CN110876707A

CN110876707A - Astaxanthin essence extract freeze-dried powder and preparation method thereof

Info

Publication number: CN110876707A
Application number: CN201911255525.9A
Authority: CN
Inventors: 王洪波
Original assignee: Individual
Current assignee: Individual
Priority date: 2019-12-10
Filing date: 2019-12-10
Publication date: 2020-03-13

Abstract

The invention discloses astaxanthin essence extract freeze-dried powder which comprises the following components in percentage by mass: 4 to 5 percent of mannitol, 3 to 4 percent of trehalose, 1.5 to 2.5 percent of astaxanthin, 0.5 to 1.5 percent of glycerol, 0.03 to 0.07 percent of adenosine, 81.5 to 2.5 percent of acetyl hexapeptide, 0.01 to 0.05 percent of fullerene, 0.03 to 0.07 percent of xanthan gum, 0.03 to 0.07 percent of carnosine, 0.5 to 1.5 percent of hyaluronic acid and 85 to 86 percent of water, wherein the preparation method comprises the following steps: s1, weighing sodium hyaluronate, mannitol and water, stirring and heating to obtain a transparent preparation I; s2, cooling the transparent first preparation liquid; s3, weighing trehalose, astaxanthin, glycerol, adenosine, acetyl hexapeptide-8, fullerene, xanthan gum and carnosine, adding into the first transparent solution, and stirring and heating to obtain a second transparent solution; and S4, filling the transparent preparation liquid II into a penicillin bottle, covering a bottle stopper, putting the penicillin bottle into freeze-drying equipment, and freeze-drying. The invention has the advantages that: can effectively whiten, lighten spots, prevent sunburn, remove free radicals in skin and delay skin aging, has no side effect and is convenient to use.

Description

Astaxanthin essence extract freeze-dried powder and preparation method thereof

Technical Field

The invention relates to the technical field of cosmetics, in particular to astaxanthin essence extract freeze-dried powder and a preparation method thereof.

Background

The modern social life of matters is more and more abundant, people also pay more and more attention to the personal appearance problem, the sun light is strongly irradiated in summer, and the ultraviolet radiation is enhanced, so that the skin is blackened and burnt; meanwhile, with the increase of age and the deterioration of living environment, the metabolism of the skin is reduced, the function of absorbing various beneficial elements is reduced, water is easy to lose, various harmful substances are easy to stay on the surface of the skin, and the skin gradually loses the original elasticity, so that the skin is aged. Nowadays, skin care products become the most popular choice for most people, especially for contemporary women, and good skin care products can play roles in promoting skin blood circulation, repairing skin injury, removing wrinkles, increasing skin elasticity and luster, caring sensitive skin, and the like.

However, although skin care products on the market are full of various types, most skin care products are fine chemical products, only the surface layer problem of the skin is solved, the effects of repairing the skin and delaying skin aging cannot be fundamentally achieved, and some cosmetics are added with components such as hormone, the beauty effect is not obvious, the negative influence is caused on the human body, and the use safety performance is poor.

Disclosure of Invention

The invention aims to solve the technical problems and provides the sea cucumber intestine egg essence extract freeze-dried powder which can effectively whiten, lighten spots, prevent sunburn, remove free radicals in skin and delay skin aging, has no side effect and is convenient to use and a preparation method thereof.

In order to solve the technical problems, the technical scheme provided by the invention is as follows: an astaxanthin essence extract freeze-dried powder comprises the following components in percentage by mass: 4 to 5 percent of mannitol, 3 to 4 percent of trehalose, 1.5 to 2.5 percent of astaxanthin, 0.5 to 1.5 percent of glycerol, 0.03 to 0.07 percent of adenosine, 81.5 to 2.5 percent of acetyl hexapeptide, 0.01 to 0.05 percent of fullerene, 0.03 to 0.07 percent of xanthan gum, 0.03 to 0.07 percent of carnosine, 0.5 to 1.5 percent of hyaluronic acid and 85 to 86 percent of water.

