CN1112416C - 亚麻籽胶生产工艺 - Google Patents

亚麻籽胶生产工艺 Download PDF

Info

Publication number
CN1112416C
CN1112416C CN00133515A CN00133515A CN1112416C CN 1112416 C CN1112416 C CN 1112416C CN 00133515 A CN00133515 A CN 00133515A CN 00133515 A CN00133515 A CN 00133515A CN 1112416 C CN1112416 C CN 1112416C
Authority
CN
China
Prior art keywords
glue
flaxseed gum
described production
drying
concentrated
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
CN00133515A
Other languages
English (en)
Other versions
CN1319634A (zh
Inventor
王琴声
孙晓冬
史峰山
赵秀峰
张贵彬
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
XINJIANG LINSEED BIOLOGIC TECHNOLOGIES CO.,LTD.
Original Assignee
CHANGJI LUQI BIOLOGICAL PRODUCTS Co Ltd XINJIANG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by CHANGJI LUQI BIOLOGICAL PRODUCTS Co Ltd XINJIANG filed Critical CHANGJI LUQI BIOLOGICAL PRODUCTS Co Ltd XINJIANG
Priority to CN00133515A priority Critical patent/CN1112416C/zh
Publication of CN1319634A publication Critical patent/CN1319634A/zh
Priority to AU2002221476A priority patent/AU2002221476A1/en
Priority to PCT/CN2001/001546 priority patent/WO2002038690A1/zh
Application granted granted Critical
Publication of CN1112416C publication Critical patent/CN1112416C/zh
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Landscapes

  • Jellies, Jams, And Syrups (AREA)

Abstract

本发明的从亚麻籽中提取亚麻籽胶的方法，包括以下步骤：亚麻籽原料经去除杂物、水洗后，用水浸提；通过液固相分离，得到提取胶液；在减压下浓缩提取胶液；浓缩液经乙醇沉淀得到絮状沉淀，并对沉淀进行压榨分离；以热风烘干淀淀物；粉碎烘干物，得到亚麻籽胶产品；或浓缩液直接进行热风或微波干燥，粉碎干燥物，得到亚麻籽胶产品。本发明的提胶方法工艺简单，提取率稳定在12%以上，产品主要技术指标-粘度稳定在5000-8000mpa·s以上，并且对环境无污染，生产成本也大大降低。本发明的亚麻籽胶可在食品、制药、化妆品等领域用作增稠剂、保湿剂、悬浮稳定剂、乳化剂和粘接剂等，具有粘度高、乳化性强、保湿性和悬浮稳定性好等优点。

