion is achieved, the oil control effect is fundamentally achieved, and the efficient oil control effect is.
(2) The oil control shampoo adopts the normal saline as the thickening agent, the normal saline is a solution, the solution can be quickly dispersed into a system, the thickening effect is well played, the preparation of the oil control shampoo is facilitated, the clear liquid with good properties and fluidity can be formed by compounding the oil control shampoo with AES, so that the oil control shampoo with stable properties can be prepared, the thickening agent adopts the normal saline which has no stimulation to skin, the normal saline is easy to obtain and has low price, and the oil control shampoo has a certain antibacterial effect, the stability of the finished oil control shampoo is further improved, the cell activity can be improved, the oil control effect can be improved by compounding the oil control complexing agent, the scalp health is improved, and the hair quality is improved.
(3) The sea salt and the cymene are compounded in the shampoo, so that the generation of bacteria around the scalp can be effectively inhibited, the antiseptic effect is achieved, other preservatives are not needed, the use of chemical reagents is reduced, the stimulation to the scalp is reduced, the formula is mild and non-irritant, the shampoo is suitable for long-term use, and the oily hair does not damage the hair and the scalp after being used every day.
Detailed Description
The present invention will be described in further detail with reference to specific examples, but the embodiments of the present invention are not limited thereto. All the raw materials and reagents used in the present invention are commercially available raw materials and reagents, unless otherwise specified. In the examples, the components are used in g and mL in parts by mass.
Example 1
In the embodiment, the oil control shampoo comprises the following components in parts by mass: 10 parts of AES, 6 parts of sodium lauroyl glutamate, 3 parts of disodium cocoyl amphodiacetate, 0.5 part of polyquaternium-7, 0.1 part of polyquaternium-10, 0.1 part of polyquaternium-22, 0.1 part of citric acid, 0.2 part of normal saline, 0.06 part of cymene, 0.2 part of OCT, 0.1 part of sea salt and 80 parts of water.
The preparation method of the oil control shampoo provided by the embodiment comprises the following steps:
(1) adding AES, sodium lauroyl glutamate, disodium cocoyl amphodiacetate and citric acid into a part of water according to a proportion, heating to 75 ℃, and uniformly stirring to obtain a mixed solution A;
(2) and (3) cooling to 42.5 ℃, adding polyquaternium-7, polyquaternium-10, polyquaternium-22, cymene, OCT, sea salt, 0.9% physiological saline and the rest of water into the mixed solution A according to the proportion, and uniformly stirring to obtain the oil control shampoo of the embodiment 1.
Example 2
In the embodiment, the oil control shampoo comprises the following components in parts by mass: 12.5 parts of AES, 8 parts of sodium lauroyl glutamate, 4 parts of disodium cocoyl amphodiacetate, 1 part of polyquaternium-7, 0.2 part of polyquaternium-10, 0.2 part of polyquaternium-22, 0.3 part of citric acid, 0.9 part of normal saline, 0.07 part of cymene, 0.25 part of OCT, 0.2 part of sea salt and 75 parts of water.
The preparation method of the oil control shampoo provided by the embodiment comprises the following steps:
(1) adding AES, sodium lauroyl glutamate, disodium cocoyl amphodiacetate and citric acid into a part of water according to a proportion, heating to 75 ℃, and uniformly stirring to obtain a mixed solution A;
(2) and (3) cooling to 42.5 ℃, adding polyquaternium-7, polyquaternium-10, polyquaternium-22, cymene, OCT, sea salt, 0.9% physiological saline and the rest of water into the mixed solution A according to the proportion, and uniformly stirring to obtain the oil control shampoo of the embodiment 2.
Example 3
In the embodiment, the oil control shampoo comprises the following components in parts by mass: 15 parts of AES, 10 parts of sodium lauroyl glutamate, 5 parts of disodium cocoyl amphodiacetate, 1.5 parts of polyquaternium-7, 0.3 part of polyquaternium-10, 0.3 part of polyquaternium-22, 0.5 part of citric acid, 1.5 parts of normal saline, 0.08 part of cymene, 0.3 part of OCT, 0.3 part of sea salt and 70 parts of water.
