CN112120987A - Roxburgh rose VC toothpaste and preparation method thereof - Google Patents

Abstract

The invention discloses roxburgh rose VC toothpaste and a preparation method thereof. Has the advantages that: the roxburgh rose is added into the toothpaste, so that impurities on teeth and gum can be cleaned, the problem of tooth oxidation is solved, the immunity of the teeth is enhanced, the health of periodontal tissues can be maintained, the decayed teeth are effectively prevented, the toothpaste can keep the oral cavity fresh, the teeth are bright and white, and the nutrients required by the periodontal tissues can be provided through vitamin C in the roxburgh rose stock solution; the addition of hydrated silica can improve the stability of the toothpaste, avoid the problems of water separation, oil separation, color change and the like, and the addition of sodium phytate can adjust the pH value of the toothpaste and improve the whitening effect of the toothpaste.

Description

Roxburgh rose VC toothpaste and preparation method thereof

Technical Field

The invention relates to the technical field of toothpaste, in particular to roxburgh rose VC toothpaste and a preparation method thereof.

Background

Toothpaste is a common cleaning product in daily life and has a long history. The toothpaste can remove films and dental plaques on the surfaces of teeth, has no stimulation and toxicity to oral mucosa, and is very important for oral cavity cleaning and oral cavity health care.

Along with the continuous development of science and technology, the requirements of people on toothpaste are more and more diversified, the requirements of the toothpaste on the market, such as tooth cleaning, breath freshening, gingival health protection, tooth brightening and whitening, and natural raw materials are required in the components of the toothpaste. The natural extract added into the toothpaste has a great challenge on the stability of the toothpaste, can cause the problems of water separation, oil separation, color change and the like of the toothpaste, and the pH value of the toothpaste is lower than the national standard requirement when the original Rosa roxburghii Tratt liquid is directly added into the toothpaste because the Rosa roxburghii Tratt is acidic.

Disclosure of Invention

The invention aims to solve the problems and provide roxburgh rose VC toothpaste and a preparation method thereof.

The invention realizes the purpose through the following technical scheme:

the roxburgh rose VC toothpaste is prepared from the following raw materials in parts by weight: 30-75g of sorbitol, 10-20g of hydrated silica, 1-2.5g of sodium lauryl sulfate, 0.2-1.5g of roxburgh rose stock solution, 0.5-1.5g of sodium phytate, 0.4-1.0g of cellulose gum, 0.2-0.5g of carrageenan, 0.1-2g of wetting agent, 0.1-0.5g of saccharin sodium, 0.1-0.5g of sodium benzoate, 0.01-0.1g of carrageen crispus extract, 0.01-0.1g of hydroxyapatite, 0.01-0.1g of xylitol, 0.01-0.1g of sodium lauroyl sarcosinate, 0.01-0.1g of sodium methyl ester, 0.01-0.1g of sodium bicarbonate and 0.01-0.1g of sodium ascorbyl phosphate.

Further, the feed is composed of the following raw materials by weight: 60g of sorbitol, 18g of hydrated silica, 2g of sodium lauryl sulfate, 0.5g of roxburgh rose stock solution, 1g of sodium phytate, 0.9g of cellulose gum, 0.5g of carrageenan, 1g of wetting agent, 0.18g of saccharin sodium, 0.3g of sodium benzoate, 0.1g of carrageen crispus extract, 0.1g of hydroxyapatite, 0.1g of xylitol, 0.1g of sodium lauroyl sarcosinate, 0.1g of sodium methyl ester, 0.1g of sodium bicarbonate and 0.05g of sodium ascorbyl phosphate.

Further, the water-saving paint also comprises 10-20g of water.

Further, 0.5-1.5g of essence is also included.

Furthermore, the paint also comprises pigment.

Further, the pigment includes CI-19140 (lemon yellow) 0.001-0.01g, and CI-15985 (sunset yellow) 0.001-0.01 g.

Further, the wetting agent is polyethylene glycol-8.

