CN113274330A - Mulberry leaf volatile oil-water mixture and application thereof in skin care products - Google Patents
Mulberry leaf volatile oil-water mixture and application thereof in skin care products Download PDFInfo
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- CN113274330A CN113274330A CN202110643050.1A CN202110643050A CN113274330A CN 113274330 A CN113274330 A CN 113274330A CN 202110643050 A CN202110643050 A CN 202110643050A CN 113274330 A CN113274330 A CN 113274330A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P17/00—Drugs for dermatological disorders
- A61P17/04—Antipruritics
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P17/00—Drugs for dermatological disorders
- A61P17/10—Anti-acne agents
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P29/00—Non-central analgesic, antipyretic or antiinflammatory agents, e.g. antirheumatic agents; Non-steroidal antiinflammatory drugs [NSAID]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
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Abstract
The application discloses a mulberry leaf volatile oil-water mixture and application thereof in skin care products, wherein the mulberry leaf volatile oil-water mixture comprises 98.0-99.5 wt% of mulberry leaf steam distillate, 0.1-2.0 wt% of preservative and 0.03-0.05% of chelating agent, and has the effects of diminishing inflammation and removing acnes.
Description
Technical Field
The invention relates to a mulberry leaf volatile oil-water mixture and application thereof in skin care products.
Background
Folium mori is the leaf of a plant of the Moraceae family (Moraceae), is rich in various active substances including flavone, alkaloid, polysaccharide, volatile oil and the like, and is a traditional Chinese medicinal material. The mulberry leaf polysaccharide and the mulberry leaf flavone are applied in daily chemicals earlier, and have anti-inflammatory and whitening effects, but the development of the mulberry leaf volatile oil component is not reported.
Disclosure of Invention
The first purpose of the invention is to provide a mulberry leaf volatile oil-water mixture which has the advantages of diminishing inflammation and removing acnes.
The technical purpose of the invention is realized by the following technical scheme:
a mulberry leaf volatile oil-water mixture comprises 98.0-99.5 wt% of mulberry leaf steam distillate, 0.1-2.0 wt% of preservative and 0.03-0.05 wt% of chelating agent.
Preferably, the mulberry leaf water vapor distillate comprises 98.0-99.5 wt% of mulberry leaf water vapor distillate, 0.0-0.5 wt% of caprylyl hydroximic acid, 0.0-0.5 wt% of ethyl hexyl glycerol, 0.1-1 wt% of hexylene glycol and 0.03-0.05 wt% of EDTA disodium.
Preferably, the mulberry leaf water vapor distillate comprises 99.0-99.5 wt% of mulberry leaf steam distillate, 0.0-0.1 wt% of caprylyl hydroximic acid, 0.0-0.2 wt% of ethyl hexyl glycerol, 0.1-0.5 wt% of hexylene glycol and 0.03-0.05 wt% of EDTA disodium.
Preferably, the mulberry leaf steam distillate is obtained by the following method:
(1) picking new leaves at 2-5 th positions on branches of mulberry leaves, wherein the picking time is in the later stage of spring silkworms or before frost fall; drying picked fresh mulberry leaves in the shade at room temperature, and storing in a dry environment for later use; the mulberry leaf is Hu mulberry, namely the mulberry is in a mulberry-based fishpond planting environment;
(2) boiling by a water distillation method, condensing and collecting steam distillate of mulberry leaves:
adding 1 kg of dried mulberry leaves into an extraction tank with a condensing device, adding 10-30 kg of water, fully soaking the mulberry leaves and the water, checking smoothness of condensed cooling water and a pipeline, heating in sections, boiling, condensing steam and collecting 6-12 kg of volatile oil water; the heating step is to heat the mixture to 70-85 ℃, and when the temperature reaches 70-85 ℃, the mixture is heated to boiling and kept constant.
The second purpose of the invention is to provide the application of the mulberry leaf volatile oil-water mixture in skin care products, which has the advantages of diminishing inflammation and removing acnes.
The technical purpose of the invention is realized by the following technical scheme:
the application of the mulberry leaf volatile oil-water mixture in skin care products is provided.