The preparation method of the oil control shampoo provided by the embodiment comprises the following steps:
(1) adding AES, sodium lauroyl glutamate, disodium cocoyl amphodiacetate and citric acid into a part of water according to a proportion, heating to 75 ℃, and uniformly stirring to obtain a mixed solution A;
(2) and (3) cooling to 42.5 ℃, adding polyquaternium-7, polyquaternium-10, polyquaternium-22, cymene, OCT, sea salt, 0.9% physiological saline and the rest of water into the mixed solution A according to the proportion, and uniformly stirring to obtain the oil control shampoo of the embodiment 3.
Example 4
In the embodiment, the oil control shampoo comprises the following components in parts by mass: 14.8 parts of AES, 9.7 parts of sodium lauroyl glutamate, 4.7 parts of disodium cocoyl amphodiacetate, 1.4 parts of polyquaternium-7, 0.28 part of polyquaternium-10, 0.28 part of polyquaternium-22, 0.45 part of citric acid, 1.35 parts of normal saline and 0.075 part of sodium lauroyl glutamate
Cymene, 0.27 parts OCT, 0.27 parts sea salt, and 78 parts water.
The preparation method of the oil control shampoo provided by the embodiment comprises the following steps:
(1) adding AES, sodium lauroyl glutamate, disodium cocoyl amphodiacetate and citric acid into a part of water according to a proportion, heating to 75 ℃, and uniformly stirring to obtain a mixed solution A;
(2) and (3) cooling to 42.5 ℃, adding polyquaternium-7, polyquaternium-10, polyquaternium-22, cymene, OCT, sea salt, 0.9% physiological saline and the rest of water into the mixed solution A according to the proportion, and uniformly stirring to obtain the oil control shampoo of the embodiment 4.
Example 5
In the embodiment, the oil control shampoo comprises the following components in parts by mass: 14.8 parts of AES, 9.7 parts of sodium lauroyl glutamate, 4.7 parts of disodium cocoyl amphodiacetate, 1.4 parts of polyquaternium-7, 0.28 part of polyquaternium-10, 0.28 part of polyquaternium-22, 0.45 part of citric acid, 1.35 parts of normal saline, 0.075 part of cymene, 0.27 part of OCT, 0.27 part of sea salt and 78 parts of water.
The preparation method of the oil control shampoo provided by the embodiment comprises the following steps:
(1) adding AES, sodium lauroyl glutamate, disodium cocoyl amphodiacetate and citric acid into a part of water according to a proportion, heating to 70 ℃, and uniformly stirring to obtain a mixed solution A;
(2) and (3) cooling to 40 ℃, adding polyquaternium-7, polyquaternium-10, polyquaternium-22, cymene, OCT, sea salt, 0.9% physiological saline and the rest of water into the mixed solution A according to the proportion, and uniformly stirring to obtain the oil control shampoo of the embodiment 5.
Example 6
In the embodiment, the oil control shampoo comprises the following components in parts by mass: 14.8 parts of AES, 9.7 parts of sodium lauroyl glutamate, 4.7 parts of disodium cocoyl amphodiacetate, 1.4 parts of polyquaternium-7, 0.28 part of polyquaternium-10, 0.28 part of polyquaternium-22, 0.45 part of citric acid, 1.35 parts of normal saline, 0.075 part of cymene, 0.27 part of OCT, 0.27 part of sea salt and 78 parts of water.
The preparation method of the oil control shampoo provided by the embodiment comprises the following steps:
(1) adding AES, sodium lauroyl glutamate, disodium cocoyl amphodiacetate and citric acid into a part of water according to a proportion, heating to 80 ℃, and uniformly stirring to obtain a mixed solution A;
(2) and (3) cooling to 45 ℃, adding polyquaternium-7, polyquaternium-10, polyquaternium-22, cymene, OCT, sea salt, 0.9% physiological saline and the rest of water into the mixed solution A according to the proportion, and uniformly stirring to obtain the oil control shampoo of the embodiment 6.
