CN110974766A

CN110974766A - Rose fragrance body lotion and preparation process thereof

Info

Publication number: CN110974766A
Application number: CN202010091681.2A
Authority: CN
Inventors: 赵金虎; 钟俊敏; 彭美兴
Original assignee: Guangzhou Barburly Cosmetic Co ltd
Current assignee: Guangzhou Barburly Cosmetic Co ltd
Priority date: 2020-02-14
Filing date: 2020-02-14
Publication date: 2020-04-10

Abstract

The invention discloses rose fragrance body lotion and a preparation process thereof. The rose fragrance body lotion contains active ingredients such as rose petals, nicotinamide, oldenlandia diffusa extracts, spot red orchid extracts and SESBANIA (SESBANIA flower extracts) and has the function of moistening skin, can supplement water and nutrients required for the skin, prevents the skin from drying and lack of water, and enables the skin to be ruddy, fair, glossy, full and elastic.

Description

Rose fragrance body lotion and preparation process thereof

Technical Field

The invention relates to the field of cosmetics, and in particular relates to rose fragrance body lotion and a preparation process thereof.

Background

The body lotion is cosmetic lotion applied on body after bath, and has effects of moisturizing whole body, whitening skin, and moistening. With the maturity and development of the technology, the body lotion can be subdivided into the functions of smoothing, sun-screening, slimming, repairing and maintaining, perfuming and getting lost and the like.

The rose is a plant of rosa in rosaceae, is originally produced in north China, Japan, Korean and the like, has bright color and strong fragrance of flowers, and is mainly used for processing food and extracting rose essential oil. Therefore, the method is widely applied to the aspects of cosmetics, foods, fine chemical engineering and the like. The rose also has high medicinal value and economic value, contains flavone, organic acid, phenols, vitamins, soluble sugar, alkaloid, and nutrient components such as more than 10 amino acids and more than mineral elements. The rose is rich in color, the pigment of the rose is anthocyanin, the rose belongs to polyphenol compounds, is an effective component of health food approved by China, and has the effects of resisting oxidation, resisting free radicals, protecting cardiovascular and central nervous systems and the like.

The common methods for extracting rose essential oil at present comprise a water vapor extraction method, an organic solvent extraction method, a squeezing method, an adsorption extraction method, an enzyme fermentation method, a lipolysis method and a supercritical CO extraction method₂Extraction methods, etc. Among the methods, the steam distillation method is convenient to operate, but takes longer time and is easy to decompose at high temperature, so that the yield is not high; the obtained essential oil has many impurities and the organic solvent is not easy to remove by an organic solvent extraction method; supercritical CO₂The extraction method has higher requirements on test equipment and larger investment.

Disclosure of Invention

The invention aims to solve the technical problem of providing the rose-fragrance body lotion which has the function of moistening skin, can supplement water and nutrients required for the skin, prevents the skin from drying and lack of water, and enables the skin to become ruddy, white, glossy, full and elastic.

The specific technical scheme of the invention is as follows:

the rose fragrance body lotion comprises 9-30% of whitening skin care composition by mass, wherein the whitening skin care composition comprises the following components in parts by mass: 1-5 parts of rose petal, 5-10 parts of nicotinamide, 1-5 parts of oldenlandia diffusa (hedyotis diffusa) extract, 1-5 parts of ORCHIS maculota (ORCHIS maculiata) flower extract and 1-5 parts of SESBANIA GRANDIFLORA (SESBANIA GRANDIFLORA) flower extract.

Preferably, the whitening skin care composition contains the following components in parts by mass: 3 parts of rose petals, 8 parts of nicotinamide, 3 parts of oldenlandia DIFFUSA (HEDYOTIS diffuis) extract, 3 parts of ORCHIS MACULATA (ORCHIS MACULATA) flower extract and 3 parts of SESBANIA GRANDIFLORA (SESBANIA GRANDIFLORA) flower extract.

Further, the formula of the rose fragrance body milk can also comprise the following components in percentage by mass: 0.001-0.01% of rose (ROSA RUGOSA) flower oil, 5-10% of humectant, 10-20% of emollient, 1-2% of emulsifier, 0.1-1% of thickener and 0.1-1% of preservative.

The humectant can be one or more of glycerol, propylene glycol, butanediol, pentanediol, hexanediol, sorbitol, ethanol, polyethylene glycol-8, polyethylene glycol-32, dipropylene glycol, diglycerol, glyceryl polyether-26, polyglycerol-10, polyglycerol-8, trehalose, biogel-4 and biogel-1.