Description

亚麻籽胶生产工艺
本发明涉及一种新型植物胶-亚麻籽胶的制造方法。
亚麻籽胶是一种纯天然、无污染、多功能、营养丰富的植物胶，是国家绿色食品发展中心认证的绿色食品添加剂，主要在食品、制药、化妆品等生产领域中用做增稠剂、保湿剂、稳定剂、乳化剂和粘接剂。
本发明的目的是：提出一种从亚麻籽中提取亚麻籽胶的新工艺。
目前亚麻籽胶的生产尚无成熟可行的生产工艺，其关键技术是胶的提取、分离及干燥方法。已有的提取方法或产率低或造成严重的环境污染。利用传统的喷雾干燥方法不能得到合格的固胶产品，真空干燥及冷冻干燥方法成本高且产率低。本发明提出的生产方法工艺简单，可大幅度降低生产成本，无环境污染，且使提胶产率稳定在12％以上，所得固胶产品与同类胶(如卡拉胶、魔芋胶等)相比，性能优越，是理想的替代产品。提胶后的亚麻籽仍可榨油，出油率与未提胶前相比无明显差别。
本发明的实现是通过以下工艺：原料(亚麻籽)→去杂→水洗→软化水洗→浸提→籽液分离→浓缩、热风干燥或酒精沉淀后干燥或微波加热干燥→粉碎→成品，其中浸提、分离与制取胶粉的方法是本发明的关键技术。首次浸提时控制料液比为1∶3-15，其后各次浸提时控制料液比为1∶2-8，并在浸提过程中保持温度为35-100℃，每次浸提时间为10-100分钟，浸提过程中需不断搅拌，但无需加入其他任何化学试剂。对浸提后的混合物进行籽液分离是生产工艺的难点之一，本发明提出采用提取罐内压滤或配合刮板进行泵吸过滤的方法很好的解决了这一问题。由提取之胶液制取干胶胶粉是本发明的又一突破，胶液采用在常压或减压500-700毫米汞柱及70-140℃热风条件下配合刮板器使之浓缩或微波浓缩，可在较短的时间内使胶液浓缩至原体积的1/2-1/20，并可直接干燥，且保持亚麻籽胶性质不发生变化；或将浓缩后混合胶液冷却并迅速搅拌后加入95％乙醇使固胶沉淀，固液分离后，再以热风吹扫干燥或将液胶于微波环境下浓缩干燥。利用上述方法，可使提胶率达12-15％本发明优选工艺为：原料→去杂→水洗→软化水洗→软化水浸提→液固相分离→浓缩干燥或酒精沉淀后干燥→粉碎→成品。优选以软化水作为浸提溶剂，分次提取亚麻籽胶，首次提取时亚麻籽与浸提溶剂的重量比为1∶3-15，其后各次提取时亚麻籽与浸提溶剂的重量比为1∶2-8。优选其浸提温度为35-100℃，常压下经10-100分钟完成一次提取。优选采用提取罐内加压或泵吸并配合刮板进行过滤的方法实施液固相分离。优选对所产胶液采用加热并配合使用刮板器的方法实施浓缩及干燥。优选提取之胶液在常压或减压500-700毫米汞柱下经刮板法浓缩至原胶液体积之1/2-1/20，采用常压或减压500-700毫米汞柱条件下热风吹扫干燥法，热风温度70-140℃，吹扫时间20-80分钟。优选胶液经浓缩至原胶液体积之1/2-1/20时，冷至室温并在100-800转/分钟速度下搅拌后，按重量比1∶0.6-1.5加入95％乙醇使固胶沉淀，固液分离后，以80-100℃热风烘干。优选胶液经微波加热浓缩至原胶液体积1/2-1/20时，涂布于适当载体上，继续使用微波加热干燥。
最佳实施方式
实施例1
1、将精选的亚麻籽，经水洗后，加入与原料重量比1∶3-15、温度35-100℃软化水，在常压下搅拌提取10-100分钟，他离籽液，得到胶液A。
2、将步骤1分离的固料加入重量比1∶2-8、温度-100℃的软化水，在常压下搅拌提取10-100分钟，浸提3次，分离籽液，得到胶液B、C、D。
3、合并胶液A、B、C、D，以70-110℃热风加热并配合使用刮板器浓缩至原胶液体积的1/2-1/20。
4、将浓缩液涂布于聚酯网上，以70-140℃热风吹扫0.5-2小时，同时用刮膜装置刮翻涂布物，干燥后粉碎即得固胶产品。实例2在前述实例1-3的基础上，将浓缩液冷却，迅速搅拌后，以1∶0.8-1.5配比(质量比)加入95％乙醇，待沉淀完全后，分离固相，以80-100℃热风烘干，粉碎后即得固胶产品。
利用本发明工艺所得亚麻籽胶产品技术分析结果见表1。
             表1 亚麻籽胶技术指标分析结果
     项目                             测定结果
     水分(％)                         11
     灰分(％)                         6-10
     pH(1％水溶液)                    6.2±0.5
     粘度(mpa·s，1％水溶液)          5000-8000
     水不溶物(％)                     1.8
     果胶酸                           ＜4

Claims (8)

