CN110894437A - Essential oil composition and preparation method thereof - Google Patents

Essential oil composition and preparation method thereof Download PDF

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Publication number
CN110894437A
CN110894437A CN201811061120.7A CN201811061120A CN110894437A CN 110894437 A CN110894437 A CN 110894437A CN 201811061120 A CN201811061120 A CN 201811061120A CN 110894437 A CN110894437 A CN 110894437A
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Prior art keywords
essential oil
parts
tea
oil
yellow tea
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Pending
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CN201811061120.7A
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Chinese (zh)
Inventor
许娟
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Suzhou Yuanzhou Biological Technology Co Ltd
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Suzhou Yuanzhou Biological Technology Co Ltd
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Priority to CN201811061120.7A priority Critical patent/CN110894437A/en
Publication of CN110894437A publication Critical patent/CN110894437A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/60Moraceae (Mulberry family), e.g. breadfruit or fig
    • A61K36/605Morus (mulberry)
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/82Theaceae (Tea family), e.g. camellia
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K47/00Medicinal preparations characterised by the non-active ingredients used, e.g. carriers or inert additives; Targeting or modifying agents chemically bound to the active ingredient
    • A61K47/44Oils, fats or waxes according to two or more groups of A61K47/02-A61K47/42; Natural or modified natural oils, fats or waxes, e.g. castor oil, polyethoxylated castor oil, montan wax, lignite, shellac, rosin, beeswax or lanolin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61PSPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P17/00Drugs for dermatological disorders
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61PSPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P17/00Drugs for dermatological disorders
    • A61P17/10Anti-acne agents
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61PSPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P31/00Antiinfectives, i.e. antibiotics, antiseptics, chemotherapeutics
    • A61P31/04Antibacterial agents
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q17/00Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
    • A61Q17/005Antimicrobial preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/02Recovery or refining of essential oils from raw materials
    • C11B9/022Refining
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/02Recovery or refining of essential oils from raw materials
    • C11B9/025Recovery by solvent extraction
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/02Recovery or refining of essential oils from raw materials
    • C11B9/027Recovery of volatiles by distillation or stripping
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/30Extraction of the material
    • A61K2236/33Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
    • A61K2236/331Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using water, e.g. cold water, infusion, tea, steam distillation, decoction
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/30Extraction of the material
    • A61K2236/35Extraction with lipophilic solvents, e.g. Hexane or petrol ether

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • General Health & Medical Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • Engineering & Computer Science (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Pharmacology & Pharmacy (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Dermatology (AREA)
  • Epidemiology (AREA)
  • Wood Science & Technology (AREA)
  • General Chemical & Material Sciences (AREA)
  • Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
  • Biotechnology (AREA)
  • Microbiology (AREA)
  • Medical Informatics (AREA)
  • Mycology (AREA)
  • Botany (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • Alternative & Traditional Medicine (AREA)
  • Communicable Diseases (AREA)
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  • Medicines Containing Plant Substances (AREA)

Abstract

The invention relates to an essential oil composition and a preparation method thereof, and the essential oil in the formula comprises, by volume, 50-60 parts of yellow tea, 20-30 parts of mulberry leaves, 5-10 parts of base oil and 5-15 parts of Biluochun tea flowers. Distilling 50 parts of yellow tea by using water vapor for 2-10H, and then condensing and separating oil and water to obtain yellow tea essential oil; putting 30 parts of mulberry leaves and 15 parts of Biluochun tea flowers into a 2000ml flask, adding 500ml of distilled water, and extracting for 5 hours by a water distillation method; after extraction, adding 30ml of ether into the extract for extraction, adding a proper amount of anhydrous Na into the ether layer2SO4Drying for 30min, filtering, and evaporating diethyl ether solvent in water bath at 40 deg.C to obtain mixed essential oil of folium Mori and Biluochun tea flower; mixing the essential oil mixture of the yellow tea essential oil and the mulberry leaf Biluochun tea flower essential oil obtained respectively with the base oil to obtain the essential oil composition. The essential oil mixture can disperse wind and heat, clear away the lung-heat and moisten dryness, calm the liver and improve eyesight, and has the functions of increasing the skin defense capability and reducing the skin tension while cooling blood and stopping bleeding.

Description

Essential oil composition and preparation method thereof
Technical Field
The invention relates to the field of essential oil, in particular to an essential oil composition and a preparation method thereof.
Background
With the improvement of living standard of people, the demand of essential oil is higher and higher, most of the essential oil widely sold in the market at present is prepared by chemical drugs, is easy to cause skin allergy, has other side effects, is expensive in price and is not suitable for being used in large quantity. Many essential oils have poor effects on skin comfort and moisture, have no anti-inflammatory effect, have low universality for whelk patients, and have an allergic phenomenon after being used; other methods are adopted for removing acnes, the acne removing paste is long in time, the deposition of melanin in a body can be increased, scars are serious, and the problem is difficult to solve fundamentally.
Disclosure of Invention
In order to solve the technical problems, the invention provides an essential oil composition according to a first aspect, wherein the essential oil comprises, by volume, 50-60 parts of yellow tea, 20-30 parts of mulberry leaves, 5-10 parts of base oil and 5-15 parts of Biluochun tea flowers.
Preferably, the formula essential oil consists of 50 parts of yellow tea, 30 parts of mulberry leaves, 5 parts of base oil and 15 parts of Biluochun tea flowers according to the volume part ratio.
Preferably, the mulberry leaves are buds of mulberry leaves; the yellow tea is Leishan yellow tea.
Preferably, the base oil is one or two of sweet almond oil, almond oil and wheat germ oil.
Compared with the conventional essential oil, the yellow tea essential oil has the effects of sterilizing and diminishing inflammation, phytol extracted from fresh mulberry leaves, also called phytol and xanthol, is an important raw material for preparing vitamin E and K, and the essential oil extracted from the biluochun tea flowers can disperse wind and heat, clear away the lung-heat, moisten dryness, calm the liver, improve eyesight, cool blood and stop bleeding, and meanwhile has the effects of increasing the skin defense capacity and reducing skin tension.
In a second aspect of the invention, there is provided a process for the preparation of an essential oil composition, the process comprising the steps of:
(1) distilling 50 parts of yellow tea by using water vapor for 2-10H, and then condensing and separating oil and water to obtain yellow tea essential oil;
(2) putting 30 parts of mulberry leaves and 15 parts of Biluochun tea flowers into a 2000ml flask, adding 500ml of distilled water, and extracting for 5 hours by a water distillation method; after extraction, adding 30ml of ether into the extract for extraction, adding a proper amount of anhydrous Na into the ether layer2SO4Drying for 30min, filtering, and evaporating diethyl ether solvent in water bath at 40 deg.C to obtain mixed essential oil of folium Mori and Biluochun tea flower;
(3) and (3) mixing the yellow tea essential oil and the mulberry leaf Biluochun tea flower essential oil mixed essential oil obtained in the steps (1) and (2) respectively with base oil to obtain the essential oil composition.
Detailed Description
The present invention will be specifically described below by way of examples. It should be noted that the following examples are only for illustrating the present invention and should not be construed as limiting the scope of the present invention, and that the insubstantial modifications and adaptations of the present invention by those skilled in the art based on the above disclosure are still within the scope of the present invention.
The disclosure may be understood more readily by reference to the following detailed description of preferred embodiments of the invention and the examples included therein. Unless defined otherwise, all technical and scientific terms used herein have the same meaning as commonly understood by one of ordinary skill in the art to which this invention belongs. In case of conflict, the present specification, including definitions, will control.
The term "prepared from …" as used herein is synonymous with "comprising". The terms "comprises," "comprising," "includes," "including," "has," "having," "contains," "containing," or any other variation thereof, as used herein, are intended to cover a non-exclusive inclusion. For example, a composition, process, method, article, or apparatus that comprises a list of elements is not necessarily limited to only those elements but may include other elements not expressly listed or inherent to such composition, process, method, article, or apparatus.
