CN110326627A - Spray for refreshing air - Google Patents
Spray for refreshing air Download PDFInfo
- Publication number
- CN110326627A CN110326627A CN201811078923.3A CN201811078923A CN110326627A CN 110326627 A CN110326627 A CN 110326627A CN 201811078923 A CN201811078923 A CN 201811078923A CN 110326627 A CN110326627 A CN 110326627A
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- CN
- China
- Prior art keywords
- extractor
- oil
- fluid reservoir
- spray
- ramulus cinnamomi
- Prior art date
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Classifications
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/02—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing liquids as carriers, diluents or solvents
- A01N25/04—Dispersions, emulsions, suspoemulsions, suspension concentrates or gels
- A01N25/06—Aerosols
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/12—Asteraceae or Compositae [Aster or Sunflower family], e.g. daisy, pyrethrum, artichoke, lettuce, sunflower, wormwood or tarragon
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/24—Lauraceae [Laurel family], e.g. laurel, avocado, sassafras, cinnamon or camphor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/34—Chemical or biological purification of waste gases
- B01D53/74—General processes for purification of waste gases; Apparatus or devices specially adapted therefor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/34—Chemical or biological purification of waste gases
- B01D53/74—General processes for purification of waste gases; Apparatus or devices specially adapted therefor
- B01D53/86—Catalytic processes
- B01D53/8668—Removing organic compounds not provided for in B01D53/8603 - B01D53/8665
Abstract
Spray for refreshing air, consisting of: Atractylis oil: 1.0%-1.5%, cassia twig oil: 0.8%-1.2%, coconut oleoyl amine DEA:0.5%-1.0%, sodium laureth sulfate: 3%-4%, TEA lauryl sodium sulfate: 2.0%-3.0%, glycerol: 5%-8%, borneol: 0.2%-0.3%, Nano titanium dioxide 1.0-2.0%, pure water surplus.Spray for refreshing air of the invention with efficient sterilizing and can remove formaldehyde, and environmentally protective, and side effect non-stimulated to human body.
Description
Technical field
The present invention relates to a kind of environmentally protective spray for refreshing air.
Background technique
Air is one of our conditions on which persons or things depend for existence, and pure and fresh air can bring pleasant mood to people, and air is also
One of main media of pathogen transmission, with the continuous development in city, population size constantly increases, and the density of population is big, air
Environment of poor quality is worsening, and harmful substance increases in air, and peculiar smell, infection through air influence the mood, health, work effect of people
Rate.In order to kill the harmful microorganism in air and remove peculiar smell, Modern Family, hospital, hotel, restaurant and some other public
Occasion often uses spray for refreshing air into air.Spray for refreshing air is also known as " environment perfume ", as its name suggests, refers to
The medicament that air can be made more pure and fresh.
Common spray for refreshing air, at being grouped as, is covered by ethyl alcohol, essence, deionized water etc. by fragrant
Peculiar smell mitigates people to the sticky feeling of peculiar smell, is a kind of chemical products for being applied to environmental sanitation field since 20th century.
Current market sales of spray for refreshing air contains artificial synthesized chemosterilant mostly, is commonly exposed to this contain
Have in the air of chemicals, certain injury may be will cause to human body.Therefore, to purify the air of a room, safety is developed
The pure and fresh sterile products of effective natural air, it appears particularly important.
Summary of the invention
The object of the present invention is to provide it is a kind of can with sterilizing, except formaldehyde, purify the spray for refreshing air of air.
According to the first aspect of the invention, a kind of spray for refreshing air is provided, consisting of: Rhzoma Atractylodis Lanceae volatile oil:
1.0%-1.5%, Ramulus Cinnamomi Volatile oil: 0.8%-1.2%, coconut oleoyl amine DEA:0.5%-1.0%, sodium laureth sulfate:
3%-4%, TEA lauryl sodium sulfate: 2.0%-3.0%, glycerol: 5%-8%, borneol: 0.2%-0.3%, nanoscale two
Titanium oxide 1.0-2.0%, pure water surplus.
