CN107333813A - A kind of indoor air disinfectant and preparation method thereof - Google Patents

A kind of indoor air disinfectant and preparation method thereof Download PDF

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CN107333813A
CN107333813A CN201710563328.8A CN201710563328A CN107333813A CN 107333813 A CN107333813 A CN 107333813A CN 201710563328 A CN201710563328 A CN 201710563328A CN 107333813 A CN107333813 A CN 107333813A
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parts
essential oil
indoor air
raw material
following part
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张安育
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Hefei Huagai Biotechnology Co Ltd
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Hefei Huagai Biotechnology Co Ltd
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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N33/00Biocides, pest repellants or attractants, or plant growth regulators containing organic nitrogen compounds
    • A01N33/02Amines; Quaternary ammonium compounds
    • A01N33/12Quaternary ammonium compounds
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
    • A01N59/04Carbon disulfide; Carbon monoxide; Carbon dioxide
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
    • A01N59/16Heavy metals; Compounds thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/40Liliopsida [monocotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L9/00Disinfection, sterilisation or deodorisation of air
    • A61L9/01Deodorant compositions
    • A61L9/013Deodorant compositions containing animal or plant extracts, or vegetable material
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L2209/00Aspects relating to disinfection, sterilisation or deodorisation of air
    • A61L2209/20Method-related aspects
    • A61L2209/21Use of chemical compounds for treating air or the like

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  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Zoology (AREA)
  • Wood Science & Technology (AREA)
  • Plant Pathology (AREA)
  • Dentistry (AREA)
  • Agronomy & Crop Science (AREA)
  • Environmental Sciences (AREA)
  • Pest Control & Pesticides (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical & Material Sciences (AREA)
  • Biotechnology (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Botany (AREA)
  • Epidemiology (AREA)
  • Animal Behavior & Ethology (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Medicines Containing Plant Substances (AREA)

Abstract

The invention discloses a kind of indoor air disinfectant and preparation method thereof, is related to disinfectant technical field, includes the raw material of following part meter:75 ~ 80 parts of 45 ~ 55 parts of extracts of Chinese herbal medicine, 35 ~ 36 parts of bactericide, 32 ~ 33 parts of plants essential oil, 20 ~ 25 parts of activated particle, 17 ~ 19 parts of auxiliary agent and deionized water.The present invention it is nontoxic it is non-stimulated, smell is pure and fresh, sterilization bacteria-eliminating efficacy is good and lasting effect is long.

Description

A kind of indoor air disinfectant and preparation method thereof
Technical field
The present invention relates to disinfectant technical field, and in particular to a kind of indoor air disinfectant and preparation method thereof.
Background technology
Room air pollution is higher 2 ~ 10 times than outdoor, serious even as high as hundreds of times.Indoor Air Microorganisms are main From following two aspects:First, the spittle, people can will parasitize human mouth, bottleneck throat when deeply breathing, speak, sneezing The microorganism of position is spread in air in the form of the spittle;Second, the scurf and dust of people, according to measuring and calculating, averagely contain on each scurf Bacterium amount is up to 40,000, and with the activity of people indoors, scurf can be suspended in air with dust pollutes air, particularly has in family During patient, corresponding pathogen can be found in atmosphere, therefore the air sterillization to interior is particularly heavy to promoting health Will.
Air sanitizer of the prior art, currently used air disinfection method are mainly the sterilization using chemical composition Agent, such as Peracetic acid, lactic acid, hydrogen peroxide, formaldehyde, glutaraldehyde chemical method and ultraviolet irradiation, smelly chlorine generator etc. Physical method.These methods can kill pathogenic microorganisms, and effect is quick, and valid density is low, obtains preferable effect.But respectively have The defects of certain, such as toxic, excitant, metal protection, lasting effect, are poor;It is many itself to form pollutant, different journeys again Degree ground influences health, uncomfortable tenant in common's environment;Peculiar smell can not eliminate quickly after sterilization, and long-term use can have accumulation to human body Danger of poisoning etc..
The content of the invention
It is an object of the invention to provide a kind of indoor air disinfectant and preparation method thereof, it is nontoxic it is non-stimulated, smell is pure and fresh, Sterilization bacteria-eliminating efficacy is good and lasting effect is long.