Approximating language, as used herein throughout the specification and claims, is intended to modify a quantity, such that the invention is not limited to the specific quantity, but includes portions that are literally received for modification without substantial change in the basic function to which the invention is related. Accordingly, the use of "about" to modify a numerical value means that the invention is not limited to the precise value. In some instances, the approximating language may correspond to the precision of an instrument for measuring the value. In the present description and claims, range limitations may be combined and/or interchanged, including all sub-ranges contained therein if not otherwise stated.
In addition, the indefinite articles "a" and "an" preceding an element or component of the invention are not intended to limit the number requirement (i.e., the number of occurrences) of the element or component. Thus, "a" or "an" should be read to include one or at least one, and the singular form of an element or component also includes the plural unless the stated number clearly indicates that the singular form is intended.
The essential oil composition comprises, by volume, 50-60 parts of yellow tea, 20-30 parts of mulberry leaves, 5-10 parts of base oil and 5-15 parts of Biluochun tea flowers.
The formula essential oil consists of 50 parts of yellow tea, 30 parts of mulberry leaves, 5 parts of base oil and 15 parts of Biluochun tea flowers according to the volume part ratio.
The mulberry leaves are buds of the mulberry leaves; the yellow tea is Leishan yellow tea.
The base oil is one or two of sweet almond oil, almond oil and wheat germ oil.
Compared with the conventional essential oil, the yellow tea essential oil has the effects of sterilizing and diminishing inflammation, phytol extracted from fresh mulberry leaves, also called phytol and xanthol, is an important raw material for preparing vitamin E and K, and the essential oil extracted from the biluochun tea flowers can disperse wind and heat, clear away the lung-heat, moisten dryness, calm the liver, improve eyesight, cool blood and stop bleeding, and meanwhile has the effects of increasing the skin defense capacity and reducing skin tension.
In a second aspect of the invention, there is provided a process for the preparation of an essential oil composition, the process comprising the steps of:
(1) distilling 50 parts of yellow tea by using water vapor for 2-10H, and then condensing and separating oil and water to obtain yellow tea essential oil;
(2) putting 30 parts of mulberry leaves and 15 parts of Biluochun tea flowers into a 2000ml flask, adding 500ml of distilled water, and extracting for 5 hours by a water distillation method; after extraction, adding 30ml of ether into the extract for extraction, adding a proper amount of anhydrous Na into the ether layer2SO4Drying for 30min, filtering, and evaporating diethyl ether solvent in water bath at 40 deg.C to obtain mixed essential oil of folium Mori and Biluochun tea flower;
(3) and (3) mixing the yellow tea essential oil and the mulberry leaf Biluochun tea flower essential oil mixed essential oil obtained in the steps (1) and (2) respectively with base oil to obtain the essential oil composition.
The product prepared by the preparation method has obvious endocrine regulating and sterilizing capabilities. The essential oil has volatility and permeability, so the essential oil molecules of the product can enter the skin and a blood circulation system in a short time, quickly discharge toxin and turbid substances accumulated in the blood and the skin, and deeply clean the skin; radically treat acnes and scars, and achieve the effects of external medicine internal treatment and endocrine regulation. In addition, the invention adopts the common coordination effect of the Leishan yellow tea, the mulberry leaf bud and the Biluochun tea tree flower, the obtained essential oil has mild performance, achieves the purposes of repairing damaged skin, delaying skin aging, whitening and beautifying, can radically remove acne and acne mark, and has good effect on skin problems such as blackheads, acnes, large pores and the like. In addition, the essential oil of the formula can form a layer of protective film on the surface of skin, so that the skin is kept moist, the damaged skin is repaired, and the growth of bacteria is inhibited.
The foregoing examples are merely illustrative and serve to explain some of the features of the method of the present invention. The appended claims are intended to claim as broad a scope as possible, and the examples presented herein are merely illustrative of selected implementations in accordance with all possible combinations of examples. Accordingly, it is applicants' intention that the appended claims are not to be limited by the choice of examples illustrating features of the invention. The use of some numerical ranges in the claims also includes sub-ranges within their range, and variations in these ranges are also to be construed as being covered by the appended claims where possible.

