CN107279199A - A kind of indoor disinfectant and preparation method thereof - Google Patents

A kind of indoor disinfectant and preparation method thereof Download PDF

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Publication number
CN107279199A
CN107279199A CN201710475706.7A CN201710475706A CN107279199A CN 107279199 A CN107279199 A CN 107279199A CN 201710475706 A CN201710475706 A CN 201710475706A CN 107279199 A CN107279199 A CN 107279199A
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parts
essential oil
herbal medicine
extracts
chinese herbal
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Chinese (zh)
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张安育
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Hefei Huagai Biotechnology Co Ltd
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Hefei Huagai Biotechnology Co Ltd
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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
    • A01N59/16Heavy metals; Compounds thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N63/00Biocides, pest repellants or attractants, or plant growth regulators containing microorganisms, viruses, microbial fungi, animals or substances produced by, or obtained from, microorganisms, viruses, microbial fungi or animals, e.g. enzymes or fermentates
    • A01N63/10Animals; Substances produced thereby or obtained therefrom
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • A01N65/12Asteraceae or Compositae [Aster or Sunflower family], e.g. daisy, pyrethrum, artichoke, lettuce, sunflower, wormwood or tarragon
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • A01N65/24Lauraceae [Laurel family], e.g. laurel, avocado, sassafras, cinnamon or camphor
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/40Liliopsida [monocotyledons]
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/40Liliopsida [monocotyledons]
    • A01N65/48Zingiberaceae [Ginger family], e.g. ginger or galangal
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D53/00Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D53/00Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/34Chemical or biological purification of waste gases
    • B01D53/74General processes for purification of waste gases; Apparatus or devices specially adapted therefor
    • B01D53/86Catalytic processes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/06Silicon, titanium, zirconium or hafnium; Oxides or hydroxides thereof
    • B01J21/063Titanium; Oxides or hydroxides thereof
    • B01J35/39
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2253/00Adsorbents used in seperation treatment of gases and vapours
    • B01D2253/10Inorganic adsorbents
    • B01D2253/102Carbon
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2255/00Catalysts
    • B01D2255/20Metals or compounds thereof
    • B01D2255/207Transition metals
    • B01D2255/20792Zinc
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2258/00Sources of waste gases
    • B01D2258/06Polluted air

Abstract

The invention discloses a kind of indoor disinfectant and preparation method thereof, it is related to disinfectant technical field, including 40 ~ 50 parts of 90 ~ 110 parts of extracts of Chinese herbal medicine, 40 ~ 50 parts of borneol, 30 ~ 40 parts of bamboo carbon powder, 20 ~ 30 parts of essential oil component, 20 ~ 30 parts of nano zine oxide, 10 ~ 15 parts of AEO, 2 ~ 10 parts of cationic surfactant, 2 ~ 8 parts of buffer, 2 ~ 4 parts of solubilizer and deionized water.The present invention have have no toxic side effect, noresidue and high safety the features such as small excitant, sprinkling can be contacted directly with skin in atmosphere, non-stimulated to skin, the bactericidal property with wide spectrum, stronger stability have good killing effect to bacterium, fungi, mould.

Description

A kind of indoor disinfectant and preparation method thereof
Technical field
The present invention relates to disinfectant technical field, and in particular to a kind of indoor disinfectant and preparation method thereof.
Background technology
With the aggravation of urban air pollution, urban air-quality is significantly reduced, and dirty air turns into various and caused The hotbed of germ, causes various infectious disease wide-scale distributions in city in recent years, influence people's life health.Existing air sterillization The how irritant smell of agent, interior is used, and a small amount of spray effect is not obvious, and a large amount of sprinkling smells are too heavy, can make one to produce nausea, The uncomfortable reaction such as vomiting.There are some air fresheners although tasteless, but it is expensive, it is unsuitable for daily sprinkling.
The content of the invention
It is an object of the invention to provide a kind of indoor disinfectant and preparation method thereof, with having no toxic side effect, noresidue and The features such as excitant is small high safety, sprinkling can be contacted directly with skin in atmosphere, killing with wide spectrum non-stimulated to skin Bacterium performance, stronger stability, have good killing effect to bacterium, fungi, mould.