1.一种以亚麻籽为原料生产亚麻籽胶的方法，其工艺为：原料→去杂→水洗→软化水洗→软化水浸提→液固相分离→浓缩干燥或酒精沉淀后干燥→粉碎→成品。
2.按照权利要求1所述生产亚麻籽胶方法，其特征在于：以软化水作为浸提溶剂，分次提取亚麻籽胶，首次提取时亚麻籽与浸提溶剂的重量比为1∶3-15，其后各次提取时亚麻籽与浸提溶剂的重量比为1∶2-8。
3.按照权利要求1所述生产亚麻籽胶的方法，其浸提温度为35-100℃，常压下经10-100分钟完成一次提取。
4.按照权利要求1所述生产亚麻籽胶的方法，其特征在于：采用提取罐内加压或泵吸并配合刮板进行过滤的方法实施液固相分离。
5.按照权利要求1所述生产亚麻籽胶的方法，其特征在于：对所产胶液采用加热并配合使用刮板器的方法实施浓缩及干燥。
6.按照权利要求1所述生产亚麻籽胶的方法，其特征在于：提取之胶液在常压或减压500-700毫米汞柱下经刮板法浓缩至原胶液体积之1/2-1/20，采用常压或减压500-700毫米汞柱条件下的热风吹扫干燥法，热风温度70-140℃，吹扫时间20-80分钟。
7.按照权利要求1所述生产亚麻籽胶的方法，其特征在于：胶液经浓缩至原胶液体积之1/2-1/20时，冷至室温并在100-800转/分钟速度下搅拌后，按重量比1∶0.6-1.5加入95％乙醇使固胶沉淀，固液分离后，以80-100℃热风烘干。
8.按照权利要求1所述生产亚麻籽胶的方法，其特征在于：胶液经微波加热浓缩至原胶液体积1/2-1/20时，涂布于适当载体上，继续使用微波加热干燥。
CN00133515A 2000-02-01 2000-11-09 亚麻籽胶生产工艺 Expired - Lifetime CN1112416C (zh)

Priority Applications (3)

Application Number Priority Date Filing Date Title
CN00133515A CN1112416C (zh) 2000-02-01 2000-11-09 亚麻籽胶生产工艺
AU2002221476A AU2002221476A1 (en) 2000-11-09 2001-11-09 A method of extracting flax gum from flax seed
PCT/CN2001/001546 WO2002038690A1 (fr) 2000-11-09 2001-11-09 Procede d'extraction de graines de lin a partir d'une gomme de lin

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
CN00101272.X 2000-02-01
CN00101272 2000-02-01
CN00133515A CN1112416C (zh) 2000-02-01 2000-11-09 亚麻籽胶生产工艺

Publications (2)

Publication Number Publication Date
CN1319634A CN1319634A (zh) 2001-10-31
CN1112416C true CN1112416C (zh) 2003-06-25

Family

ID=25739180

Family Applications (1)

Application Number Title Priority Date Filing Date
CN00133515A Expired - Lifetime CN1112416C (zh) 2000-02-01 2000-11-09 亚麻籽胶生产工艺

Country Status (1)

Country Link
CN (1) CN1112416C (zh)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1330725C (zh) * 2003-03-07 2007-08-08 清华大学 一种从亚麻籽皮中提取亚麻籽胶的方法
CN101838406B (zh) * 2010-05-21 2011-12-07 甘肃亚兰特种药材饮片生产有限公司 从亚麻籽中同时提取分离亚麻籽胶和亚麻木酚素的方法
CN105037573B (zh) * 2015-07-03 2017-10-03 暨南大学 一种具有抗病毒和免疫活性的亚麻籽多糖的制备及其应用
CN110663774A (zh) * 2019-11-01 2020-01-10 辽宁晟麦实业股份有限公司 一种冲调性良好的高膳食纤维亚麻籽粉及其制备方法

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1211602A (zh) * 1998-08-17 1999-03-24 清华大学 一种从亚麻子壳中干法提取亚麻胶的方法
CN1263139A (zh) * 1999-02-12 2000-08-16 清华大学 一种从亚麻子中湿法提取亚麻胶的方法

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1211602A (zh) * 1998-08-17 1999-03-24 清华大学 一种从亚麻子壳中干法提取亚麻胶的方法
CN1263139A (zh) * 1999-02-12 2000-08-16 清华大学 一种从亚麻子中湿法提取亚麻胶的方法