Comparative example 1
In the comparative example, the oil control shampoo comprises the following components in parts by mass: 14.8 parts of AES, 9.7 parts of sodium lauroyl glutamate, 4.7 parts of disodium cocoyl amphodiacetate, 1.4 parts of polyquaternium-7, 0.28 part of polyquaternium-10, 0.28 part of polyquaternium-22, 0.45 part of citric acid, 1.35 parts of normal saline and 78 parts of water.
The preparation method of the oil control shampoo provided by the comparative example comprises the following steps:
(1) adding AES, sodium lauroyl glutamate, disodium cocoyl amphodiacetate and citric acid into a part of water according to a proportion, heating to 75 ℃, and uniformly stirring to obtain a mixed solution A;
(2) and cooling to 42.5 ℃, adding polyquaternium-7, polyquaternium-10, polyquaternium-22, 0.9% physiological saline and the rest water into the mixed solution A according to the proportion, and uniformly stirring to obtain the oil control shampoo of the comparative example 1.
Comparative example 2
In the embodiment, the oil control shampoo comprises the following components in parts by mass: 14.8 parts of AES, 9.7 parts of sodium lauroyl glutamate, 4.7 parts of disodium cocoyl amphodiacetate, 1.4 parts of polyquaternium-7, 0.28 part of polyquaternium-10, 0.28 part of polyquaternium-22, 0.45 part of citric acid, 1.35 parts of normal saline, 0.27 part of OCT, 0.27 part of sea salt and 78 parts of water.
The preparation method of the oil control shampoo provided by the comparative example comprises the following steps:
(1) adding AES, sodium lauroyl glutamate, disodium cocoyl amphodiacetate and citric acid into a part of water according to a proportion, heating to 75 ℃, and uniformly stirring to obtain a mixed solution A;
(2) and cooling to 42.5 ℃, adding polyquaternium-7, polyquaternium-10, polyquaternium-22, OCT, sea salt, 0.9% normal saline and the rest water into the mixed solution A according to the proportion, and uniformly stirring to obtain the oil control shampoo of the comparative example 2.
Comparative example 3
In the embodiment, the oil control shampoo comprises the following components in parts by mass: 14.8 parts of AES, 9.7 parts of sodium lauroyl glutamate, 4.7 parts of disodium cocoyl amphodiacetate, 1.4 parts of polyquaternium-7, 0.28 part of polyquaternium-10, 0.28 part of polyquaternium-22, 0.45 part of citric acid, 1.35 parts of normal saline, 0.075 part of cymene, 0.27 part of sea salt and 78 parts of water.
The preparation method of the oil control shampoo provided by the comparative example comprises the following steps:
(1) adding AES, sodium lauroyl glutamate, disodium cocoyl amphodiacetate and citric acid into a part of water according to a proportion, heating to 75 ℃, and uniformly stirring to obtain a mixed solution A;
(2) and cooling to 42.5 ℃, adding polyquaternium-7, polyquaternium-10, polyquaternium-22, cymene, sea salt, 0.9% physiological saline and the rest water into the mixed solution A according to the proportion, and uniformly stirring to obtain the oil control shampoo of the comparative example 3.
Comparative example 4
In the embodiment, the oil control shampoo comprises the following components in parts by mass: 14.8 parts of AES, 9.7 parts of sodium lauroyl glutamate, 4.7 parts of disodium cocoyl amphodiacetate, 1.4 parts of polyquaternium-7, 0.28 part of polyquaternium-10, 0.28 part of polyquaternium-22, 0.45 part of citric acid, 1.35 parts of normal saline, 0.075 part of cymene, 0.27 part of OCT and 78 parts of water.
The preparation method of the oil control shampoo provided by the comparative example comprises the following steps:
(1) adding AES, sodium lauroyl glutamate, disodium cocoyl amphodiacetate and citric acid into a part of water according to a proportion, heating to 75 ℃, and uniformly stirring to obtain a mixed solution A;
(2) and cooling to 42.5 ℃, adding polyquaternium-7, polyquaternium-10, polyquaternium-22, cymene, OCT, 0.9% physiological saline and the rest water into the mixed solution A according to the proportion, and uniformly stirring to obtain the oil control shampoo of the comparative example 4.