Preferably, the composition comprises the following components in percentage by mass: 4.2 to 4.8 percent of mannitol, 3.2 to 3.8 percent of trehalose, 1.7 to 2.3 percent of astaxanthin, 0.7 to 1.3 percent of glycerol, 0.04 to 0.06 percent of adenosine, 81.7 to 2.3 percent of acetyl hexapeptide, 0.02 to 0.04 percent of fullerene, 0.04 to 0.06 percent of xanthan gum, 0.04 to 0.06 percent of carnosine, 0.7 to 1.3 percent of hyaluronic acid and 85.2 to 85.9 percent of water.

Preferably, the composition comprises the following components in percentage by mass: 4.5% of mannitol, 3.5% of trehalose, 2% of astaxanthin, 1% of glycerol, 0.05% of adenosine, 0.82% of acetyl hexapeptide, 0.03% of fullerene, 0.05% of xanthan gum, 0.05% of carnosine, 1% of hyaluronic acid and 85.82% of water.

Preferably, the water is purified water after secondary filtration.

Preferably, the preparation method of the astaxanthin essence extract freeze-dried powder comprises the following steps:

s1, weighing hyaluronic acid, mannitol and water, stirring for 12-30 minutes, heating to 70-80 ℃ to obtain a first transparent preparation solution;

s2, cooling the transparent first preparation solution to enable the transparent first preparation solution to be cooled to 15-30 ℃ at a constant speed;

s3, weighing trehalose, astaxanthin, glycerol, adenosine, acetyl hexapeptide-8, fullerene, xanthan gum and carnosine, adding the weighed materials into the first transparent solution, stirring for 15-30 minutes, heating at the temperature of 40-60 ℃ to obtain a second transparent solution;

s4, filling the transparent preparation liquid II into a penicillin bottle, covering a bottle stopper, putting the penicillin bottle into a freeze-drying device, and freeze-drying at the temperature of-15 to-5 ℃.

Compared with the prior art, the invention has the advantages that: according to the astaxanthin essence extract freeze-dried powder and the preparation method thereof, trehalose can form a unique protective film on the cell surface under severe environmental conditions such as high temperature, high cold, high osmotic pressure, drying and dehydration and the like, so that protein molecules can be effectively protected from inactivation without denaturation, and skin cells can be well protected; acetyl hexapeptide-8 is a bioactive polypeptide, can locally block nerve transmission muscle contraction information, influence skin sac nerve conduction, relax facial muscles, smooth dynamic lines, static lines and fine lines, effectively reorganize collagen elasticity, increase elastin activity, relax facial lines, smooth wrinkles and improve skin relaxation; the fullerene has strong oxidation resistance, and can play a role in activating skin cells and preventing skin decay; the xanthan gum can supplement moisture to the skin, prevent moisture loss, prevent wrinkles of the skin and resist aging; astaxanthin has effects of resisting oxidation, resisting aging, scavenging oxygen free radicals, whitening skin, removing speckle, preventing sunburn, and relieving skin dullness and melanin pigmentation; glycerin can keep skin moist; carnosine can prevent skin aging and whiten skin, and can prevent free radicals generated by smoking and protect skin; meanwhile, the freeze-drying synthesis process is adopted to fully extract the effective components in the raw materials, so that the freeze-drying powder is smeared on the face when in use, and the face mask is convenient to use and good in absorptivity.

Detailed Description

Example one

An astaxanthin essence extract freeze-dried powder comprises the following components in percentage by mass: 4.3% of mannitol, 3.7% of trehalose, 1.8% of astaxanthin, 1.2% of glycerol, 0.04% of adenosine, 81.8% of acetyl hexapeptide, 0.04% of fullerene, 0.04% of xanthan gum, 0.06% of carnosine, 1.15% of hyaluronic acid and 85.87% of water.