Claims (5)

1. An essential oil composition characterized by: the formula essential oil consists of 50-60 parts of yellow tea, 20-30 parts of mulberry leaves, 5-10 parts of base oil and 5-15 parts of Biluochun tea flowers according to parts by volume.
2. The essential oil composition according to claim 1, characterized in that: the formula essential oil consists of 50 parts of yellow tea, 30 parts of mulberry leaves, 5 parts of base oil and 15 parts of Biluochun tea flowers according to the volume part ratio.
3. An essential oil composition according to claim 2, characterized in that: the mulberry leaves are buds of the mulberry leaves; the yellow tea is Leishan yellow tea.
4. An essential oil composition according to claim 2, characterized in that: the base oil is one or two of sweet almond oil, almond oil and wheat germ oil.
5. A process for the preparation of an essential oil composition according to claim 1, characterized in that: the preparation method comprises the following steps:
(1) distilling 50 parts of yellow tea by using water vapor for 2-10H, and then condensing and separating oil and water to obtain yellow tea essential oil;
(2) putting 30 parts of mulberry leaves and 15 parts of Biluochun tea flowers into a 2000ml flask, adding 500ml of distilled water, and extracting for 5 hours by a water distillation method; after extraction, adding 30ml of ether into the extract for extraction, adding a proper amount of anhydrous Na into the ether layer2SO4Drying for 30min, filtering, and evaporating diethyl ether solvent in water bath at 40 deg.C to obtain mixed essential oil of folium Mori and Biluochun tea flower;
(3) and (3) mixing the yellow tea essential oil and the mulberry leaf Biluochun tea flower essential oil mixed essential oil obtained in the steps (1) and (2) respectively with base oil to obtain the essential oil composition.
CN201811061120.7A 2018-09-12 2018-09-12 Essential oil composition and preparation method thereof Pending CN110894437A (en)

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Application Number Priority Date Filing Date Title
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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113274330A (en) * 2021-06-09 2021-08-20 浙江曲蔓地生物科技有限公司 Mulberry leaf volatile oil-water mixture and application thereof in skin care products

Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101343597A (en) * 2008-07-29 2009-01-14 红云烟草(集团)有限责任公司 Yellow tea oil, preparation and application thereof
CN102229862A (en) * 2010-10-15 2011-11-02 华芳烟用香料有限公司 Preparation of mulberry leaf volatile oil and application thereof in tobacco flavoring
CN103497837A (en) * 2013-09-27 2014-01-08 福建中烟工业有限责任公司 Tea flower essential oil, preparation method and application of essential oil to cigarette
CN104887604A (en) * 2015-05-29 2015-09-09 陈文创 Health-preserving jasmine essential oil
CN104997702A (en) * 2015-08-18 2015-10-28 云南同方科技有限公司 Acne-removing essential oil
CN106937922A (en) * 2017-05-23 2017-07-11 邓子坚 A kind of anti-acne compound essential oil
CN107488515A (en) * 2017-09-30 2017-12-19 江苏农林职业技术学院 A kind of extract solution and the method using extract solution extraction essential oil of the flower of Camellia sinensis
CN107669560A (en) * 2017-11-16 2018-02-09 佘利平 A kind of nutrition mediation type essential oil and preparation method thereof

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101343597A (en) * 2008-07-29 2009-01-14 红云烟草(集团)有限责任公司 Yellow tea oil, preparation and application thereof
CN102229862A (en) * 2010-10-15 2011-11-02 华芳烟用香料有限公司 Preparation of mulberry leaf volatile oil and application thereof in tobacco flavoring
CN103497837A (en) * 2013-09-27 2014-01-08 福建中烟工业有限责任公司 Tea flower essential oil, preparation method and application of essential oil to cigarette
CN104887604A (en) * 2015-05-29 2015-09-09 陈文创 Health-preserving jasmine essential oil
CN104997702A (en) * 2015-08-18 2015-10-28 云南同方科技有限公司 Acne-removing essential oil
CN106937922A (en) * 2017-05-23 2017-07-11 邓子坚 A kind of anti-acne compound essential oil
CN107488515A (en) * 2017-09-30 2017-12-19 江苏农林职业技术学院 A kind of extract solution and the method using extract solution extraction essential oil of the flower of Camellia sinensis
CN107669560A (en) * 2017-11-16 2018-02-09 佘利平 A kind of nutrition mediation type essential oil and preparation method thereof

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113274330A (en) * 2021-06-09 2021-08-20 浙江曲蔓地生物科技有限公司 Mulberry leaf volatile oil-water mixture and application thereof in skin care products

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