The invention provides following technical scheme:A kind of indoor disinfectant, includes the raw material of following part meter:Chinese herbal medicine is carried Take 90 ~ 110 parts of liquid, 40 ~ 50 parts of borneol, 30 ~ 40 parts of bamboo carbon powder, 20 ~ 30 parts of essential oil component, 20 ~ 30 parts of nano zine oxide, fat 10 ~ 15 parts of alcohol APEO, 2 ~ 10 parts of cationic surfactant, 2 ~ 8 parts of buffer, 2 ~ 4 parts of solubilizer and deionized water 40 ~ 50 parts;
The extracts of Chinese herbal medicine includes the raw material that following part is counted:20 ~ 30 parts of Chinese gall, 20 ~ 30 parts of the coptis, 10 ~ 20 parts of folium artemisiae argyi, The white palm 10 ~ 15 parts, 10 ~ 15 parts of honeysuckle, 2 ~ 10 parts of magnolia obovata;
The essential oil component includes the raw material that following part is counted:10 ~ 15 parts of ginger essential oil, 5 ~ 10 parts of chamomile essential oil and cinnamon essential oil 2 ~ 4 parts.
Preferably, the raw material of following part meter is included:100 parts of extracts of Chinese herbal medicine, 45 parts of borneol, 35 parts of bamboo carbon powder, essential oil 25 parts of component, 25 parts of nano zine oxide, 12.5 parts of AEO, 6 parts of cationic surfactant, 5 parts of buffer, 45 parts of 3 parts of solubilizer and deionized water;
The extracts of Chinese herbal medicine includes the raw material that following part is counted:25 parts of Chinese gall, 25 parts of the coptis, 15 parts of folium artemisiae argyi, 12.5 are slapped in vain Part, 12.5 parts of honeysuckle, 6 parts of magnolia obovata;
The essential oil component includes the raw material that following part is counted:12.5 parts of ginger essential oil, 7.5 parts of chamomile essential oil and cinnamon essential oil 3 Part.
Preferably, the preparation method of the nano zine oxide is:Into 0.1 ~ 0.3mol/L zinc acetate solutions add 0.2 ~ The volume ratio of 0.6mol/L urea liquid, zinc acetate solution and urea liquid is 3:2, both are well mixed, then controlled Temperature is 80 ~ 90 DEG C of 3 ~ 4h of reaction, after question response terminates, and will react obtained product and filters, collect after filter residue, filter residue and drying 2 ~ 4h is calcined at 300 ~ 400 DEG C, that is, obtains nano zine oxide.
Preferably, the cationic surfactant is zephiran or alkyldimethylbenzylammonium bromine Change ammonium, the buffer is the one or more in dipotassium hydrogen phosphate, disodium hydrogen phosphate, potassium dihydrogen phosphate, sodium dihydrogen phosphate.
Preferably, the borneol extracts the knot obtained for the resin and volatile oil processed goods of Spore density kapur It is brilliant.
Preferably, the solubilizer is rilanit special.
Preferably, the preparation method of the ginger essential oil is:Ginger is weighed, is cleaned with clear water, 90 ~ 100 is put into after section 8 ~ 10min of boiling in DEG C water, taking-up, which is drained, to be put into heating container, adds the hydromel that mass concentration is 20 ~ 30%, heating plus Heat, keep heating-up temperature be 90 ~ 95 DEG C, the heat time be 50 ~ 60min, obtain mixed liquor after cooling, into mixed liquor add 1 ~ After 40 ~ 50% ethanol solutions of 2 times of parts by weight, 6 ~ 8h of immersion refluxing extraction, obtained extract solution is the ginger essential oil.
The present invention provides a kind of preparation method of indoor disinfectant, comprises the following steps:
(1), prepare extracts of Chinese herbal medicine
Chinese gall, the coptis, folium artemisiae argyi, the white palm, honeysuckle magnolia obovata are weighed according to proportioning, is crushed and crosses 40~60 mesh sieves, mixed Conjunction uniformly obtains pulvis;
Ultrasonic assistant ethanol extraction is carried out to pulvis, 50 ~ 65% ethanol of 5~10 times of parts by weight are added into pulvis, in ultrasound Under ripple booster action, 30~50min of refluxing extraction under the conditions of 60~80 DEG C is extracted 3 times, and the filtrate of extraction is merged, and refrigeration is put Put after 10~20h, be concentrated under reduced pressure recovery ethanol under the conditions of 55~85 DEG C, it is the extracts of Chinese herbal medicine to obtain concentrate, It is standby;
(2), prepare finished product
Surplus stock and step are weighed according to proportioning(1)Obtained extracts of Chinese herbal medicine mixing, is put into homogenizer 900 It is mixed evenly under the conditions of ~ 1000r/min, packing produces the indoor disinfectant after standing.