Preferred embodiment in accordance with the present invention, wherein Nano titanium dioxide is partial size 100nm anatase titanium dioxide dioxy below
Change titanium.This titanium dioxide has significant catalysis, can generate similar photosynthetic light-catalyzed reaction, make in spray
The ingredient of rhizoma atractylodis and Ramulus Cinnamomi Volatile oil produces the extremely strong free hydroxy of oxidability and active oxygen, which has very strong
Photoredox function, oxidable to decompose various organic compounds and part inorganic matter, the efficient indoor remaining formaldehyde of removal.
According to the second aspect of the invention, the production method of above-mentioned spray for refreshing air is provided, comprising:
Pure water and glycerol are uniformly mixed；
It is then respectively adding coconut oleoyl amine DEA, sodium laureth sulfate, TEA lauryl sodium sulfate, stirs and fills it
Divide dissolution；
Atractylis oil and cassia twig oil and Nano titanium dioxide are added, and is stirred evenly；
It is eventually adding borneol, it is filling.
In accordance with the present production process, wherein Atractylis oil and/or cassia twig oil are continuously prepared preferably through following techniques:
Rhizoma atractylodis rhizome powder and/or ramulus cinnamomi powder are added to the extractor for being equipped with auger conveyor；
First fluid reservoir of the heating equipped with pure water is to generate vapor；
Vapor is passed through extractor after cooler is condensed into liquid water to submerge rhizoma atractylodis rhizome powder and/or ramulus cinnamomi powder
End；
When the liquid level in extractor is higher than the highest point of the siphon pipe of connection extractor and the first fluid reservoir, in extractor
Extracting solution automatically by siphon pipe enter the first fluid reservoir；
When the extracting solution in extractor becomes colorless, start the auger conveyor in extractor with by rhizoma atractylodis rhizome wet-milling
And/or extractor is discharged in ramulus cinnamomi wet-milling, while (fresh) rhizoma atractylodis rhizome powder and/or ramulus cinnamomi powder is added into extractor again；
Stop the first fluid reservoir of heating and starts the second fluid reservoir simultaneously to continue above-mentioned steps；And
The extracting solution in the first fluid reservoir is separated to obtain Atractylis oil and/or cassia twig oil.
Preferred embodiment in accordance with the present invention executes plant after mixing rhizoma atractylodis rhizome powder and ramulus cinnamomi powder in proportion again
Oil extract process.In this case, due to experienced pyroreaction cohesive process between each active botanical ingredient at the extraction, therefore
And it is capable of forming stronger synergic remove.
Rhizoma atractylodis (volatilization) oil of the invention can be extracted from the dry rhizome of composite family rhizoma atractylodis platymiscium Atractylis lancea or Atractylis chinensis
It obtains.Rhzoma Atractylodis Lanceae volatile oil mainly contains the volatile materials such as β-cineol, Atisine chloride Atractydin, atractylone, atractylol, elemi oleyl alcohol.No
Can only there be certain killing effect to mycobacterium tuberculosis, the pseudomonas aeruginosa etc. in air, also to Escherichia coli and gold
Staphylococcus aureus has very strong killing effect.
(ramulus cinnamomi) volatile oil of the invention can be extracted from the dry twig of lauraceae plant cortex cinnamomi and be obtained.Ramulus Cinnamomi Volatile oil
The volatile materials such as benzaldehyde, benzenpropanal, trans- cinnaldehydrum, cinnaldehydrum are mainly contained, there is significant antibacterial, calmness, analgesia
And other effects.
Inventor has found in practice process, main active atractylol in Rhzoma Atractylodis Lanceae volatile oil etc. and Ramulus Cinnamomi Volatile oil
In main active cinnaldehydrum etc. there is synergic remove, the two is shared with specific proportion, is reducing the same of total dosage
When can have to staphylococcus aureus, streptococcus and streptococcus anaerobius it is apparent kill inhibiting effect, mechanism or be rhizoma atractylodis
Pure and mild cinnaldehydrum collaboration inhibition bacteria cell wall synthesis, i.e. inhibition cell wall mucopeptide synzyme (including transpeptidase, carboxylic tire enzyme, interior peptide
Enzyme) synthesis make cell wall defective thus the synthesis of block cell wall peptide glycan, thallus rupture is dead.