Preferably, the skin care product adopts a face cleaning cream which comprises 10 wt% of the mulberry leaf volatile oil-water mixture, 3 wt% of butanediol, 4 wt% of glycerol, 45 wt% of amino acid surfactant and 38 wt% of water.
The technical effects of the invention are mainly reflected in the following aspects:
1. has effects of tranquilizing skin, remarkably improving itching symptom of inflamed skin, and relieving skin redness.
2. The mulberry leaf volatile oil extract can be applied to common formulas of skin care products, and has the effects of diminishing inflammation and removing acnes. The active ingredients in the mulberry leaf volatile oil can relieve the inflammation of the skin surface layer and reduce the release of inflammatory factors, thereby playing the role of diminishing inflammation and removing acnes.
3. The invention also regulates the variety, the part and the picking time of the mulberry leaves, and ensures the uniqueness and the efficacy of the finished product.
Detailed Description
Example 1: a folium Mori volatile oil water mixture comprises folium Mori steam distillate 99.17 wt%, caprylyl hydroximic acid 0.1%, ethylhexyl glycerol 0.2%, hexanediol 0.5% and disodium EDTA 0.03%.
The preparation method of the mulberry leaf volatile oil mixture comprises the following steps:
(1) picking new leaves at 2-5 th positions on branches of mulberry leaves, wherein the picking time is in the later stage of spring silkworms or before frost fall; drying picked fresh mulberry leaves in the shade at room temperature for 1-2 days generally, and storing the fresh mulberry leaves in a dry environment for later use; the mulberry leaf is Hu mulberry, namely the mulberry is in a mulberry-based fishpond planting environment;
(2) boiling by a water distillation method, condensing and collecting steam distillate of mulberry leaves:
adding 1 kg of dried mulberry leaves into an extraction tank with a condensing device, adding 15 kg of water, fully soaking the mulberry leaves and the water, checking the smoothness of condensed cooling water and a pipeline, heating in sections, boiling, condensing steam, and collecting 9 kg of volatile oil water; the heating step is to heat the mixture to 75 ℃ and to boil the mixture and keep the mixture constant when the temperature reaches 75 ℃;
(3) preservatives (caprylhydroxamic acid, ethylhexyl glycerol, hexylene glycol in this example) and chelating agents (disodium EDTA) were added and stirred at 60 ℃ until completely dissolved.
Example 2: a mulberry leaf volatile oil-water mixture is different from that of example 1 in that it comprises 98.87 wt% of mulberry leaf steam distillate, 0.5 wt% of caprylyl hydroximic acid, 0.5 wt% of ethylhexyl glycerin, 0.1% of hexylene glycol and 0.03 wt% of disodium EDTA.
Example 3: a mulberry leaf volatile oil-water mixture is different from that in example 1 in that the mulberry leaf volatile oil-water mixture comprises 98.95 wt% of mulberry leaf steam distillate, 0.5% of caprylyl hydroximic acid, 0.5% of hexylene glycol and 0.05% of disodium EDTA.
Example 4: a mulberry leaf volatile oil-water mixture is different from that in example 1 in that the mulberry leaf volatile oil-water mixture comprises 98.46 wt% of mulberry leaf steam distillate, 0.5% of ethylhexyl glycerol, 1% of hexanediol and 0.04% of disodium EDTA.
Example 5: a mulberry leaf volatile oil-water mixture is different from that in example 1 in that the preparation method of the mulberry leaf volatile oil-water mixture comprises the following steps:
(1) picking new leaves at 2-5 th positions on branches of mulberry leaves, wherein the picking time is in the later stage of spring silkworms or before frost fall; drying picked fresh mulberry leaves in the shade at room temperature for 1-2 days generally, and storing the fresh mulberry leaves in a dry environment for later use; the mulberry leaf is Hu mulberry, namely the mulberry is in a mulberry-based fishpond planting environment;
(2) boiling by a water distillation method, condensing and collecting steam distillate of mulberry leaves:
adding 1 kg of dried mulberry leaves into an extraction tank with a condensing device, adding 10 kg of water, fully soaking the mulberry leaves and the water, checking the smoothness of condensed cooling water and a pipeline, heating in sections, boiling, condensing steam, and collecting 6 kg of volatile oil water; the heating step is to heat up to 70 ℃ at first, when the temperature reaches 75 ℃, heat up to boiling and keep constant;
(3) adding antiseptic and chelating agent, and stirring at 60 deg.C to dissolve completely.
