CN111317707A - Gorgonia pseudopterogorgia hydrating and moisturizing mask and preparation method thereof - Google Patents
Gorgonia pseudopterogorgia hydrating and moisturizing mask and preparation method thereof Download PDFInfo
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
- A61K8/442—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof substituted by amido group(s)
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/005—Preparations for sensitive skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
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Abstract
The invention discloses a gorgonian moisturizing mask and a preparation method thereof. The facial mask consists of essence and facial mask cloth which is cut into the shape of an adult face, wherein the essence consists of the following raw materials in parts by weight: 0.01-0.1 part of hydroxyethyl acrylate/sodium acryloyldimethyl taurate copolymer, 0.01-0.3 part of xanthan gum, 0.01-0.1 part of sclerotium rolfsii gum, 1-10 parts of glycerol, 1-5 parts of butanediol, 0.01-0.5 part of gorgonian extract, 0.15-0.5 part of CAB-35 (cocamidopropyl betaine), 0.01-0.3 part of olivem300 emulsifier, 0.01-2 parts of A165 (glyceryl stearate/PEG-100 stearate), 0.01-0.5 part of GTCC (composed of caprylic/capric acid and triglyceride), 0.01-0.5 part of grape seed essential oil and water to 100 parts by weight. Human body experiments prove that the mask product has obvious moisturizing effect, is safe and has no stimulation.
Description
Technical Field
The invention relates to a mask and a preparation method thereof, in particular to a moisturizing mask containing an aucuba japonica extract and a preparation method thereof. The invention belongs to the technical field of cosmetics.
Background
With the increase of age, various skin problems can occur to many people under the influence of environmental factors and living habits, so that daily care and beautification of skin are more and more popular and more emphasized by people. The water content of the stratum corneum of normal skin is 10-30% so as to maintain the elasticity and softness of the skin and ensure the health of the skin. When the external environment climate changes and stimulates (such as wind blowing, solarization, cold and the like) or the skin health is in a problem, the water content of the skin stratum corneum is reduced, so that the skin is dry and various skin problems are caused. Skin problems due to water deficit are by no means as simple as dryness, and almost every skin problem is associated with water deficit. Moisture is the first element of beautiful skin, whitening, oil control, sun protection, sensitivity resistance, aging resistance and the like are all completed on the basis of water replenishing and moisture preserving, and water replenishing is needed in any season. Because of the wide function and specificity, the convenient use and the rapid water replenishing and repairing, the water replenishing mask is more and more popular and sought after by people.
The facial mask is a carrier of facial skin care or beauty care products, is coated or stuck on the face for a certain time, and is removed by cleaning or stripping after beneficial substances in the care or beauty care products are absorbed by the skin or substances harmful to the health of the skin in the surface of the skin are absorbed by the facial mask, so that the purposes of facial skin care or beauty are achieved, such as moisturizing, whitening, anti-aging and oil balancing. However, most of the active ingredients of the existing facial mask are chemical synthesis preparations, and although the facial mask has the effects of moisturizing, moistening skin, whitening, beautifying, removing wrinkles and the like, the facial mask contains various chemical additives, belongs to strong drug irritation treatment and has toxic and side effects of stimulating skin and the like; the skin is caused to generate drug dependence, and the drug resistance is generated after long-term use.
Therefore, a mask product which can effectively replenish water and moisturize and has higher safety is urgently needed in the market at present.
Disclosure of Invention
The invention aims to provide a mask product with moisturizing and moisture-keeping functions.
In order to achieve the purpose, the invention adopts the following technical means:
the invention provides a gorgonian hydrating and moisturizing mask which is composed of essence and mask cloth cut into an adult face shape, wherein the essence is composed of the following raw materials in parts by weight:
0.01-0.1 part of hydroxyethyl acrylate/sodium acryloyldimethyl taurate copolymer, 0.01-0.3 part of xanthan gum, 0.01-0.1 part of sclerotium rolfsii gum, 1-10 parts of glycerol, 1-5 parts of butanediol, 0.01-0.5 part of gorgonian extract, 0.15-0.5 part of CAB-35 (cocamidopropyl betaine), 0.01-0.3 part of olivem300 emulsifier, 0.01-2 parts of A165 (glyceryl stearate/PEG-100 stearate), 0.01-0.5 part of GTCC (composed of caprylic/capric acid and triglyceride), 0.01-0.5 part of grape seed essential oil and water to 100 parts by weight.
Wherein, preferably, the mask cloth is non-woven fabrics, silk or biological fibers.