The invention provides following technical scheme:A kind of indoor air disinfectant, include the raw material of following part meter:Medium-height grass 45 ~ 55 parts of medicament extracting solution, 35 ~ 36 parts of bactericide, 32 ~ 33 parts of plants essential oil, 20 ~ 25 parts of activated particle, 17 ~ 19 parts of auxiliary agent and go 75 ~ 80 parts of ionized water;
The extracts of Chinese herbal medicine includes the raw material of following part meter:15 ~ 17 parts of Chinese gall, 12 ~ 13 parts of the coptis, in vain slap 10 ~ 11 parts, 7 ~ 9 parts of honeysuckle, 4 ~ 6 parts of magnolia obovata;
The bactericide includes the raw material of following part meter:15 ~ 17 parts of stability carrier, 12 ~ 13 parts of nano zine oxide, nano-silica Change 20 ~ 23 parts of 10 ~ 11 parts of carbon, 8 ~ 9 parts of nano silicon, 8 ~ 9 parts of chlorine dioxide and deionized water;
The plants essential oil includes the raw material of following part meter:12 ~ 13 parts of wormwood essential oil, 10 ~ 11 parts of Peppermint essential oil and lavender essence 8 ~ 9 parts of oil;
The auxiliary agent includes the raw material of following part meter:8 ~ 9 parts of cationic surfactant, 6 ~ 8 parts of preservative, 4 ~ 5 parts of thickener With 3 ~ 4 parts of dispersant.
Wherein, the preparation method of the wormwood essential oil is:Take wormwood and crush, cross 80 ~ 90 mesh sieves and obtain wormwood powder, add Enter the ethanol solution of 10 ~ 15 times of mass parts, soak 8 ~ 10h, the concentration of ethanol solution is 45 ~ 50%, and microwave carries after immersion 40 ~ 50min is taken, microwave power is 500 ~ 600W, and extraction is filtered after terminating, and by filtrate concentrated by rotary evaporation untill without alcohol taste, is obtained The wormwood essential oil.
Wherein, the preparation method of the Peppermint essential oil is:Take dried peppermint leaf and crush, cross 110 ~ 120 mesh sieves and obtain dried peppermint leaf Powder, add the ethanol solution of 4 ~ 6 times of mass parts, soak 6 ~ 8h, the concentration of ethanol solution is 30 ~ 50%, immersion finish after 50 ~ 55 degrees Celsius of lower 30 ~ 40min of ultrasonic extraction, after extraction terminates, filtering, filtrate is rotated into concentrated by rotary evaporation, untill without alcohol taste Obtain the Peppermint essential oil.
Wherein, the preparation method of the Lavender is:Take lavender and crush, cross 50 ~ 80 mesh sieves and obtain lavender Powder, it is placed in beaker, adds the deionized water of 2 ~ 3 times of parts by weight, is placed on 40 ~ 50min of heating on electric furnace, after cooling, uses cloth Family name's funnel is filtered, and is retained filtrate and is obtained the Lavender.
Wherein, the activated particle is one in citric acid, tartaric acid, oxalic acid, boric acid, sulfamic acid and sodium dihydrogen phosphate Kind is several.
Wherein, the stability carrier is the one or more in diatomite, sepiolite, zeolite and silica.
Wherein, the cationic surfactant is quarternary ammonium salt compound, and the thickener is hydroxypropyl methyl cellulose, The preservative is methylisothiazolinone, and the dispersant is calgon.
The present invention provides a kind of preparation method of indoor air disinfectant, comprises the following steps:
(1), prepare extracts of Chinese herbal medicine
Chinese gall, the coptis, the white palm, honeysuckle magnolia obovata are weighed according to proportioning, is crushed and crosses 40~60 mesh sieves, be well mixed Obtain pulvis;
Ultrasonic assistant ethanol extraction is carried out to pulvis, 35 ~ 45% ethanol of 10~15 times of parts by weight are added into pulvis, super Under sound wave booster action, 20~30min of refluxing extraction under 60~80 degrees celsius, extract 3 times, the filtrate of extraction merged, After 6~8h is placed in refrigeration, be concentrated under reduced pressure recovery ethanol under 55~85 degrees celsius, and it is the Chinese herbal medicine to obtain concentrate Extract solution, it is standby;
(2), prepare bactericide
Chlorine dioxide is dissolved in deionized water, then sequentially adds stability carrier, nano zine oxide, nano-silica according to proportioning Change carbon and nano silicon, be well mixed, obtain the bactericide;
(3), by step(1)Obtained extracts of Chinese herbal medicine and step(2)Obtained bactericide mixing, then according to proportioning successively Surplus stock is added, is stirred with 200 ~ 300r/min rotating speed, obtains the indoor air disinfectant.