Example 6: a mulberry leaf volatile oil-water mixture is different from that in example 1 in that the preparation method of the mulberry leaf volatile oil-water mixture comprises the following steps:
(1) picking new leaves at 2-5 th positions on branches of mulberry leaves, wherein the picking time is in the later stage of spring silkworms or before frost fall; drying picked fresh mulberry leaves in the shade at room temperature for 1-2 days generally, and storing the fresh mulberry leaves in a dry environment for later use; the mulberry leaf is Hu mulberry, namely the mulberry is in a mulberry-based fishpond planting environment;
(2) boiling by a water distillation method, condensing and collecting steam distillate of mulberry leaves:
adding 1 kg of dried mulberry leaves into an extraction tank with a condensing device, adding 20 kg of water, fully soaking the mulberry leaves and the water, checking the smoothness of condensed cooling water and a pipeline, heating in sections, boiling, condensing steam, and collecting 12 kg of volatile oil water; the heating step is to heat the mixture to 85 ℃ first, and when the temperature reaches 85 ℃, the mixture is heated to boiling and kept constant;
(3) adding antiseptic and chelating agent, and stirring at 60 deg.C to dissolve completely.
Example 7: a face wash comprises 10 wt% of a mulberry leaf volatile oil water mixture (from example 1), 3 wt% of butylene glycol, 4 wt% of glycerin, 45 wt% of an amino acid surfactant and 38 wt% of water.
Evaluation of Using Effect
To examine the anti-inflammatory and anti-acne properties of the product, 30 female subjects with skin inflamed and slightly acne (cheeks and chin) were selected, with an age between 25-40 years.
The using method comprises the following steps: after the skin is thoroughly cleaned in example 7, the sample prepared in example 1 is uniformly applied to the skin, gently patted, and is used once in the morning and evening, wherein each 28 days is a treatment course and 1-2 treatment courses are used.
And (4) judging the standard:
the method has the following advantages: the user feels very satisfactory, the skin is obviously reduced in redness, the pox is eliminated, and the test subjects have no allergy or other toxic and side effects.
The effect is shown: the user feels generally satisfactory, the skin redness is reduced, and the pox is reduced.
And (4) invalidation: the user feels dissatisfied with the skin, the skin redness is reduced, and the pox is not obviously reduced.
The 20 cases were recorded and reviewed, and the specific results are shown in the following table.
| Total number of people | Is effective | Show effect | Invalidation |
| 30 | 12 | 17 | 1 |
During use, no allergic or other toxic side effects occurred in the subjects. The total effective rate reaches 96 percent.
And (4) conclusion: the experimental data show that the acne cream can reduce skin inflammation and remove acnes, and has a good calming effect on damaged skin.
The above are only typical examples of the present invention, and besides, the present invention may have other embodiments, and all the technical solutions formed by equivalent substitutions or equivalent changes are within the scope of the present invention as claimed.
Claims (6)
1. The mulberry leaf volatile oil-water mixture is characterized by comprising 98.0-99.5 wt% of mulberry leaf steam distillate, 0.1-2.0 wt% of preservative and 0.03-0.05% of chelating agent.
2. The mulberry leaf volatile oil-water mixture as claimed in claim 1, comprising 98.0-99.5 wt% of mulberry leaf steam distillate, 0.0-0.5 wt% of caprylyl hydroximic acid, 0.0-0.5 wt% of ethyl hexyl glycerol, 0.1-1 wt% of hexylene glycol and 0.03-0.05 wt% of disodium EDTA.
3. The mulberry leaf volatile oil-water mixture as claimed in claim 1, comprising 99.0-99.5 wt% of mulberry leaf steam distillate, 0.0-0.1 wt% of caprylyl hydroximic acid, 0.0-0.2 wt% of ethyl hexyl glycerol, 0.1-0.5 wt% of hexylene glycol and 0.03-0.05 wt% of disodium EDTA.