Although the present invention can also pass through conventional extraction techniques such as CO2Overcritical (or subcritical) fluid extraction mentions
Plant (volatilization) oily such as Rhzoma Atractylodis Lanceae volatile oil and/or Ramulus Cinnamomi Volatile oil are taken, but the present invention is preferably by following extraction system come real
The fast industrialization scale of existing vegetable oil is extracted.
Therefore, according to the third aspect of the invention we, a kind of plant (volatilization) oil extract system is additionally provided, comprising:
Extractor with feed opening and discharge gate, is provided with auger conveyor；
First fluid reservoir passes through the first gas-liquid partial circuit and the first siphon partial circuit and extractor selectivity respectively
Connection；
Second fluid reservoir passes through the second gas-liquid partial circuit and the second siphon partial circuit and extractor selectivity respectively
Connection；
Cooler is arranged on the first gas-liquid partial circuit and the second gas-liquid partial circuit close to extractor.
Extraction system according to the present invention, wherein the first gas-liquid partial circuit includes being connected to the top of the first fluid reservoir
Both first vertical pipeline, the shared vertical pipeline being connected to the top of extractor and connection and the valvular level of setting
Pipeline；Second gas-liquid partial circuit includes the second vertical pipeline being connected to the top of the second fluid reservoir, the top with extractor
Both the shared vertical pipeline of connection and connection and the valvular horizontal pipeline of setting；And the first siphon partial circuit and
Second siphon partial circuit is respectively arranged with valve.
Extraction system according to the present invention, the first siphon partial circuit and the second siphon partial circuit are respectively provided with and are bent up
Folding part point and its highest point are lower than the top of extractor.
Spray for refreshing air according to the present invention, plant efficient sterilization component are aoxidized by Titanium Dioxide, such as
Hu Tianyi, significantly improves sterilization and except formaldehyde ability, and to human body is non-stimulated and side effect.
Detailed description of the invention
Fig. 1 is the schematic diagram of vegetable oil extraction system (device) according to the present invention.
Specific embodiment
Plant oil extract
The present invention devises quick (uninterrupted) vegetable oil extraction system, to meet industrialized production fruits and vegetables cleaning solution when institute
Need vegetable oil raw materials.In the present invention, vegetable oil, essential oil and volatile oil meaning are identical, are mentioning for corresponding plant referenced below
Take liquid.
Referring to Fig. 1, vegetable oil extraction system of the invention includes the first fluid reservoir 10 and the second fluid reservoir 20, cooler 30
And extractor 40.
The bottom of first fluid reservoir 10 is equipped with the drain pipe 11 for being mounted with valve 12 thereon, and top passes through the first gas-liquid part
Circuit is connected to the top of extractor 40, and upper lateral part then passes through the first siphon partial circuit 50 and is connected to the bottom of extractor 40.
First gas-liquid partial circuit includes the first vertical pipeline 13 being connected to the top of the first fluid reservoir 10, the top with extractor 40
Both the shared vertical pipeline 33 of connection and connection and the horizontal pipeline for being provided with valve 14.First siphon partial circuit 50
It is provided with valve 51.As shown in Figure 1, the first siphon partial circuit 50 is lower than extractor with part and its highest point is folded upward at
40 top.
Similarly, the bottom of the second fluid reservoir 20 is equipped with the drain pipe 21 for being mounted with valve 22 thereon, and top passes through second
Gas-liquid partial circuit is connected to the top of extractor 40, and upper lateral part then passes through the bottom of the second siphon partial circuit 60 and extractor 40
Portion's connection.Second gas-liquid partial circuit includes the second vertical pipeline 23 and extractor being connected to the top of the second fluid reservoir 20
Both the shared vertical pipeline 33 of 40 top connection and connection and the horizontal pipeline for being provided with valve 24.Second siphon portion
Point circuit 60 is provided with valve 61.As shown in Figure 1, the first siphon partial circuit 60, which also has, is folded upward at part and its highest point
Lower than the top of extractor 40.
In Fig. 1, shown first gas-liquid partial circuit and the second gas-liquid partial circuit are shared with vertical pipeline 33 is shared
Vertical pipeline 33 passes through cooler 30.In alternative embodiments, the first gas-liquid partial circuit and the second gas-liquid partial circuit can also
Vertical pipeline 33 is shared not have, but respectively there is the vertical pipeline across cooler 30, can be omitted in this case
Valve 14 and valve 24.