Beneficial effects of the present invention:It is nontoxic it is non-stimulated, smell is pure and fresh, sterilization bacteria-eliminating efficacy is good and lasting effect is long, specifically It is as follows:
(1), the present invention nano zine oxide, nanometer titanium dioxide carbon and nano silicon are added in bactericide, have very strong Photoredox function, it is oxidable to decompose various organic compounds and part inorganic matter, organic pollution is resolved into pollution-free Water and carbon dioxide;
(2), the present invention chlorine dioxide is added in bactericide, chlorine dioxide is slowly discharged by stability carrier, to human body and dynamic Thing is harmless, and has bactericidal effect, and chlorine dioxide has stronger absorption and penetration capacity to the cell membrane of bacterium, quick to suppress Microprotein synthesis destroys microorganism, and chlorine dioxide can have with sulfur oxide compound, cyanide, phenol and formaldehyde etc. Sterilize, eliminate the unusual smell, going the effect of formaldehyde;
(3), the present invention add quarternary ammonium salt compound in the feed as cationic surfactant, while sterilization can also be played The effect of sterilization, quarternary ammonium salt compound can make protein denaturation, change membrane passage, moisture is entered in thalline, So as to swelling rupture, therefore quarternary ammonium salt compound can high aggregation in phage surface, the metabolism of bacterium is influenceed, so as to reach Sterilization, sterilization functions;
(4), the present invention disinfectant it is non-stimulated to human body skin, respiratory system is not damaged, it is easy to use, in use, not It can only be sprayed, but also can be mounted in humidifier mounted in watering can, interior is carried out disinfection, is effectively improved indoor ring Border, protect the health of people;
(5), the present invention add plants essential oil in the feed, extracted from natural plants, plant itself to human body without any injury, It can suppress and remove the bacterium in space, also act as net taste effect, volatilization is slow, and continuation is long, easy to use;
(6), the present invention add extracts of Chinese herbal medicine in the feed, it is environment-protecting and non-poisonous, various pathogens can be killed, prevent pathogenic bacteria from passing through Cross air, droplet transmission and the cross-infection to keep off infection.
Embodiment
With reference to specific embodiment, the present invention is expanded on further.These embodiments are merely to illustrate the present invention and not had to In limitation the scope of the present invention.
Embodiment 1
A kind of indoor air disinfectant, include the raw material of following part meter:45 parts of extracts of Chinese herbal medicine, 35 parts of bactericide, plant essence 75 parts of 32 parts of oil, 20 parts of activated particle, 17 parts of auxiliary agent and deionized water;
The extracts of Chinese herbal medicine includes the raw material of following part meter:15 parts of Chinese gall, 12 parts of the coptis, the white palm 10 parts, 7 parts of honeysuckle 4 parts of magnolia obovata;
The bactericide includes the raw material of following part meter:15 parts of stability carrier, 12 parts of nano zine oxide, nanometer titanium dioxide carbon 10 Part, 8 parts of nano silicon, 8 parts of chlorine dioxide and 20 parts of deionized water;
The plants essential oil includes the raw material of following part meter:8 parts of 12 parts of wormwood essential oil, 10 parts of Peppermint essential oil and Lavender;
The auxiliary agent includes the raw material of following part meter:8 parts of cationic surfactant, 6 parts of preservative, 4 parts of thickener and scattered 3 parts of agent.
Wherein, the preparation method of the wormwood essential oil is:Take wormwood and crush, cross 80 mesh sieves and obtain wormwood powder, add The ethanol solution of 10 times of mass parts, 8h is soaked, the concentration of ethanol solution is 45%, Microwave Extraction 40min, microwave after immersion Power is 500W, and extraction is filtered after terminating, and by filtrate concentrated by rotary evaporation untill without alcohol taste, obtains the wormwood essential oil.
Wherein, the preparation method of the Peppermint essential oil is:Take dried peppermint leaf and crush, cross 110 mesh sieves and obtain dried peppermint leaf powder, The ethanol solution of 4 times of mass parts is added, soaks 6h, the concentration of ethanol solution is 30%, and immersion is finished after super under 50 degrees Celsius Sound extracts 30min, after extraction terminates, filtering, filtrate is rotated into concentrated by rotary evaporation, the Peppermint essential oil is obtained untill without alcohol taste.