Preferably, the step(1)Middle ultrasonic power is 150 ~ 250W.
Beneficial effects of the present invention:With having no toxic side effect, noresidue and high safety the features such as small excitant, be sprayed at Directly it can be contacted in air with skin, bactericidal property with wide spectrum, stronger stability non-stimulated to skin, to bacterium, very Bacterium, mould have good killing effect, specific as follows:
(1), the bamboo carbon powder that adds refers to the powdered substance of bamboo charcoal in the present invention, can be rapid with fabulous adsorption capacity Effectively absorb pernicious gas in air;
(2), the nano zine oxide that adds, as photocatalyst, produces the extremely strong free hydroxy of oxidability and work in the present invention Property oxygen, with photoredox function, the oxidable various organic compounds of decomposition and part inorganic matter, killing bacterium and decomposition has Organic pollution, is resolved into free of contamination water and carbon dioxide by organic pollutants, can effectively degradation of formaldehyde, benzene, toluene, two The pollutants such as toluene, ammonia, VOC, and the antiseptic property with high-efficiency broad spectrum, can also effectively kill various bacteria, antibiotic rate in addition Up to 99.99%;
(4), the present invention realize sterilization while can also effectively remove air in peculiar smell, it is applied widely;
(5), the present invention in addition AEO (AEO), applied in disinfectant, one played to skin and mucosa Determine the protective effect of degree, reduce stimulation of the disinfectant to skin;
(6), add extracts of Chinese herbal medicine in the present invention, can effectively kill various harmful bacterias and virus in air, reduce various The generation of infectious disease, beneficial health, the raw material synergy of addition is good, and bacterium is not developed immunity to drugs;Wherein, addition Chinese gall has preferable bacteriostasis, to Pseudomonas aeruginosa, shigella dysenteriae, proteus, Escherichia coli, typhoid bacillus, enteritis Bacillus etc. has inhibitory action;The coptis is to staphylococcus aureus, hemolytic streptococcus, pneumococcus, diplococcus meningitidis, charcoal The pathogenic bacteria such as subcutaneous ulcer bacillus are viral with good inhibiting effect with influenza virus, hepatitis B etc.;
(7), the present invention in add essential oil component, fully used the restraining and sterilizing bacteria of these natural components to act on, antioxidation, It is nontoxic, harmless, have no side effect, it is non-stimulated to human body;Wherein, chamomile essential oil has releive pressure, fatigue-relieving, mosquito expelling Effect, cinnamon essential oil, which has, relaxes slow muscle cramp and rheumatism, improves arthralgia, digestion, or a kind of antiseptic, It is all effective in cure to flu or respiratory tract infection;
(8), addition surfactant improves disinfectant to the wettability of body surface in the present invention, promotes disinfectant and object The contact action on surface.
Embodiment
With reference to specific embodiment, the present invention is expanded on further.These embodiments be merely to illustrate the present invention and without In limitation the scope of the present invention.
Embodiment 1
A kind of indoor disinfectant, includes the raw material of following part meter:
90 parts of extracts of Chinese herbal medicine;
40 parts of borneol;
30 parts of bamboo carbon powder;
20 parts of essential oil component;
20 parts of nano zine oxide;
10 parts of AEO;
2 parts of cationic surfactant;
2 parts of buffer;
2 parts of solubilizer;
40 parts of deionized water;
The extracts of Chinese herbal medicine includes the raw material that following part is counted:20 parts of Chinese gall, 20 parts of the coptis, 10 parts of folium artemisiae argyi, white 10 parts of the palm, 10 parts of honeysuckle, 2 parts of magnolia obovata;
The essential oil component includes the raw material that following part is counted:2 parts of 10 parts of ginger essential oil, 5 parts of chamomile essential oil and cinnamon essential oil.