Comparative example 5
In the embodiment, the oil control shampoo comprises the following components in parts by mass: 14.8 parts of AES, 9.7 parts of sodium lauroyl glutamate, 4.7 parts of disodium cocoyl amphodiacetate, 1.4 parts of polyquaternium-7, 0.28 part of polyquaternium-10, 0.28 part of polyquaternium-22, 0.45 part of citric acid, 1.35 parts of sodium carboxymethyl cellulose, 0.075 part of cymene, 0.27 part of OCT, 0.27 part of sea salt and 78 parts of water.
The preparation method of the oil control shampoo provided by the comparative example comprises the following steps:
(1) adding AES, sodium lauroyl glutamate, disodium cocoyl amphodiacetate and citric acid into a part of water according to a proportion, heating to 75 ℃, and uniformly stirring to obtain a mixed solution A;
(2) and cooling to 42.5 ℃, adding polyquaternium-7, polyquaternium-10, polyquaternium-22, cymene, OCT, sea salt, sodium carboxymethylcellulose and the rest of water into the mixed solution A according to the proportion, and uniformly stirring to obtain the oil control shampoo of the comparative example 5.
Comparative example 6
In the embodiment, the oil control shampoo comprises the following components in parts by mass: 10 parts of AES, 6 parts of sodium lauroyl glutamate, 3 parts of disodium cocoyl amphodiacetate, 0.5 part of polyquaternium-7, 0.1 part of polyquaternium-10, 0.1 part of polyquaternium-22, 0.1 part of citric acid, 0.2 part of normal saline, 0.05 part of cymene, 0.18 part of OCT, 0.08 part of sea salt and 80 parts of water.
(1) Adding AES, sodium lauroyl glutamate, disodium cocoyl amphodiacetate and citric acid into a part of water according to a proportion, heating to 75 ℃, and uniformly stirring to obtain a mixed solution A;
(2) and cooling to 42.5 ℃, adding polyquaternium-7, polyquaternium-10, polyquaternium-22, cymene, OCT, sea salt, physiological saline with the concentration of 0.9 percent and the rest water into the mixed solution A according to the proportion, and uniformly stirring to obtain the oil control shampoo of the comparative example 6.
Clinical effect experiment:
test subjects: the hair had 240 oily hair substances (half of men and women): the patients with the excessive oil secretion are tried out, 240 patients (half of men and women respectively) with the excessive oil secretion are randomly divided into 12 groups, and each group comprises 20 patients;
the using method comprises the following steps: after hair is wetted, a proper amount of the product is taken and coated on the hair, the hair is rubbed and foamed, the hair is washed by warm water after being massaged for 3-5 minutes, and the hair is washed once every two days and is continuously used for 2 weeks.
Grading standard: the testers grade the evaluation items according to the use feelings of the testers, and the grade standard adopts a 10-point system.
The results, tested after 2 weeks of use by the subjects, were as follows:
TABLE 1 evaluation results of subjects after 2 weeks of use
As can be seen from table 1, the oil removal and scurf removal capability, scalp itching relieving situation, scalp water-moist feeling, hair smoothness and oil control effect of the oil control shampoo of examples 1-6 are comprehensively superior to those of comparative examples 1-6, and excellent oil control effect can be achieved after long-term use, through the mutual cooperation of three components of cymene, OCT and sea salt and the synergistic effect of the three components compared with comparative examples 1-4 in examples 1-6, the remarkable oil control and oil removal effect is achieved, and simultaneously scalp is well nourished and hair is cared, through the comparison of examples 1-6 with comparative example 5, the thickener adopts physiological saline, not only can the stable oil control shampoo be prepared, but also has the synergistic effect, the oil control effect can be remarkably improved, the quality of the oil control shampoo is improved, through the comparison of example 1 with comparative example 6, the reduction of the content of cymene, OCT and sea salt can remarkably affect the oil control effect, the quality of the oil control shampoo is reduced, and the oil control shampoo disclosed by the invention can resist and inhibit bacteria by compounding the components, so that the effect of remarkably reducing oil secretion is achieved, the oil control effect is fundamentally achieved, and the high-efficiency oil control effect is synergistically exerted.
