CN112315893A - Beautifying cream mask with whitening and moisturizing effects and preparation method thereof - Google Patents
Beautifying cream mask with whitening and moisturizing effects and preparation method thereof Download PDFInfo
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- CN112315893A CN112315893A CN202011441251.5A CN202011441251A CN112315893A CN 112315893 A CN112315893 A CN 112315893A CN 202011441251 A CN202011441251 A CN 202011441251A CN 112315893 A CN112315893 A CN 112315893A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
- A61K8/988—Honey; Royal jelly, Propolis
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/673—Vitamin B group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/673—Vitamin B group
- A61K8/675—Vitamin B3 or vitamin B3 active, e.g. nicotinamide, nicotinic acid, nicotinyl aldehyde
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/676—Ascorbic acid, i.e. vitamin C
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/736—Chitin; Chitosan; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
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Abstract
The invention relates to a beautifying cream mask with whitening and moisturizing effects and a preparation method thereof. The whitening and moisturizing facial mask is prepared by taking the bletilla jelly dry powder, the pearl powder, the chitosan, the yam and propolis zymocyte powder, the aloe extract and the vitamins as raw materials and proportioning according to a proper weight ratio, and has good whitening, freckle removing and moisturizing effects, the regeneration of skin cells is promoted, the skin aging is delayed, the skin elasticity is effectively increased, and the skin is fine, smooth and glossy; meanwhile, the cosmetic can effectively adsorb heavy metals excreted to subcutaneous deep layers, solves the problem of heavy metal residue caused by long-term use of cosmetics, has a good protective effect on skin, promotes metabolism, and improves the absorption of skin on nutrient components; the facial mask of the facial mask cream disclosed by the invention uses natural components as raw materials, is safe, has no side effect, and can be used as a facial mask skin care product for a long time.
Description
Technical Field
The invention belongs to the technical field of cosmetics, and particularly relates to a beautifying cream mask with whitening and moisturizing effects and a preparation method thereof.
Background
With the improvement of life quality, people are more and more urgent to pursue beauty, so that the variety of cosmetics is more and more, and the facial mask is an important member of the cosmetics. At present, the facial masks are various in types, and are divided into a patch facial mask, a tear facial mask and a gel facial mask. The gel mask is a gel paste which is easy to be uniformly applied to the face, can block the contact of the skin of the face and the air, effectively prevents the evaporation of water, increases the humidity of the horny layer and softens the horny layer; can also dilate pores on the surface of the skin, and is beneficial to the absorption of nutrient components.
Bletilla striata (Bletilla striata) is a perennial herb of Bletilla striata in Orchidaceae, and is a commonly used Chinese medicinal material in China. The dried tuber is used as a medicine, has the effects of stopping bleeding and astringing, clearing heat and promoting diuresis, and reducing swelling and promoting granulation, and is mainly used for treating lung injury hemoptysis, surgical wounds, ulcer pyogenic infections and the like. The rhizoma bletillae is mainly produced in Guizhou, Sichuan, Hubei and other places, and has the highest yield and the highest quality in Guizhou, wherein Guizhou Anlong and Xingzhen are the most suitable planting areas for the rhizoma bletillae. Rhizoma bletillae is a rare hemostatic material, and the pharmacological effects of the rhizoma bletillae mainly comprise antibiosis, blood circulation promotion and hemostasis, wound healing promotion, gastrointestinal tract mucous membrane injury repair promotion, bone marrow hematopoiesis promotion, virus resistance, tumor resistance and the like. The chemical components of the bletilla striata mainly comprise bibenzyl, dihydrophenanthrene, diphenanthrene ether, phenanthropyran, bibenzyl glucoside, polysaccharide, steroid, triterpene, lignin, anthraquinone and the like, and the bletilla striata is rich in chemical components and various in types.
Rhizoma Bletillae has effects of improving local blood circulation, promoting epithelial cell repair, stopping bleeding, healing sore, moistening skin and promoting granulation. Bletilla striata is a good medicine for beauty treatment from the old and is known as whitening fairy, so the bletilla striata is often used in skin care products with the functions of stopping bleeding, eliminating scars, whitening and the like. However, some of the skin care products in the prior art contain a large amount of chemical synthetic substances, and long-term use of the products cannot solve the problem of skin, but also increase the burden of skin and cause some allergic reactions.