Wherein, the preparation method of the Lavender is:Take lavender and crush, cross 50 mesh sieves and obtain lavender powder End, it is placed in beaker, adds the deionized water of 2 times of parts by weight, be placed on electric furnace and heat 40min, after cooling, entered with Buchner funnel Row filters, and retains filtrate and obtains the Lavender.
Wherein, the activated particle is citric acid.
Wherein, the stability carrier is diatomite.
Wherein, the cationic surfactant is quarternary ammonium salt compound, and the thickener is hydroxypropyl methyl cellulose, The preservative is methylisothiazolinone, and the dispersant is calgon.
A kind of preparation method of indoor air disinfectant is provided in the present embodiment, comprised the following steps:
(1), prepare extracts of Chinese herbal medicine
Chinese gall, the coptis, the white palm, honeysuckle magnolia obovata are weighed according to proportioning, is crushed and crosses 40 mesh sieves, it is well mixed to obtain Pulvis;
Ultrasonic assistant ethanol extraction is carried out to pulvis, 35% ethanol of 10 times of parts by weight is added into pulvis, in ultrasonic assistant Under effect, refluxing extraction 20min under 60 degrees celsius, extract 3 times, the filtrate of extraction is merged, after 6h is placed in refrigeration, 55 Be concentrated under reduced pressure recovery ethanol under degrees celsius, and it is the extracts of Chinese herbal medicine to obtain concentrate, standby;
(2), prepare bactericide
Chlorine dioxide is dissolved in deionized water, then sequentially adds stability carrier, nano zine oxide, nano-silica according to proportioning Change carbon and nano silicon, be well mixed, obtain the bactericide;
(3), by step(1)Obtained extracts of Chinese herbal medicine and step(2)Obtained bactericide mixing, then according to proportioning successively Surplus stock is added, is stirred with 200r/min rotating speed, obtains the indoor air disinfectant.
Embodiment 2
A kind of indoor air disinfectant, include the raw material of following part meter:55 parts of extracts of Chinese herbal medicine, 36 parts of bactericide, plant essence 80 parts of 33 parts of oil, 25 parts of activated particle, 19 parts of auxiliary agent and deionized water;
The extracts of Chinese herbal medicine includes the raw material of following part meter:17 parts of Chinese gall, 13 parts of the coptis, the white palm 11 parts, 9 parts of honeysuckle 6 parts of magnolia obovata;
The bactericide includes the raw material of following part meter:17 parts of stability carrier, 13 parts of nano zine oxide, nanometer titanium dioxide carbon 11 Part, 9 parts of nano silicon, 9 parts of chlorine dioxide and 23 parts of deionized water;
The plants essential oil includes the raw material of following part meter:9 parts of 13 parts of wormwood essential oil, 11 parts of Peppermint essential oil and Lavender;
The auxiliary agent includes the raw material of following part meter:9 parts of cationic surfactant, 8 parts of preservative, 5 parts of thickener and scattered 4 parts of agent.
Wherein, the preparation method of the wormwood essential oil is:Take wormwood and crush, cross 90 mesh sieves and obtain wormwood powder, add The ethanol solution of 15 times of mass parts, 10h is soaked, the concentration of ethanol solution is 50%, and Microwave Extraction 50min, micro- after immersion Wave power is 600W, and extraction is filtered after terminating, and by filtrate concentrated by rotary evaporation untill without alcohol taste, obtains the wormwood essential oil.
Wherein, the preparation method of the Peppermint essential oil is:Take dried peppermint leaf and crush, cross 120 mesh sieves and obtain dried peppermint leaf powder, The ethanol solution of 6 times of mass parts is added, soaks 8h, the concentration of ethanol solution is 50%, and immersion is finished after super under 55 degrees Celsius Sound extracts 40min, after extraction terminates, filtering, filtrate is rotated into concentrated by rotary evaporation, the Peppermint essential oil is obtained untill without alcohol taste.
Wherein, the preparation method of the Lavender is:Take lavender and crush, cross 80 mesh sieves and obtain lavender powder End, it is placed in beaker, adds the deionized water of 3 times of parts by weight, be placed on electric furnace and heat 50min, after cooling, entered with Buchner funnel Row filters, and retains filtrate and obtains the Lavender.
Wherein, the activated particle is tartaric acid.
Wherein, the stability carrier is sepiolite.
