KR101375865B1 - Oral spray type natural vitamins composition and Process of Treating thereof - Google Patents

Oral spray type natural vitamins composition and Process of Treating thereof Download PDF

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KR101375865B1
KR101375865B1 KR1020120061780A KR20120061780A KR101375865B1 KR 101375865 B1 KR101375865 B1 KR 101375865B1 KR 1020120061780 A KR1020120061780 A KR 1020120061780A KR 20120061780 A KR20120061780 A KR 20120061780A KR 101375865 B1 KR101375865 B1 KR 101375865B1
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extract
vitamin
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enzyme
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김유리
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김영옥
김유리
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K31/00Medicinal preparations containing organic active ingredients
    • A61K31/33Heterocyclic compounds
    • A61K31/335Heterocyclic compounds having oxygen as the only ring hetero atom, e.g. fungichromin
    • A61K31/365Lactones
    • A61K31/375Ascorbic acid, i.e. vitamin C; Salts thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/45Ericaceae or Vacciniaceae (Heath or Blueberry family), e.g. blueberry, cranberry or bilberry
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/73Rosaceae (Rose family), e.g. strawberry, chokeberry, blackberry, pear or firethorn
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
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    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/87Vitaceae or Ampelidaceae (Vine or Grape family), e.g. wine grapes, muscadine or peppervine
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/67Vitamins
    • A61K8/676Ascorbic acid, i.e. vitamin C
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
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    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/02Preparations for care of the skin for chemically bleaching or whitening the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2121/00Preparations for use in therapy
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2300/00Mixtures or combinations of active ingredients, wherein at least one active ingredient is fully defined in groups A61K31/00 - A61K41/00

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  • Health & Medical Sciences (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
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Abstract

이 발명은 액상으로 조성한 천연 비타민을 필요시마다 수시로 피 음용 자들의 구강 내에 분무하여 음용 할 수 있게 하여, 음용 상의 편리성은 물론, 구강 내의 분무로 음용 자들에게 보다 청량감을 느낄 수 있게 한 구강스프레이용 천연 액상 비타민 용액 조성물 및 그 제조방법을 개시하고 있다.The present invention is to spray the natural vitamins prepared in liquid form as needed in the oral cavity of the drink from time to time to drink, so that the convenience of drinking, as well as spraying in the oral spray to make the drinkers feel more refreshing natural A liquid vitamin solution composition and a method of preparing the same are disclosed.

Description

구강스프레이용 천연 비타민 용액 조성물 및 그 제조방법{Oral spray type natural vitamins composition and Process of Treating thereof} Oral spray natural vitamin solution composition and preparation method thereof {Oral spray type natural vitamins composition and Process of Treating etc}

본 발명은 기미,주근깨 등을 개선하는데 일조할 수 있게 한 구강 스프레이용 천연 비타민 용액 조성물 및 그 제조방법에 관한 것으로, 특히 구강(口腔) 내에 직접 분무하여 음용할 수 있도록 하여 청량감과 더불어 천연 비타민C의 생리활성기능이 효율적으로 작용되게 하여 기미,주근깨의 개선 혹은 발생 방지에 일조를 할 수 있게 한 구강스프레이용 천연 비타민 용액 조성물 및 그 제조방법에 관한 것이다. The present invention relates to a natural vitamin solution composition for oral sprays and a method for preparing the same, which can help improve blemishes, freckles, and the like. In particular, the present invention relates to a refreshing natural vitamin C by spraying directly into the oral cavity. The present invention relates to a natural vitamin solution composition for oral spray and a method for producing the same, which effectively contributes to the improvement of blemishes, freckles, and prevention of occurrence.

일반적으로 비타민 C는 멜라닌 색소의 합성작용을 저해하여 주근깨와 미백효과 등의 피부미용에 탁월하고, 또한 흡연이나 스트레스로 인한 산화 손상 방지(항산화작용)를 하고, 면역체계에서 백혈구를 활성화시켜 감염부위로의 이동을 빠르게 하고, 바이러스나 박테리아 같은 침입자와 싸우게 하며, 콜라겐을 생성시켜 피부와 점막을 강하게 유지하도록 하고, 상처 회복을 돕는 기능도 하고 감기 등의 호흡기 감염의 기간을 단축하여, 콧물 기침등의 증상을 줄여주고 철의 흡수를 향상시켜주고 있음은 주지된 사실이다.In general, vitamin C inhibits the action of melanin pigment, which is excellent for skin care such as freckles and whitening effects, and also prevents oxidative damage caused by smoking or stress (antioxidative action), and activates white blood cells in the immune system to infect areas. Speeds up the movement, fights invaders such as viruses and bacteria, produces collagen to keep skin and mucous membranes strong, helps to heal wounds, shortens the duration of respiratory infections such as colds, and coughs It is well known to reduce symptoms and improve iron absorption.