Auger conveyor 44 is installed, (drying) that will be added from the top-feed mouth 41 of extractor 40 in extractor 40
Plant granule or powder are transmitted along extractor length direction (being illustrated as horizontal direction), until near extractor discharge gate 42.Spiral shell
Powder particle in rotation conveyer 44 will directly be contacted with the liquid in extractor 40.
The working principle of said extracted system is briefly described below.
Firstly, plant granule or powder such as rhizoma atractylodis rhizome particle or ramulus cinnamomi is added in the feed opening 41 by extractor 40
Grain, and starting auger conveyor 44 spreads plant granule to the discharge gate 42 of extractor 40 along 40 horizontal direction of extractor.
Valve 12 and valve 22 are closed, is then added in the first fluid reservoir 10 and the second fluid reservoir 20 respectively and accounts for about tank body
Two or so the pure water accumulated score of three.
Close valve 24 and valve 61；Open valve 14 and 51.
Start cooler 30.
The first fluid reservoir 10 is heated until and keeping pure water constantly boiling therein constantly to form vapor.
The vapor formed in first fluid reservoir 10 leads to upwardly through after the first vertical pipeline 13 and horizontal pipeline to lower
It crosses and shares vertical pipeline 33, and become condensed water when via cooler 30 and be passed through extractor 40.
When liquid level in extractor 40 is more than the highest point of the first siphon partial circuit 50, extracting solution therein will
The first fluid reservoir 10 is returned by the first siphon partial circuit 50.
When becoming colorless substantially by the extracting solution of the first siphon partial circuit 50, stop the first fluid reservoir 10 of heating,
And start auger conveyor 44 so that extractor 40 is discharged via outlet 42 in plant wet-milling therein.
Simultaneously or and then with the discharging operation of above-mentioned auger conveyor 44, then by the feed opening 41 of extractor 40 it is added
(fresh) plant granule, still through auger conveyor 44 until near the discharge gate 42 of extractor 40.
Close valve 14 and valve 51；Open valve 24 and 61.
The second fluid reservoir 20 is heated to execute same extraction process.
Valve 12 is opened so that the extracting solution in first fluid reservoir 10 to be discharged by drain pipe 11, and distillation is subsequently isolated into
Water and plant (extraction) oil.
As described above, the first fluid reservoir 10 and the second fluid reservoir 20 work alternatively, and cooperate with the fast of auger conveyor 44
Fast conveying/discharge, so that (uninterrupted) the fast industrialization scale for realizing vegetable oil is extracted.
The preparation of spray
Pure water and glycerol are uniformly mixed；
It is then respectively adding coconut oleoyl amine DEA, sodium laureth sulfate, TEA lauryl sodium sulfate, mechanical stirring 15 is divided
Clock, 200 revs/min of mixing speed；
Add Atractylis oil and cassia twig oil and Nano titanium dioxide, and mechanical stirring 20 minutes, mixing speed 200
Rev/min；
It is eventually adding borneol, it is filling.
In above-mentioned auxiliary agent, DEA represents diethylin, and TEA represents triethyamino.
Embodiment 1 (spray weight proportion composition, similarly hereinafter)
Rhzoma Atractylodis Lanceae volatile oil: 1.0%, Ramulus Cinnamomi Volatile oil: 0.8%, coconut oleoyl amine DEA:0.5%, sodium laureth sulfate:
3%, TEA lauryl sodium sulfate: 2.0%, glycerol: 5%, borneol: 0.2%, Wastewater by Nanometer Anatase titanium dioxide 1.0%, pure
Water surplus.
Embodiment 2
Rhzoma Atractylodis Lanceae volatile oil: 1.0%, Ramulus Cinnamomi Volatile oil: 1.0%, coconut oleoyl amine DEA:0.5%, sodium laureth sulfate:
3%, TEA lauryl sodium sulfate: 2.0%, glycerol: 5%, borneol: 0.2%, Wastewater by Nanometer Anatase titanium dioxide 1.0%, pure
Water surplus.