The above embodiments are the best mode for carrying out the present invention, but the embodiments of the present invention are not limited to the above embodiments, and any other changes, modifications, substitutions, combinations, and simplifications which do not depart from the spirit and principle of the present invention should be regarded as equivalent substitutions and are included in the scope of the present invention.
Claims (10)
1. The oil control shampoo is characterized by comprising the following components: surfactant, hair conditioner, pH regulator, viscosity regulator, oil control complexing agent and water;
wherein, the oil control complexing agent comprises cymene, OCT and sea salt.
2. The oil control shampoo as claimed in claim 1, characterized by comprising the following components in parts by mass: 19-30 parts of surfactant, 0.7-2.1 parts of conditioner for hair, 0.1-0.5 part of pH regulator, 2-10 parts of viscosity regulator, 0.06-0.08 part of cymene, 0.2-0.3 part of OCT, 0.1-0.3 part of sea salt and 70-80 parts of water.
3. The oil control shampoo as in claim 2 wherein the surfactant comprises AES, sodium lauroyl glutamate and disodium cocoamphodiacetate.
4. The oil control shampoo as claimed in claim 3 wherein the surfactant comprises 10 to 15 parts by mass of AES, 6 to 10 parts by mass of sodium lauroyl glutamate and 3 to 5 parts by mass of disodium cocoamphodiacetate.
5. The oil control shampoo as claimed in claim 4 wherein the hair conditioner comprises at least one of polyquaternium-7, polyquaternium-10 and polyquaternium-22.
6. The oil control shampoo as defined in claim 5 wherein the pH adjuster is citric acid.
7. The oil control shampoo of claim 6 wherein the viscosity modifier is a physiological saline.
8. The oil control shampoo as defined in claim 7 wherein the normal saline is at a concentration of 0.9%.
9. The oil control shampoo as claimed in claim 8, wherein the oil control shampoo comprises the following components in parts by mass: 10-15 parts of AES, 6-10 parts of sodium lauroyl glutamate, 3-5 parts of disodium cocoyl amphodiacetate, 0.5-1.5 parts of polyquaternium-7, 0.1-0.3 part of polyquaternium-10, 0.1-0.3 part of polyquaternium-22, 0.1-0.5 part of citric acid, 2-10 parts of normal saline, 0.06-0.08 part of cymene, 0.2-0.3 part of OCT, 0.1-0.3 part of sea salt and 70-80 parts of water.
10. Method for preparing an oil control shampoo according to any of claims 1 to 9, comprising the following steps:
(1) adding a surfactant and a pH regulator into a part of water according to a proportion, heating to 70-80 ℃, and uniformly stirring to obtain a mixed solution A;
(2) and cooling to 40-45 ℃, adding the hair conditioner, the oil control complexing agent, the viscosity regulator and the rest amount of water into the mixed solution A in proportion, and uniformly stirring to obtain the oil control shampoo.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202011642308.8A CN112641658A (en) | 2020-12-31 | 2020-12-31 | Oil control shampoo and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202011642308.8A CN112641658A (en) | 2020-12-31 | 2020-12-31 | Oil control shampoo and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN112641658A true CN112641658A (en) | 2021-04-13 |
Family
ID=75367005
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202011642308.8A Pending CN112641658A (en) | 2020-12-31 | 2020-12-31 | Oil control shampoo and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN112641658A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114869801A (en) * | 2022-04-26 | 2022-08-09 | 彭氏(惠州)实业发展有限公司 | Hair care composition |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20190040339A1 (en) * | 2016-01-29 | 2019-02-07 | Colgate-Palmolive Company | Cleansing Compositions |