그런데 인체는 비타민C를 스스로 생산하지 못하므로 비타민C가 함유된 식품이나 비타민C 제품 등의 섭취를 충분히 해야만 건강에 도움이 되고 있다.However, the human body does not produce vitamin C by itself, so it is helpful to health only by ingesting enough foods containing vitamin C or vitamin C products.

그러나 종래의 비타민C 제품은 분말이나 정제로 만들어서 섭취하도록 하고 있어, 섭취시 어려움이 있었으나, 현재는 하기 특허 문헌1의 표시와 같은 비타민 음료 제품으로 만들어서 판매되고 있다. 그러나 특허 문헌1의 비타민 음료는 마실수 있게 만들어진 비타민이므로 누구든 쉽게 음용할 수 있는 장점은 있으나, 기존의 비타민 음료는 한번에 마시든 아니면 두번 혹은 여러 번에 나눠서 복용하든 어차피 마시는 제품이기 때문에 장시간을 두고,두고 음용 함에는 비타민 음료라는 제품에서 여러 가지의 약점이 있다.However, the conventional vitamin C product is made of powder or tablets to be ingested, and there was a difficulty in ingestion, but is currently sold as a vitamin beverage product as indicated in Patent Document 1 below. However, the vitamin drink of Patent Document 1 is a drinkable vitamin, so anyone can easily drink it, but the existing vitamin drink is a product that can be taken anytime, twice or several times, so you can leave it for a long time. Drinking drinks have several weaknesses in products called vitamin drinks.

따라서 비타민 음료를 간편하게 휴대하여 음용할 수 있게 하되, 피 음용자들로 하여금 필요시마다 수시로 꺼내서 음용 할 수 있게 하는 것이 절실하게 요구되고 있다. Therefore, it is easy to carry and drink vitamin beverages, it is urgently required that the drinkers to take out and drink whenever necessary.

1.국내 등록특허 제0141971호, 종합비타민 음료 조성물.1. Domestic registered patent No. 0141971, multivitamin beverage composition.

본 발명의 목적은, 피 음용 자들의 구강 내에 분무하여 액상 비타민을 음용 할 수 있게 한 것에 의해, 피 음용자들로 하여금 필요시마다 상시 분무형태로 음용 할 수 있게 한 음용 상의 편리성을 제공하고, 또한 구강 내의 분무로 음용 자들에게 보다 청량감과 기호 감을 부여하게 한 구강스프레이용 천연 비타민용액 조성물 및 그 제조방법을 제공하는 데 있다. It is an object of the present invention to provide a drink convenience by allowing the drinkers to drink liquid vitamins by spraying them in the mouth of the drinkers, so that the drinkers can drink in the form of a regular spray whenever necessary, The present invention also provides a natural vitamin solution composition for oral spray and a method for preparing the same, which gives the drinkers a refreshing feeling and a taste.

상기 목적을 달성하기 위한, 본 발명의 구강스프레이용 천연 비타민용액 조성물은, 청구항1기재의 비타민 음료 총량1L를 기준으로 하여 생 로얄제리 0.5~60g, 아스코르브산10~97g, 효소분해 사과추출물0.02~100g, 산자 나무열매추출물0.02~100g, 블루베리추출물0.02~100g,효소분해 포도추출물0.02~100g, 효소분해 키위추출물0.02~100g, 및 효소분해 수박추출물0.02~100g을 함유하여 혼합 조성한 것을 특징으로 한다. In order to achieve the above object, the natural vitamin solution composition for oral spray of the present invention, based on the total amount of the vitamin beverage 1L of claim 1, raw royal jelly 0.5-60g, ascorbic acid 10-97g, enzyme-degraded apple extract0.02 ~ 100 g, hawthorn fruit extract 0.02 to 100 g, blueberry extract 0.02 to 100 g, enzymatic grape extract 0.02 to 100 g, enzymatic kiwi extract 0.02 to 100 g, and enzymatic watermelon extract 0.02 to 100 g, characterized in that the mixed composition .