Disclosure of Invention
In order to solve the problems in the prior art, the invention provides a beautifying cream mask with whitening and moisturizing effects and a preparation method thereof. The facial mask of the facial mask cream has good whitening, freckle removing and moisturizing effects, can promote skin cell regeneration, delay skin aging, effectively increase skin elasticity, and enable skin to be fine, smooth and glossy, is safe and free of any side effect due to the use of natural components, and can be used as a facial mask skin care product for a long time.
The technical scheme adopted by the invention is as follows:
a facial mask of a beautifying cream with whitening and moisturizing effects comprises the following raw material components:
15-25 parts of bletilla striata gel lyophilized powder, 2-8 parts of pearl powder, 1-3 parts of chitosan, 1-3 parts of yam and propolis zymocyte powder, 1-5 parts of aloe extract and 0.1-2 parts of vitamin.
Further preferably, the skin-beautifying cream mask with the skin-whitening and moisturizing effects comprises the following raw material components:
20 parts of bletilla striata gel lyophilized powder, 5 parts of pearl powder, 2 parts of chitosan, 2 parts of yam and propolis zymocyte powder, 3 parts of aloe extract and 1 part of vitamin.
The bletilla striata gel dry powder is prepared by the following method:
(S1) drying and crushing rhizoma bletillae tubers to obtain rhizoma bletillae fine powder, adding ethanol into the rhizoma bletillae fine powder for reflux extraction, and filtering to obtain medicine residues after extraction is finished;
(S2) after the ethanol contained in the medicine residues is completely volatilized, adding water for heating and leaching, and filtering after leaching to obtain filtrate;
(S3) passing the filtrate through an ion exchange resin and eluting with deionized water, and collecting the eluate;
(S4) concentrating the eluent, and sequentially carrying out alcohol precipitation, filtration, washing and freeze drying to obtain the bletilla striata freeze-dried powder.
The yam propolis zymocyte powder is prepared by the following method:
(a) drying and crushing 1-3 parts by weight of Chinese yam to obtain Chinese yam fine powder;
(b) adding water into the yam fine powder, fully and uniformly mixing, adding 0.1-0.3 part by weight of propolis, and uniformly mixing to obtain a yam-propolis mixed solution;
(c) adding 0.05-0.1 part by weight of peptone, 0.01-0.02 part by weight of dipotassium hydrogen phosphate and 0.02-0.04 part by weight of magnesium sulfate heptahydrate into the yam and propolis mixed solution, fully mixing, sterilizing, inoculating a microbial agent, fermenting, sterilizing, and freeze-drying to obtain the yam and propolis zymocyte powder.
The microbial agent is a mixed microbial agent consisting of lactobacillus and yeast according to the mass ratio of 1-2: 1-2.
The vitamin is a mixture of vitamin C, vitamin B and vitamin E according to the mass ratio of 2:1: 1.
5-7% of nicotinamide by mass is also added into the mask.
The preparation method of the beauty cream mask with the whitening and moisturizing effects comprises the following steps:
(1) pulverizing Margarita powder and chitosan to obtain Margarita powder and chitosan powder, mixing to obtain a first mixture:
(2) taking the bletilla striata lyophilized powder and the yam propolis zymocyte powder, carrying out superfine grinding to obtain superfine powder of the bletilla striata lyophilized powder and superfine powder of the yam propolis zymocyte powder, and fully mixing to obtain a second mixture;
(3) and mixing the first mixture and the second mixture, adding the rest raw material components, uniformly mixing, adding warm water, homogenizing, and cooling to room temperature to obtain the skin beautifying cream mask with the effects of whitening and moisturizing.
In the step (1), the particle diameters of the pearl powder superfine powder and the chitosan superfine powder are 300-500 meshes;
in the step (2), the particle size of the ultrafine powder of the bletilla striata gel dry powder and the ultrafine powder of the yam propolis zymocyte powder is 300-500 meshes.
In the step (3), the homogenizing treatment is performed under the conditions of 800-900rpm for 4-6min, and then the rotation speed is reduced to 120-150rpm, and the treatment is performed at 120-150rpm for 10-20 min.
According to the facial mask, the yam and propolis zymocyte powder is adopted, so that the tyrosinase activity can be inhibited, the generation of melanin can be blocked, the inhibition activity of the bletilla jelly dry powder on tyrosinase can be improved, the synergy can be realized, and the whitening effect of the facial mask can be improved. And the fermented components in the yam and propolis zymocyte powder effectively promote the regeneration of skin cells, increase the skin elasticity and delay the skin aging.
According to the facial mask, the adopted pearl powder is rich in calcium carbonate, so that the chitosan can be promoted to play a better moisturizing and adsorbing effect, heavy metals excreted to the subcutaneous deep layer can be effectively adsorbed, the problem of heavy metal residue caused by long-term use of cosmetics is solved, a good protective effect is achieved on skin, metabolism is promoted, and the skin nutrition absorption effect is improved.