Wherein, the preparation method of the nano zine oxide is:Add 0.2mol/L's into 0.1mol/L zinc acetate solutions The volume ratio of urea liquid, zinc acetate solution and urea liquid is 3:2, both are well mixed, it is 80 DEG C then to control temperature 3h is reacted, after question response terminates, the product that reaction is obtained is filtered, and 2h is calcined at 300 DEG C after collecting filter residue, filter residue and drying, Obtain nano zine oxide.
Wherein, the cationic surfactant is zephiran, and the buffer is phosphoric acid hydrogen two Potassium.
Wherein, the borneol extracts the crystallization obtained for the resin and volatile oil processed goods of Spore density kapur.
Wherein, the solubilizer is rilanit special.
Wherein, the preparation method of the ginger essential oil is:Ginger is weighed, is cleaned, is put into after section in 90 DEG C of water with clear water Boiling 8min, taking-up, which is drained, to be put into heating container, adds the hydromel that mass concentration is 20%, and heating heating keeps heating temperature Spend for 90 DEG C, the heat time is to obtain mixed liquor after 50min, cooling, and 40% ethanol that 1 times of parts by weight is added into mixed liquor is molten After liquid, immersion refluxing extraction 6h, obtained extract solution is the ginger essential oil.
A kind of preparation method of indoor disinfectant is provided in the present embodiment, comprised the following steps:
(1), prepare extracts of Chinese herbal medicine
Chinese gall, the coptis, folium artemisiae argyi, the white palm, honeysuckle magnolia obovata are weighed according to proportioning, is crushed and crosses 40 mesh sieves, mixing is equal It is even to obtain pulvis;
Ultrasonic assistant ethanol extraction is carried out to pulvis, 50% ethanol of 5 times of parts by weight is added into pulvis, in ultrasonic assistant Under effect, refluxing extraction 30min under the conditions of 60 DEG C is extracted 3 times, and the filtrate of extraction is merged, and refrigeration is placed after 10h, at 55 DEG C Under the conditions of be concentrated under reduced pressure recovery ethanol, it is the extracts of Chinese herbal medicine to obtain concentrate, standby;
(2), prepare finished product
Surplus stock and step are weighed according to proportioning(1)Obtained extracts of Chinese herbal medicine mixing, is put into homogenizer It is mixed evenly under the conditions of 900r/min, packing produces the indoor disinfectant after standing.
Wherein, the step(1)Middle ultrasonic power is 150W.
Embodiment 2
A kind of indoor disinfectant, includes the raw material of following part meter:
110 parts of extracts of Chinese herbal medicine;
50 parts of borneol;
40 parts of bamboo carbon powder;
30 parts of essential oil component;
30 parts of nano zine oxide;
15 parts of AEO;
10 parts of cationic surfactant;
8 parts of buffer;
4 parts of solubilizer;
50 parts of deionized water;
The extracts of Chinese herbal medicine includes the raw material that following part is counted:30 parts of Chinese gall, 30 parts of the coptis, 20 parts of folium artemisiae argyi, white 15 parts of the palm, 15 parts of honeysuckle, 10 parts of magnolia obovata;
The essential oil component includes the raw material that following part is counted:4 parts of 15 parts of ginger essential oil, 10 parts of chamomile essential oil and cinnamon essential oil.
The preparation method of the nano zine oxide is:The urea that 0.6mol/L is added into 0.3mol/L zinc acetate solutions is molten The volume ratio of liquid, zinc acetate solution and urea liquid is 3:2, both are well mixed, it is 90 DEG C of reaction 4h then to control temperature, After question response terminates, the product that reaction is obtained is filtered, and 4h is calcined at 400 DEG C after collecting filter residue, filter residue and drying, that is, is received Rice zinc oxide.
Wherein, the cationic surfactant is Alkyl dimethyl benzyl ammonium bromide, and the buffer is phosphoric acid hydrogen two Sodium.
Wherein, the borneol extracts the crystallization obtained for the resin and volatile oil processed goods of Spore density kapur.
Wherein, the solubilizer is rilanit special.
Wherein, the preparation method of the ginger essential oil is:Ginger is weighed, is cleaned, is put into after section in 100 DEG C of water with clear water Boiling 10min, taking-up, which is drained, to be put into heating container, adds the hydromel that mass concentration is 30%, and heating heating keeps heating Temperature is 95 DEG C, and the heat time is to obtain mixed liquor after 60min, cooling, and 50% ethanol of 2 times of parts by weight is added into mixed liquor After solution, immersion refluxing extraction 8h, obtained extract solution is the ginger essential oil.