또한, 상기 목적을 달성하기 위한, 본 발명의 구강스프레이용 천연 비타민 용액 조성물의 제조방법은, 청구항2 기재의 하기와 같은 원료를 칭량하는 단계[생 로얄제리 0.5~60g, 아스코르브산10~97g, 효소분해 사과추출물0.02~100g, 산자 나무열매추출물0.02~100g, 블루베리추출물0.02~100g,효소분해포도추출물0.02~100g, 효소분해 키위추출물0.02~100g, 효소분해 수박추출물0.02~100g]; 상기와 같이 칭량한 원료들을 교반기에 투입후, 60~80℃의 온도를 가하여 20~60분 교반 하여 혼합하는 단계; 혼합물을 300mesh의 입도를 갖는 망에 넣고 비타민 용액을 여과하는 단계; 비타민 음료 총량lL를 기준으로 하여 상기 단계에서 수득한 비타민 여과액을 함유되게 하여 혼합하는 단계를 포함하는 것을 특징으로 한다.In addition, in order to achieve the above object, the method for producing a natural vitamin solution composition for oral spray of the present invention comprises the steps of weighing the following raw materials described in claim 2 [raw royal jelly 0.5-60g, ascorbic acid 10-97g, Enzyme degrading apple extract 0.02 ~ 100g, hawthorn fruit extract 0.02 ~ 100g, blueberry extract 0.02 ~ 100g, enzyme decomposition grape extract 0.02 ~ 100g, enzyme digestion kiwi extract 0.02 ~ 100g, enzyme decomposition watermelon extract 0.02 ~ 100g; Putting the raw materials weighed as above into a stirrer, adding a temperature of 60 to 80 ° C., and then stirring the mixture for 20 to 60 minutes; Filtering the vitamin solution into a mixture having a mesh size of 300 mesh; It is characterized in that it comprises the step of mixing and containing the vitamin filtrate obtained in the above step based on the total amount of vitamin beverage lL.

본 발명에 의하면, 피 사용자들의 구강 내에 분무하여 음용 할 수 있게 하여,피 음용자들로 하여금 필요시마다 꺼내서 비타민을 보충할 수 있게 한 효과를 제공하고, 또한 구강 내의 분무로 음용 자들에게 청량감과 기호감을 더 갖게 한 효과를 제공한다. According to the present invention, by spraying in the oral cavity of the user to drink, it provides the effect that the drinkers can take out as needed to supplement the vitamins, and also to the drinkers by the spray in the oral cavity Provides an effect that gives more sense.

이하, 본 발명의 구강스프레이용 천연 액상 비타민 조성물 및 그 제조방법의 보다 바람 직한 실시 예를 상세하게 설명한다.Hereinafter, preferred embodiments of the natural liquid vitamin composition for oral spray of the present invention and a preparation method thereof will be described in detail.

<참고예1 : 효소분해 사과추출물>Reference Example 1: Enzymatically Degraded Apple Extract

사과의 미숙과(未熟果)를 음용수와 같은 깨끗한 물로 세척하여 선별하고, 이를 기 준비한 분쇄기에 착즙하여 펄프(과육)을 분리한 후 얻은 상층의 맑은 부분을 10 ~ 60℃ 내지 40~80℃에서 36~60시간 효소 처리하여 3차 정제하여 얻은 것이다. The immature fruits of apples are washed with clean water, such as drinking water, sorted, and juiced in a crusher prepared in advance. The pulp (pulp) is separated, and the clear portion of the upper layer obtained at 10 to 60 to 40 to 80 36-60 hours of enzymatic treatment was obtained by the third purification.

<참고예2: 효소분해 산자 열매 추출물>Reference Example 2: Enzymatically Decomposed Sanja Fruit Extract

산자 나무로부터 채취한 열매를 음용수와 같은 깨끗한 물로 세척하여 선별하고, 이를 분쇄기에 착즙하여 펄프를 분리한 후 얻은 상층의 맑은 부분을 10~60℃ 내지 40~80℃에서 36~ 60시간 효소 처리하여 3차 정제하여 얻었다. The fruit collected from the hawthorn tree is washed with clean water, such as drinking water, and then screened. The juice is crushed to separate the pulp, and the clear portion of the upper layer obtained is subjected to enzyme treatment for 36 to 60 hours at 10 to 60 to 40 to 80 ℃. Obtained by tertiary purification.

<참고예3: 블루베리 추출물>Reference Example 3: Blueberry Extract

블루베리 나무로부터 채취한 열매를 음용수와 같은 깨끗한 물로 세척하여 선별하고, 이를 분쇄기에 착즙하여 펄프를 분리한 후, 얻은 상층의 맑은 부분을 10~60℃ 내지 40~80℃에서 36~ 60시간 효소 처리하여 3차 정제하여 얻었다.The fruit collected from the blueberry tree is washed with clean water such as drinking water and screened. The juice is separated by a pulverizer and the pulp is separated, and the clear portion of the upper layer obtained is subjected to enzymes for 36 to 60 hours at 10 to 60 to 40 to 80 degrees Treatment was carried out to obtain tertiary purification.