The invention also provides a preparation method for preparing the roxburgh rose VC toothpaste, which comprises the following steps:

s1, weighing the raw materials according to the weight;

s2, dissolving sodium phytate, saccharin sodium, sodium benzoate, xylitol, methyl ester sodium, sodium bicarbonate, ascorbic acid sodium phosphate, lemon yellow, and sunset yellow in water, and mixing with sorbitol and extractive solution of Chondrus crispus;

s3, mixing the essence with polyethylene glycol-8;

s4, uniformly mixing hydrated silica, sodium lauryl sulfate, cellulose gum, carrageenan and hydroxyapatite;

s5, mixing the mixture prepared in the steps S2, S3 and S4 with sodium lauroyl sarcosine, stirring for 30 minutes, adding the roxburgh rose stock solution, continuously mixing and stirring, and vacuumizing and degassing;

and S6, discharging paste, and filling into an aluminum plastic pipe.

The raw material efficacy and effect are as follows:

sorbitol (sugar) alcohol: sorbitol is also known as sorbitol and has the molecular formula C₆H₁₄O₆Is the main photosynthesis product of rosaceous plants. Is white hygroscopic powder or crystalline powder, tablet or granule, and has no odor. The melting point varied from 88 to 102 ℃ depending on the crystallization conditions, and the relative density was about 1.49. Readily soluble in water (1g in about 0.45mL water), slightly soluble in ethanol and acetic acid. Has cool sweet taste, sweetness about half of that of cane sugar, calorific value similar to that of cane sugar, and no dental caries when used as a sweetening agent. In the food industry, sorbitol solution with content of 69-71% is mostly used. Can be used as humectant for toothpaste, cosmetics, and tobacco. Is a substitute of glycerol, and has mild moisture retention and good taste. Can be used in combination with other moisturizers to achieve synergistic effect. Also used in the pharmaceutical industry as a raw material for the manufacture of vitamin C.

Hydrated silica: the material is one of extremely important high-tech superfine inorganic new materials, has special performances in the aspects of small particle size, large specific surface area, strong surface adsorption force, large surface energy, high chemical purity, good stability and dispersion performance, thermal resistance, electric resistance and the like, and can be used as an additive, a catalyst carrier, petrochemical industry, a decolorizing agent, a delustering agent, a rubber reinforcing agent, a plastic filling agent, an ink thickening agent, a metal soft polishing agent, an insulating and heat insulating filling agent, an electronic packaging material, a resin composite material, a high-grade daily cosmetic filling material, a spraying material, a medicine, environmental protection and other various fields.

Sodium lauryl sulfate: is an organic substance with a chemical formula of C₁₂H₂₅SO₄Na, white or light yellow powder, is soluble in water and is not sensitive to alkali and hard water. Has the advantages of decontamination, emulsification and excellent foaming power. Is an anionic surfactant which is slightly toxic to human bodies. Degree of biodegradation thereof>90％。

And (3) roxburgh rose: 1. enhancing the resistance of the body to infection; 2. preventing and resisting cancer; 3. treating scurvy; 4. lead removal effect; 5. anti-aging; 6. treating beriberi; 7. treating oral inflammation. Vitamin B2 (riboflavin) is one of the most deficient vitamins in chinese diets. Cheilitis and glossitis are common in the absence of B2. The daily requirement of male adult is 1.8mg, the daily requirement of female adult is 1.3mg, and the fructus Rosae Normalis juice contains Vb20 of 0.3mg/100g, and can be used for treating oral inflammation after a certain amount of fructus Rosae Normalis juice is taken; 8. it contains superoxide dismutase (SOD) and flavone. Therefore, the roxburgh rose can not only strengthen the spleen and stomach, tonify the kidney and strengthen yang, but also have the functions of enhancing the human body resistance, preventing cancer, maintaining beauty and keeping young, reducing the contents of cholesterol and triglyceride, and preventing hypertension, hyperlipidemia, hyperglycemia, cardiovascular and cerebrovascular diseases and the like.

