CN110734274A - 一种陶瓷材料及其制备方法 - Google Patents

一种陶瓷材料及其制备方法 Download PDF

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CN110734274A
CN110734274A CN201911166010.1A CN201911166010A CN110734274A CN 110734274 A CN110734274 A CN 110734274A CN 201911166010 A CN201911166010 A CN 201911166010A CN 110734274 A CN110734274 A CN 110734274A
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许木顺
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Shanghai Zhuyi Culture Communication Co Ltd
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Abstract

本发明属于陶瓷材料技术领域，尤其为一种陶瓷材料及其制备方法，包括以下按重量份数计组分：聚丁二烯环氧树10‑30份，氧化铝20‑30份，高岭土10‑25份，稳定剂5‑10份，烧结助剂5‑10份，环己烷溶液10‑30份，硅藻土8‑12份，甲基三乙酰氧基硅烷2‑4份，锗0.5‑0.9份，泡沫镍0.05‑0.8份，钼0.02‑0.05份，二氧化铱0.01‑0.02份；采用多次烧制，一件作品要反复烧制3次，自制的有色，烧制过程中有两种自制的特殊的釉，烧制过程中用温度控制来达到釉色的最后呈现，采用多次上釉法，在烧制好的成品的釉上再次上釉色。

Description

一种陶瓷材料及其制备方法
技术领域
本发明属于陶瓷材料技术领域，具体涉及一种陶瓷材料及其制备方法。
背景技术
陶瓷材料是用天然或合成化合物经过成型或高温煅烧制成的一类无机非金属材料，陶瓷的种类很多，用途各异，电容器的外壳等大多都是陶瓷制成。
原有的陶瓷挂釉难度非常高，同时不同的釉的伸缩比例不同，容易破釉，开裂，很难烧制出成品。
发明内容
为解决上述背景技术中提出的问题。本发明提供了一种陶瓷材料及其制备方法。
为实现上述目的，本发明提供如下技术方案：一种陶瓷材料，包括以下按重量份数计组分：聚丁二烯环氧树10-30份，氧化铝20-30份，高岭土10-25份，稳定剂5-10份，烧结助剂5-10份，环己烷溶液10-30份，硅藻土8-12份，甲基三乙酰氧基硅烷2-4份，锗0.5-0.9份，泡沫镍0.05-0.8份，钼0.02-0.05份，二氧化铱0.01-0.02份。
作为本发明的一种陶瓷材料优选技术方案，所述烧结助剂为La2O3，所述稳定剂为SiO2。
作为本发明的一种陶瓷材料优选技术方案，还包括炭黑0.02份和钛白粉0.05份。
作为本发明的一种陶瓷材料优选技术方案，还包括三聚磷酸钠0.01-0.03份。
作为本发明的一种陶瓷材料优选技术方案，包括以下按重量份数计组分：聚丁二烯环氧树脂20份，氧化铝25份，高岭土20份，稳定剂7份，烧结助剂7份，环己烷溶液20份，硅藻土10份，甲基三乙酰氧基硅烷3份，锗0.7份，泡沫镍0.4份，钼0.03份，二氧化铱0.01份，炭黑0.02份，钛白粉0.05份和三聚磷酸钠0.02份。
本发明提供一种陶瓷材料的制造方法，包括如下步骤：
S1、称取聚丁二烯环氧树脂20份，氧化铝25份，高岭土20份，稳定剂7份，烧结助剂7份，环己烷溶液20份，硅藻土10份，甲基三乙酰氧基硅烷3份，锗0.7份，泡沫镍0.4份，钼0.03份，二氧化铱0.01份，炭黑0.02份，钛白粉0.05份和三聚磷酸钠0.02份；
S2、将所述S1中的材料放置到研磨机中，研磨10-30分钟；
S3、将研磨后的物料混合均匀后，在850-1050℃、50-80Mpa下混合8-18分钟，在真空条件下逐步降温，得到陶瓷材料。
作为本发明的一种陶瓷材料的制造方法优选技术方案，所述逐步降温的过程具体包括：在700-750℃保温10分钟，在500-550℃保温5分钟，在300-350℃保温2分钟。
作为本发明的一种陶瓷材料的制造方法优选技术方案，包括如下步骤：
S1、称取聚丁二烯环氧树脂20份，氧化铝25份，高岭土20份，稳定剂7份，烧结助剂7份，环己烷溶液20份，硅藻土10份，甲基三乙酰氧基硅烷3份，锗0.7份，泡沫镍0.4份，钼0.03份，二氧化铱0.01份，炭黑0.02份，钛白粉0.05份和三聚磷酸钠0.02份；