Wherein, the cationic surfactant is quarternary ammonium salt compound, and the thickener is hydroxypropyl methyl cellulose, The preservative is methylisothiazolinone, and the dispersant is calgon.
A kind of preparation method of indoor air disinfectant is provided in the present embodiment, comprised the following steps:
(1), prepare extracts of Chinese herbal medicine
Chinese gall, the coptis, the white palm, honeysuckle magnolia obovata are weighed according to proportioning, is crushed and crosses 60 mesh sieves, it is well mixed to obtain Pulvis;
Ultrasonic assistant ethanol extraction is carried out to pulvis, 45% ethanol of 15 times of parts by weight is added into pulvis, in ultrasonic assistant Under effect, refluxing extraction 30min under 80 degrees celsius, extract 3 times, the filtrate of extraction is merged, after 8h is placed in refrigeration, Be concentrated under reduced pressure recovery ethanol under 85 degrees celsius, and it is the extracts of Chinese herbal medicine to obtain concentrate, standby;
(2), prepare bactericide
Chlorine dioxide is dissolved in deionized water, then sequentially adds stability carrier, nano zine oxide, nano-silica according to proportioning Change carbon and nano silicon, be well mixed, obtain the bactericide;
(3), by step(1)Obtained extracts of Chinese herbal medicine and step(2)Obtained bactericide mixing, then according to proportioning successively Surplus stock is added, is stirred with 300r/min rotating speed, obtains the indoor air disinfectant.
Embodiment 3
A kind of indoor air disinfectant, include the raw material of following part meter:50 parts of extracts of Chinese herbal medicine, 35.5 parts of bactericide, plant 77.5 parts of 32.5 parts of essential oil, 22.5 parts of activated particle, 18 parts of auxiliary agent and deionized water;
The extracts of Chinese herbal medicine includes the raw material of following part meter:16 parts of Chinese gall, 12.5 parts of the coptis, the white palm 10.5 parts, gold and silver Spend 8 parts of 5 parts of magnolia obovatas;
The bactericide includes the raw material of following part meter:16 parts of stability carrier, 12.5 parts of nano zine oxide, nanometer titanium dioxide carbon 21.5 parts of 10.5 parts, 8.5 parts of nano silicon, 8.5 parts of chlorine dioxide and deionized water;
The plants essential oil includes the raw material of following part meter:12.5 parts of wormwood essential oil, 10.5 parts of Peppermint essential oil and Lavender 8.5 part;
The auxiliary agent includes the raw material of following part meter:8.5 parts of cationic surfactant, 7 parts of preservative, 4.5 parts of thickener and 3.5 parts of dispersant.
Wherein, the preparation method of the wormwood essential oil is:Take wormwood and crush, cross 85 mesh sieves and obtain wormwood powder, add The ethanol solution of 12 times of mass parts, 9h is soaked, the concentration of ethanol solution is 47%, Microwave Extraction 45min, microwave after immersion Power is 550W, and extraction is filtered after terminating, and by filtrate concentrated by rotary evaporation untill without alcohol taste, obtains the wormwood essential oil.
Wherein, the preparation method of the Peppermint essential oil is:Take dried peppermint leaf and crush, cross 115 mesh sieves and obtain dried peppermint leaf powder, The ethanol solution of 5 times of mass parts is added, soaks 7h, the concentration of ethanol solution is 40%, and immersion is finished after super under 52 degrees Celsius Sound extracts 35min, after extraction terminates, filtering, filtrate is rotated into concentrated by rotary evaporation, the Peppermint essential oil is obtained untill without alcohol taste.
Wherein, the preparation method of the Lavender is:Take lavender and crush, cross 70 mesh sieves and obtain lavender powder End, it is placed in beaker, adds the deionized water of 2 times of parts by weight, be placed on electric furnace and heat 45min, after cooling, entered with Buchner funnel Row filters, and retains filtrate and obtains the Lavender.
Wherein, the activated particle is oxalic acid.
Wherein, the stability carrier is zeolite.
Wherein, the cationic surfactant is quarternary ammonium salt compound, and the thickener is hydroxypropyl methyl cellulose, The preservative is methylisothiazolinone, and the dispersant is calgon.