<참고예4: 효소분해 포도추출물>Reference Example 4: Enzymatically Decomposed Grape Extracts

포도를 음용수와 같은 깨끗한 물로 세척하여 선별하고, 이를 분쇄기에 착즙하여 펄프를 분리한 후, 얻은 상층의 맑은 부분을 10~60℃ 내지 40~80℃에서 36~ 60시간 효소 처리하여 3차 정제하여 얻었다.The grapes were washed with clean water, such as drinking water, sorted, and juiced in a grinder to separate the pulp, and the purified upper part of the obtained upper layer was purified by enzymatic treatment at 36 to 60 hours at 10 to 60 ℃ to 40 to 80 ℃. Got it.

<참고예5: 효소분해 키위 추출물> Reference Example 5: Enzymatic Degradation Kiwi Extract

키위의 미숙과를 음용수와 같은 깨끗한 물로 세척하여 선별하고, 이를 분쇄기에 착즙하여 펄프를 분리한 후, 얻은 상층의 맑은 부분을 10~60℃ 내지 40~80℃에서 36~ 60시간 효소 처리하여 3차 정제하여 얻었다.The kiwifruit is washed with clean water such as drinking water and screened. The juice is crushed in a grinder to separate the pulp, and the clear portion of the obtained upper layer is subjected to enzyme treatment for 36 to 60 hours at 10 to 60 ℃ to 40 to 80 ℃. It was obtained by tea purification.

<참고예6: 효소분해 수박 추출물>Reference Example 6: Enzymatic Watermelon Extract

수박의 미숙과를 음용수와 같은 깨끗한 물로 세척하여 선별하고, 이를 분쇄기에 착즙하여 펄프를 분리한 후, 얻은 상층의 맑은 부분을 10~60℃ 내지 40~80℃에서 36~ 60시간 효소 처리하여 3차 정제하여 얻었다.After washing the immature fruit of watermelon with clean water such as drinking water, sift it, and separate the pulp by pulverizing it, and then the clear portion of the upper layer obtained by enzyme treatment for 36 to 60 hours at 10 ~ 60 ℃ ~ 40 ~ 80 ℃ 3 It was obtained by tea purification.

<제조예><Production Example>

단계1: 원료 칭량 Step 1: Raw weighing

상기 참고예 1 내지 6으로부터 수득한 추출물과 다른 원료들을 하기의 표1과 같이 칭량 한다.Extracts and other raw materials obtained from Reference Examples 1 to 6 are weighed as shown in Table 1 below.

성분 ingredient 함량content 생로얄제리Saint Royal Jerry 0.5 ~ 60g0.5 to 60 g 아스코르브산 Ascorbic acid 10~97g10-97 g 효소분해 사과 추출물 Enzymatic Apple Extract 0.02~ 100g0.02-100 g 효소분해 산자열매 추출물 Enzymatic Degradation Coconut Extract 0.02~ 100g0.02-100 g 효소분해블루베리추출물 Enzymatically Decomposed Blueberry Extract 0.02~ 100g0.02-100 g 효소분해 포도추출물Enzymatic Grape Extract 0.02~ 100g0.02-100 g 효소분해 키위 추출물Enzymatic Digestion Kiwi Extract 0.02~ 100g0.02-100 g 효소분해 수박추출물Enzymatic Watermelon Extract 0.02~ 100g0.02-100 g

상기 표1에서 생 로얄제리의 첨가는 체내에 영양을 공급하여 간장활동 촉진, 간장해독기능 등 인체의 면역력을 증가시켜 줌으로서 피부에 색소 침착을 방지하는 면역 기능을 주도록 하기 위함이다. 따라서 첨가량이 0.5g의 미만 시에는 위와 같은 기능이 약화 되고, 반대 60g을 초과시에는 약리 효능이 더 좋아지는 점은 있으나, 원가 상승의 요인이 있고, 또한 같이 첨가되는 성분들의 약리 기능 저하시 킬 우려가 있다.The addition of raw royal jelly in Table 1 is intended to give the immune function to prevent pigmentation on the skin by supplying nutrition to the body to increase the body's immunity, such as promoting liver activity, liver detoxification function. Therefore, when the addition amount is less than 0.5g, the above function is weakened, whereas when the amount exceeds 60g, the pharmacological effect is better, but there is a factor of cost increase, and there is a concern that the pharmacological function of the components added together may be lowered. have.