Also Published As

Publication number Publication date
CN1319634A (zh) 2001-10-31

Similar Documents

Publication Publication Date Title
CN102732050B (zh) 一种从栀子中制备栀子色素的方法
CN1970578B (zh) 豆渣中水溶性大豆多糖的微波提取方法
CN101613418A (zh) 一种提取双孢蘑菇多糖的方法
CN104757191A (zh) 一种用于制造速溶茶粉的酶解工艺
CN105852189A (zh) 一种利用废次烟叶制备烟草浸膏的方法
CN107686773A (zh) 一种从迷迭香中提取迷迭香精油和抗氧化剂的方法
CN105237654A (zh) 一种利用柑橘皮提取果胶的方法
CN105646301B (zh) 从大蒜中提取蒜氨酸联产蒜多糖和蒜粉的方法
CN106866397B (zh) 一种低本高效的姜黄素提取方法
JPH06254382A (ja) マイクロカプセルの製造法およびその製造装置
CN102492054B (zh) 一种大豆种皮果胶类凝胶多糖的制备方法
CN108179065A (zh) 一种茉莉花精油的提取方法
CN102757515A (zh) 一种从柑橘果皮中提取高纯度类黄酮和果胶的方法
CN1112416C (zh) 亚麻籽胶生产工艺
CN107011457B (zh) 一种从红薯废水中提取制备非淀粉多糖及小分子营养分子的方法
CN1163155C (zh) 一种微胶囊植物素的生产方法
CN104970418A (zh) 一种生物复合酶法桂花汁的生产方法
CN1220094A (zh) 一种亚麻籽综合利用方法
CN106916801A (zh) 一种木瓜酶制剂的产业化制备方法及其应用
CN105566944A (zh) 辣椒精粗品中分离脱色辣椒精和辣椒色素的方法
CN106136117A (zh) 一种用高红素鲜番茄生产番茄红和浓缩番茄汁的方法
CN105362346A (zh) 一种从厚朴皮中制备高纯度厚朴总酚的方法
CN105924536B (zh) 一种改进的沙蒿胶乳化剂的加工方法
CN107149075A (zh) 一种澄清猕猴桃粉及其制备方法
WO2002038690A1 (fr) Procede d'extraction de graines de lin a partir d'une gomme de lin

Legal Events

Date Code Title Description
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C06 Publication
PB01 Publication
C14 Grant of patent or utility model
GR01 Patent grant
C57 Notification of unclear or unknown address
DD01 Delivery of document by public notice

Addressee: Chen Peng

Document name: payment instructions

C57 Notification of unclear or unknown address
DD01 Delivery of document by public notice

Addressee: Chen Peng

Document name: payment instructions

C57 Notification of unclear or unknown address
DD01 Delivery of document by public notice

Addressee: Chen Peng

Document name: Notification to Pay the Fees

C57 Notification of unclear or unknown address
DD01 Delivery of document by public notice

Addressee: Chen Peng

Document name: Notification that Application Deemed not to be Proposed

ASS Succession or assignment of patent right

Owner name: BEIJING LVQI ANKANG FLAXSEED GUM INSTITUTE

Free format text: FORMER OWNER: XINJIANG LV QI BIOLOGY SCIENCE (GROUP)CO., LTD.

Effective date: 20080523

C41 Transfer of patent application or patent right or utility model
C56 Change in the name or address of the patentee

Owner name: XINJIANG LVQI COMPANY (GROUP)BIOLOGY SCIENCE CO.,

Free format text: FORMER NAME OR ADDRESS: GREEN FLAG BIOLOGICAL PRODUCTS CO., LTD., CHANGJI CITY, XINJIANG

Owner name: XINJIANG LV QI BIOLOGY SCIENCE (GROUP)CO., LTD.

Free format text: FORMER NAME OR ADDRESS: XINJIANG LVQI COMPANY (GROUP)BIOLOGY SCIENCE CO., LTD.

CP03 Change of name, title or address

Address after: No. 8, Beijing North Road, Changji, the Xinjiang Uygur Autonomous Region: 831100

Patentee after: Xinjiang green flag Biotechnology (Group) Co.,Ltd.