The beautifying cream mask disclosed by the invention can effectively inhibit the irritation of nicotinamide to the skin, improve the appropriate use concentration of the nicotinamide and enhance the whitening effect under the combined action of the aloe extract and the vitamins serving as raw material components.
The invention has the beneficial effects that:
according to the beautifying cream mask with whitening and moisturizing effects, the bletilla jelly dry powder, the pearl powder, the chitosan, the yam and propolis zymocyte powder, the aloe extract and the vitamins are adopted as raw materials and are proportioned according to a proper weight ratio, so that the finally prepared beautifying cream mask has good whitening, freckle removing and moisturizing effects, can promote skin cell regeneration, delay skin aging, effectively increase skin elasticity, and enable the skin to be fine, smooth and glossy; meanwhile, the cosmetic can effectively adsorb heavy metals excreted to subcutaneous deep layers, solves the problem of heavy metal residue caused by long-term use of cosmetics, has a good protective effect on skin, promotes metabolism, and improves the absorption of skin on nutrient components; the facial mask of the facial mask cream disclosed by the invention uses natural components as raw materials, is safe, has no side effect, and can be used as a facial mask skin care product for a long time.
Detailed Description
In order to make the objects, technical solutions and advantages of the present invention more apparent, the technical solutions of the present invention will be described in detail below. It is to be understood that the described embodiments are merely exemplary of the invention, and not restrictive of the full scope of the invention. All other embodiments, which can be derived by a person skilled in the art from the examples given herein without any inventive step, are within the scope of the present invention.
In the following examples, 100g is represented by 1 part by weight. The starting materials used in the following examples and comparative examples were all commercially available products except for the specific ones.
Example 1
The embodiment provides a beauty cream mask with whitening and moisturizing effects, which comprises the following raw material components:
15 parts of bletilla striata gel freeze-dried powder;
8 parts of pearl powder;
1 part by weight of chitosan;
3 parts of yam and propolis zymocyte powder;
1 part by weight of aloe extract;
2 parts by weight of a mixture consisting of vitamin C, vitamin B and vitamin E according to a mass ratio of 2:1: 1.
The bletilla striata gel dry powder is prepared by the following method:
(S1) drying and crushing rhizoma bletillae tubers to obtain fine rhizoma bletillae powder with the particle size of 80nm, adding 2 times of ethanol with the mass and volume concentration of 80% into the fine rhizoma bletillae powder, carrying out reflux extraction under the heating condition, and filtering after extraction is finished to obtain medicine residues;
(S2) after the ethanol contained in the medicine residues is completely volatilized, adding 2 times of water by mass, heating and leaching for 5 hours at 100 ℃, and filtering after leaching is finished to obtain filtrate;
(S3) passing the filtrate through macroporous weakly-basic anion resin and macroporous weakly-acidic cation resin in sequence, eluting with deionized water, and collecting the eluate;
(S4) concentrating the eluent to the relative density of 1.1, adding 80% ethanol by volume concentration for alcohol precipitation, filtering the precipitate, washing the precipitate with alcohol, and freeze-drying to obtain the bletilla striata freeze-dried powder.
The yam propolis zymocyte powder is prepared by the following method:
(a) taking 1 part by weight of Chinese yam, drying and crushing to obtain Chinese yam fine powder with the particle size of 80 meshes;
(b) adding 2 times of water by mass into the yam fine powder, fully and uniformly mixing, adding 0.1 part by weight of propolis, and uniformly mixing to obtain yam and propolis mixed solution;
(c) adding 0.05 weight part of peptone, 0.01 weight part of dipotassium hydrogen phosphate and 0.02 weight part of magnesium sulfate heptahydrate into the yam and propolis mixed solution, fully mixing, sterilizing, inoculating a lactobacillus and yeast mixed microbial inoculum (the mass ratio of lactobacillus to yeast is 1:2) according to the inoculation amount of 2%, fermenting for 60 hours at 25 ℃, sterilizing at high temperature, and freeze-drying to obtain yam and propolis zymocyte powder.