A kind of preparation method of indoor disinfectant is provided in the present embodiment, comprised the following steps:
(1), prepare extracts of Chinese herbal medicine
Chinese gall, the coptis, folium artemisiae argyi, the white palm, honeysuckle magnolia obovata are weighed according to proportioning, is crushed and crosses 60 mesh sieves, mixing is equal It is even to obtain pulvis;
Ultrasonic assistant ethanol extraction is carried out to pulvis, 65% ethanol of 10 times of parts by weight is added into pulvis, in ultrasonic assistant Under effect, refluxing extraction 50min under the conditions of 80 DEG C is extracted 3 times, and the filtrate of extraction is merged, and refrigeration is placed after 20h, at 85 DEG C Under the conditions of be concentrated under reduced pressure recovery ethanol, it is the extracts of Chinese herbal medicine to obtain concentrate, standby;
(2), prepare finished product
Surplus stock and step are weighed according to proportioning(1)Obtained extracts of Chinese herbal medicine mixing, is put into homogenizer It is mixed evenly under the conditions of 1000r/min, packing produces the indoor disinfectant after standing.
Wherein, the step(1)Middle ultrasonic power is 250W.
Embodiment 3
A kind of indoor disinfectant, includes the raw material of following part meter:
100 parts of extracts of Chinese herbal medicine;
45 parts of borneol;
35 parts of bamboo carbon powder;
25 parts of essential oil component;
25 parts of nano zine oxide;
12.5 parts of AEO;
6 parts of cationic surfactant;
5 parts of buffer;
3 parts of solubilizer;
45 parts of deionized water;
The extracts of Chinese herbal medicine includes the raw material that following part is counted:25 parts of Chinese gall, 25 parts of the coptis, 15 parts of folium artemisiae argyi, 12.5 are slapped in vain Part, 12.5 parts of honeysuckle, 6 parts of magnolia obovata;
The essential oil component includes the raw material that following part is counted:12.5 parts of ginger essential oil, 7.5 parts of chamomile essential oil and cinnamon essential oil 3 Part.
Wherein, the preparation method of the nano zine oxide is:Add 0.4mol/L's into 0.2mol/L zinc acetate solutions The volume ratio of urea liquid, zinc acetate solution and urea liquid is 3:2, both are well mixed, it is 85 DEG C then to control temperature 3.5h is reacted, after question response terminates, the product that reaction is obtained is filtered, collect and calcined after filter residue, filter residue and drying at 350 DEG C 3h, that is, obtain nano zine oxide.
Wherein, the cationic surfactant is Alkyl dimethyl benzyl ammonium bromide, and the buffer is biphosphate Potassium.
Wherein, the borneol extracts the crystallization obtained for the resin and volatile oil processed goods of Spore density kapur.
Wherein, the solubilizer is rilanit special.
Wherein, the preparation method of the ginger essential oil is:Ginger is weighed, is cleaned, is put into after section in 95 DEG C of water with clear water Boiling 9min, taking-up, which is drained, to be put into heating container, adds the hydromel that mass concentration is 25%, and heating heating keeps heating temperature Spend for 93 DEG C, the heat time is to obtain mixed liquor after 55min, cooling, and 45% ethanol of 1.5 times of parts by weight is added into mixed liquor After solution, immersion refluxing extraction 7h, obtained extract solution is the ginger essential oil.
The present embodiment provides a kind of preparation method of indoor disinfectant, comprises the following steps:
(1), prepare extracts of Chinese herbal medicine
Chinese gall, the coptis, folium artemisiae argyi, the white palm, honeysuckle magnolia obovata are weighed according to proportioning, is crushed and crosses 50 mesh sieves, mixing is equal It is even to obtain pulvis;
Ultrasonic assistant ethanol extraction is carried out to pulvis, 55% ethanol of 7 times of parts by weight is added into pulvis, in ultrasonic assistant Under effect, refluxing extraction 40min under the conditions of 70 DEG C is extracted 3 times, and the filtrate of extraction is merged, and refrigeration is placed after 15h, at 70 DEG C Under the conditions of be concentrated under reduced pressure recovery ethanol, it is the extracts of Chinese herbal medicine to obtain concentrate, standby;
(2), prepare finished product
Surplus stock and step are weighed according to proportioning(1)Obtained extracts of Chinese herbal medicine mixing, is put into homogenizer It is mixed evenly under the conditions of 950r/min, packing produces the indoor disinfectant after standing.