S2、将所述S1中的材料放置到研磨机中，研磨10-30分钟；
S3、把所述S2中的研磨材料分批烧制；
S31、第一次，素胚烧制，在800℃温度下把白胚烧制定型，并上第一次釉烧制，白胚定型完成后，等冷却后，上自制白釉；
S32、第二次釉并烧制，白釉烧制完成后，冷却后，再上自制的红釉。
作为本发明的一种陶瓷材料的制造方法优选技术方案，白釉是用长石釉加入适当比例(100：9)的草木灰调和，温度控制在1180℃-1260℃；红釉是长石釉加入适当比例(100：3)的红原矿石调和，温度控制在1260℃-1310°C。
与现有技术相比，本发明的有益效果是：采用多次烧制，一件作品要反复烧制3次，自制的有色，烧制过程中有两种自制的特殊的釉，烧制过程中用温度控制来达到釉色的最后呈现，采用多次上釉法，在烧制好的成品的釉上再次上釉色。
具体实施方式
下面将对本发明实施例中的技术方案进行清楚、完整地描述，显然，所描述的实施例仅仅是本发明一部分实施例，而不是全部的实施例。基于本发明中的实施例，本领域普通技术人员在没有做出创造性劳动前提下所获得的所有其他实施例，都属于本发明保护的范围。
一种陶瓷材料，其特征在于，包括以下按重量份数计组分：聚丁二烯环氧树脂10-30份，氧化铝20-30份，高岭土10-25份，稳定剂5-10份，烧结助剂5-10份，环己烷溶液10-30份，硅藻土8-12份，甲基三乙酰氧基硅烷2-4份，锗0.5-0.9份，泡沫镍0.05-0.8份，钼0.02-0.05份，二氧化铱0.01-0.02份。
在一个可选的实施例中：所述烧结助剂为La2O3，所述稳定剂为SiO2。
在一个可选的实施例中：还包括炭黑0.02份和钛白粉0.05份。
在一个可选的实施例中：还包括三聚磷酸钠0.01-0.03份。
实施例1
一种陶瓷材料，包括以下按重量份数计组分：聚丁二烯环氧树脂20份，氧化铝25份，高岭土20份，稳定剂7份，烧结助剂7份，环己烷溶液20份，硅藻土10份，甲基三乙酰氧基硅烷3份，锗0.7份，泡沫镍0.4份，钼0.03份，二氧化铱0.01份，炭黑0.02份，钛白粉0.05份和三聚磷酸钠0.02份。
一种陶瓷材料的制造方法，包括如下步骤：
S1、称取聚丁二烯环氧树脂20份，氧化铝25份，高岭土20份，稳定剂7份，烧结助剂7份，环己烷溶液20份，硅藻土10份，甲基三乙酰氧基硅烷3份，锗0.7份，泡沫镍0.4份，钼0.03份，二氧化铱0.01份，炭黑0.02份，钛白粉0.05份和三聚磷酸钠0.02份；
S2、将所述S1中的材料放置到研磨机中，研磨10-30分钟；
S3、将研磨后的物料混合均匀后，在850-1050℃、50-80Mpa下混合8-18分钟，在真空条件下逐步降温，得到陶瓷材料。
在一个可选的实施例中：所述逐步降温的过程具体包括：在700-750℃保温10分钟，在500-550℃保温5分钟，在300-350℃保温2分钟。
实施例2
一种陶瓷材料，包括以下按重量份数计组分：聚丁二烯环氧树脂20份，氧化铝25份，高岭土20份，稳定剂7份，烧结助剂7份，环己烷溶液20份，硅藻土10份，甲基三乙酰氧基硅烷3份，锗0.7份，泡沫镍0.4份，钼0.03份，二氧化铱0.01份，炭黑0.02份，钛白粉0.05份和三聚磷酸钠0.02份。
一种陶瓷材料的制造方法，包括如下步骤：
S1、称取聚丁二烯环氧树脂20份，氧化铝25份，高岭土20份，稳定剂7份，烧结助剂7份，环己烷溶液20份，硅藻土10份，甲基三乙酰氧基硅烷3份，锗0.7份，泡沫镍0.4份，钼0.03份，二氧化铱0.01份，炭黑0.02份，钛白粉0.05份和三聚磷酸钠0.02份；
S2、将所述S1中的材料放置到研磨机中，研磨10-30分钟；
S3、把所述S2中的研磨材料分批烧制；
S31、第一次，素胚烧制，在800℃温度下把白胚烧制定型，并上第一次釉烧制，白胚定型完成后，等冷却后，上自制白釉；
S32、第二次釉并烧制，白釉烧制完成后，冷却后，再上自制的红釉。
在一个可选的实施例中：白釉是用长石釉加入适当比例(100：9)的草木灰调和，温度控制在1180℃-1260℃；红釉是长石釉加入适当比例(100：3)的红原矿石调和，温度控制在1260℃-1310℃。
本发明的有益效果是：采用多次烧制，一件作品要反复烧制3次，自制的有色，烧制过程中有两种自制的特殊的釉，烧制过程中用温度控制来达到釉色的最后呈现，采用多次上釉法，在烧制好的成品的釉上再次上釉色。
最后应说明的是：以上所述仅为本发明的优选实施例而已，并不用于限制本发明，尽管参照前述实施例对本发明进行了详细的说明，对于本领域的技术人员来说，其依然可以对前述各实施例所记载的技术方案进行修改，或者对其中部分技术特征进行等同替换。凡在本发明的精神和原则之内，所作的任何修改、等同替换、改进等，均应包含在本发明的保护范围之内。