Further, the embodiment provides a preparation method of the facial mask cream with whitening and moisturizing effects, which comprises the following steps:
(1) pulverizing Margarita powder and chitosan into superfine powder with particle size of 300 meshes, and mixing to obtain a first mixture:
(2) taking the bletilla striata lyophilized powder and the yam propolis zymocyte powder, carrying out superfine grinding to obtain bletilla striata lyophilized powder superfine powder and the yam propolis zymocyte powder superfine powder which have the grain sizes of 300 meshes, and fully mixing to obtain a second mixture;
(3) and mixing the first mixture and the second mixture, adding the rest raw material components, uniformly mixing, adding 70 parts by weight of 60 ℃ warm water, homogenizing for 6min under the condition of 800rpm, then reducing the rotating speed to 120rpm, treating for 20min at 120rpm, and reducing to room temperature to obtain the beautifying cream mask with whitening and moisturizing effects.
Example 2
The embodiment provides a beauty cream mask with whitening and moisturizing effects, which comprises the following raw material components:
25 parts of bletilla striata gel freeze-dried powder;
2 parts of pearl powder;
3 parts of chitosan;
1 part of yam and propolis zymocyte powder;
5 parts by weight of aloe extract;
0.1 part of a mixture of vitamin C, vitamin B and vitamin E according to the mass ratio of 2:1: 1.
The bletilla striata gel dry powder is prepared by the following method:
(S1) drying and crushing rhizoma bletillae tubers to obtain rhizoma bletillae fine powder with the particle size of 120nm, adding 3 times of ethanol with the mass and volume concentration of 95% into the rhizoma bletillae fine powder, carrying out reflux extraction under the heating condition, and filtering after extraction is finished to obtain medicine residues;
(S2) after the ethanol contained in the dregs of a decoction is completely volatilized, adding 8 times of mass water, heating and leaching at 82 ℃ for 5-8h, and filtering after leaching is finished to obtain filtrate;
(S3) passing the filtrate through macroporous weakly-basic anion resin and macroporous weakly-acidic cation resin in sequence, eluting with deionized water, and collecting the eluate;
(S4) concentrating the eluent to the relative density of 1.3, adding ethanol with the volume concentration of 95% for alcohol precipitation, filtering the precipitate, washing the precipitate with alcohol, and freeze-drying to obtain the bletilla striata freeze-dried powder.
The yam propolis zymocyte powder is prepared by the following method:
(a) taking 3 parts by weight of Chinese yam, drying and crushing to obtain Chinese yam fine powder with the particle size of 120 meshes;
(b) adding 4 times of water by mass into the yam fine powder, fully and uniformly mixing, adding 0.3 part by weight of propolis, and uniformly mixing to obtain a yam-propolis mixed solution;
(c) adding 0.1 weight part of peptone, 0.02 weight part of dipotassium hydrogen phosphate and 0.04 weight part of magnesium sulfate heptahydrate into the yam and propolis mixed solution, fully mixing, sterilizing, inoculating a lactobacillus and yeast mixed microbial inoculum (the mass ratio of lactobacillus to yeast is 2:1) according to the inoculation amount of 3%, fermenting for 48 hours at 35 ℃, sterilizing at high temperature, and freeze-drying to obtain yam and propolis zymocyte powder.
Further, the embodiment provides a preparation method of the facial mask cream with whitening and moisturizing effects, which comprises the following steps:
(1) pulverizing Margarita powder and chitosan into superfine powder with particle size of 500 meshes, and mixing to obtain a first mixture:
(2) taking the bletilla striata freeze-dried powder and the Chinese yam and propolis zymocyte powder, carrying out superfine grinding to obtain superfine powder of the bletilla striata freeze-dried powder and the Chinese yam and propolis zymocyte powder which have the particle sizes of 500 meshes, and fully mixing the superfine powder to obtain a second mixture;
(3) and mixing the first mixture and the second mixture, adding the rest raw material components, uniformly mixing, adding 63.9 parts by weight of warm water at 80 ℃, homogenizing for 4min at 900rpm, reducing the rotation speed to 150rpm, treating for 10min at 150rpm, and reducing to room temperature to obtain the beautifying cream mask with whitening and moisturizing effects.
Example 3
The embodiment provides a beauty cream mask with whitening and moisturizing effects, which comprises the following raw material components:
20 parts of bletilla striata gel freeze-dried powder;
5 parts of pearl powder;
2 parts of chitosan;
2 parts of yam and propolis zymocyte powder;
3 parts of aloe extract;
1 part by weight of a mixture of vitamin C, vitamin B and vitamin E in a mass ratio of 2:1: 1;
nicotinamide, 7 parts by weight.