Wherein, the step(1)Middle ultrasonic power is 200W.
The present invention is described in detail with reference to the foregoing embodiments, for those skilled in the art, its according to The technical scheme described in foregoing embodiments can so be modified, or which part technical characteristic is equally replaced Change.Within the spirit and principles of the invention, any modification, equivalent substitution and improvements made etc., should be included in the present invention Protection domain within.

Claims (9)

1. a kind of indoor disinfectant, it is characterised in that the raw material counted including following part:90 ~ 110 parts of extracts of Chinese herbal medicine, borneol 40 ~ 50 parts, 30 ~ 40 parts of bamboo carbon powder, 20 ~ 30 parts of essential oil component, 20 ~ 30 parts of nano zine oxide, AEO 10 ~ 15 40 ~ 50 parts of part, 2 ~ 10 parts of cationic surfactant, 2 ~ 8 parts of buffer, 2 ~ 4 parts of solubilizer and deionized water;
The extracts of Chinese herbal medicine includes the raw material that following part is counted:20 ~ 30 parts of Chinese gall, 20 ~ 30 parts of the coptis, 10 ~ 20 parts of folium artemisiae argyi, The white palm 10 ~ 15 parts, 10 ~ 15 parts of honeysuckle, 2 ~ 10 parts of magnolia obovata;
The essential oil component includes the raw material that following part is counted:10 ~ 15 parts of ginger essential oil, 5 ~ 10 parts of chamomile essential oil and cinnamon essential oil 2 ~ 4 parts.
2. indoor disinfectant according to claim 1, it is characterised in that the raw material counted including following part:Chinese herbal medicine is extracted 100 parts of liquid, 45 parts of borneol, 35 parts of bamboo carbon powder, 25 parts of essential oil component, 25 parts of nano zine oxide, AEO 12.5 Part, 6 parts of cationic surfactant, 5 parts of buffer, 3 parts of solubilizer and 45 parts of deionized water;
The extracts of Chinese herbal medicine includes the raw material that following part is counted:25 parts of Chinese gall, 25 parts of the coptis, 15 parts of folium artemisiae argyi, 12.5 are slapped in vain Part, 12.5 parts of honeysuckle, 6 parts of magnolia obovata;
The essential oil component includes the raw material that following part is counted:12.5 parts of ginger essential oil, 7.5 parts of chamomile essential oil and cinnamon essential oil 3 Part.
3. indoor disinfectant according to claim 1, it is characterised in that the preparation method of the nano zine oxide is:To The volume of 0.2 ~ 0.6mol/L urea liquid, zinc acetate solution and urea liquid is added in 0.1 ~ 0.3mol/L zinc acetate solutions Than for 3:2, both are well mixed, it is 80 ~ 90 DEG C of 3 ~ 4h of reaction then to control temperature, and after question response terminates, reaction is obtained Product filtering, collect filter residue, calcine 2 ~ 4h after filter residue and drying at 300 ~ 400 DEG C, that is, obtain nano zine oxide.
4. indoor disinfectant according to claim 1, it is characterised in that the cationic surfactant is alkyl-dimethyl Base benzyl ammonium chloride or Alkyl dimethyl benzyl ammonium bromide, the buffer are dipotassium hydrogen phosphate, disodium hydrogen phosphate, di(2-ethylhexyl)phosphate One or more in hydrogen potassium, sodium dihydrogen phosphate.
5. indoor disinfectant according to claim 1, it is characterised in that the borneol is Spore density kapur Resin and volatile oil processed goods extract the crystallization obtained.
6. indoor disinfectant according to claim 1, it is characterised in that the solubilizer is rilanit special.
7. indoor disinfectant according to claim 1, it is characterised in that the preparation method of the ginger essential oil is:Weigh Ginger, is cleaned with clear water, and 8 ~ 10min of boiling in 90 ~ 100 DEG C of water is put into after section, and taking-up, which is drained, to be put into heating container, is added Mass concentration is 20 ~ 30% hydromel, and heating heating, holding heating-up temperature is 90 ~ 95 DEG C, and the heat time is 50 ~ 60min, cold But mixed liquor is obtained afterwards, is added into mixed liquor after 40 ~ 50% ethanol solutions of 1 ~ 2 times of parts by weight, 6 ~ 8h of immersion refluxing extraction, Obtained extract solution is the ginger essential oil.