Embodiment 3
Rhzoma Atractylodis Lanceae volatile oil: 1.5%, Ramulus Cinnamomi Volatile oil: 0.8%, coconut oleoyl amine DEA:0.5%, sodium laureth sulfate:
3%, TEA lauryl sodium sulfate: 2.0%, glycerol: 5%, borneol: 0.2%, Wastewater by Nanometer Anatase titanium dioxide 1.0%, pure
Water surplus.
Embodiment 4
Rhzoma Atractylodis Lanceae volatile oil: 1.5%, Ramulus Cinnamomi Volatile oil: 1.0%, coconut oleoyl amine DEA:0.5%, sodium laureth sulfate:
3%, TEA lauryl sodium sulfate: 2.0%, glycerol: 5%, borneol: 0.2%, Wastewater by Nanometer Anatase titanium dioxide 1.0%, pure
Water surplus.
Embodiment 5
Rhzoma Atractylodis Lanceae volatile oil: 1.5%, Ramulus Cinnamomi Volatile oil: 1.2%, coconut oleoyl amine DEA:0.5%, sodium laureth sulfate:
3%, TEA lauryl sodium sulfate: 2.0%, glycerol: 5%, borneol: 0.2%, Wastewater by Nanometer Anatase titanium dioxide 1.0%, pure
Water surplus.
Test 1 --- taste removal test
Different tests place is chosen, toilet, basement, laboratory, kitchen, air-conditioned room, garbage house, finishing room are as examination
Test place.Above-mentioned place is used into spray for refreshing air obtained by Examples 1 to 5 respectively, comparative example, which uses, is free of rhizoma atractylodis and osmanthus
Branch extract component spray as control (conventional amount used, by spraying use 1-3 times, continue to carry out tracking assessment after five minutes,
It the results are shown in Table 1.
Evaluation standard are as follows: √ √ √-free from extraneous odour；√ √-peculiar smell is weaker；√-has obvious peculiar smell
The different spray evaluating results of table 1
| Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 | Comparative example | |
| Toilet | √√√ | √√√ | √√√ | √√√ | √√√ | √ |
| Basement | √√√ | √√√ | √√√ | √√√ | √√ | √ |
| Laboratory | √√√ | √√ | √√√ | √√√ | √√√ | √√ |
| Kitchen | √√√ | √√√ | √√ | √√√ | √√ | √ |
| Air-conditioned room | √√√ | √√√ | √√√ | √√ | √√√ | √ |
| Garbage house | √√√ | √√√ | √√√ | √√√ | √√√ | √ |
| Fit up room | √√√ | √√√ | √√√ | √√√ | √√√ | √ |
The result shows that: the various embodiments described above spray has the function of significantly adsorbing peculiar smell and have significantly except formaldehyde
Effect.
Test 2 --- Suspension quantitative bactericidal test
(1) three kinds of staphylococcus aureus, streptococcus, streptococcus anaerobius bacterial strains is selected to press disinfection technology standard preparation respectively
Experiment bacteria suspension, concentration are 1 × 108cfu/ml~5 × 108cfu/ml.
(2) the sterile Boiling tube of sterilizing test is taken, 0.5ml test bacteria suspension is first added, adds the organic interference of 0.5ml
Substance,
It mixes, sets in 20 DEG C of ± 1 DEG C of water-baths after 5min, the liquid with fresh air of each embodiment preparation is drawn with aseptic straw
4.0ml sample, injection wherein, are mixed rapidly and are clocked immediately.
(3) bacterium to be tested and air-atomizing agent interacted to each predetermined time, drew 0.5ml test organisms and air respectively
Spray mixed liquor is added in the sterilized neutralizer of 4.5ml, is mixed.
(4) after each pipe test organisms and air-atomizing agent mixed liquor are added neutralizer effect 10min, 1.0ml sample is drawn respectively
Liquid, by viable bacteria culture method of counting measurement survival bacterium number, every pipe sample liquid is inoculated with 2 plates.Such as the bacterium colony grown on plate
When number is more, after 10 times of dilutions of series can be carried out, then carries out viable bacteria culture and count.
(5) air-atomizing agent is replaced with dilution simultaneously, parallel test is carried out, as positive control.
(6) all test samples are cultivated in 37 DEG C of incubators, observe final result to bacterial propagule culture 48h；It is right
Bacterial spore need to cultivate 72h observation final result.