A kind of preparation method of indoor air disinfectant is provided in the present embodiment, comprised the following steps:
(1), prepare extracts of Chinese herbal medicine
Chinese gall, the coptis, the white palm, honeysuckle magnolia obovata are weighed according to proportioning, is crushed and crosses 50 mesh sieves, it is well mixed to obtain Pulvis;
Ultrasonic assistant ethanol extraction is carried out to pulvis, 40% ethanol of 12 times of parts by weight is added into pulvis, in ultrasonic assistant Under effect, refluxing extraction 25min under 70 degrees celsius, extract 3 times, the filtrate of extraction is merged, after 7h is placed in refrigeration, 75 Be concentrated under reduced pressure recovery ethanol under degrees celsius, and it is the extracts of Chinese herbal medicine to obtain concentrate, standby;
(2), prepare bactericide
Chlorine dioxide is dissolved in deionized water, then sequentially adds stability carrier, nano zine oxide, nano-silica according to proportioning Change carbon and nano silicon, be well mixed, obtain the bactericide;
(3), by step(1)Obtained extracts of Chinese herbal medicine and step(2)Obtained bactericide mixing, then according to proportioning successively Surplus stock is added, is stirred with 250r/min rotating speed, obtains the indoor air disinfectant.
The present invention is described in detail with reference to the foregoing embodiments, for those skilled in the art, its according to The technical scheme described in foregoing embodiments can so be modified, or which part technical characteristic is equally replaced Change.Within the spirit and principles of the invention, any modification, equivalent substitution and improvements made etc., should be included in the present invention Protection domain within.

Claims (9)

1. a kind of indoor air disinfectant, it is characterised in that include the raw material of following part meter:45 ~ 55 parts of extracts of Chinese herbal medicine, kill 75 ~ 80 parts of 35 ~ 36 parts of microbial inoculum, 32 ~ 33 parts of plants essential oil, 20 ~ 25 parts of activated particle, 17 ~ 19 parts of auxiliary agent and deionized water;
The extracts of Chinese herbal medicine includes the raw material of following part meter:15 ~ 17 parts of Chinese gall, 12 ~ 13 parts of the coptis, in vain slap 10 ~ 11 parts, 7 ~ 9 parts of honeysuckle, 4 ~ 6 parts of magnolia obovata;
The bactericide includes the raw material of following part meter:15 ~ 17 parts of stability carrier, 12 ~ 13 parts of nano zine oxide, nano-silica Change 20 ~ 23 parts of 10 ~ 11 parts of carbon, 8 ~ 9 parts of nano silicon, 8 ~ 9 parts of chlorine dioxide and deionized water;
The plants essential oil includes the raw material of following part meter:12 ~ 13 parts of wormwood essential oil, 10 ~ 11 parts of Peppermint essential oil and lavender essence 8 ~ 9 parts of oil;
The auxiliary agent includes the raw material of following part meter:8 ~ 9 parts of cationic surfactant, 6 ~ 8 parts of preservative, 4 ~ 5 parts of thickener With 3 ~ 4 parts of dispersant.
2. indoor air disinfectant according to claim 1, it is characterised in that include the raw material of following part meter:Chinese herbal medicine 50 parts of extract solution, 35.5 parts of bactericide, 32.5 parts of plants essential oil, 22.5 parts of activated particle, 18 parts of auxiliary agent and deionized water 78.5 Part;
The extracts of Chinese herbal medicine includes the raw material of following part meter:16 parts of Chinese gall, 12.5 parts of the coptis, the white palm 10.5 parts, gold and silver Spend 8 parts of 5 parts of magnolia obovatas;
The bactericide includes the raw material of following part meter:16 parts of stability carrier, 12.5 parts of nano zine oxide, nanometer titanium dioxide carbon 21.5 parts of 10.5 parts, 8.5 parts of nano silicon, 8.5 parts of chlorine dioxide and deionized water;
The plants essential oil includes the raw material of following part meter:12.5 parts of wormwood essential oil, 10.5 parts of Peppermint essential oil and Lavender 8.5 part;
The auxiliary agent includes the raw material of following part meter:8.5 parts of cationic surfactant, 7 parts of preservative, 4.5 parts of thickener and 3.5 parts of dispersant.
3. indoor air disinfectant according to claim 1, it is characterised in that the preparation method of the wormwood essential oil is: Take wormwood and crush, cross 80 ~ 90 mesh sieves and obtain wormwood powder, add the ethanol solution of 10 ~ 15 times of mass parts, soak 8 ~ 10h, second The concentration of alcoholic solution is 45 ~ 50%, and 40 ~ 50min of Microwave Extraction after immersion, microwave power is 500 ~ 600W, and extraction terminates After filter, by filtrate concentrated by rotary evaporation untill without alcohol taste, obtain the wormwood essential oil.