Address before: No. 8, Beijing North Road, Changji, the Xinjiang Uygur Autonomous Region: 831100

Patentee before: Xinjiang green flag enterprise (Group) biological science and Technology Co.,Ltd.

Address after: No. 8, Beijing North Road, Changji, the Xinjiang Uygur Autonomous Region: 831100

Patentee after: Xinjiang green flag enterprise (Group) biological science and Technology Co.,Ltd.

Address before: No. 8, Beijing North Road, Changji, the Xinjiang Uygur Autonomous Region: 831100

Patentee before: XINJIANG LVQI BIOLOGICAL PRODUCTS Co.,Ltd.

TR01 Transfer of patent right

Effective date of registration: 20080523

Address after: Executive Hotel, 2 North Taiping Road, 201, Beijing, Haidian District

Patentee after: Beijing green flag Ankang flaxseed gum Research Institute

Address before: No. 8, Beijing North Road, Changji, the Xinjiang Uygur Autonomous Region

Patentee before: Xinjiang green flag Biotechnology (Group) Co.,Ltd.

C56 Change in the name or address of the patentee
CP01 Change in the name or title of a patent holder

Address after: Executive Hotel, 2 North Taiping Road, 201, Beijing, Haidian District

Patentee after: Beijing DeLong sunshine hydrocolloid Institute

Address before: Executive Hotel, 2 North Taiping Road, 201, Beijing, Haidian District

Patentee before: Beijing green flag Ankang flaxseed gum Research Institute

C56 Change in the name or address of the patentee

Owner name: BEIJING DELANG YANGGUANG HYDROCOLLOIDS INSTITUTE

Free format text: FORMER NAME: BEIJING LVQI ANKANG FLAXSEED GUM INSTITUTE

ASS Succession or assignment of patent right

Owner name: WANG QINSHENG

Free format text: FORMER OWNER: BEIJING DELANG SUNSHINE HYDROCOLLOIDS INSTITUTE

Effective date: 20110707

C41 Transfer of patent application or patent right or utility model
COR Change of bibliographic data

Free format text: CORRECT: ADDRESS; FROM: 100088 201, DEHENG BUSINESS CENTER, NO. 2, BEITAIPINGZHUANG ROAD, HAIDIAN DISTRICT, BEIJING TO: 100088 602, UNIT 5, BUILDING 4, LUOZHUANG DONGLI RESIDENTIAL QUARTER, ZHICHUN ROAD, HAIDIAN DISTRICT, BEIJING

TR01 Transfer of patent right

Effective date of registration: 20110707

Address after: 100088, Beijing, Zhichun Road, Luozhuang, Haidian District East Lane 4, building 5, 602

Patentee after: Wang Qinsheng

Address before: 100088, Executive Hotel, 2 Taiping Road, 201, Beijing, Haidian District

Patentee before: Beijing DeLong sunshine hydrocolloid Institute

DD01 Delivery of document by public notice

Addressee: Lu Liping

Document name: Notification of Passing Examination on Formalities

ASS Succession or assignment of patent right

Owner name: XINJIANG LINSEED BIOLOGIC TECHNOLOGIES CO., LTD.

Free format text: FORMER OWNER: WANG QINSHENG

Effective date: 20120426

C41 Transfer of patent application or patent right or utility model
COR Change of bibliographic data

Free format text: CORRECT: ADDRESS; FROM: 100088 HAIDIAN, BEIJING TO: 835400 ILI KAZAKH AUTONOMOUS PREFECTURE, XINJIANG UYGUR AUTONOMOUS REGION

TR01 Transfer of patent right

Effective date of registration: 20120426

Address after: 835400 the Xinjiang Uygur Autonomous Region, Yili, Gongliu County town on the north side of the mirror Road

Patentee after: XINJIANG LINSEED BIOLOGIC TECHNOLOGIES CO.,LTD.

Address before: 100088, Beijing, Zhichun Road, Luozhuang, Haidian District East Lane 4, building 5, 602

Patentee before: Wang Qinsheng

CX01 Expiry of patent term
CX01 Expiry of patent term

Granted publication date: 20030625