CN111902384B - 在氯化烷烃生产中回收催化剂的方法 - Google Patents

在氯化烷烃生产中回收催化剂的方法 Download PDF

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CN111902384B
CN111902384B CN201980021941.4A CN201980021941A CN111902384B CN 111902384 B CN111902384 B CN 111902384B CN 201980021941 A CN201980021941 A CN 201980021941A CN 111902384 B CN111902384 B CN 111902384B
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effluent stream
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CN111902384A (zh
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J·D·迈尔斯
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Blue Cube Intellectual Property Co ltd
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/26—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton
    • C07C17/272—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by addition reactions
    • C07C17/275—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by addition reactions of hydrocarbons and halogenated hydrocarbons
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/74—Iron group metals
    • B01J23/745—Iron
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/26—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton
    • C07C17/272—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by addition reactions
    • C07C17/278—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by addition reactions of only halogenated hydrocarbons
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/38—Separation; Purification; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/38—Separation; Purification; Stabilisation; Use of additives
    • C07C17/383—Separation; Purification; Stabilisation; Use of additives by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/38—Separation; Purification; Stabilisation; Use of additives
    • C07C17/395—Separation; Purification; Stabilisation; Use of additives by treatment giving rise to a chemical modification of at least one compound
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C19/00—Acyclic saturated compounds containing halogen atoms
    • C07C19/01—Acyclic saturated compounds containing halogen atoms containing chlorine
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C19/00—Acyclic saturated compounds containing halogen atoms
    • C07C19/08—Acyclic saturated compounds containing halogen atoms containing fluorine
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C21/00—Acyclic unsaturated compounds containing halogen atoms
    • C07C21/02—Acyclic unsaturated compounds containing halogen atoms containing carbon-to-carbon double bonds
    • C07C21/04—Chloro-alkenes
    • C07C21/06—Vinyl chloride
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C21/00—Acyclic unsaturated compounds containing halogen atoms
    • C07C21/02—Acyclic unsaturated compounds containing halogen atoms containing carbon-to-carbon double bonds
    • C07C21/04—Chloro-alkenes
    • C07C21/073—Dichloro-alkenes
    • C07C21/08—Vinylidene chloride
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/584—Recycling of catalysts

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
CN201980021941.4A 2018-04-03 2019-04-02 在氯化烷烃生产中回收催化剂的方法 Active CN111902384B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US201862652107P 2018-04-03 2018-04-03
US62/652,107 2018-04-03
PCT/US2019/025334 WO2019195248A1 (en) 2018-04-03 2019-04-02 Method for recycling catalyst in the production of chlorinated alkanes

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CN111902384A CN111902384A (zh) 2020-11-06
CN111902384B true CN111902384B (zh) 2024-05-14

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US (1) US11192840B2 (https=)
EP (1) EP3774703B1 (https=)
JP (1) JP7187573B2 (https=)
CN (1) CN111902384B (https=)
WO (1) WO2019195248A1 (https=)

Families Citing this family (5)

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MX2021008678A (es) * 2019-01-22 2021-10-26 Bisichem Co Ltd Compuesto de heteroarilo de anillo fusionado como inhibidor del receptor de tipo i de la activina (alk4) y/o el receptor de tipo i del factor beta de crecimiento transformante (tgf-beta) (alk5).
WO2022115151A1 (en) 2020-11-30 2022-06-02 Blue Cube Ip Llc Method for treating a heavy byproduct stream from chlorinated propane production
CN114349594B (zh) * 2021-12-16 2024-02-20 西安近代化学研究所 一种制备多卤代烃的方法及反应器
CN116265097B (zh) 2021-12-17 2024-10-08 中国科学院宁波材料技术与工程研究所 用于气固相反应连续生产1,1,1,3-四氯丙烷的催化剂、其制备方法与应用
WO2025264758A1 (en) * 2024-06-21 2025-12-26 The Chemours Company Fc, Llc Process for (hydro)chloro(fluoro)carbon recovery

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GB1023423A (en) * 1961-09-28 1966-03-23 Meir Asscher Production of adducts of carbon tetrachloride and alkenes
JPH09249587A (ja) * 1996-03-18 1997-09-22 Tokuyama Corp ポリ塩素化アルカンの製造方法
WO2000035839A1 (en) * 1998-12-15 2000-06-22 Alliedsignal Inc. Process for addition of haloalkanes to alkenes catalyzed by an organophosphite compound
BE1012972A6 (fr) * 1998-02-24 2001-07-03 Solvay Procede de preparation d'hydrocarbures halogenes.
US6313360B1 (en) * 2000-09-29 2001-11-06 Vulcan Materials Company Process for the manufacture of 1, 1, 1, 3, 3-pentachloropropane
WO2008037657A1 (en) * 2006-09-26 2008-04-03 Solvay (Société Anonyme) Process for the preparation of halogenated hydrocarbons with at least 3 carbon atoms in the presence of a ruthenium compound
JP2008531474A (ja) * 2005-01-19 2008-08-14 グレート・レイクス・ケミカル・コーポレイション ハロゲン化炭素生成方法、ハロゲン化炭素分離方法及びハロゲン化炭素生成システム
CN101535226A (zh) * 2006-10-06 2009-09-16 索尔维公司 在铁和亚磷酸酯存在下制备具有至少3个碳原子的卤代烃的方法
CN101903312A (zh) * 2007-12-19 2010-12-01 西方化学股份有限公司 制备氯化烃的方法
CN103373894A (zh) * 2012-04-13 2013-10-30 中化蓝天集团有限公司 一种制备c3饱和卤代烷烃的连续方法
CN103562165A (zh) * 2011-06-03 2014-02-05 霍尼韦尔国际公司 在卤代烷化合物生产过程中减缓副产物形成的方法
CN103648640A (zh) * 2011-06-03 2014-03-19 霍尼韦尔国际公司 用于捕集和循环卤代烷化合物生产中使用的铁催化剂的方法
CN106146247A (zh) * 2015-03-24 2016-11-23 中化近代环保化工(西安)有限公司 一种连续法制备1,1,1,3-四氯丙烷的工艺方法
CN107001191A (zh) * 2014-10-16 2017-08-01 化学和冶金生产联合体股份公司 方法
JP2017137263A (ja) * 2016-02-04 2017-08-10 株式会社トクヤマ １，１，１，３−テトラクロロプロパンの製造方法
WO2017178857A1 (en) * 2016-04-13 2017-10-19 Arkema France Process for the manufacture of 2,3,3,3-tetrafluoropropene