Preferably, the gorgonian extract is prepared by the following method:
1) extraction of
(1) Pulverizing and sieving herba Salicornia Herbacea raw material to obtain 50-70 mesh fine granules, and extracting with deionized water at 55-60 deg.C; extracting for three times, wherein the ratio of the first material to the liquid is 1: 6, 1 for the second time: 4, third time is 1: 3, 2 hours each time;
(2) after extraction, combining the three filtrates, concentrating at low temperature by using an MVR evaporator to obtain a feed liquid with a specific gravity of 1.11-1.13, and discharging the feed liquid for later use;
2) per resin
Purifying the extracted and concentrated feed liquid by adopting a macroporous adsorption resin column, wherein the sample loading amount is 2 column volumes, eluting by using 16-20 vol% low-concentration ethanol, the elution volume is 3-5 column volumes, then eluting by using 95 vol% high-concentration ethanol, the elution volume is 2-2.5 column volumes, and collecting the eluent at this time;
3) concentrating
Concentrating the high concentration ethanol solution collected by the resin at low temperature by an MVR evaporator to one fifth of the volume of the solution, discharging, standing the discharged solution in a cold storage for precipitation, controlling the temperature at-3 to-5 ℃, standing for 8 hours, and filtering;
4) drying
Drying the filtered precipitate in an oven at 50 deg.C for 5 hr to obtain the final product.
Wherein, preferably, the macroporous absorption resin column is nonpolar macroporous absorption resin, and comprises one or more of HP20, HPD100, HPD300 and D101 macroporous absorption resin.
Furthermore, the invention also provides application of the mask in preparing a skin care product with moisturizing and moisture-keeping functions.
Compared with the prior art, the invention has the beneficial effects that:
the invention provides a mask product with moisturizing and moisture-keeping functions, wherein the mask contains an gorgonian extract component, and the gorgonian extract is a natural extract of pseudopterogorgia (also known as verbena) and is an antiallergic component which is safe, efficient and environmentally-friendly. According to the invention, hydroxyethyl acrylate/sodium acryloyldimethyl taurate copolymer, xanthan gum, sclerotium rolfsii gum, glycerol, butanediol, a gorgonian extract, CAB-35 (cocamidopropyl betaine), an olive 300 emulsifier, A165 (glyceryl stearate/PEG-100 stearate), GTCC (caprylic acid/capric acid and triglyceride) and grape seed essential oil are matched for use, and the dosage of the A165 and the A165 is determined appropriately, so that the mask product is finally prepared.
Drawings
Fig. 1 is a radar chart for testing the overall performance of the mask.
Detailed Description
The invention will be further described with reference to specific embodiments, and the advantages and features of the invention will become apparent as the description proceeds. These examples are illustrative only and do not limit the scope of the present invention in any way. It will be understood by those skilled in the art that various changes in form and details may be made therein without departing from the spirit and scope of the invention, and that such changes and modifications may be made without departing from the spirit and scope of the invention.
Example 1 preparation of an extract of gorgonian
1) Extraction of
(1) Pulverizing and sieving the raw materials of the gorgonia pseudopterodonta to obtain fine particles of 60 meshes, and extracting the fine particles by using deionized water with the temperature controlled at 55 ℃; extracting for three times, wherein the ratio of the first material to the liquid is 1: 6, 1 for the second time: 4, third time is 1: 3, 2 hours each time;
(2) after extraction, combining the three filtrates, concentrating at low temperature by using an MVR evaporator to obtain a feed liquid with a specific gravity of 1.12, and discharging the feed liquid for later use;
2) per resin
Purifying the extracted and concentrated feed liquid by using a macroporous adsorption resin column HP20, wherein the sample loading amount is 2 column volumes, eluting by using 20 vol% low-concentration ethanol, the elution volume is 4 column volumes, then eluting by using 95 vol% high-concentration ethanol, the elution volume is 2 column volumes, and collecting the eluent at this time;
3) concentrating
Concentrating the high-concentration ethanol solution collected by the resin at low temperature by using an MVR evaporator to one fifth of the volume of the feed liquid, discharging, standing the discharged feed liquid in a cold storage for precipitation, controlling the temperature at-4 ℃, standing for 8 hours, and filtering;
4) drying
Drying the filtered precipitate in an oven at 50 deg.C for 5 hr to obtain the final product.
HPLC high performance liquid chromatography detection shows that the content of gorgonian acid is 1% and the content of methyl ester of gorgonian is 2%.