(7) test is repeated 3 times, and is calculated the viable bacteria concentration (cfu/ml) of each group, and be scaled logarithm (N), is then pressed
Formula, which calculates, kills logarithm:
Kill logarithm (No)-test group viable bacteria concentration logarithm of logarithm (KL)=control group mean viable concentration
(Nx) test result is as shown in table 1.
The different embodiment sterilization test evaluating results (action time < 10min) of table 2
Compared with the similar products of market, the present invention has set up a kind of natural green spray for refreshing air, have it is resistant to high temperatures, resist
Oxidation, the characteristic of long-time moisturizing, some smell substances that can either be removed in air can keep room aroma for a long time again；
Two kinds of essential oils of rhizoma atractylodis and ramulus cinnamomi, which combine to supplement and complement each other, simultaneously has synergistic effect, then by the catalysed oxidn of titanium dioxide,
It significantly can efficiently remove indoor formaldehyde and have to common bacteria gram-positive bacteria, Gram-negative bacteria, fungi, saccharomycete etc.
Quickly, sterilization persistently rather than bacteriostasis have good air purification effect.
Claims (3)
1. a kind of spray for refreshing air, consisting of: Atractylis oil: 1.0%-1.5%, cassia twig oil: 0.8%-1.2%, cocounut oil
Amide DEA:0.5%-1.0%, sodium laureth sulfate: 3%-4%, TEA lauryl sodium sulfate: 2.0%-3.0%, sweet
Oil: 5%-8%, borneol: 0.2%-0.3%, Nano titanium dioxide 1.0-2.0%, pure water surplus.
2. a kind of production method of spray for refreshing air as claimed in claim 1, comprising:
Pure water and glycerol are uniformly mixed；
It is then respectively adding coconut oleoyl amine DEA, sodium laureth sulfate, TEA lauryl sodium sulfate, stir and keeps it sufficiently molten
Solution；
Atractylis oil and cassia twig oil and Nano titanium dioxide are added, and is stirred evenly；
It is eventually adding borneol and carries out filling.
3. production method according to claim 2, wherein Atractylis oil and/or cassia twig oil are continuously prepared by following techniques:
Rhizoma atractylodis rhizome powder and/or ramulus cinnamomi powder are added to the extractor for being equipped with auger conveyor；
First fluid reservoir of the heating equipped with pure water is to generate vapor；
Vapor is passed through extractor after cooler is condensed into liquid water to submerge rhizoma atractylodis rhizome powder and/or ramulus cinnamomi powder；
When the liquid level in extractor is higher than the highest point of the siphon pipe of connection extractor and the first fluid reservoir, mentioning in extractor
Liquid is taken to enter the first fluid reservoir automatically by siphon pipe；
When the extracting solution in extractor becomes colorless, start extractor in auger conveyor with by rhizoma atractylodis rhizome wet-milling and/
Or extractor is discharged in ramulus cinnamomi wet-milling, while rhizoma atractylodis rhizome powder and/or ramulus cinnamomi powder is added into extractor again；
Stop the first fluid reservoir of heating and starts the second fluid reservoir simultaneously to continue above-mentioned steps；And
The extracting solution in the first fluid reservoir is separated to obtain Atractylis oil and/or cassia twig oil.
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811078923.3A CN110326627B (en) | 2018-09-17 | 2018-09-17 | Air refreshing spray |
| PCT/CN2019/099838 WO2020057285A1 (en) | 2018-09-17 | 2019-08-08 | Atractylodes oil and/or cassia twig oil, production method therefor and use thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811078923.3A CN110326627B (en) | 2018-09-17 | 2018-09-17 | Air refreshing spray |
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| Publication Number | Publication Date |
|---|---|
| CN110326627A true CN110326627A (en) | 2019-10-15 |
| CN110326627B CN110326627B (en) | 2021-08-31 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811078923.3A Active CN110326627B (en) | 2018-09-17 | 2018-09-17 | Air refreshing spray |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2021022562A1 (en) * | 2019-08-08 | 2021-02-11 | 中国医学科学院药用植物研究所 | Pure natural compound essential oil having broad-spectrum bactericidal activity and preparation and application thereof |
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