4. indoor air disinfectant according to claim 1, it is characterised in that the preparation method of the Peppermint essential oil is: Take dried peppermint leaf and crush, cross 110 ~ 120 mesh sieves and obtain dried peppermint leaf powder, add the ethanol solution of 4 ~ 6 times of mass parts, immersion 6 ~ 8h, the concentration of ethanol solution is 30 ~ 50%, and immersion finishes to be terminated after 50 ~ 55 degrees Celsius of lower 30 ~ 40min of ultrasonic extraction, extraction Afterwards, filter, filtrate is rotated into concentrated by rotary evaporation, the Peppermint essential oil is obtained untill without alcohol taste.
5. indoor air disinfectant according to claim 1, it is characterised in that the preparation method of the Lavender For:Take lavender and crush, cross 50 ~ 80 mesh sieves and obtain lavender powder, be placed in beaker, add 2 ~ 3 times of parts by weight go from Sub- water, 40 ~ 50min of heating on electric furnace is placed on, after cooling, is filtered with Buchner funnel, retained filtrate and obtain the lavender Essential oil.
6. indoor air disinfectant according to claim 1, it is characterised in that the activated particle is citric acid, winestone One or more in acid, oxalic acid, boric acid, sulfamic acid and sodium dihydrogen phosphate.
7. indoor air disinfectant according to claim 1, it is characterised in that the stability carrier is diatomite, sea One or more in afrodite, zeolite and silica.
8. indoor air disinfectant according to claim 1, it is characterised in that the cationic surfactant is quaternary ammonium Salt compound, the thickener are hydroxypropyl methyl cellulose, and the preservative is methylisothiazolinone, and the dispersant is Calgon.
A kind of 9. preparation method of indoor air disinfectant according to any one of claim 1 ~ 8, it is characterised in that including Following steps:
(1), prepare extracts of Chinese herbal medicine
Chinese gall, the coptis, the white palm, honeysuckle magnolia obovata are weighed according to proportioning, is crushed and crosses 40~60 mesh sieves, be well mixed Obtain pulvis;
Ultrasonic assistant ethanol extraction is carried out to pulvis, 35 ~ 45% ethanol of 10~15 times of parts by weight are added into pulvis, super Under sound wave booster action, 20~30min of refluxing extraction under 60~80 degrees celsius, extract 3 times, the filtrate of extraction merged, After 6~8h is placed in refrigeration, be concentrated under reduced pressure recovery ethanol under 55~85 degrees celsius, and it is the Chinese herbal medicine to obtain concentrate Extract solution, it is standby;
(2), prepare bactericide
Chlorine dioxide is dissolved in deionized water, then sequentially adds stability carrier, nano zine oxide, nano-silica according to proportioning Change carbon and nano silicon, be well mixed, obtain the bactericide;
(3), by step(1)Obtained extracts of Chinese herbal medicine and step(2)Obtained bactericide mixing, then according to proportioning successively Surplus stock is added, is stirred with 200 ~ 300r/min rotating speed, obtains the indoor air disinfectant.
CN201710563328.8A 2017-07-12 2017-07-12 A kind of indoor air disinfectant and preparation method thereof Withdrawn CN107333813A (en)

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CN108079355A (en) * 2017-12-08 2018-05-29 英德市东顺精细化工实业有限公司 A kind of extracting method of Chinese herbal medicine extract for air freshener
CN108144097A (en) * 2018-03-16 2018-06-12 广州市凯卫莎环保科技有限公司 Fragrant essential oil and preparation method and application
CN108295654A (en) * 2018-02-07 2018-07-20 合肥华盖生物科技有限公司 A kind of plant source indoor air purification agent and preparation method thereof
CN108295642A (en) * 2018-03-18 2018-07-20 国润生物科技(深圳)有限公司 A kind of efficiently removal sulfur-bearing contamination gas build air purifying preparation composition
CN108552239A (en) * 2018-05-23 2018-09-21 马鞍山市金农牧业有限公司 A kind of livestock-raising disinfection formula of liquid