The emollient described in the present invention may be one or a mixture of caprylic/capric triglyceride, isopropyl myristate, isononyl isononanoate, ethylhexyl palmitate, ethylene glycol distearate, glycerol tri (ethylhexanoate), cyclopentadimethylsiloxane, trimethylsiloxysilicate, polydimethylsiloxane, dimethiconol, lanolin, emu oil, horse fat, sea buckthorn fruit oil, ginger root oil, soybean oil, safflower seed oil, olive oil, evening primrose oil, rose hip oil, avocado oil, jojoba oil, grape seed oil, meadowfoam seed oil, shea butter oil, cocoa butter, macadamia nut oil, camellia seed oil, palm kernel oil, camellia seed oil, rosa canina fruit oil, wheat germ oil, and sweet almond oil.

The emulsifier of the invention can be one of coco glucoside, polyglyceryl-2 dipolyhydroxystearate, polysorbate-60, ceteareth-25, sorbitan sesquioleate, glyceryl stearate, PEG-100 stearate, coco glucoside, methyl glucose sesquistearate, PEG-20 methyl glucose sesquistearate, potassium lauryl phosphate, polysorbate-20, hydrogenated lecithin or a mixture thereof.

The thickener of the present invention may be cetostearyl alcohol, hydroxypropyl methylcellulose, xanthan gum, sodium carbomer, polyacrylate cross-linked polymer-6, sodium magnesium lithium silicate, sodium alginate, acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, polyvinylpyrrolidone, magnesium aluminum silicate, hydroxyethyl cellulose, acrylic acid (ester) copolymer, sodium hyaluronate, chondroitin sulfate, or a mixture of one or more of gums.

The preservative can be one or the mixture of more than one of phenoxyethanol, methyl hydroxybenzoate, ethylparaben, p-hydroxyacetophenone, hexanediol, pentanediol, potassium sorbate and sodium benzoate.

The embodiment of the invention also provides a preparation method of the rose petals, which comprises the following steps:

(1) picking rose petals, drying the rose petals in the shade indoors, adding the rose petals into hot saturated sucrose aqueous solution, and uniformly stirring;

(2) adding Mel, and stirring; cooling to room temperature, taking out the treated rose petals, and air drying.

In some of these embodiments, the temperature of the saturated aqueous sucrose solution in step (1) is 70-80 ℃.

In some of these embodiments, the honey in step (1) is added in an amount of 10-20% by weight of the saturated aqueous sucrose solution.

The technical scheme provided by the embodiment of the invention has the following beneficial effects:

(1) the invention selects rose petals, nicotinamide, oldenlandia DIFFUSA (HEDYOTIS diffuis) extract, ORCHIS MACULATA (ORCHIS MACULATA) flower extract and SESBANIA GRANDIFLORA (SESBANIA GRANDIFLORA) flower extract as the whitening skin care composition, and the whitening skin care composition has the function of moisturizing skin when being applied to body milk, can supplement water and nutrients required for the skin, prevents the skin from drying and water shortage, and ensures that the skin becomes more ruddy, white, glossy, full and elastic;

(2) the invention provides a preparation method of rose petals, which reserves the beautiful appearance and all nutrient components of roses and is also beneficial to long-term storage.

Drawings

FIG. 1 is a graph of skin elasticity test results;

fig. 2 is a graph of skin whitening test results.

Detailed Description

The embodiments in the description are only for illustrating the present invention and do not limit the scope of the present invention. The scope of the present invention is defined only by the appended claims, and any omissions, substitutions, or modifications made based on the embodiments disclosed herein will fall within the scope of the present invention.

The following detailed description of preferred embodiments of the invention and the examples included therein will make the present invention more readily understandable. Unless defined otherwise, all technical and scientific terms used herein have the same meaning as commonly understood by one of ordinary skill in the art to which this invention belongs. In case of conflict, the present specification, including definitions, will control.

The term "prepared from …" as used herein is synonymous with "comprising". The terms "comprises," "comprising," "includes," "including," "has," "having," "contains," "containing," or any other variation thereof, as used herein, are intended to cover a non-exclusive inclusion. For example, a composition, process, method, article, or apparatus that comprises a list of elements is not necessarily limited to only those elements but may include other elements not expressly listed or inherent to such composition, process, method, article, or apparatus.