| CN110585087A (en) * | 2019-10-11 | 2019-12-20 | 茂名市瑜丰沉香创意产业有限公司 | Agilawood essential oil shampoo and preparation method thereof |
-
2020
- 2020-12-31 CN CN202011642308.8A patent/CN112641658A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20190040339A1 (en) * | 2016-01-29 | 2019-02-07 | Colgate-Palmolive Company | Cleansing Compositions |
| CN110585087A (en) * | 2019-10-11 | 2019-12-20 | 茂名市瑜丰沉香创意产业有限公司 | Agilawood essential oil shampoo and preparation method thereof |
Non-Patent Citations (4)
| Title |
|---|
| 李东光，等: "《实用化妆品制造技术》", 30 April 1998, 金盾出版社 * |
| 潮妈妈: "唯伊丝洗发水好不好用？唯伊丝柔顺大粉瓶洗发水怎么样", 《HTTP://WWW.FASHIONMM.CN/HUAZHUANGPIN/2020/0710/22508.HTML》 * |
| 电子凭证-国产非特殊用途化妆品备案信息服务平台: "香依伴海盐均衡洗发露", 《HTTP://FTBA.NMPA.GOV.CN:8181/FTBAN/ITOWNET/HZP_BA/FW/PZ.JSP?PROCESSID=20200724154710EHTNS&NID=20200724154710EHTNS》 * |
| 黄楼生活网: "敷完生理盐水要洗脸吗 生理盐水敷脸后需洗吗", 《HTTPS://WWW.HUANGLOUBLOG.COM/SHCS/40321.HTML》 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114869801A (en) * | 2022-04-26 | 2022-08-09 | 彭氏(惠州)实业发展有限公司 | Hair care composition |
| CN114869801B (en) * | 2022-04-26 | 2024-03-22 | 彭氏(惠州)实业发展有限公司 | Hair care compositions |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN106038330B (en) | A kind of mildy wash and preparation method thereof | |
| CN102716044B (en) | Low-stimulation hair-cleaning compound | |
| CN111110577B (en) | Mild mite-removing itching-relieving shower gel and preparation method thereof | |
| CN1270688C (en) | Emulsified salt type skin-cleaning product and its preparation method | |
| CN109568187B (en) | Multi-effect nursing bath foam for pet dogs and preparation method thereof | |
| US7125544B2 (en) | Kit for promoting the growth of human hair and its method of use | |
| CN108852940A (en) | A kind of anti-hair shampoo and preparation method thereof | |
| CN112107533A (en) | Composition with effects of controlling oil, tendering skin and collecting fine pores and preparation method and application thereof | |
| CN109875951B (en) | Hair cleaning care solution | |
| CN112641658A (en) | Oil control shampoo and preparation method thereof | |
| CN113908095A (en) | Oil-control moisturizing hair composition containing double proteins | |
| CN116509774A (en) | Anti-dandruff shampoo preparation containing sweet wormwood herb extract and preparation method thereof | |
| CN108158921B (en) | Plant composition containing tea bran and rosemary as well as preparation method and application of plant composition | |
| CN112336662B (en) | Soothing shower gel and preparation method and application thereof | |
| CN113081889A (en) | Three-stage washing and protecting integrated composition | |
| CN110237008A (en) | A kind of grape pip elastic force mildy wash and preparation method thereof | |
| CN116585245B (en) | Shampoo containing ginger root extract and preparation method thereof | |
| CN115590798B (en) | Double-component bath lotion with anti-allergy and skin tendering effects and preparation method thereof | |
| CN114795989B (en) | Composition with hair care and hair growth functions and preparation thereof | |
| CN113616558B (en) | Plant extract composition and application thereof | |
| CN115444766B (en) | Bi-component shampoo with scalp nourishing effect and preparation method thereof | |
| CN115414272B (en) | Female bubble shampoo without irritation in eyes and preparation method thereof | |
| TWI704930B (en) | Set for deep cleaning pores and method for deep cleaning pores | |
| CN114099386A (en) | Bacteriostatic and fragrance-releasing foam shampoo | |
| CN115487094A (en) | Sleep-aiding skin-care cleaning composition and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20210413 |