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US4650914A (en) 1983-07-06 1987-03-17 Monsanto Company Process for producing 1,1,2,3-tetrachloropropene
US6720466B2 (en) * 2002-04-17 2004-04-13 Vulcan Chemicals, a division of Vulcan Materials Company 1,1,1,3,3-pentachloropropane process purge stream concentration using a secondary refluxed evaporator and secondary product recovery
US7102041B2 (en) * 2004-12-08 2006-09-05 Honeywell International Inc. Continuous process for preparing halogenated compounds
US8907147B2 (en) 2013-02-04 2014-12-09 Honeywell International Inc. Synthesis of 1,1,2,3-tetrachloropropene
CN103530055A (zh) 2013-10-22 2014-01-22 北京奇虎科技有限公司 屏幕图像的截取方法及设备
JP2017178897A (ja) 2016-03-31 2017-10-05 株式会社トクヤマ クロロプロパン類の製造方法
US20190202759A1 (en) 2016-09-09 2019-07-04 Blue Cube Ip Llc Processes for the dehydrochlorination of a chlorinated alkane

Patent Citations (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1023423A (en) * 1961-09-28 1966-03-23 Meir Asscher Production of adducts of carbon tetrachloride and alkenes
JPH09249587A (ja) * 1996-03-18 1997-09-22 Tokuyama Corp ポリ塩素化アルカンの製造方法
BE1012972A6 (fr) * 1998-02-24 2001-07-03 Solvay Procede de preparation d'hydrocarbures halogenes.
WO2000035839A1 (en) * 1998-12-15 2000-06-22 Alliedsignal Inc. Process for addition of haloalkanes to alkenes catalyzed by an organophosphite compound
US6313360B1 (en) * 2000-09-29 2001-11-06 Vulcan Materials Company Process for the manufacture of 1, 1, 1, 3, 3-pentachloropropane
JP2008531474A (ja) * 2005-01-19 2008-08-14 グレート・レイクス・ケミカル・コーポレイション ハロゲン化炭素生成方法、ハロゲン化炭素分離方法及びハロゲン化炭素生成システム
WO2008037657A1 (en) * 2006-09-26 2008-04-03 Solvay (Société Anonyme) Process for the preparation of halogenated hydrocarbons with at least 3 carbon atoms in the presence of a ruthenium compound
CN101535226A (zh) * 2006-10-06 2009-09-16 索尔维公司 在铁和亚磷酸酯存在下制备具有至少3个碳原子的卤代烃的方法
CN101903312A (zh) * 2007-12-19 2010-12-01 西方化学股份有限公司 制备氯化烃的方法
CN103562165A (zh) * 2011-06-03 2014-02-05 霍尼韦尔国际公司 在卤代烷化合物生产过程中减缓副产物形成的方法
CN103648640A (zh) * 2011-06-03 2014-03-19 霍尼韦尔国际公司 用于捕集和循环卤代烷化合物生产中使用的铁催化剂的方法
CN103373894A (zh) * 2012-04-13 2013-10-30 中化蓝天集团有限公司 一种制备c3饱和卤代烷烃的连续方法
CN107001191A (zh) * 2014-10-16 2017-08-01 化学和冶金生产联合体股份公司 方法
CN106146247A (zh) * 2015-03-24 2016-11-23 中化近代环保化工(西安)有限公司 一种连续法制备1,1,1,3-四氯丙烷的工艺方法
JP2017137263A (ja) * 2016-02-04 2017-08-10 株式会社トクヤマ １，１，１，３−テトラクロロプロパンの製造方法
WO2017178857A1 (en) * 2016-04-13 2017-10-19 Arkema France Process for the manufacture of 2,3,3,3-tetrafluoropropene

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EP3774703A1 (en) 2021-02-17
US11192840B2 (en) 2021-12-07
EP3774703B1 (en) 2022-04-27
CN111902384A (zh) 2020-11-06
WO2019195248A1 (en) 2019-10-10
JP7187573B2 (ja) 2022-12-12
JP2021520376A (ja) 2021-08-19
US20210009490A1 (en) 2021-01-14

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