When an amount, concentration, or other value or parameter is expressed as a range, preferred range, or as a range of upper preferable values and lower preferable values, this is to be understood as specifically disclosing all ranges formed from any pair of any upper range limit or preferred value and any lower range limit or preferred value, regardless of whether ranges are separately disclosed. For example, when a range of "1 to 5" is disclosed, the described range should be interpreted to include the ranges "1 to 4", "1 to 3", "1 to 2 and 4 to 5", "1 to 3 and 5", and the like. When a range of values is described herein, unless otherwise stated, the range is intended to include the endpoints thereof and all integers and fractions within the range.

In addition, the indefinite articles "a" and "an" preceding an element or component of the invention are not intended to limit the number requirement (i.e., the number of occurrences) of the element or component. Thus, "a" or "an" should be read to include one or at least one, and the singular form of an element or component also includes the plural unless the stated number clearly indicates that the singular form is intended.

For the purpose of enhancing understanding of the present invention, the present invention will be further described in detail with reference to the following examples, which are provided for illustration only and are not to be construed as limiting the scope of the present invention.

The oldenlandia DIFFUSA (HEDYOTIS DIFFUSA) extract is a standard extract prepared by extracting oldenlandia DIFFUSA. The preparation method comprises pulverizing fresh herba Hedyotidis Diffusae, extracting with 70% ethanol water solution, centrifuging, and filtering.

The extract of the flowers of the ORCHIS MACULATA (ORCHIS MACULATA) is a standard extract prepared by extracting the flowers of the ORCHIS MACULATA. The preparation method comprises pulverizing flos Magnoliae, extracting with 70% ethanol water solution, centrifuging, and filtering.

The SESBANIA GRANDIFLORA (SESBANIA GRANDIFLORA) flower extract is a standard extract prepared by extracting SESBANIA GRANDIFLORA flowers. The preparation method comprises pulverizing Sesbania grandiflora, extracting with 70% ethanol water solution as extraction solvent, centrifuging the extractive solution, and filtering.

Example 1

A preparation method of rose petals comprises the following steps:

(1) picking rose petals, drying in the shade indoors, adding into a saturated sucrose aqueous solution at 70 ℃, and uniformly stirring;

(2) adding honey, and uniformly stirring, wherein the adding amount of the honey is 20% of the weight of the saturated sucrose aqueous solution; cooling to room temperature, taking out the treated rose petals, and air drying.

Example 2

A preparation method of rose petals comprises the following steps:

(1) picking rose petals, drying in the shade indoors, adding into 80 ℃ saturated sucrose aqueous solution, and stirring uniformly;

(2) adding honey, and uniformly stirring, wherein the adding amount of the honey is 10% of the weight of the saturated sucrose aqueous solution; cooling to room temperature, taking out the treated rose petals, and air drying.

Example 3

The rose fragrance body lotion comprises the following components in percentage by mass:

rose petal 5% prepared in example 1

5 percent of nicotinamide

Herba Hedyotidis Diffusae (HEDYOTIS DIFFUSA) extract 1%

Extract of Orchis maculatus (ORCHIS MACULATA) flower 5%

Sesbania GRANDIFLORA (Sesbania GRANDIFLORA) flower extract 1%

Rose (ROSA RUGOSA) flower oil 0.001%

5 percent of glycerin

10 percent of propylene glycol

Caprylic/capric triglyceride 1%

Jojoba oil 5%

1% of polydimethylsiloxane

Potassium lauryl phosphate 1.5%

PEG-100 stearate 0.1%

Cetearyl alcohol 3%

Carbomer 0.3%

Xanthan gum 0.3%

0.3 percent of phenoxyethanol

0.2 percent of methyl hydroxybenzoate

Arginine 0.3%

0.1 percent of hexanediol

The balance of water.

Example 4

rose petal 1% prepared in example 2

10% of nicotinamide

Herba Hedyotidis Diffusae (HEDYOTIS DIFFUSA) extract 5%

Extract of Orchis maculatus (ORCHIS MACULATA) flower 1%

Sesbania GRANDIFLORA (Sesbania GRANDIFLORA) flower extract 5%

Rose (ROSA RUGOSA) flower oil 0.01%

10 percent of glycerin

Propylene glycol 5%

Caprylic/capric triglyceride 5%

Jojoba oil 1%

3 percent of polydimethylsiloxane

Lauryl alcohol potassium phosphate 0.5%

PEG-100 stearate 0.5%

Cetearyl alcohol 1%

Carbomer 0.5%

Xanthan gum 0.1%

0.5 percent of phenoxyethanol

0.1 percent of methyl hydroxybenzoate

0.5 percent of hexanediol

Arginine 0.5%

The balance of water.