Example 2 preparation of an extract of Pseudopterogorgia elisahethae
1) Extraction of
(1) Pulverizing and sieving herba Salicornia Herbacea raw material to obtain 50 mesh fine granules, and extracting with deionized water at 60 deg.C; extracting for three times, wherein the ratio of the first material to the liquid is 1: 6, 1 for the second time: 4, third time is 1: 3, 2 hours each time;
(2) after extraction, combining the three filtrates, concentrating at low temperature by using an MVR evaporator to obtain a feed liquid with a specific gravity of 1.11, and discharging the feed liquid for later use;
2) per resin
Purifying the extracted and concentrated feed liquid by using a macroporous adsorption resin column D101, wherein the sample loading amount is 2 column volumes, eluting by using 16 vol% low-concentration ethanol, the elution volume is 3 column volumes, then eluting by using 95 vol% high-concentration ethanol, the elution volume is 2.5 column volumes, and collecting the eluate;
3) concentrating
Concentrating the high-concentration ethanol solution collected by the resin at low temperature by using an MVR evaporator to one fifth of the volume of the feed liquid, discharging, standing the discharged feed liquid in a cold storage for precipitation, controlling the temperature at-3 ℃, standing for 8 hours, and filtering;
4) drying
Drying the filtered precipitate in an oven at 50 deg.C for 5 hr to obtain the final product.
Example 3 preparation of an extract of Elaeagnus angustifolia
1) Extraction of
(1) Pulverizing and sieving herba Salicornia Herbacea raw material to obtain 70 mesh fine granules, and extracting with deionized water at 55 deg.C; extracting for three times, wherein the ratio of the first material to the liquid is 1: 6, 1 for the second time: 4, third time is 1: 3, 2 hours each time;
(2) after extraction, combining the three filtrates, concentrating at low temperature by using an MVR evaporator to obtain a feed liquid with a specific gravity of 1.13, and discharging the feed liquid for later use;
2) per resin
Purifying the extracted and concentrated feed liquid by using a macroporous adsorption resin column HPD300, wherein the sample loading amount is 2 column volumes, eluting by using low-concentration ethanol with the concentration of 20 vol% firstly, the elution volume is 5 column volumes, then eluting by using high-concentration ethanol with the concentration of 95 vol%, the elution volume is 2 column volumes, and collecting the eluent at this time;
3) concentrating
Concentrating the high-concentration ethanol solution collected by the resin at low temperature by using an MVR evaporator to one fifth of the volume of the feed liquid, discharging, standing the discharged feed liquid in a cold storage for precipitation, controlling the temperature at-5 ℃, standing for 8 hours, and filtering;
4) drying
Drying the filtered precipitate in an oven at 50 deg.C for 5 hr to obtain the final product.
Example 4 preparation of a gorgonian hydrating moisturizing mask
The essence of the facial mask consists of the following raw materials in parts by weight: 0.05 part by weight of hydroxyethyl acrylate/sodium acryloyldimethyl taurate copolymer, 0.1 part by weight of xanthan gum, 0.05 part by weight of sclerotium rolfsii gum, 5 parts by weight of glycerin, 3 parts by weight of butylene glycol, 0.3 part by weight of gorgonian extract (prepared in example 1), 0.3 part by weight of CAB-35 (cocamidopropyl betaine), 0.2 part by weight of olivem300 emulsifier, 1 part by weight of a165 (glyceryl stearate/PEG-100 stearate), 0.3 part by weight of GTCC (caprylic/capric acid and triglyceride), 0.3 part by weight of grape seed essential oil, and water to 100 parts by weight.
Detecting according to cosmetic safety technical Specification (2015 edition), QB/T2872-2017, and filling into facial mask bag containing non-woven fabric cut into adult face shape.
Example 5 preparation of a Lissaria pseudopterogorgia moisturizing mask
The essence of the facial mask consists of the following raw materials in parts by weight: 0.1 part by weight of hydroxyethyl acrylate/sodium acryloyldimethyl taurate copolymer, 0.3 part by weight of xanthan gum, 0.01 part by weight of sclerotium rolfsii gum, 10 parts by weight of glycerin, 5 parts by weight of butylene glycol, 0.5 part by weight of gorgonian extract (prepared in example 2), 0.15 part by weight of CAB-35 (cocamidopropyl betaine), 0.05 part by weight of olivem300 emulsifier, 0.05 part by weight of a165 (glyceryl stearate/PEG-100 stearate), 0.05 part by weight of GTCC (from caprylic/capric acid and triglyceride), 0.5 part by weight of grape seed essential oil, and water to 100 parts by weight.
Detecting according to cosmetic safety technical Specification (2015 edition), QB/T2872-2017, and filling into facial mask bag containing non-woven fabric cut into adult face shape.