또한, 상기 아스코르브산은 비타민C로서, 첨가 이유는 체내에서 멜라닌 색소의 합성작용을 억제하여 주근깨, 기미의 발생을 없게 하는 미백 기능과 아울러 콜라겐의 먹이 역활을 하여 피부의 윤기뿐만 아니라 피부를 탱탱하게 해주는 효능을 한다. 그밖에 비타민C는 뼈들의 성장 재생에 중요 역활을 하며, 또 유해산소의 공격으로부터 세포를 보호하여 신체가 산성화되는 것을 방지하는 강력한 항산화 작용을 한다. 이러한 이유로 첨가량이 10g 미만 시에는 위와 같은 기능을 약화시킬 우려가 있고, 반대로 첨가량이 97g을 초과시에는 효능이 더 좋아지는 점은 있으나, 같이 첨가되는 성분들의 기능을 저하시 킬 우려가 있다.In addition, the ascorbic acid is a vitamin C, the reason for the addition is to inhibit the synthesis of melanin pigment in the body to prevent the occurrence of freckles, blemishes, as well as to serve as a food for collagen to make the skin not only shiny but also firm skin Efficacy. In addition, vitamin C plays an important role in the growth and regeneration of bones, and a powerful antioxidant that protects the cells from the attack of harmful oxygen to prevent the body from acidifying. For this reason, when the added amount is less than 10g, there is a risk of weakening the above function, on the contrary, when the added amount exceeds 97g there is a point that the efficacy is better, but there is a risk of lowering the function of the components added together.

또, 효소분해 사과추출물, 산자 나무열매추출물, 블루베리추출물, 효소분해 포도추출물, 효소분해 키위추출물 및 효소분해 수박추출물의 첨가 이유는 타 과일에 비하여 비타민C를 많이 함유하고 있어, 천연 비타민C의 함유를 위하여 첨가하는 것으로, 이들의 효능은 상기 아스코르브산과 같이 체내에서 멜라닌 색소의 합성작용을 억제하여 주근깨, 기미의 발생을 없게 하는 미백 효능과, 그리고 체내에서 콜라겐의 먹이 역활을 하여 피부의 윤기뿐만 아니라 피부를 탱탱하게 해주는 효능을 발휘하기 위함이 주 효능이고, 그밖에 뼈들의 성장 재생, 유해산소의 공격으로부터 세포를 보호하여 신체가 산성화되는 것을 방지하는 강력한 항산화 작용을 한다.Also, the reason for the addition of enzymatic apple extract, berry fruit extract, blueberry extract, enzymatic grape extract, enzymatic kiwi extract and enzymatic watermelon extract contains more vitamin C than other fruits. It is added for the purpose of containing, their efficacy is the whitening effect of inhibiting the synthesis of melanin pigment in the body like the ascorbic acid to avoid the occurrence of freckles and blemishes, and serves as a food of collagen in the body to serve as a skin luster In addition, the main effect is to make the skin firm, and other powerful antioxidants that protect the body from acid growth by protecting the cells from the growth and regeneration of bones and harmful oxygen attack.

이러한 이유로 각 첨가량이 0.02g 미만 시에는 위와 같은 기능을 약화시킬 우려가 있고, 반대로 첨가량이 각 100g을 초과시에는 효능이 더 좋아지는 점은 있으나, 원가 상승의 요인이 발생 될 우려와 아울러 같이 첨가되는 성분들의 기능을 저하시 킬 우려가 있다. For this reason, if each amount is less than 0.02g, there is a concern that the above function is weakened. On the contrary, if the amount is more than 100g, the effect is better, but the ingredients are added together with the concern that a cost increase may occur. It may lower their function.

단계2 : 원료의 교반혼합Step 2: Mixing the raw materials with stirring

상기 단계1과 같이 칭량한 원료들을 기준비한 교반기 내부로 투입 후, 60~80℃의 온도를 가하면서 20~60분 교반 하면서 골고루 혼합한다.The raw materials weighed as in step 1 are introduced into a stirrer and mixed at a temperature of 60 to 80 ° C with stirring for 20 to 60 minutes.

단계3 : 여과Step 3: Filtration

단계2로부터 얻은 혼합물을 300mesh의 입도를 갖는 망에 넣고 여과하여 순수한 액상만을 얻는다.The mixture obtained in step 2 is placed in a mesh having a particle size of 300 mesh and filtered to obtain only a pure liquid phase.

단계4 : 혼합Step 4: Mix

비타민 음료 총량lL를 기준으로 하여 상기 단계에서 수득한 비타민 여과액을 표1과 같은 함량으로 함유되게 하는 것이고, 나머지는 정제수이다. The vitamin filtrate obtained in the above step is contained in the content shown in Table 1 based on the total amount of the vitamin beverage lL, and the rest is purified water.