Example 5

3% of the petals of Rose obtained in example 2

8 percent of nicotinamide

Herba Hedyotidis Diffusae (HEDYOTIS DIFFUSA) extract 3%

Extract of Orchis maculatus (ORCHIS MACULATA) flower 3%

Sesbania GRANDIFLORA (Sesbania GRANDIFLORA) flower extract 3%

Rose (ROSA RUGOSA) flower oil 0.05%

Glycerol 7%

Propylene glycol 7%

Caprylic/capric triglyceride 3%

Jojoba oil 3%

2% of polydimethylsiloxane

1 percent of potassium lauryl phosphate

PEG-100 stearate 0.3%

Cetostearyl alcohol 2%

Carbomer 0.4%

Xanthan gum 0.2%

0.4 percent of phenoxyethanol

0.15 percent of methyl hydroxybenzoate

0.3 percent of hexanediol

Arginine 0.4%

The balance of water.

The preparation of the above examples 3-5 was as follows:

(1) putting water, glycerol, propylene glycol, methyl hydroxybenzoate, carbomer and xanthan gum into an emulsifying pot, heating to 85 deg.C under stirring, homogenizing for 3-5 min, dissolving and dispersing uniformly, adding potassium lauryl phosphate, and stirring for dissolving;

(2) putting caprylic/capric triglyceride, jojoba oil, polydimethylsiloxane, PEG-100 stearate, and cetostearyl alcohol into an oil phase pan, and heating for dissolving;

(3) pumping the oil phase into an emulsifying pot under stirring, starting homogenizing for 5-10 minutes, adding arginine, keeping the temperature at 85 ℃, and stirring for 30 minutes;

(4) cooling to 48 deg.C, adding flos Rosae Rugosae, nicotinamide, herba Hedyotidis Diffusae (HEDYOTIS diffuis) extract, Orchis maculita (ORCHIS MACULATA) flower extract, Sesbania GRANDIFLORA (SESBANIA GRANDIFLORA) flower extract, flos Rosae Rugosae (ROSA RUGOSA) flower oil, phenoxyethanol, and hexanediol, and stirring; cooling to room temperature, inspecting and discharging.

Experiment 1 stability test

The rose fragrance body lotion prepared in examples 3 to 5 was placed at-15 ℃, room temperature, and 45 ℃ for one month, and then compared with each other to determine whether abnormal conditions such as off-flavor, emulsion breaking, delamination, and petal discoloration occurred, and the abnormal conditions were recorded as being unqualified, otherwise, as being qualified. The details are shown in Table 1.

TABLE 1 stability Table

As can be seen from Table 1, the rose-fragrance body milks obtained in examples 3 to 5 passed the one-month stability test and did not suffer from abnormal conditions such as discoloration of the petals. The rose fragrance body lotion prepared by the embodiment of the invention has good stability, and the prepared rose petals can be used as an active substance to be added into a skin care product without influencing the quality of the skin care product.

Experiment 2 evaluation of efficacy of volunteers

The rose-fragrance body milks obtained in examples 3 to 5 were evaluated for efficacy, and comparative examples 1 to 6 were set as controls. Wherein comparative example 1 differs from example 5 in that the formulation does not contain ingredients of the whitening composition; comparative example 2 differs from example 5 in that the whitening composition active ingredient in its formulation contains only 3wt% rose petals; comparative 3 differs from example 5 in that the formulation contains only 8% by weight of niacinamide as the active ingredient of the whitening composition; comparative example 4 is different from example 5 in that the whitening composition active ingredient in the formulation thereof contains only oldenlandia DIFFUSA (HEDYOTIS DIFFUSA) extract 3 wt%; comparative example 5 differs from example 5 in that the formulation of the whitening composition contains only 3wt% of the extract of the flowers of the ORCHIS MACULATA (ORCHIS MACULATA) plant; comparative example 6 differs from example 5 in that the formulation of the whitening composition contains only 3wt% of the extract of the flowers of SESBANIA grandiflorum (SESBANIA GRANDIFLORA).