8. the preparation method of a kind of indoor disinfectant according to any one of claim 1 ~ 7, it is characterised in that including following Step:
(1), prepare extracts of Chinese herbal medicine
Chinese gall, the coptis, folium artemisiae argyi, the white palm, honeysuckle magnolia obovata are weighed according to proportioning, is crushed and crosses 40~60 mesh sieves, mixed Conjunction uniformly obtains pulvis;
Ultrasonic assistant ethanol extraction is carried out to pulvis, 50 ~ 65% ethanol of 5~10 times of parts by weight are added into pulvis, in ultrasound Under ripple booster action, 30~50min of refluxing extraction under the conditions of 60~80 DEG C is extracted 3 times, and the filtrate of extraction is merged, and refrigeration is put Put after 10~20h, be concentrated under reduced pressure recovery ethanol under the conditions of 55~85 DEG C, it is the extracts of Chinese herbal medicine to obtain concentrate, It is standby;
(2), prepare finished product
Surplus stock and step are weighed according to proportioning(1)Obtained extracts of Chinese herbal medicine mixing, is put into homogenizer 900 It is mixed evenly under the conditions of ~ 1000r/min, packing produces the indoor disinfectant after standing.
9. the preparation method of indoor disinfectant according to claim 8, it is characterised in that the step(1)Middle ultrasonic wave Power is 150 ~ 250W.
CN201710475706.7A 2017-06-21 2017-06-21 A kind of indoor disinfectant and preparation method thereof Withdrawn CN107279199A (en)

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CN108651382A (en) * 2018-05-05 2018-10-16 谈玉靓 A kind of sterilization method reducing disease infectious rate
CN108669099A (en) * 2018-05-05 2018-10-19 谈玉靓 A kind of preparation method for the disinfectant reducing disease infectious rate
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CN111449092A (en) * 2020-04-14 2020-07-28 深圳大学总医院 Preparation method of disinfectant for emergency diagnosis room
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CN108014624A (en) * 2018-01-11 2018-05-11 史书亭 The preparation method of green smell scavenger and its application method and its application
CN108184915A (en) * 2018-01-24 2018-06-22 合肥华盖生物科技有限公司 A kind of Household floor thimerosal and preparation method thereof
CN108651382A (en) * 2018-05-05 2018-10-16 谈玉靓 A kind of sterilization method reducing disease infectious rate
CN108669099A (en) * 2018-05-05 2018-10-19 谈玉靓 A kind of preparation method for the disinfectant reducing disease infectious rate
CN110326627B (en) * 2018-09-17 2021-08-31 中国医学科学院药用植物研究所 Air refreshing spray
CN110326627A (en) * 2018-09-17 2019-10-15 中国医学科学院药用植物研究所 Spray for refreshing air
CN109699686A (en) * 2019-01-07 2019-05-03 甘肃康承动物保健有限公司 A kind of disinfectant for killing avian influenza virus
CN110506738A (en) * 2019-08-27 2019-11-29 江苏瑞丰科技实业有限公司 A kind of efficient sterilizing air cleaning spray
CN111418615A (en) * 2019-12-17 2020-07-17 江苏天嘉生物科技有限公司 Preparation method of disinfectant
CN111449092A (en) * 2020-04-14 2020-07-28 深圳大学总医院 Preparation method of disinfectant for emergency diagnosis room
WO2021217324A1 (en) * 2020-04-27 2021-11-04 陕西高源体外诊断试剂有限公司 Disinfectant composition, preparation method therefor, and use thereof
CN113631155A (en) * 2020-04-27 2021-11-09 陕西高源体外诊断试剂有限公司 Disinfectant composition, preparation method and application thereof
CN114573015A (en) * 2022-03-18 2022-06-03 上海健康医学院 Nano zinc oxide composite antibacterial agent dispersion liquid and preparation method thereof
CN114573015B (en) * 2022-03-18 2023-10-27 上海健康医学院 Nanometer zinc oxide composite antibacterial agent dispersion liquid and preparation method thereof

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