The bletilla striata gel dry powder is prepared by the following method:
(S1) drying and crushing rhizoma bletillae tubers to obtain rhizoma bletillae fine powder with the particle size of 100nm, adding 2.5 times of ethanol with the volume concentration of 90% into the rhizoma bletillae fine powder, carrying out reflux extraction under the heating condition, and filtering after the extraction is finished to obtain medicine residues;
(S2) after the ethanol contained in the medicine residues is completely volatilized, adding 5 times of mass water, heating and leaching at 90 ℃ for 6 hours, and filtering after leaching is finished to obtain filtrate;
(S3) passing the filtrate through macroporous weakly-basic anion resin and macroporous weakly-acidic cation resin in sequence, eluting with deionized water, and collecting the eluate;
(S4) concentrating the eluent to the relative density of 1.2, adding ethanol with the volume concentration of 90% for alcohol precipitation, filtering the precipitate, washing the precipitate with alcohol, and freeze-drying to obtain the bletilla striata freeze-dried powder.
The yam propolis zymocyte powder is prepared by the following method:
(a) taking 2 parts by weight of Chinese yam, drying and crushing to obtain Chinese yam fine powder with the particle size of 100 meshes;
(b) adding 3 times of water by mass into the yam fine powder, fully and uniformly mixing, adding 0.2 part by weight of propolis, and uniformly mixing to obtain a yam-propolis mixed solution;
(c) adding 0.075 weight part of peptone, 0.015 weight part of dipotassium phosphate and 0.03 weight part of magnesium sulfate heptahydrate into the yam and propolis mixed solution, fully mixing, sterilizing, inoculating a lactobacillus and yeast mixed microbial inoculum (the mass ratio of lactobacillus to yeast is 1:1) according to the inoculation amount of 2.5%, fermenting at 30 ℃ for 54h, sterilizing at high temperature, and freeze-drying to obtain yam and propolis zymocyte powder.
Further, the embodiment provides a preparation method of the facial mask cream with whitening and moisturizing effects, which comprises the following steps:
(1) pulverizing Margarita powder and chitosan into superfine powder with particle size of 400 meshes, and mixing to obtain a first mixture:
(2) taking the bletilla striata freeze-dried powder and the Chinese yam and propolis zymocyte powder, carrying out superfine grinding to obtain superfine powder of the bletilla striata freeze-dried powder and the Chinese yam and propolis zymocyte powder which have the particle sizes of 400 meshes, and fully mixing the superfine powder to obtain a second mixture;
(3) and mixing the first mixture and the second mixture, adding the rest raw material components, uniformly mixing, adding 60 parts by weight of warm water at 70 ℃, homogenizing for 5min under the condition of 850rpm, then reducing the rotating speed to 135rpm, treating for 15min at 135rpm, and reducing to room temperature to obtain the beautifying cream mask with whitening and moisturizing effects.
Example 4
The embodiment provides a beauty cream mask with whitening and moisturizing effects, which comprises the following raw material components:
20 parts of bletilla striata gel freeze-dried powder;
5 parts of pearl powder;
2 parts of chitosan;
2 parts of yam and propolis zymocyte powder;
3 parts of aloe extract;
1 part by weight of a mixture of vitamin C, vitamin B and vitamin E in a mass ratio of 2:1: 1;
6 parts of nicotinamide.
The bletilla striata gel dry powder is prepared by the following method:
(S1) drying and crushing rhizoma bletillae tubers to obtain rhizoma bletillae fine powder with the particle size of 100nm, adding 2.5 times of ethanol with the volume concentration of 90% into the rhizoma bletillae fine powder, carrying out reflux extraction under the heating condition, and filtering after the extraction is finished to obtain medicine residues;
(S2) after the ethanol contained in the medicine residues is completely volatilized, adding 5 times of mass water, heating and leaching at 90 ℃ for 6 hours, and filtering after leaching is finished to obtain filtrate;
(S3) passing the filtrate through macroporous weakly-basic anion resin and macroporous weakly-acidic cation resin in sequence, eluting with deionized water, and collecting the eluate;
(S4) concentrating the eluent to the relative density of 1.2, adding ethanol with the volume concentration of 90% for alcohol precipitation, filtering the precipitate, washing the precipitate with alcohol, and freeze-drying to obtain the bletilla striata freeze-dried powder.
The yam propolis zymocyte powder is prepared by the following method:
(a) taking 2 parts by weight of Chinese yam, drying and crushing to obtain Chinese yam fine powder with the particle size of 100 meshes;
(b) adding 3 times of water by mass into the yam fine powder, fully and uniformly mixing, adding 0.2 part by weight of propolis, and uniformly mixing to obtain a yam-propolis mixed solution;
(c) adding 0.075 weight part of peptone, 0.015 weight part of dipotassium phosphate and 0.03 weight part of magnesium sulfate heptahydrate into the yam and propolis mixed solution, fully mixing, sterilizing, inoculating a lactobacillus and yeast mixed microbial inoculum (the mass ratio of lactobacillus to yeast is 1:1) according to the inoculation amount of 2.5%, fermenting at 30 ℃ for 54h, sterilizing at high temperature, and freeze-drying to obtain yam and propolis zymocyte powder.
Further, the embodiment provides a preparation method of the facial mask cream with whitening and moisturizing effects, which comprises the following steps:
(1) pulverizing Margarita powder and chitosan into superfine powder with particle size of 400 meshes, and mixing to obtain a first mixture:
(2) taking the bletilla striata freeze-dried powder and the Chinese yam and propolis zymocyte powder, carrying out superfine grinding to obtain superfine powder of the bletilla striata freeze-dried powder and the Chinese yam and propolis zymocyte powder which have the particle sizes of 400 meshes, and fully mixing the superfine powder to obtain a second mixture;
(3) and mixing the first mixture and the second mixture, adding the rest raw material components, uniformly mixing, adding 61 parts by weight of warm water at 70 ℃, homogenizing for 5min under the condition of 850rpm, then reducing the rotating speed to 135rpm, treating for 15min at 135rpm, and reducing to room temperature to obtain the beautifying cream mask with whitening and moisturizing effects.
Example 5
The embodiment provides a beauty cream mask with whitening and moisturizing effects, which comprises the following raw material components:
20 parts of bletilla striata gel freeze-dried powder;
5 parts of pearl powder;
2 parts of chitosan;
2 parts of yam and propolis zymocyte powder;
3 parts of aloe extract;
1 part by weight of a mixture of vitamin C, vitamin B and vitamin E in a mass ratio of 2:1: 1;
5 parts of nicotinamide.
The bletilla striata gel dry powder is prepared by the following method:
(S1) drying and crushing rhizoma bletillae tubers to obtain rhizoma bletillae fine powder with the particle size of 100nm, adding 2.5 times of ethanol with the volume concentration of 90% into the rhizoma bletillae fine powder, carrying out reflux extraction under the heating condition, and filtering after the extraction is finished to obtain medicine residues;
(S2) after the ethanol contained in the medicine residues is completely volatilized, adding 5 times of mass water, heating and leaching at 90 ℃ for 6 hours, and filtering after leaching is finished to obtain filtrate;
(S3) passing the filtrate through macroporous weakly-basic anion resin and macroporous weakly-acidic cation resin in sequence, eluting with deionized water, and collecting the eluate;
(S4) concentrating the eluent to the relative density of 1.2, adding ethanol with the volume concentration of 90% for alcohol precipitation, filtering the precipitate, washing the precipitate with alcohol, and freeze-drying to obtain the bletilla striata freeze-dried powder.
The yam propolis zymocyte powder is prepared by the following method:
(a) taking 2 parts by weight of Chinese yam, drying and crushing to obtain Chinese yam fine powder with the particle size of 100 meshes;
(b) adding 3 times of water by mass into the yam fine powder, fully and uniformly mixing, adding 0.2 part by weight of propolis, and uniformly mixing to obtain a yam-propolis mixed solution;
(c) adding 0.075 weight part of peptone, 0.015 weight part of dipotassium phosphate and 0.03 weight part of magnesium sulfate heptahydrate into the yam and propolis mixed solution, fully mixing, sterilizing, inoculating a lactobacillus and yeast mixed microbial inoculum (the mass ratio of lactobacillus to yeast is 1:1) according to the inoculation amount of 2.5%, fermenting at 30 ℃ for 54h, sterilizing at high temperature, and freeze-drying to obtain yam and propolis zymocyte powder.
Further, the embodiment provides a preparation method of the facial mask cream with whitening and moisturizing effects, which comprises the following steps:
(1) pulverizing Margarita powder and chitosan into superfine powder with particle size of 400 meshes, and mixing to obtain a first mixture:
(2) taking the bletilla striata freeze-dried powder and the Chinese yam and propolis zymocyte powder, carrying out superfine grinding to obtain superfine powder of the bletilla striata freeze-dried powder and the Chinese yam and propolis zymocyte powder which have the particle sizes of 400 meshes, and fully mixing the superfine powder to obtain a second mixture;
(3) and mixing the first mixture and the second mixture, adding the rest raw material components, uniformly mixing, adding 62 parts by weight of warm water at 70 ℃, homogenizing for 5min under the condition of 850rpm, then reducing the rotating speed to 135rpm, treating for 15min at 135rpm, and reducing to room temperature to obtain the beautifying cream mask with whitening and moisturizing effects.