CN108782628A (en) * 2018-07-30 2018-11-13 合肥华盖生物科技有限公司 A kind of pure and fresh disinfectant of environment-friendly type air and preparation method thereof
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CN110271391A (en) * 2019-07-24 2019-09-24 广州市佰分佰环境治理有限公司 A kind of vehicle-mounted air purification magic square and its application method
CN110432290A (en) * 2019-08-19 2019-11-12 三门华迈化工产品有限公司 Compound central air conditioner system fungicide
CN111248235A (en) * 2020-03-14 2020-06-09 王立强 Chinese and western medicine compound disinfectant/bacteriostatic agent capable of killing coronavirus and preparation method thereof
CN111296508A (en) * 2020-03-20 2020-06-19 呼和浩特市万登环境科技有限公司 Disinfectant for indoor air disinfection
CN111330387A (en) * 2020-03-31 2020-06-26 上海开亿信息科技有限公司 Nano chlorine dioxide air filter element material, preparation method, air filter element and module
CN111449092A (en) * 2020-04-14 2020-07-28 深圳大学总医院 Preparation method of disinfectant for emergency diagnosis room
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CN112352785A (en) * 2020-10-29 2021-02-12 青岛翼科新程生物科技有限公司 Chlorine dioxide nano zinc disinfection and bacteriostasis tablet
CN112369430A (en) * 2020-11-04 2021-02-19 青岛翼科新程生物科技有限公司 Chlorine dioxide nano zinc disinfection and bacteriostasis solution
CN112641987A (en) * 2019-10-12 2021-04-13 苏州淳雨净化科技有限公司 Sterilization equipment and sterilization system for enclosed space
CN113509582A (en) * 2021-04-19 2021-10-19 湖南普泰尔环境股份有限公司 Preparation method of composite deodorant containing natural plant extract
CN114011377A (en) * 2021-07-13 2022-02-08 武汉晏合环境科学技术有限公司 Air sterilizing and purifying material and preparation method thereof

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CN108079355A (en) * 2017-12-08 2018-05-29 英德市东顺精细化工实业有限公司 A kind of extracting method of Chinese herbal medicine extract for air freshener
CN108295654A (en) * 2018-02-07 2018-07-20 合肥华盖生物科技有限公司 A kind of plant source indoor air purification agent and preparation method thereof
CN108144097A (en) * 2018-03-16 2018-06-12 广州市凯卫莎环保科技有限公司 Fragrant essential oil and preparation method and application
CN108295642A (en) * 2018-03-18 2018-07-20 国润生物科技(深圳)有限公司 A kind of efficiently removal sulfur-bearing contamination gas build air purifying preparation composition
CN108552239A (en) * 2018-05-23 2018-09-21 马鞍山市金农牧业有限公司 A kind of livestock-raising disinfection formula of liquid
CN108782628A (en) * 2018-07-30 2018-11-13 合肥华盖生物科技有限公司 A kind of pure and fresh disinfectant of environment-friendly type air and preparation method thereof
CN109045956A (en) * 2018-08-07 2018-12-21 赵文辉 A kind of vaccary deodorizing disinfectant and preparation method thereof
CN110271391A (en) * 2019-07-24 2019-09-24 广州市佰分佰环境治理有限公司 A kind of vehicle-mounted air purification magic square and its application method
CN110432290A (en) * 2019-08-19 2019-11-12 三门华迈化工产品有限公司 Compound central air conditioner system fungicide
CN112641987A (en) * 2019-10-12 2021-04-13 苏州淳雨净化科技有限公司 Sterilization equipment and sterilization system for enclosed space
CN111248235A (en) * 2020-03-14 2020-06-09 王立强 Chinese and western medicine compound disinfectant/bacteriostatic agent capable of killing coronavirus and preparation method thereof
CN111296508A (en) * 2020-03-20 2020-06-19 呼和浩特市万登环境科技有限公司 Disinfectant for indoor air disinfection
CN111330387A (en) * 2020-03-31 2020-06-26 上海开亿信息科技有限公司 Nano chlorine dioxide air filter element material, preparation method, air filter element and module
CN111449092A (en) * 2020-04-14 2020-07-28 深圳大学总医院 Preparation method of disinfectant for emergency diagnosis room
CN111771907A (en) * 2020-08-03 2020-10-16 中山大学 Antivirus nano material for slowly releasing chlorine dioxide and preparation method and application thereof
CN112352785A (en) * 2020-10-29 2021-02-12 青岛翼科新程生物科技有限公司 Chlorine dioxide nano zinc disinfection and bacteriostasis tablet
CN112369430A (en) * 2020-11-04 2021-02-19 青岛翼科新程生物科技有限公司 Chlorine dioxide nano zinc disinfection and bacteriostasis solution
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Application publication date: 20171110