필요에 따라서는 본 발명에서는 상기의 주 성분 이외에 보조성분을 더 첨가할 수 있다. 보조성분은 감미제, 점도조절제, 향료 등이다. 감미제는 D-솔비톨, 자일리톨과 같은 다가 알콜, 서당, 글루코스, 말토스, 후락토스 등이 사용될 수 있고, 향료는 천연향(허벌, 민트, 스트로베리향 등)이고, 점도조절제는 겔란검, 구아검, 알기닌산 나트륨염, CMC 소디움에서 선택된 점도 조절제를 사용할 수 있다. 또한, 본 발명에서는 보존성을 향상시키기 위하여 방부제 또는 보존제를 첨가할 수도 있는데, 방부제 또는 보존제로서는 안식향산 나트륨, p-메틸 안식향산, p-에틸안식향산, p-프로필안식향산을 사용할 수 있으나, 가능한 천연 방부제를 사용함이 바람직하다. If necessary, in the present invention, an auxiliary component may be further added in addition to the main component. Auxiliary ingredients are sweeteners, viscosity modifiers, fragrances and the like. Sweetening agents may be polyhydric alcohols such as D-sorbitol, xylitol, sucrose, glucose, maltose, fructose, and the like, and flavors are natural flavors (herbal, mint, strawberry flavors, etc.), and viscosity modifiers are gellan gum, guar. Viscosity modifiers selected from gums, sodium alginate salts, CMC sodium can be used. In the present invention, a preservative or a preservative may be added in order to improve preservability. As a preservative or preservative, sodium benzoate, p-methylbenzoic acid, p-ethylbenzoic acid or p-propylbenzoic acid may be used. .

단계5 : 용기 충전Step 5: Charging the container

상기 단계4에서 조성된 액상의 비타민은 보통의 펌프식 분무노즐을 갖는 용기에 소정 단위로 수용하여 필요시마다 구강 내에 적절하게 분무하여 비타민c를 복용 내지는 음용하게 할 수 있다.The liquid vitamin prepared in step 4 may be accommodated in a predetermined unit in a container having a normal pump spray nozzle and sprayed appropriately in the mouth whenever necessary to take or drink vitamin c.

성분 ingredient 실시예1Example 1 실시예2Example 2 실시예3Example 3 실시예4Example 4 실시예5Example 5 생로얄제리Saint Royal Jerry 0.5 g0.5 g 60g60g 5g5g 15g15g 50g50g 아스코르브산 Ascorbic acid 10g10g 97g97g 15g15g 60g60g 85g85 g 효소분해 사과 추출물 Enzymatic Apple Extract 100g100g 0.02g0.02 g 50g50g 70g70g 90g90 g 효소분해 산자열매 추출물 Enzymatic Degradation Coconut Extract 0.02g0.02 g 100g100g 50g50g 70g70g 90g90 g 효소분해블루베리추출물 Enzymatically Decomposed Blueberry Extract 0.02g0.02 g 100g100g 50g50g 70g70g 90g90 g 효소분해 포도추출물Enzymatic Grape Extract 0.02g0.02 g 100g100g 50g50g 70g70g 90g90 g 효소분해 키위 추출물Enzymatic Digestion Kiwi Extract 0.02g0.02 g 100g100g 50g50g 70g70g 90g90 g 효소분해 수박추출물Enzymatic Watermelon Extract 0.02g0.02 g 100g100g 50g50g 70g70g 90g90 g 정제수Purified water 잔량Balance 잔량Balance 잔량Balance 잔량Balance 잔량Balance 합계Sum 1L1L 1L1L 1L1L 1L1L 1L1L

상기 표2의 실시 예1과 같이 칭량한 함량으로 혼합 조성된 액상의 비타민 용액 조성물을 수득하였고, 이를 기준비한 분무 용기에 충진하여 구강 내에 스프레이 형태로 분무할 수 있게 하였다. As shown in Example 1 of Table 2 to obtain a liquid vitamin solution composition of a mixed composition in a weighed content, it was filled in a spray container prepared by reference to be able to spray in the form of a spray in the oral cavity.

상기 표2의 실시 예2와 같이 칭량한 함량으로 혼합 조성된 액상의 비타민 용액 조성물을 수득하였고, 이를 기준비한 분무 용기에 충진하여 구강 내에 스프레이형태로 분무할 수 있게 하였다.As shown in Example 2 of Table 2 to obtain a liquid vitamin solution composition mixed composition in a weighed content, it was filled in a spray container prepared by reference to be able to spray in the form of a spray in the oral cavity.

상기 표2의 실시 예3과 같이 칭량한 함량으로 혼합 조성된 액상의 비타민 용액 조성물을 수득하였고, 이를 기준비한 분무 용기에 충진하여 구강 내에 스프레이형태로 분무할 수 있게 하였다.As shown in Example 3 of Table 2 to obtain a liquid vitamin solution composition mixed composition in a weighed content, it was filled in a spray container prepared by reference to be able to spray in the form of a spray in the oral cavity.

상기 표2의 실시 예4와 같이 칭량한 함량으로 혼합 조성된 액상의 비타민 용액 조성물을 수득하였고, 이를 기준비한 분무 용기에 충진하여 구강 내에 스프레이형태로 분무할 수 있게 하였다.As shown in Example 4 of Table 2, a liquid vitamin solution composition was obtained, which was mixed in a weighed amount, and filled in a spray container prepared in a standard ratio so as to be sprayed in the oral cavity.

상기 표2의 실시 예5와 같이 칭량한 함량으로 혼합조성된 액상의 비타민 용액 조성물을 수득하였고, 이를 기준비한 분무 용기에 충진하여 구강 내에 스프레이형태로 분무할 수 있게 하였다.As shown in Example 5 of Table 2 to obtain a liquid vitamin solution composition mixed composition in a weighed content, it was filled in a spray container prepared by reference to the spray can be sprayed in the oral cavity.

<실험예 1><Experimental Example 1>

본 실험 예에서는 비타민 음료에 대한 기호도, 미감 등을 조사하기 위해 10세 이상의 남녀 50명을 대상으로, 상기 실시 예에 따라 제조한 본 발명과 기존의 비타민 음료를 대략 10g 이하의 범위에서, 본 발명은 구강 내에 분무하는 형태로 음용하는 반면 기존의 비타민 음료는 그대로 마시게 하였다. 그 결과는 하기 표3에 표시하였다.In the present experimental example, the present invention and the existing vitamin beverage prepared in accordance with the above embodiment in the range of about 10g or less to 50 men and women over 10 years old to investigate the preference, taste and the like for the vitamin beverage, the present invention While drinking in the form of a spray in the mouth while drinking the existing vitamin beverages. The results are shown in Table 3 below.

특징Characteristic 본발명
(응답자수)
Invention
(Number of respondents)
대조용
(응답자수)
Control
(Number of respondents)
모르겠다
(응답자수)
I do not know
(Number of respondents)
더 상쾌한 맛을 준다.Gives a more refreshing taste 28 28 20 20 22 기호성이 우수하다.Excellent palatability. 3030 1616 44 좋은 향기가 느껴진다I feel a good fragrance 2525 2121 44

이상의 실험 결과에서 나타난 바와 같이 본 발명은 대조용의 일반 마시는 비타민 음료보다 우수하거나 필적할 만하다는 것이 입증되었다.As shown in the above experimental results, the present invention proved to be superior or comparable to that of the control general drinking vitamin beverage.

<실험예 2><Experimental Example 2>

기미, 주근깨가 있는 성인남녀 50명을 대상으로 상기 실시 예에 따라 제조한 비타민을 1일 6회(0.5g정도)씩 30일간 계속하여 수시로 분무하는 형태로 음용 토록 하고,설문 조사에 의해 효과를 평가하였다. 결과는 하기 표4에 표시하였다.For 50 adult men and women with blemishes and freckles, the vitamins prepared in accordance with the above embodiments were continuously sprayed continuously for 6 days (about 0.5 g) for 30 days, and the effect was investigated by a survey. Evaluated. The results are shown in Table 4 below.

별무효과Separate effect 효과
있음
effect
has exist
상당한
효과
considerable
effect
완치근접
효과
Cure proximity
effect
system
10(20%)10 (20%) 30(60%)30 (60%) 9(18%)9 (18%) 1(2%)1 (2%) 50(100%)50 (100%)

상기 실험 결과에서 나타난 바와 같이, 본 제품을 꾸준히 차로서 사용할 경우 기미,주근깨 등이 완화되어 건강 보조 식품으로서의 효과가 있음을 알 수 있다.As shown in the experimental results, it can be seen that when the product is used continuously as a tea, blemishes, freckles, etc. are alleviated to have an effect as a dietary supplement.

본 발명은 기재된 실시 예에 한정되는 것은 아니고, 본 발명의 사상 및 범위를 벗어나지 않고 다양하게 수정 변형할 수 있음은 이 기술의 분야에서 통상의 지식을 가진자에게는 자명하다. 따라서 그러한 변형예 또는 수정예들은 본 발명의 특허청구범위에 속한다 해야할 것이다.
It will be apparent to those skilled in the art that various modifications and variations can be made in the present invention without departing from the spirit and scope of the invention as set forth in the appended claims. It is therefore intended that such variations and modifications fall within the scope of the appended claims.

Claims (2)

비타민 음료 총량1L를 기준으로 하여 생 로얄제리 0.5~60g, 아스코르브산10~97g, 효소분해 사과추출물0.02~100g, 산자 나무열매추출물0.02~100g, 블루베리추출물0.02~100g, 효소분해 포도추출물0.02~100g, 효소분해 키위추출물0.02~100g, 및 효소분해 수박추출물0.02~100g을 함유되게 하여 혼합 조성한 것을 특징으로 하는 구강 스프레이용 천연 비타민 용액 조성물.Based on the total amount of vitamin drink 1L, raw royal jelly 0.5-60g, ascorbic acid 10-97g, enzyme-degraded apple extract 0.02--100g, hawthorn fruit extract 0.02--100g, blueberry extract 0.02--100g, enzyme-degraded grape extract 0.02- ~ A natural vitamin solution composition for oral sprays, comprising 100 g, enzymatic kiwi extract 0.02 to 100 g, and enzymatic watermelon extract 0.02 to 100 g. ①하기와 같이 원료를 칭량하는 단계;
생 로얄제리 0.5~60g, 아스코르브산10~97g, 효소분해 사과추출물0.02~100g, 산자 나무열매추출물0.02~100g, 블루베리추출물0.02~100g, 효소분해포도추출물0.02~100g, 효소분해 키위추출물0.02~100g, 및 효소분해 수박추출물0.02~100g.
②상기와 같이 칭량한 원료들을 교반기에 투입후, 60~80℃의 온도를 가하여 20~60분 교반 하여 혼합하는 단계;
③혼합물을 300mesh의 입도를 갖는 망에 넣고 여과하여 비타민 여과액을 얻는 단계;및
④비타민 음료 총량lL를 기준으로 하여 상기 단계에서 수득한 비타민 여과액을 넣고 혼합하는 단계로 이루어진 구강 스프레이용 천연 비타민 용액 조성물의 제조방법.
① weighing the raw materials as follows;
Raw Royal Jelly 0.5 ~ 60g, Ascorbic Acid 10 ~ 97g, Enzymatic Apple Extract 0.02 ~ 100g, Hazel Fruit Extract 0.02 ~ 100g, Blueberry Extract 0.02 ~ 100g, Enzyme Degraded Grape Extract 0.02 ~ 100g, Enzymatic Kiwi Extract 0.02 ~ 100 g, and enzymatic watermelon extract 0.02-100 g.
② the raw materials weighed as described above are added to the stirrer, and then mixed by stirring for 20 to 60 minutes by adding a temperature of 60 ~ 80 ℃;
(3) mixing the mixture into a mesh having a particle size of 300 mesh to obtain a vitamin filtrate; and
④ The method of producing a natural vitamin solution composition for oral spray consisting of mixing and adding the vitamin filtrate obtained in the above step based on the total amount of vitamin L of the beverage.
KR1020120061780A 2012-06-08 2012-06-08 Oral spray type natural vitamins composition and Process of Treating thereof KR101375865B1 (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20220163133A (en) 2021-06-02 2022-12-09 최이교 Manufacturing method of natural antiseptic spray composition for oral spray

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KR970018926A (en) * 1995-09-28 1997-04-30 원본미기재 Method and apparatus for noise reduction of switched magnetoresistive motors by current profile
KR970032507A (en) * 1995-12-05 1997-07-22 손경식 Hangover preventive beverage composition
JPH11266840A (en) * 1998-03-24 1999-10-05 Tekunooto:Kk Drinking of propolis extract solution
JP2005287318A (en) 2004-03-31 2005-10-20 Mitani Valve Co Ltd Concentrated carbonated beverage packaged in aerosol container

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR970018926A (en) * 1995-09-28 1997-04-30 원본미기재 Method and apparatus for noise reduction of switched magnetoresistive motors by current profile
KR970032507A (en) * 1995-12-05 1997-07-22 손경식 Hangover preventive beverage composition
JPH11266840A (en) * 1998-03-24 1999-10-05 Tekunooto:Kk Drinking of propolis extract solution
JP2005287318A (en) 2004-03-31 2005-10-20 Mitani Valve Co Ltd Concentrated carbonated beverage packaged in aerosol container

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20220163133A (en) 2021-06-02 2022-12-09 최이교 Manufacturing method of natural antiseptic spray composition for oral spray

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