Comparative example 1
The facial mask of the facial cream provided by the comparative example is different from the facial mask of the example 3 only in that the yam propolis zymophyte powder is not added in the raw materials, and other raw materials and the preparation method are the same.
Comparative example 2
The facial mask of the facial cream provided by the comparative example is different from that of example 3 only in that the aloe extract is not added to the raw materials, and other raw materials and preparation methods are the same.
Comparative example 3
The facial mask of the facial cream provided by the comparative example is different from the facial mask of the example 3 only in that the raw materials are not added with vitamins, and other raw materials and preparation methods are the same.
Comparative example 4
The facial mask of the facial beautifying cream provided by the comparative example is different from the facial mask of the example 3 only in that pearl powder is not added to the raw materials, and other raw materials and preparation methods are the same.
Examples of the experiments
1. Whitening effect detection
The whitening effects of the facial mask of the beauty creams prepared in examples 1-3 and comparative examples 1-4 were evaluated, 70 women with speckles on the face and dark skin color were invited as volunteers, the volunteers were used 3 times a week for one month continuously, 10 volunteers were selected for each facial mask sample for trial use, and the whitening effects were classified into three grades.
The whitening effect is obvious: the skin is obviously whitened, spots on the face are lightened and reduced, and the skin is moist and bright;
the whitening effect is general: the skin becomes white and not obvious, the spots on the face begin to fade but become small and not obvious, and the skin is moist and bright;
the whitening effect is not changed: the skin did not whiten, nor did the face blemishes show signs of thinning or lightening.
The results are shown in Table 1.
TABLE 1 whitening Effect test results
Sample (I) | Is obvious | In general | Without change |
Example 1 | 9 | 1 | 0 |
Example 2 | 9 | 1 | 0 |
Example 3 | 10 | 0 | 0 |
Comparative example 1 | 5 | 3 | 2 |
Comparative example 2 | 6 | 3 | 1 |
Comparative example 3 | 6 | 3 | 1 |
Comparative example 4 | 7 | 2 | 1 |
As can be seen from table 1, the whitening effect of the facial mask cream prepared by the methods described in examples 1 to 3 of the present invention is better, particularly, the whitening effect of the facial mask cream prepared by the method described in example 3 is the best, while the whitening effect of the facial mask prepared by the methods described in comparative examples 1 to 4 is not ideal, so that the raw material components of the present invention exert a synergistic effect, and the added nicotinamide component can exert a synergistic effect with other components, so as to effectively improve the whitening effect of the facial mask.
2. Water replenishment effect detection
In addition, 70 women with dry and spotty skin and dark skin were invited to the test subjects and randomly divided into 7 groups, and the beauty cream masks prepared in examples 1 to 3 and comparative examples 1 to 4 were tried respectively. The method comprises the following steps of cleaning the face of a volunteer with clear water, testing the moisture content of the skin of the forehead, the left face, the right face and the chin respectively by using a skin moisture detector of Ficus Keel SK-III, taking an arithmetic average value, uniformly coating the facial mask on the face by using the facial mask of the facial mask beautifying cream, wiping off the facial mask after using the facial mask for 20min, respectively testing the moisture content of the skin of the forehead, the left face, the right face and the chin respectively by using the skin moisture detector after using the facial mask for 12h, and taking the arithmetic average value. The results were arithmetically averaged for each group of 10 volunteers. The average increase and decrease rate of the moisture content of the skin after 20min and 12h is calculated, and the result is shown in Table 2.
The skin moisture content increase and decrease rate after 20min of using the facial mask is the average skin moisture after 20min of using the facial mask-the average skin moisture before using the facial mask.
After the mask is used for 12 hours, the skin moisture content increase and decrease rate is equal to the average moisture of the skin after the mask is used for 12 hours, and the average moisture of the skin before the mask is used.
TABLE 2 skin moisture content test results using different masks
As can be seen from table 2, the moisturizing effect of the facial mask cream in examples 1 to 3 of the present invention is relatively good, especially, the moisturizing effect of the facial mask cream prepared by the method in example 3 is the best, while the moisturizing effect of the facial mask prepared by the method in comparative examples 1 to 4 is relatively poor, so that the raw material components of the present invention exert the synergistic effect, and the added niacinamide component can exert the synergistic effect with other components to enhance the moisturizing effect of the facial mask as a whole.
The present invention is not limited to the above-mentioned preferred embodiments, and any other products in various forms can be obtained by anyone in the light of the present invention, but any changes in the shape or structure thereof, which have the same or similar technical solutions as those of the present application, fall within the protection scope of the present invention.
Claims (10)
1. The beautifying cream mask with the whitening and moisturizing effects is characterized by comprising the following raw material components:
15-25 parts of bletilla striata gel lyophilized powder, 2-8 parts of pearl powder, 1-3 parts of chitosan, 1-3 parts of yam and propolis zymocyte powder, 1-5 parts of aloe extract and 0.1-2 parts of vitamin.
2. The beauty cream mask with whitening and moisturizing effects as claimed in claim 1, which is characterized by comprising the following raw material components:
20 parts of bletilla striata gel lyophilized powder, 5 parts of pearl powder, 2 parts of chitosan, 2 parts of yam and propolis zymocyte powder, 3 parts of aloe extract and 1 part of vitamin.
3. The beauty cream mask with the whitening and moisturizing effects as claimed in claim 1, is characterized in that the bletilla striata gel lyophilized powder is prepared by the following method:
(S1) drying and crushing rhizoma bletillae tubers to obtain rhizoma bletillae fine powder, adding ethanol into the rhizoma bletillae fine powder for reflux extraction, and filtering to obtain medicine residues after extraction is finished;
(S2) after the ethanol contained in the medicine residues is completely volatilized, adding water for heating and leaching, and filtering after leaching to obtain filtrate;
(S3) passing the filtrate through an ion exchange resin and eluting with deionized water, and collecting the eluate;
(S4) concentrating the eluent, and sequentially carrying out alcohol precipitation, filtration, washing and freeze drying to obtain the bletilla striata freeze-dried powder.
4. The beauty cream mask with whitening and moisturizing effects as claimed in claim 1, wherein the yam propolis zymocyte powder is prepared by the following method:
(a) drying and crushing 1-3 parts by weight of Chinese yam to obtain Chinese yam fine powder;
(b) adding water into the yam fine powder, fully and uniformly mixing, adding 0.1-0.3 part by weight of propolis, and uniformly mixing to obtain a yam-propolis mixed solution;
(c) adding 0.05-0.1 part by weight of peptone, 0.01-0.02 part by weight of dipotassium hydrogen phosphate and 0.02-0.04 part by weight of magnesium sulfate heptahydrate into the yam and propolis mixed solution, fully mixing, sterilizing, inoculating a microbial agent, fermenting, sterilizing, and freeze-drying to obtain the yam and propolis zymocyte powder.
5. The beauty cream mask with whitening and moisturizing effects as claimed in claim 4, wherein the microbial agent is a mixed microbial agent consisting of lactobacillus and yeast at a mass ratio of 1-2: 1-2.
6. The beauty cream mask with the effects of whitening and moisturizing as claimed in claim 1, wherein the vitamin C, the vitamin B and the vitamin E are a mixture in a mass ratio of 2:1: 1.
7. The facial mask of the beautifying cream with the effects of whitening and moisturizing as claimed in claim 1, wherein 5-7% by mass of niacinamide is further added into the facial mask.
8. The preparation method of the beauty cream mask with whitening and moisturizing effects as claimed in claims 1 to 7, which is characterized by comprising the following steps:
(1) pulverizing Margarita powder and chitosan to obtain Margarita powder and chitosan powder, mixing to obtain a first mixture:
(2) taking the bletilla striata lyophilized powder and the yam propolis zymocyte powder, carrying out superfine grinding to obtain superfine powder of the bletilla striata lyophilized powder and superfine powder of the yam propolis zymocyte powder, and fully mixing to obtain a second mixture;
(3) and mixing the first mixture and the second mixture, adding the rest raw material components, uniformly mixing, adding warm water, homogenizing, and cooling to room temperature to obtain the skin beautifying cream mask with the effects of whitening and moisturizing.
9. The method according to claim 8, wherein in the step (1), the particle size of the ultrafine pearl powder and the ultrafine chitosan powder is 300-500 mesh;
in the step (2), the particle size of the ultrafine powder of the bletilla striata gel dry powder and the ultrafine powder of the yam propolis zymocyte powder is 300-500 meshes.
10. The method as claimed in claim 8, wherein in the step (3), the homogenizing treatment is performed under the conditions of 800-900rpm for 4-6min, and then the rotation speed is decreased to 120-150rpm, and the treatment is performed at 120-150rpm for 10-20 min.
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