4. The mulberry leaf volatile oil and water mixture according to claim 1, wherein the mulberry leaf steam distillate is obtained by the following method:
(1) picking new leaves at 2-5 th positions on branches of mulberry leaves, wherein the picking time is in the later stage of spring silkworms or before frost fall; drying picked fresh mulberry leaves in the shade at room temperature, and storing in a dry environment for later use; the mulberry leaf is Hu mulberry, namely the mulberry is in a mulberry-based fishpond planting environment;
(2) boiling by a water distillation method, condensing and collecting steam distillate of mulberry leaves:
adding 1 kg of dried mulberry leaves into an extraction tank with a condensing device, adding 10-30 kg of water, fully soaking the mulberry leaves and the water, checking smoothness of condensed cooling water and a pipeline, heating in sections, boiling, condensing steam and collecting 6-12 kg of volatile oil water; the heating step is to heat the mixture to 70-85 ℃, and when the temperature reaches 70-85 ℃, the mixture is heated to boiling and kept constant.
5. The use of the mulberry leaf volatile oil-water mixture according to any one of claims 1 to 4 in skin care products.
6. The use of the mulberry leaf volatile oil water mixture in the skin care product according to claim 5, wherein the skin care product is a facial cleanser, and the facial cleanser comprises 10 wt% of the mulberry leaf volatile oil water mixture, 3 wt% of butanediol, 4 wt% of glycerol, 45 wt% of an amino acid surfactant and 38 wt% of water.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202110643050.1A CN113274330A (en) | 2021-06-09 | 2021-06-09 | Mulberry leaf volatile oil-water mixture and application thereof in skin care products |
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| Application Number | Priority Date | Filing Date | Title |
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| CN202110643050.1A CN113274330A (en) | 2021-06-09 | 2021-06-09 | Mulberry leaf volatile oil-water mixture and application thereof in skin care products |
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| CN113274330A true CN113274330A (en) | 2021-08-20 |
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| CN202110643050.1A Pending CN113274330A (en) | 2021-06-09 | 2021-06-09 | Mulberry leaf volatile oil-water mixture and application thereof in skin care products |
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Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1733194A (en) * | 2004-08-15 | 2006-02-15 | 江苏中康药物科技有限公司 | Extract of combined Chinese traditional medicinal crops for curing diseases of respiratory system and extracting method |
| CN102100653A (en) * | 2009-12-22 | 2011-06-22 | 李慧娟 | Bath lotion containing extracts of chinese mugwort leaf and grass-leaved sweetflag rhizome |
| CN102229862A (en) * | 2010-10-15 | 2011-11-02 | 华芳烟用香料有限公司 | Preparation of mulberry leaf volatile oil and application thereof in tobacco flavoring |
| CN108670915A (en) * | 2018-08-30 | 2018-10-19 | 佛山市欧若拉生物科技有限公司 | A kind of lavender type Essence and preparation method thereof |
| CN110894437A (en) * | 2018-09-12 | 2020-03-20 | 苏州市元使生物科技有限公司 | Essential oil composition and preparation method thereof |
| CN112168744A (en) * | 2020-09-24 | 2021-01-05 | 广州美物生物科技有限公司 | Plant essential oil composition and application thereof |
-
2021
- 2021-06-09 CN CN202110643050.1A patent/CN113274330A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1733194A (en) * | 2004-08-15 | 2006-02-15 | 江苏中康药物科技有限公司 | Extract of combined Chinese traditional medicinal crops for curing diseases of respiratory system and extracting method |
| CN102100653A (en) * | 2009-12-22 | 2011-06-22 | 李慧娟 | Bath lotion containing extracts of chinese mugwort leaf and grass-leaved sweetflag rhizome |
| CN102229862A (en) * | 2010-10-15 | 2011-11-02 | 华芳烟用香料有限公司 | Preparation of mulberry leaf volatile oil and application thereof in tobacco flavoring |
| CN108670915A (en) * | 2018-08-30 | 2018-10-19 | 佛山市欧若拉生物科技有限公司 | A kind of lavender type Essence and preparation method thereof |
| CN110894437A (en) * | 2018-09-12 | 2020-03-20 | 苏州市元使生物科技有限公司 | Essential oil composition and preparation method thereof |
| CN112168744A (en) * | 2020-09-24 | 2021-01-05 | 广州美物生物科技有限公司 | Plant essential oil composition and application thereof |
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