Example 6 preparation of a Lissaria pseudopterogorgia moisturizing mask
The essence of the facial mask consists of the following raw materials in parts by weight: 0.01 part by weight of hydroxyethyl acrylate/sodium acryloyldimethyl taurate copolymer, 0.05 part by weight of xanthan gum, 0.1 part by weight of sclerotium rolfsii gum, 2 parts by weight of glycerin, 2 parts by weight of butylene glycol, 0.03 part by weight of gorgonian extract (prepared in example 3), 0.05 part by weight of CAB-35 (cocamidopropyl betaine), 0.3 part by weight of olivem300 emulsifier, 0.05 part by weight of a165 (glyceryl stearate/PEG-100 stearate), 0.01 part by weight of GTCC (caprylic/capric acid and triglyceride), 0.2 part by weight of grape seed essential oil, and water to 100 parts by weight.
Detecting according to cosmetic safety technical Specification (2015 edition), QB/T2872-2017, and filling into facial mask bag containing non-woven fabric cut into adult face shape.
Clinical test example mask Performance test
1. Mask integrity Performance test
6 volunteers with basic knowledge of cosmetics of different ages, sexes and skin types are selected to score each index of the facial mask (prepared in example 4), the score of each index is from 1 to 10, the larger the numerical value is, the better the evaluation is represented, and the scoring result is shown in the following figure 1.
2. Mask moisturizing Performance test
The moisture retention of the mask (prepared in example 4) was tested by selecting 6 volunteers with basic knowledge of cosmetics of different ages, sexes, and skin types. The test method is as follows: the skin of the face was washed with clean water and facial cleanser at room temperature of 25 ℃ and a relative humidity of 50%, and then dried with a paper towel, and the left half of each test person was applied with a mask cloth soaked with ultrapure water, and the right half was applied with a mask cloth soaked with the essence prepared in example 4 (the same as the mask cloth used for the left face). Removing the mask cloth after 30min and 60min, respectively, and measuring the facial skin of the subject with a digital skin moisture tester 0min, 60min, 120 min and 240min after removing the mask to obtain the skin moisture content. The results are shown in Table 1 below
TABLE 1 skin moisture content
The results show that the mask disclosed by the invention has good moisturizing effect, is safe and has no irritation.
Claims (5)
1. The gorgonia hydrating and moisturizing mask is characterized by consisting of essence and mask cloth cut into the shape of an adult face, wherein the essence consists of the following raw materials in parts by weight:
0.01-0.1 part of hydroxyethyl acrylate/sodium acryloyldimethyl taurate copolymer, 0.01-0.3 part of xanthan gum, 0.01-0.1 part of sclerotium rolfsii gum, 1-10 parts of glycerol, 1-5 parts of butanediol, 0.01-0.5 part of gorgonian extract, 0.15-0.5 part of CAB-35 (cocamidopropyl betaine), 0.01-0.3 part of olivem300 emulsifier, 0.01-2 parts of A165 (glyceryl stearate/PEG-100 stearate), 0.01-0.5 part of GTCC (composed of caprylic/capric acid and triglyceride), 0.01-0.5 part of grape seed essential oil and water to 100 parts by weight.
2. The mask of claim 1, wherein the mask cloth is a non-woven fabric, silk or bio-fiber.
3. The mask of claim 1, wherein the gorgonian extract is prepared by the following method:
1) extraction of
(1) Pulverizing and sieving herba Salicornia Herbacea raw material to obtain 50-70 mesh fine granules, and extracting with deionized water at 55-60 deg.C; extracting for three times, wherein the ratio of the first material to the liquid is 1: 6, 1 for the second time: 4, third time is 1: 3, 2 hours each time;
(2) after extraction, combining the three filtrates, concentrating at low temperature by using an MVR evaporator to obtain a feed liquid with a specific gravity of 1.11-1.13, and discharging the feed liquid for later use;
2) per resin
Purifying the extracted and concentrated feed liquid by adopting a macroporous adsorption resin column, wherein the sample loading amount is 2 column volumes, eluting by using 16-20 vol% low-concentration ethanol, the elution volume is 3-5 column volumes, then eluting by using 95 vol% high-concentration ethanol, the elution volume is 2-2.5 column volumes, and collecting the eluent at this time;
3) concentrating
Concentrating the high concentration ethanol solution collected by the resin at low temperature by an MVR evaporator to one fifth of the volume of the solution, discharging, standing the discharged solution in a cold storage for precipitation, controlling the temperature at-3 to-5 ℃, standing for 8 hours, and filtering;
4) drying
Drying the filtered precipitate in an oven at 50 deg.C for 5 hr to obtain the final product.
4. The mask pack of claim 3, wherein the macroporous adsorbent resin column is a non-polar macroporous adsorbent resin comprising one or more of HP20, HPD100, HPD300, and D101 macroporous adsorbent resins.
5. Use of the mask pack according to any one of claims 1 to 4 for preparing a skin care product having moisturizing and hydrating functions.
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