Claims (9)

1.一种陶瓷材料及其制备方法，其特征在于，包括以下按重量份数计组分：聚丁二烯环氧树脂10-30份，氧化铝20-30份，高岭土10-25份，稳定剂5-10份，烧结助剂5-10份，环己烷溶液10-30份，硅藻土8-12份，甲基三乙酰氧基硅烷2-4份，锗0.5-0.9份，泡沫镍0.05-0.8份，钼0.02-0.05份，二氧化铱0.01-0.02份。
2.根据权利要求1所述的陶瓷材料，其特征在于：所述烧结助剂为La2O3，所述稳定剂为SiO2。
3.根据权利要求1所述的陶瓷材料，其特征在于：还包括炭黑0.02份和钛白粉0.05份。
4.根据权利要求1所述的陶瓷材料，其特征在于：还包括三聚磷酸钠0.01-0.03份。
5.根据权利要求1所述的陶瓷材料，其特征在于，包括以下按重量份数计组分：聚丁二烯环氧树脂20份，氧化铝25份，高岭土20份，稳定剂7份，烧结助剂7份，环己烷溶液20份，硅藻土10份，甲基三乙酰氧基硅烷3份，锗0.7份，泡沫镍0.4份，钼0.03份，二氧化铱0.01份，炭黑0.02份，钛白粉0.05份和三聚磷酸钠0.02份。
6.如权利要求1-5任意一项所述的陶瓷材料的制造方法，其特征在于，包括如下步骤：
S1、称取聚丁二烯环氧树脂20份，氧化铝25份，高岭土20份，稳定剂7份，烧结助剂7份，环己烷溶液20份，硅藻土10份，甲基三乙酰氧基硅烷3份，锗0.7份，泡沫镍0.4份，钼0.03份，二氧化铱0.01份，炭黑0.02份，钛白粉0.05份和三聚磷酸钠0.02份；
S2、将所述S1中的材料放置到研磨机中，研磨10-30分钟；
S3、将研磨后的物料混合均匀后，在850-1050℃、50-80Mpa下混合8-18分钟，在真空条件下逐步降温，得到陶瓷材料。
7.根据权利要求6所述的陶瓷材料的制造方法，其特征在于，所述逐步降温的过程具体包括：在700-750℃保温10分钟，在500-550℃保温5分钟，在300-350℃保温2分钟。
8.根据权利要求6所述的陶瓷材料的制造方法，其特征在于，包括如下步骤：
S1、称取聚丁二烯环氧树脂20份，氧化铝25份，高岭土20份，稳定剂7份，烧结助剂7份，环己烷溶液20份，硅藻土10份，甲基三乙酰氧基硅烷3份，锗0.7份，泡沫镍0.4份，钼0.03份，二氧化铱0.01份，炭黑0.02份，钛白粉0.05份和三聚磷酸钠0.02份；
S2、将所述S1中的材料放置到研磨机中，研磨10-30分钟；
S3、把所述S2中的研磨材料分批烧制；
S31、第一次，素胚烧制，在800℃温度下把白胚烧制定型，并上第一次釉烧制，白胚定型完成后，等冷却后，上自制白釉；
S32、第二次釉并烧制，白釉烧制完成后，冷却后，再上自制的红釉。
9.根据权利要求8所述的陶瓷材料的制造方法，其特征在于：白釉是用长石釉加入适当比例(100：9)的草木灰调和，温度控制在1180℃-1260℃；红釉是长石釉加入适当比例(100：3)的红原矿石调和，温度控制在1260℃-1310℃。
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Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103803951A (zh) * 2013-12-23 2014-05-21 苏州宏泉高压电容器有限公司 一种陶瓷材料及其制备方法
CN104803679A (zh) * 2015-04-16 2015-07-29 苏州靖羽新材料有限公司 一种陶瓷材料及其制备方法
CN106477888A (zh) * 2016-10-20 2017-03-08 沈阳建筑大学 一种氧化铜桃红色钾长石釉及其制备方法

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103803951A (zh) * 2013-12-23 2014-05-21 苏州宏泉高压电容器有限公司 一种陶瓷材料及其制备方法
CN104803679A (zh) * 2015-04-16 2015-07-29 苏州靖羽新材料有限公司 一种陶瓷材料及其制备方法
CN106477888A (zh) * 2016-10-20 2017-03-08 沈阳建筑大学 一种氧化铜桃红色钾长石釉及其制备方法

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