Sodium phytate: can be widely used as antioxidant and color fixative for fruit and vegetable juice beverage, meat product, and marine product. The sodium phytate is white hygroscopic powder, and is easily soluble in water. The method is widely applied to the fields of medicine, food, daily chemicals, paint, coating, printing, metallurgy and other industries.

Cellulose gum: the cellulose gum has excellent thickening property under the conditions of low pH value and high temperature, and is used as a stabilizer to resist precipitation. The cellulose gum has the characteristics similar to xanthan gum, can improve the fluid adsorption capacity and the adsorption rate, stabilize an oil-in-water emulsion turbidity system and improve the mouthfeel. Can be mixed with water-soluble high molecular compound to obtain uniform solution with higher viscosity. Such as polyvinyl alcohol, starch ether, vegetable gum, etc.

Carrageenin: it is commonly used in the food industry as a thickener, gelling agent, suspending agent, emulsifier and stabilizer.

Polyethylene glycol-8: polyethylene glycol-8 is used as humectant and solvent in cosmetic. The composition is soft, and can be added into scrub cream after sufficient grinding to be used as a mild abrasive. And the addition of a trace amount of polyethylene glycol in the cosmetic helps to keep the product stable.

Sodium saccharin: a synthetic sweetener.

Sodium benzoate: it is mainly used as food preservative, and also used for preparing medicines, dyes, etc. Used in the pharmaceutical industry and plant genetic research, and also used as dye intermediate, bactericide and preservative. A preservative; an antimicrobial agent. Sodium benzoate is also an important acid-type food preservative. When used, the compound is converted into the effective form of benzoic acid. The range and amount of use is referred to benzoic acid. In addition, the compound can also be used as a preservative of feed. The product can be used as food additive (antiseptic), bactericide in pharmaceutical industry, mordant in dye industry, plasticizer in plastic industry, and intermediate for organic synthesis such as perfume. The compound is used as a cosolvent for serum bilirubin test, a food additive (preservative), a bactericide in the pharmaceutical industry, a mordant in the dye industry, a plasticizer in the plastic industry, and an intermediate for organic synthesis such as perfume.

Chondrus crispus extract: is a water-retaining and moisture-keeping raw material for cosmetics extracted from natural seaweed, and in the cosmetics, the surface activity and water absorbability of the raw material are used as an emulsifier and a stabilizer, so that the separation of suspended matters can be prevented, and the skin absorption is good. In addition, the aqueous solution of Chondrus crispus extract has good consistency and can be used as thickener for cosmetic. And simultaneously can lock water and promote skin absorption.

Hydroxyapatite: can realize chemical bond combination with organism tissue on an interface, has certain solubility in vivo, can release ions harmless to the organism, can participate in vivo metabolism, has stimulation or induction effect on hyperosteogeny, can promote the repair of defective tissue, shows bioactivity, is a main inorganic composition of bones and teeth of vertebrates, has the hydroxyapatite content of about 96 Wt.% (92 Vol.%) in human enamel and accounts for about 69 Wt.% (69 Wt.%). The hydroxyapatite has excellent biocompatibility and bioactivity, can be used as an induction factor of bones or teeth, and has better remineralization, desensitization and whitening effects on the teeth in the field of oral health care. Experiments prove that the HAP particles have good biocompatibility and high affinity with enamel, and the mineralized liquid can effectively form remineralization deposition, prevent calcium ions from losing, solve the problem of enamel demineralization and fundamentally prevent dental caries. The toothpaste containing HAP material has strong adsorption effect on salivary protein and dextran, can reduce dental plaque in oral cavity of patient, promote gingivitis healing, and has good prevention and treatment effect on dental caries and periodontal disease.

Xylitol: the anti-caries property of the xylitol has the best effect in all sweeteners, firstly, the xylitol can not be fermented and utilized by bacteria which generate caries in the oral cavity, and the growth of streptococcus and the generation of acid are inhibited; secondly, when the xylitol is chewed, the saliva secretion can be promoted, more saliva can wash bacteria in oral cavity and teeth, the concentration of basic amino acid and ammonia at saliva and decayed tooth spots can be increased, the decrease of the pH value in the oral cavity is slowed down, acidic substances which harm the teeth are neutralized and diluted, and the adsorption of the bacteria on the surfaces of the teeth is inhibited, so that the acid erosion of the teeth is reduced, the decayed teeth are prevented, the generation of dental plaque is reduced, and the teeth are consolidated; the xylitol has cool mouthfeel and better effect after being frozen, and can be used in refreshing cold drink, desserts, milk, coffee and other industries. Can also be used in health beverage, throat moistening medicine, and cough syrup; xylitol is a polyhydric alcohol, can be used as a moisture regulator for cosmetics, and has no irritation to human skin. For example: face lotions, cosmetic creams, lotions, and the like; xylitol has the functions of hygroscopicity and caries prevention, and liquid xylitol has good sweet taste, so that the xylitol can replace glycerin to be used as flavoring, antifreezing humectant and the like of cut tobacco, caries prevention toothpaste and mouthwash; xylitol is a functional sugar alcohol with anti-inflammatory and antibacterial effects.

Sodium lauroyl sarcosinate: (1) in the aspect of mineral flotation, the amino acid type anionic surfactant has good synergistic effect with a cationic surfactant to achieve higher flotation efficiency, and is a novel amino acid type anionic surfactant; (2) has the characteristics of washing, emulsification, infiltration, solubilization and the like; (3) excellent foamability, fine and durable foam, and is suitable for being used as raw materials of foaming agent, shampoo and shaving cream of toothpaste and cosmetics; (4) has antibacterial and bactericidal properties, mildew resistance, corrosion resistance and antistatic ability; (5) low toxicity and low irritation; (6) the biodegradability is good, and the environment is not polluted; (7) in the petroleum industry, the additive can be compounded into a thick oil viscosity reducer, an antirust agent, a heat stabilizer, a combustion promoter and the like; (8) in the biological aspect, the product can be used for RNA and DNA isolation, can be used as a dissolving agent in cell purification, can be used as an additive in the process of separating DNA from human serum, can also be added to increase the nitrogen fixation capacity of leguminous plant rhizobium, and has a plurality of applications in the immunochemistry aspect; (9) corrosion inhibitors, rust removers and the like are used in metal processing; (10) in the aspects of pharmacology and pharmacy: n-sodium lauroyl sarcosine can relieve the stimulation of vitamin E to skin, increase the absorption of vitamin, and increase the antibacterial property and durability of the eye ointment, and can be used as anesthetic additive and intermediate of anticancer drug; (11) in agrochemicals and bioregulators. The compound can be used as a pesticide blending agent to reduce the irritation and toxicity of the pesticide and increase the activity of the pesticide; (12) a lubricant additive; (13) the paint and the ink additive can increase the compatibility and the stability; (14) in the electroplating industry, the coating can be used as a polishing agent for a noble metal coating; (15) in the dye industry, the formation of exciplex between dyes is facilitated.

Sodium methyl ester: water-soluble preservatives, widely used in medicine, food, textile industry and other fields such as cosmetics, feed, daily industrial products, namely in dairy products, pickled products, beverages, fruit juices, jellies, cakes and the like.

Sodium bicarbonate: the sodium bicarbonate can be directly used as raw material in pharmaceutical industry for treating hyperacidity; in food processing, the carbon dioxide-containing aerated beverage is a loosening agent which is most widely applied, is used for producing biscuits, bread and the like, and is a generating agent of carbon dioxide in aerated beverages; can be compounded with alum to obtain alkaline fermentation powder, and can also be compounded with soda to obtain civil caustic soda; can also be used as butter preservative; the pharmaceutical industry is used as a raw material for antacids.

Sodium ascorbyl phosphate: the vitamin C is stable in property and water-soluble, has an antioxidant function, and also has a strong whitening effect.

The invention has the beneficial effects that: the roxburgh rose is added into the toothpaste, so that impurities on teeth and gum can be cleaned, the problem of tooth oxidation is solved, the immunity of the teeth is enhanced, the health of periodontal tissues can be maintained, decayed teeth are effectively prevented, the toothpaste can keep the oral cavity fresh, the teeth are bright and white, and the nutrients required by the periodontal tissues can be provided through vitamin C in the roxburgh rose stock solution; the addition of hydrated silica can improve the stability of the toothpaste, avoid the problems of water separation, oil separation, color change and the like, and the addition of sodium phytate can adjust the pH value of the toothpaste and improve the whitening effect of the toothpaste.

Detailed Description

The technical solutions of the present invention will be described clearly and completely with reference to the following embodiments, and it should be understood that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.

The first embodiment is as follows:

the roxburgh rose VC toothpaste is prepared from the following raw materials in parts by weight: 60g of sorbitol (sugar) alcohol, 18g of hydrated silica, 2g of sodium lauryl sulfate, 0.5g of roxburgh rose stock solution, 1g of sodium phytate, 0.9g of cellulose gum, 0.5g of carrageenan, 1g of wetting agent (polyethylene glycol-8), 0.18g of saccharin sodium, 0.3g of sodium benzoate, 0.1g of a Chondrus crispus extractive solution, 0.1g of hydroxyapatite, 0.1g of xylitol, 0.1g of sodium lauroyl sarcosinate, 0.1g of sodium methyl ester, 0.1g of sodium bicarbonate, 0.05g of sodium ascorbyl phosphate, 13.75g of water and 1g of essence; CI-19140 (lemon yellow) 0.005g, and CI-15985 (sunset yellow) 0.002 g.

Example two:

the roxburgh rose VC toothpaste is prepared from the following raw materials in parts by weight: 40g of sorbitol (sugar) alcohol, 12g of hydrated silica, 1.5g of sodium lauryl sulfate, 0.3g of roxburgh rose stock solution, 0.8g of sodium phytate, 0.5g of cellulose gum, 0.3g of carrageenan, 0.5g of wetting agent (polyethylene glycol-8), 0.12g of saccharin sodium, 0.1g of sodium benzoate, 0.2g of carrageenin extract, 0.02g of hydroxyapatite, 0.02g of xylitol, 0.02g of sodium lauroyl sarcosinate, 0.02g of sodium methyl ester, 0.02g of sodium bicarbonate, 0.02g of sodium ascorbyl phosphate, 11g of water and 1g of essence; CI-19140 (lemon yellow) 0.003g, and CI-15985 (sunset yellow) 0.002 g.

Example three:

the roxburgh rose VC toothpaste is prepared from the following raw materials in parts by weight: 70g of sorbitol (sugar) alcohol, 20g of hydrated silica, 2g of sodium lauryl sulfate, 1.5g of roxburgh rose stock solution, 1.2g of sodium phytate, 0.8g of cellulose gum, 0.5g of carrageenan, 1.8g of wetting agent (polyethylene glycol-8), 0.2g of saccharin sodium, 0.4g of sodium benzoate, 0.1g of Chondrus crispus extract, 0.08g of hydroxyapatite, 0.08g of xylitol, 0.08g of sodium lauroyl sarcosinate, 0.08g of sodium methyl ester, 0.08g of sodium bicarbonate, 0.08g of sodium ascorbyl phosphate, 18g of water and 1g of essence; CI-19140 (lemon yellow) 0.006g, and CI-15985 (sunset yellow) 0.006 g.

The invention also provides a preparation method for preparing the roxburgh rose VC toothpaste, which comprises the following steps:

s1, weighing the raw materials according to the weight;

s2, dissolving sodium phytate, saccharin sodium, sodium benzoate, xylitol, methyl ester sodium, sodium bicarbonate, ascorbic acid sodium phosphate, lemon yellow, and sunset yellow in water, and mixing with sorbitol and extractive solution of Chondrus crispus;

s3, mixing the essence with polyethylene glycol-8;

s4, uniformly mixing hydrated silica, sodium lauryl sulfate, cellulose gum, carrageenan and hydroxyapatite;

s5, mixing and stirring the mixture prepared in the steps S2, S3 and S4 and sodium lauroyl sarcosine for 30min under the condition of 2000r/min, keeping the paste temperature below 37 ℃, adding the roxburgh rose stock solution, continuously mixing and stirring, vacuumizing to-0.096 MPa, and degassing for 20 min;

and S6, discharging paste, and filling into an aluminum plastic pipe.

In the embodiment, when the roxburgh rose stock solution is prepared from roxburgh rose, high-quality and high-nutrition roxburgh rose is selected through strict screening and examination, and vitamin C in the roxburgh rose is extracted.

The foregoing illustrates and describes the principles, general features, and advantages of the present invention. It will be understood by those skilled in the art that the present invention is not limited to the embodiments described above, which are described in the specification and illustrated only to illustrate the principle of the present invention, but that various changes and modifications may be made therein without departing from the spirit and scope of the present invention, which fall within the scope of the invention as claimed.

Claims (8)

1. A roxburgh rose VC toothpaste is characterized in that: the composition is characterized by comprising the following raw materials in parts by weight: 30-75g of sorbitol, 10-20g of hydrated silica, 1-2.5g of sodium lauryl sulfate, 0.2-1.5g of roxburgh rose stock solution, 0.5-1.5g of sodium phytate, 0.4-1.0g of cellulose gum, 0.2-0.5g of carrageenan, 0.1-2g of wetting agent, 0.1-0.5g of saccharin sodium, 0.1-0.5g of sodium benzoate, 0.01-0.1g of carrageen crispus extract, 0.01-0.1g of hydroxyapatite, 0.01-0.1g of xylitol, 0.01-0.1g of sodium lauroyl sarcosinate, 0.01-0.1g of sodium methyl ester, 0.01-0.1g of sodium bicarbonate and 0.01-0.1g of sodium ascorbyl phosphate.

2. The roxburgh rose VC toothpaste as claimed in claim 1, wherein: the composition is prepared from the following raw materials in parts by weight: 60g of sorbitol, 18g of hydrated silica, 2g of sodium lauryl sulfate, 0.5g of roxburgh rose stock solution, 1g of sodium phytate, 0.9g of cellulose gum, 0.5g of carrageenan, 1g of wetting agent, 0.18g of saccharin sodium, 0.3g of sodium benzoate, 0.1g of carrageen crispus extract, 0.1g of hydroxyapatite, 0.1g of xylitol, 0.1g of sodium lauroyl sarcosinate, 0.1g of sodium methyl ester, 0.1g of sodium bicarbonate and 0.05g of sodium ascorbyl phosphate.

3. The roxburgh rose VC toothpaste as claimed in claim 2, wherein: also comprises 10-20g of water.

4. The roxburgh rose VC toothpaste as claimed in claim 3, wherein: also comprises 0.5-1.5g of essence.

5. The roxburgh rose VC toothpaste according to claim 4, wherein: also comprises pigment.

6. The roxburgh rose VC toothpaste as claimed in claim 5, wherein: the pigment comprises CI-19140 (lemon yellow) 0.001-0.01g, and CI-15985 (sunset yellow) 0.001-0.01 g.

7. The roxburgh rose VC toothpaste as claimed in claim 6, wherein: the wetting agent adopts polyethylene glycol-8.

8. A process for preparing the rosa roxburghii VC toothpaste of any of claim 7, wherein: the method comprises the following steps:

s1, weighing the raw materials according to the weight;

s2, dissolving sodium phytate, saccharin sodium, sodium benzoate, xylitol, methyl ester sodium, sodium bicarbonate, ascorbic acid sodium phosphate, lemon yellow, and sunset yellow in water, and mixing with sorbitol and extractive solution of Chondrus crispus;

s3, mixing the essence with polyethylene glycol-8;

s4, uniformly mixing hydrated silica, sodium lauryl sulfate, cellulose gum, carrageenan and hydroxyapatite;

s5, mixing the mixture prepared in the steps S2, S3 and S4 with sodium lauroyl sarcosine, stirring for 30 minutes, adding the roxburgh rose stock solution, continuously mixing and stirring, and vacuumizing and degassing;

and S6, discharging paste, and filling into an aluminum plastic pipe.