90 volunteers were summoned in 9 groups of 10 persons each. Inclusion criteria were: the complexion of the face is dull, the eye corners have obvious fine lines, and the skin lacks elasticity; the test can be well matched, and the life rule can be kept during the research period; all the contents of the informed consent can be read and understood and signed voluntarily; during the test period, the skin care products were discontinued, no further clinical trials were involved in any other research center, and no use of any cosmetics, drugs and nutraceuticals affecting the outcome was agreed to. Exclusion criteria: the skin disease at the tested part may affect the judgment of the test result; those with high allergic constitution; a female who is pregnant, lactating, or intended to be pregnant during the test; severe center of gravity, liver and kidney function damage and severe immunologic hypofunction; those with mental disorders, severe endocrine disorders, and oral contraceptives; adding drugs into clinical testers or other testers of the drugs within 30 days, or patients who have systemic effect on the test result within nearly 1 week; those who had oral and topical cosmetic products within 2 weeks that may have an effect on the outcome of the test; the test person can not be matched; researchers considered unsuitable participants.

After bathing, a proper amount of sample to be tested is smeared on the skin of the body for 1 time every day and is continuously used for 3 months. The elasticity of the back skin of the volunteer before and after the test was measured by a skin elasticity measuring instrument Cutomer MPA580, R2 was measured and averaged for 3 times, the R2 value is the ratio of the amount of springback of the skin without negative pressure to the maximum amount of stretching with negative pressure, and the R2 value is closer to 1, indicating that the skin elasticity is better. Meanwhile, a skin melanin tester MX 18 instrument is used for detecting the melanin content of the back skin of the volunteer before and after the test. The results of the test for the change rate of the specific R2 values are shown in FIG. 1, and the results of the test for the change rate of the melanin content are shown in FIG. 2. Rate of change = (post test value-pre test value)/post test value 100%.

As can be seen in FIG. 1, examples 3-5, which had the complete whitening composition added thereto, had better skin elasticity.

As can be seen from fig. 2, the skin whitening effects of examples 3 to 5, to which the complete whitening composition was added, were more excellent.

The technical features of the above embodiments can be arbitrarily combined, and for the sake of brevity, all possible combinations of the technical features in the above embodiments are not described, but should be considered as the scope of the present specification as long as there is no contradiction between the combinations of the technical features.

The above examples only show some embodiments of the present invention, and the description thereof is more specific and detailed, but not construed as limiting the scope of the invention. It should be noted that, for a person skilled in the art, several variations and modifications can be made without departing from the inventive concept, which falls within the scope of the present invention. Therefore, the protection scope of the present patent shall be subject to the appended claims.

Claims

1. The rose fragrance body lotion is characterized by comprising 9-30% by mass of a whitening skin care composition, wherein the whitening skin care composition comprises the following components in parts by mass: 1-5 parts of rose petal, 5-10 parts of nicotinamide, 1-5 parts of oldenlandia DIFFUSA (HEDYOTIS diffuis) extract, 1-5 parts of ORCHIS MACULATA (ORCHIS MACULATA) flower extract and 1-5 parts of SESBANIA GRANDIFLORA (SESBANIA GRANDIFLORA) flower extract.

2. The rose-fragrance body lotion according to claim 1, wherein the whitening and skin-care composition comprises the following components in parts by mass: 3 parts of rose petals, 8 parts of nicotinamide, 3 parts of oldenlandia DIFFUSA (HEDYOTIS diffuis) extract, 3 parts of ORCHIS MACULATA (ORCHIS MACULATA) flower extract and 3 parts of SESBANIA GRANDIFLORA (SESBANIA GRANDIFLORA) flower extract.

3. The rose fragrance body lotion according to claim 1 or 2, further comprising the following components in percentage by mass: 0.001-0.01% of rose (ROSA RUGOSA) flower oil, 5-10% of humectant, 10-20% of emollient, 1-2% of emulsifier, 0.1-1% of thickener and 0.1-1% of preservative.

4. The rose fragrance body lotion according to claim 1, wherein the preparation method of rose petals comprises the following steps:

5. The rose-scented body milk according to claim 4, wherein the temperature of the saturated sucrose aqueous solution in step (1) is 70-80 ℃.

6. The rose-scented body milk according to claim 4, wherein the honey is added in step (1) in an amount of 10-20% by weight of the saturated sucrose aqueous solution.