The preparation method comprises the following steps:

s1, weighing hyaluronic acid, mannitol and water, stirring for 20 minutes, heating to 80 ℃ to obtain a first transparent preparation solution;

s2, cooling the transparent first preparation solution to enable the temperature to be reduced to 25 ℃ at a constant speed;

s3, weighing trehalose, astaxanthin, glycerol, adenosine, acetyl hexapeptide-8, fullerene, xanthan gum and carnosine, adding the weighed materials into the first transparent solution, stirring for 30 minutes, heating to the temperature of 60 ℃ to obtain a second transparent solution;

s4, filling the transparent preparation liquid II into a penicillin bottle, covering a bottle stopper, putting the penicillin bottle into freeze-drying equipment, and freeze-drying at the temperature of-5 ℃.

Example two

An astaxanthin essence extract freeze-dried powder comprises the following components in percentage by mass: 4.5% of mannitol, 3.5% of trehalose, 2% of astaxanthin, 1% of glycerol, 0.05% of adenosine, 0.82% of acetyl hexapeptide, 0.03% of fullerene, 0.05% of xanthan gum, 0.05% of carnosine, 1% of hyaluronic acid and 85.82% of water.

The preparation method comprises the following steps:

s1, weighing hyaluronic acid, mannitol and water, stirring for 25 minutes, heating to 75 ℃ to obtain a first transparent preparation solution;

s2, cooling the transparent first preparation solution to ensure that the temperature is reduced to 22 ℃ at a constant speed;

s3, weighing trehalose, astaxanthin, glycerol, adenosine, acetyl hexapeptide-8, fullerene, xanthan gum and carnosine, adding the weighed materials into the first transparent solution, stirring for 25 minutes, heating to 50 ℃ to obtain a second transparent solution;

s4, filling the transparent preparation liquid II into a penicillin bottle, covering a bottle stopper, putting the penicillin bottle into freeze-drying equipment, and freeze-drying at the temperature of-12 ℃.

The above embodiments are preferred embodiments of the present invention, but the present invention is not limited to the above embodiments, and any other changes, modifications, substitutions, combinations, and simplifications which do not depart from the spirit and principle of the present invention should be construed as equivalents thereof, and all such changes, modifications, substitutions, combinations, and simplifications are intended to be included in the scope of the present invention.

Claims

1. The astaxanthin essence extract freeze-dried powder is characterized by comprising the following components in percentage by mass: 4 to 5 percent of mannitol, 3 to 4 percent of trehalose, 1.5 to 2.5 percent of astaxanthin, 0.5 to 1.5 percent of glycerol, 0.03 to 0.07 percent of adenosine, 81.5 to 2.5 percent of acetyl hexapeptide, 0.01 to 0.05 percent of fullerene, 0.03 to 0.07 percent of xanthan gum, 0.03 to 0.07 percent of carnosine, 0.5 to 1.5 percent of hyaluronic acid and 85 to 86 percent of water.

2. The astaxanthin essence extract freeze-dried powder according to claim 1, which is characterized by comprising the following components in percentage by mass: 4.2 to 4.8 percent of mannitol, 3.2 to 3.8 percent of trehalose, 1.7 to 2.3 percent of astaxanthin, 0.7 to 1.3 percent of glycerol, 0.04 to 0.06 percent of adenosine, 81.7 to 2.3 percent of acetyl hexapeptide, 0.02 to 0.04 percent of fullerene, 0.04 to 0.06 percent of xanthan gum, 0.04 to 0.06 percent of carnosine, 0.7 to 1.3 percent of hyaluronic acid and 85.2 to 85.9 percent of water.

3. The astaxanthin essence extract freeze-dried powder according to claim 1, which is characterized by comprising the following components in percentage by mass: 4.5% of mannitol, 3.5% of trehalose, 2% of astaxanthin, 1% of glycerol, 0.05% of adenosine, 0.82% of acetyl hexapeptide, 0.03% of fullerene, 0.05% of xanthan gum, 0.05% of carnosine, 1% of hyaluronic acid and 85.82% of water.

4. The astaxanthin essence extract freeze-dried powder according to claim 1, characterized in that: the water is purified water after secondary filtration.

5. The preparation method of the astaxanthin essence extract freeze-dried powder according to claim 1, which is characterized by comprising the following steps of: