CN105504966B - A kind of offset litho printing ink - Google Patents

A kind of offset litho printing ink Download PDF

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Publication number
CN105504966B
CN105504966B CN201610093677.3A CN201610093677A CN105504966B CN 105504966 B CN105504966 B CN 105504966B CN 201610093677 A CN201610093677 A CN 201610093677A CN 105504966 B CN105504966 B CN 105504966B
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weight
parts
essential oil
oil
extraction
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CN201610093677.3A
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CN105504966A (en
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魏本武
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唐玉乐
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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/50Improvements relating to the production of products other than chlorine, adipic acid, caprolactam, or chlorodifluoromethane, e.g. bulk or fine chemicals or pharmaceuticals
    • Y02P20/54Improvements relating to the production of products other than chlorine, adipic acid, caprolactam, or chlorodifluoromethane, e.g. bulk or fine chemicals or pharmaceuticals characterised by the solvent
    • Y02P20/544Supercritical solvents, e.g. supercritical H2O or CO2

Abstract

A kind of offset litho printing ink can not only discharge negative aeroion for a long time, purify air, be conducive to health;Also there are certain inhibition, killing effect to a variety of germs such as staphylococcus, Escherichia coli, gram-positive bacteria and fungi;Simultaneously fragrant odour, pure and fresh to soothe the spirit, pressure of releiving can leave lasting fragrance after use, have refresh the mind, the health-care efficacy of dispelling fatigue, be suitable for each age groups, have very extensive application prospect.

Description

A kind of offset litho printing ink

Technical field

The present invention relates to a kind of ink, more particularly to a kind of offset litho printing ink.

Background technology

Ink is a kind of common consumptive material, can be used for routine office work or textile printing field, but traditional general ink is only There is writing function, without refreshing oneself and generating the health-care effects such as anion, user, which uses to use when long, generates taediumvitae, due to Conventional inks have a single function, and have been unable to meet the multi-demands of people.

Invention content

In view of the deficienciess of the prior art, for the user of ink to provide a kind of smell pure and fresh by the present invention, have and refresh oneself The ink of effect and negative ion health effect, it can not only discharge negative aeroion for a long time, purify air, strong conducive to human body Health;Also there are certain inhibition, killing effect to a variety of germs such as staphylococcus, Escherichia coli, gram-positive bacteria and fungi;Together When fragrant odour, pure and fresh to soothe the spirit, pressure of releiving, can also expelling mosquito, harmful effect will not be generated to human body, had very extensive Application prospect.

The purpose of the present invention is what is be achieved through the following technical solutions:

A kind of offset litho printing ink, it is characterised in that:By weight by following component:23 weight of dispersible pigment color paste Part, 19 parts by weight of bisphenol-A, 4.5 parts by weight of glycerine, 2.3 parts by weight of anhydrous sodium sulfate, 2.7 parts by weight of triethanolamine, triethylamine 3.3 parts by weight, 3.6 parts by weight of acetone, 0.25 parts by weight of double thiocarbamates, 1.7 parts by weight of active mineral matter powder, surface 1.2 parts by weight of activating agent compound, 0.55 parts by weight of sustained release agent, 3.85 parts by weight of essential oil of traditional Chinese medicine, 62 parts by weight of deionized water, institute The pigment for stating mill base is high-carbon black pigment, and the average grain diameter of the dispersible pigment color paste is 75nm, and the active mineral matter powder is germanium Stone, fluorite, tourmaline, gahnite are by weight 2.5:3:3.7:2 mixture, wherein tourmaline are dravite and lithium electricity Gas stone is by weight 5:3 mixture, grain size≤13 μm of the active mineral matter powder, wherein the essential oil of traditional Chinese medicine passes through such as Lower step is prepared,

S1,35 parts by weight of fly expelling plum are taken to clean, naturally dry is subsequently placed in 90 DEG C of frying pans and fries to savory effusion, so 17 parts by weight of Air washer afterwards are placed in 60 DEG C or less drying, water content≤6.5% in constant temperature oven;

S2,21 parts by weight of perilla leaf are cleaned, is put into brine and impregnates 3.5 hours, salt water is is impregnated spice quality 3.7 times, be put into pot and steam saturating, take out, dry, a concentration of the 27% of brine;

S3, by 17 parts by weight of lavender, 4 parts by weight of anemone vitifolia, 1.5 parts by weight of Moschus, 2 parts by weight of marjoram, 1 parts by weight decontamination of ambergris puts into micronizer together with the made bulk pharmaceutical chemicals of step S1 and S2 and is crushed to 60 mesh, is made Bulk pharmaceutical chemicals powder, it is spare;

S4, bulk pharmaceutical chemicals powder obtained in step S3 is put into the extraction kettle of supercritical carbon dioxide extraction apparatus, is adjusted Save extracting pressure 27.65MPa, 45.10 DEG C of extraction temperature, carbon dioxide flow 0.6m3/ h, dynamic extraction 2.5h, directly exists Separating still outlet triangular flask collection volatile oil A, it is spare;

S5, by 7 parts by weight of elm bark, 5 parts by weight of cordate houttuynia, 4.5 parts by weight of corydlis bungeana, 3.5 parts by weight of agalloch eaglewood, camphorwood 11 parts by weight, 3 parts by weight of calamus, 1.75 parts by weight of peppermint clean drying, put into micronizer be crushed to 70 mesh together, so Afterwards plus deionized water is impregnated 6 hours, and amount of water is institute 6.5 times of immersion bulk pharmaceutical chemicals quality, is dispersed with stirring and mixes well, and obtained Chinese medicine mixes Object is closed, it is spare;

S6, Traditional Chinese drug mixture made from step S5 is decocted 2 hours in 80 DEG C, collects distillate, and ether extraction is added, The volume ratio of distillate and ether is 2:1, then plus anhydrous sodium sulfate drying upper oil phase is taken, obtains volatile oil B, it is spare;

S7, the made volatile oil A of step S4 and S6 and volatile oil B are mixed and mix well obtained miscella, then while stirring successively Wheat malt essential oil, Geranium Essential, snow lotus herb soap essential oil, lemon and grapefruit essential oil is added, is sufficiently stirred 35 minutes, stands It 30 minutes, is sufficiently stirred and mixes well, filtering and impurity removing is to get essential oil of traditional Chinese medicine, wherein the miscella and wheat malt essential oil, fish pelargonium Essential oil, snow lotus herb soap essential oil, lemon and grapefruit essential oil mass ratio be 1.3:0.4:0.75:0.6:0.5:0.3.

In a preferred embodiment, also include 1.3 parts by weight of origanum oil and white flower in the bulk pharmaceutical chemicals powder of step S3 1.5 parts by weight of Dalmatian chrysanthemum.

In a preferred embodiment, in the Traditional Chinese drug mixture of step S5 also include 0.6 parts by weight of borneol and lotus leaf 0.4 Parts by weight.

In a preferred embodiment, in the essential oil of traditional Chinese medicine of step S7 also include 0.3 parts by weight of eucalyptus oil.

Equipment, raw material and method according to the present invention, are equipment, raw material and method that the industry usually uses, This is repeated no more.

Wherein each essential oil component must be sufficiently mixed with surfactant, sustained release agent, to reach slow release effect, each essential oil and The additive amount of anion natural mineral powder is had in right amount, not only antibiotic and sterilizing, moreover it is possible to stable mood, so to the not normal heart Reason state has positive effect, can purify, pacify soul, can mitigate indignation and beaten feeling, making one can be with the flat gas of the heart It is helpful to alarmed and dejected state because it can balance nervous centralis with ground in face of living, also have apparent flat It is quiet with releive function, there is fairly good easypro put to be consoled with spirit insomniac, for pacify it is hot-tempered into or moody temper have Fairly good effect, can be improved working efficiency.

The present invention refers to modern Chinese medicine pharmacological research, verifies from the drug screening of existing Chinese medicine and repeatedly, gives full play to respectively Group parts by weight synergistic effect, wherein each traditional Chinese medicinal components are described as follows.

Fly expelling plum:Verenaceae Lantana, belongs to perennial plant, evergreen half tendril shrub, four prismatic of sprig, it is long and under Hanging down has reverse sharp thorn, and the smell of mosquitos and flies sensitivity is volatilized in its branches and leaves and flower, has effects that very strong expulsion mosquitos and flies, And to human body without any injury, there is " mosquito repellent seven becomes flower " good reputation.

Perilla leaf:For the dried leaf of labiate purple perilla(Or with spray), there is relieving exterior syndrome and dispelling cold, the work(of relieving QI stagnancy in the stomach Effect is used for anemofrigid cold, and evil of vomitting of coughing has inhibiting effect to staphylococcus.

Lavender can remove ant, except roach, except mite, when being placed under wardrobe, pillow, can not only replace camphor ball, moreover it is possible to stay The fragrance of one lower people that oozes, research find that it is lavender that lavender, which has apparent antibacterial action, the linalool contained in lavender, The main component of antibacterial, it can inhibit 17 kinds of bacteriums(Including gram-negative bacteria and gram-positive bacteria), 10 kinds of fungies life It is long.

Anemone vitifolia:①《Shaanxi Chinese herbal medicine》:" it is bitter, it is cool, it is slightly poisonous.”②《Often use Chinese herbal medicine in Sichuan》:" toil, temperature, It is slightly poisonous." removing toxic substances, apocenosis myogenic, scattered stasis detumescence, with maggot, wriggler, change product is killed, detumescence dissipates the stasis of blood, controls stubborn dermatitis, the favus of the scalp, malaria Disease, infantile malnutrition, dysentery, carbuncle furuncle sore is swollen, scrofula, traumatic injury.

Elm bark:It is sweet, flat for the dry bark or root skin of Ulmaceae, it is nontoxic;Li Shui, treating stranguria, detumescence is used for urine It is obstructed, stranguria with turbid discharge, oedema, ulcer carbuncle on the back, erysipelas, mange.

Cordate houttuynia:Have the effects that antibacterial, antiviral, raising immunity of organisms, to various microorganisms(Especially saccharomycete And mould)There is inhibiting effect, to the streptococcus of hemolytic, staphylococcus aureus, Bacillus influenzae, micrococcus catarrhalis, pneumonia ball Bacterium has apparent inhibiting effect.Also there is effect to Escherichia coli, shigella dysenteriae, typhoid bacillus.

Corydlis bungeana:For the herb of bloodroot corydalis bungeana, to alpha streptococcus, pneumococcus, micrococcus catarrhalis, dysentery Bacillus, Escherichia coli, Pseudomonas aeruginosa have inhibition, also have inhibiting effect to parainfluenza Sendai virus.

Agalloch eaglewood:" Compendium of Materia Medica " records wood, and there is strong antibacterial efficacy, fragrance to enter spleen, clear refreshing qi-regulating, tonifying five zang organs, cough-relieving Resolving sputum, ventilation analgesic therapy, can be used as medicine at warm stomach temperature spleen, be first-class medicinal material superfine product.

Camphorwood:Aiphyllium, bark yellowish-brown have an irregular longitudinal crack, on the south main product the Changjiang river and southwestern various regions.Winter It cuts down trees and splits broken or be sawn into bulk, dry or air-dry.Timber bulk is not of uniform size, surface rufous to burgundy, and cross section is visible Annual ring.Matter is heavy and hard.There is strong camphor fragrance, taste is refrigerant, there is pungent sense, warm-natured, acrid flavour;Can it is sensible ward off dirty, warm in pain, Dampness removing desinsection.

Calamus:It spends, stem aromatic flavour, have effects that have one's ideas straightened out, eliminating the phlegm, relieve heat, the epidemic disease that can dispel intelligence development keeps fit and healthy, can Make fragrance or mosquito dispersing.

Peppermint:For the dry aerial parts of labiate peppermint, dispelling wind and heat from the body, head clearing, relieving sore-throat promoting eruption, soothing the liver row Gas.

Moschus:The effect of with having one's ideas straightened out, warding off dirty, dredging collateral, dissipating the stasis of blood;Control apoplexy, coma due to blocking of the respiratory system, frightened epilepsy, middle evil unhappiness, Xin Fubao The pain, Disorder lump in the abdomen hypochondriac lumps, traumatic injury, swollen ulcer drug.《This warp》:Master wards off bad odor, a kind of malaria, and epilepsy convulsion goes three worms.

Marjoram:Can improve that mood is depressed and addictive disease, it is especially effective to liberal-mindedness and vigorous endurance stress symptom, can expand blood vessel, Blood pressure lowering, mitigation and burden, help eliminate palpitaition, have excellent nerve to pacify and calm function.

Ambergris:It is the most lasting fragrance of lasting, any type fragrance cannot all compare favourably therewith in the world, be known as " dragon The perfume of saliva coexists with life " saying.《Compendium of Materia Medica》It carries:It can invigorate blood circulation, benefiting quintessence, supporing yang road, promoting blood circulation, resolving sputum is flat Asthma;A lump in the abdomen causing distension and pain;Trusted subordinate's pain;Coma;Liao Yongyan:Promoting diuresis for stranguria, San Disorder knots, knot of cooling down, by labor worm.

Wheat malt essential oil:There is overpowering odor to contain and enrich high unit vitamin e, is famous natural(Anti-corrosion Agent), the essential oil of each ingredient can be stablized, keep the effect of perfume more lasting.There is overpowering odor to contain and enrich high unit vitamin e, is Famous natural(Preservative), the essential oil of each ingredient can be stablized, keep the effect of perfume more lasting.

Geranium Essential:With hemostasis, vasoconstriction, asthma, liver and expelling toxin, gall stone, kidney toxin expelling, kidney stone, diuresis, flesh Carnic acid pain, Oily, aging skin activation, bleb, ochrodermia, weight-reducing promote to scab, eczema, sunburn of burning, tinea, the moon Through having some setbacks, engorgement of breasts inflammation mitigates melancholy uneasiness, has deodorization, antibacterial, the effect of sterilization.

Snow lotus herb soap essential oil:With physiological activity active ingredient.Wherein lanatechead saussurea herb with flower umbelliferone has apparent antibacterial, drop Pressure calmness, spasmolysis;Scopoletin has wind-dispelling, anti-inflammatory, analgesic, eliminating the phlegm and antitumor action, and clinically it is acute to treat asthma for the Chinese Chronic bronchitis effective percentage, which is 96.6% apiolin, has smooth muscle spasmolysis and anti-ulcer effect;Have obviously to antelope base benzophenone Choleretic effect.

Lemon:It is effective cardiotonic, commonly used in reducing blood pressure with biocidal efficacies.The characteristic energy of its antibacterial Mitigation has a sore throat, coughs, catching a cold and influenza, can mitigate headache, migraine, gout and arthritis.Feel hot agitation When, pure and fresh impression, help can be brought to clarify the state of mind, effectively improve working efficiency.

Grapefruit essential oil:Smell is pure and fresh, fragrant and sweet, there is the fruit flavor of citrus, has the benefits of heat-clearing, quench the thirst, can nurse tissue The disease of cell, increase muscle power, bronchitis of releiving, diuresis, oedema and lymph glandular system, it is anti-infective.Grapefruit essential oil may be used also With anti-melancholy, the symptoms such as melancholy or drowsy especially occurred in winter can make one to refresh, and be that seasonal spirit is lost The conditioning agent of tune.

Origanum oil:The herb of Labiatae origanum wild marjoram ORIGZNUM VUL-GAREL., also known as stop dysentery grass, wild chaste tree The ground such as mustard accord with name, with the extremely strong sterilization of heat-clearing, dampness elimination, driving away summer heat, inducing diaphoresis, qi-regulating, bacteriostasis, the volatilization extracted from wild marjoram Oil, cause enteritis bacterium common to 31 kinds and shigella flexneri are the pure Chinese medicine additives of most broad-spectrum antiseptic.

Chrysanthemum cinesariaefolium:Chrysanthemum artemisia(Tanacetum)The general designation of several plants, removing dampness and destroying parasites kill crab louse, head louse, body Lice, removes the effect of mosquito desinsection at flea.

Borneol:It is pungent, it is bitter, it is cool.With inducing resuscitation of having one's ideas straightened out, heat-clearing dissipates poison, removing nebula.Cure mainly high fever apoplexy coma due to blocking of the respiratory system shies epilepsy, middle wind phlegm It faints frightened epilepsy, summer-heat and damp blinds clear key, throat deafness, aphtha tooth swells, sore carbuncle infantile malnutrition due to digestive disturbances or intestinalparasites hemorrhoid, red eye, swell pain, pterygium.

Lotus leaf:For the leaf of nymphaeaceae plant lotus, there are clearing heat and detoxicating, cool blood, hemostasis.There is clearing summer-heat and damp, liter hair clearly Sun, cooling blood and hemostasis and other effects.

Eucalyptus oil:One of most common and widest essential oil of purposes has good health-care effect, helps focal attention Power.Sinus infection, influenza, bronchitis, cold nasal obstruction and other respiratory diseases can be effectively relieved.With good anti- Bacterium and sterilization idiocratic, in some certain foods, eucalyptus oil is also used as fragrance component.This essential oil is carried in travelling, it can be with Mosquito bite and insect bite is effectively resisted, skin measles are treated.It is good culicifuge.One kind can be become by, which being mixed with water, simply and effectively disappears Toxic agent.

Beneficial effects of the present invention:

The present invention provides that a kind of smell is pure and fresh for user, has effects that the ink of stimulating effect and negative ion health, it Negative aeroion can be not only discharged for a long time, purifies air, be conducive to health;Also to staphylococcus, Escherichia coli, the blue sun of leather A variety of germs such as property bacterium and fungi have certain inhibition, killing effect;Fragrant odour simultaneously, pure and fresh to soothe the spirit, pressure of releiving, also Can expelling mosquito, will not to human body generate harmful effect, be suitable for each age groups, add other function ingredients in right amount After still be able to keep original effect and quality.

1, tourmaline is a kind of silicate mineral, and chemical formula is Na (Mg, Fe, Mn, Li, Al) 3Al6 (Si6O18) (Bo3) 3 (OH, F) 4, it is contacted with hydrone under electrostatic field, can hydrone be ionized into hydrogen ion(H+)And hydrogen-oxygen Radical ion (OH-), hydroxide ion form basic hydroxide group anion with water molecules(H2O•OH-), as " air bear from Son ", scientific research at present proves:Anion can not only facilitate human body synthesis and vitamin storage, strengthen the life with human activin Reason activity has highly important influence to the vital movement of human body and other biological, is referred to as " air vitamin ".Anion Harmful substance in effective adsorption chamber, such as formaldehyde, toluene construction and decoration harmful substance, not only itself do not increase pollution, Er Qieqing Purifying room air is inherently eliminated construction and decoration syndrome, ensures that health is unaffected.

2, the traditional Chinese medicine ingredients contained in the present invention, it is not only thin to staphylococcus, tubercle bacillus, Pseudomonas aeruginosa, Grain-negative A variety of germs such as bacterium and gram-positive bacteria and fungi have certain inhibition, killing effect;Fragrant odour simultaneously, property is mild, It is pure and fresh to soothe the spirit, help hormone secretion, the effect of anxiety of releiving, while also there is certain mosquito-repelling effect, more it is essential that The present invention, which is used for a long time, to generate harmful effect to human body, be suitable for each age groups, before having very extensive application Scape.

Specific implementation mode

Embodiment.

A kind of offset litho printing ink, it is characterised in that:By weight by following component:23 weight of dispersible pigment color paste Part, 19 parts by weight of bisphenol-A, 4.5 parts by weight of glycerine, 2.3 parts by weight of anhydrous sodium sulfate, 2.7 parts by weight of triethanolamine, triethylamine 3.3 parts by weight, 3.6 parts by weight of acetone, 0.25 parts by weight of double thiocarbamates, 1.7 parts by weight of active mineral matter powder, surface 1.2 parts by weight of activating agent compound, 0.55 parts by weight of sustained release agent, 3.85 parts by weight of essential oil of traditional Chinese medicine, 62 parts by weight of deionized water, institute The pigment for stating mill base is high-carbon black pigment, and the average grain diameter of the dispersible pigment color paste is 75nm, and the active mineral matter powder is germanium Stone, fluorite, tourmaline, gahnite are by weight 2.5:3:3.7:2 mixture, wherein tourmaline are dravite and lithium electricity Gas stone is by weight 5:3 mixture, grain size≤13 μm of the active mineral matter powder, wherein the essential oil of traditional Chinese medicine passes through such as Lower step is prepared,

S1,35 parts by weight of fly expelling plum are taken to clean, naturally dry is subsequently placed in 90 DEG C of frying pans and fries to savory effusion, so 17 parts by weight of Air washer afterwards are placed in 60 DEG C or less drying, water content≤6.5% in constant temperature oven;

S2,21 parts by weight of perilla leaf are cleaned, is put into brine and impregnates 3.5 hours, salt water is is impregnated spice quality 3.7 times, be put into pot and steam saturating, take out, dry, a concentration of the 27% of brine;

S3, by 17 parts by weight of lavender, 4 parts by weight of anemone vitifolia, 1.5 parts by weight of Moschus, 2 parts by weight of marjoram, 1 parts by weight decontamination of ambergris puts into micronizer together with the made bulk pharmaceutical chemicals of step S1 and S2 and is crushed to 60 mesh, is made Bulk pharmaceutical chemicals powder, it is spare;

S4, bulk pharmaceutical chemicals powder obtained in step S3 is put into the extraction kettle of supercritical carbon dioxide extraction apparatus, is adjusted Save extracting pressure 27.65MPa, 45.10 DEG C of extraction temperature, carbon dioxide flow 0.6m3/ h, dynamic extraction 2.5h, directly exists Separating still outlet triangular flask collection volatile oil A, it is spare;

S5, by 7 parts by weight of elm bark, 5 parts by weight of cordate houttuynia, 4.5 parts by weight of corydlis bungeana, 3.5 parts by weight of agalloch eaglewood, camphorwood 11 parts by weight, 3 parts by weight of calamus, 1.75 parts by weight of peppermint clean drying, put into micronizer be crushed to 70 mesh together, so Afterwards plus deionized water is impregnated 6 hours, and amount of water is institute 6.5 times of immersion bulk pharmaceutical chemicals quality, is dispersed with stirring and mixes well, and obtained Chinese medicine mixes Object is closed, it is spare;

S6, Traditional Chinese drug mixture made from step S5 is decocted 2 hours in 80 DEG C, collects distillate, and ether extraction is added, The volume ratio of distillate and ether is 2:1, then plus anhydrous sodium sulfate drying upper oil phase is taken, obtains volatile oil B, it is spare;

S7, the made volatile oil A of step S4 and S6 and volatile oil B are mixed and mix well obtained miscella, then while stirring successively Wheat malt essential oil, Geranium Essential, snow lotus herb soap essential oil, lemon and grapefruit essential oil is added, is sufficiently stirred 35 minutes, stands It 30 minutes, is sufficiently stirred and mixes well, filtering and impurity removing is to get essential oil of traditional Chinese medicine, wherein the miscella and wheat malt essential oil, fish pelargonium Essential oil, snow lotus herb soap essential oil, lemon and grapefruit essential oil mass ratio be 1.3:0.4:0.75:0.6:0.5:0.3.

In a preferred embodiment, also include 1.3 parts by weight of origanum oil and white flower in the bulk pharmaceutical chemicals powder of step S3 1.5 parts by weight of Dalmatian chrysanthemum.

In a preferred embodiment, in the Traditional Chinese drug mixture of step S5 also include 0.6 parts by weight of borneol and lotus leaf 0.4 Parts by weight.

In a preferred embodiment, in the essential oil of traditional Chinese medicine of step S7 also include 0.3 parts by weight of eucalyptus oil.

The ink in the above-described embodiment is tested using air ion static method of testing, anion burst size is in 430-650 A/m3, and sustained release negative aeroion, it is more advantageous to long-term purification air, reaches the basic demand of health of people.

Reference examples.

Colour carbon black 20g, phenol 11g, glycerine 4g, benzotriazole 3g, triethanolamine 1g, triethylamine 3g, sodium bicarbonate 5g, polyoxyethylene groups ethers nonionic fluorocarbon surfactant 1.5g, sustained release agent 0.4g, marjoram essential oil 0.6g, wheat Bud essential oil 0.5g, Lavender 0.5g, RADIX PAEONIAE ALBA essential oil 0.4g, cypress essential oil 0. 4g, eucalyptus quintessence oil 0.4g, folium artemisiae argyi essence Oil 0. 4g, Peppermint essential oil 0.4g, deionized water 75g.

The ink in the above-mentioned reference examples is tested using air ion static method of testing, anion burst size is in 0/m3, Function without release negative aeroion.

(1)Acute toxicity test is carried out to obtained essential oil of traditional Chinese medicine, it is as a result as follows:

1. Mouse oral acute toxicity test:The LD50 of Mouse oral essential oil of traditional Chinese medicine be 383.55g/kg, 95% it is credible It is limited to 294.68g/kg~499.31g/kg.And the toxicity criterion of air freshener is:The anxious poison LD50 of Mouse oral >= 5g/kg is determined as nontoxic.The LD50 of this essential oil of traditional Chinese medicine is higher than 76 times of nontoxic standard, therefore, it is determined that being nontoxic.

2. chmice acute toxicity on inhalation is tested:Chmice acute suck essential oil of traditional Chinese medicine LC50 be 24863.99g/m3,95% Credible be limited to 16837.34g/m3~33387.46g/m3.And the toxicity criterion of air freshener is:Chmice acute Suck (2h) LC50 > 10000mg/m3, the true nontoxic grade in border.The LC50 of this essential oil of traditional Chinese medicine is higher than the 2486 of nontoxic standard Times, therefore, it is determined that being nontoxic.

Through examining, fragrance, color and luster, refraction index, relative density, arsenic content, heavy metal contain obtained essential oil of traditional Chinese medicine Amount, pH values meet the requirement of national standard.

(2)Examine above-mentioned ink performance test result such as table 1:

(3)To improving the test of the state of mind.

Main method is that ink is tested using volunteer, recruits 60 people, uses the ink in above-mentioned 2 kinds of embodiments respectively, Pass through SCL-90 questionnaires(I.e.《Self-reporting inventory-SCL90》, it is one of foremost Mental health test scale in the world), It is tracked by continuous use in 1 week, to judge actual efficacy effect of the present invention at aspect of refreshing oneself, wherein 3 people are without impression;7 people Impression is general;1 people thinks that this product is invalid for stimulating effect;Having 49 people to feed back this product has preferable effect of refreshing oneself, and can make People's attention is concentrated, and effective percentage is 81.67%.

(4)Repelling effect is tested.

Repelling effect according to ink in ordinary ink in the prior art and above-described embodiment carries out contrast test, test Data are shown in Table 2.

Conclusion:Ink in the embodiment of the present invention has preferable repelling effect.

The foregoing is merely presently preferred embodiments of the present invention, is not intended to limit the invention, for the common of fields For technical staff, other different forms of changes or modifications may be made based on the above description, is not necessarily to here All embodiments can not be exhaustive, all within the spirits and principles of the present invention, any modification for being made equally is replaced It changes, improve, be still included within protection scope of the present invention.

Claims (1)

1. a kind of offset litho printing ink, it is characterised in that:By weight by following component:23 weight of dispersible pigment color paste Part, 19 parts by weight of bisphenol-A, 4.5 parts by weight of glycerine, 2.3 parts by weight of anhydrous sodium sulfate, 2.7 parts by weight of triethanolamine, triethylamine 3.3 parts by weight, 3.6 parts by weight of acetone, 0.25 parts by weight of double thiocarbamates, 1.7 parts by weight of active mineral matter powder, surface 1.2 parts by weight of activating agent compound, 0.55 parts by weight of sustained release agent, 3.85 parts by weight of essential oil of traditional Chinese medicine, 62 parts by weight of deionized water, institute The pigment for stating mill base is high-carbon black pigment, and the average grain diameter of the dispersible pigment color paste is 75nm, and the active mineral matter powder is germanium Stone, fluorite, tourmaline, gahnite are by weight 2.5:3:3.7:2 mixture, wherein tourmaline are dravite and lithium electricity Gas stone is by weight 5:3 mixture, grain size≤13 μm of the active mineral matter powder, wherein the essential oil of traditional Chinese medicine passes through such as Lower step is prepared,
S1,35 parts by weight of fly expelling plum are taken to clean, naturally dry is subsequently placed in 90 DEG C of frying pans and fries to savory effusion, then sprays 17 parts by weight of deionized water are drenched, 60 DEG C or less drying, water content≤6.5% in constant temperature oven are placed in;
S2,21 parts by weight of perilla leaf are cleaned, is put into a concentration of 27% brine and impregnates 3.5 hours, salt water is is impregnated medicine Expect quality 3.7 times are put into pot and steam thoroughly, take out, dry;
S3, by 17 parts by weight of lavender, 4 parts by weight of anemone vitifolia, 1.5 parts by weight of Moschus, 2 parts by weight of marjoram, imperial saliva Fragrant 1 parts by weight decontamination, puts into micronizer together with the made bulk pharmaceutical chemicals of step S1 and S2 and is crushed to 60 mesh, and raw material is made Medicinal powder end, it is spare;
S4, bulk pharmaceutical chemicals powder obtained in step S3 is put into the extraction kettle of supercritical carbon dioxide extraction apparatus, adjusts extraction Pressure power 27.65MPa, 45.10 DEG C of extraction temperature, carbon dioxide flow 0.6m3/ h, dynamic extraction 2.5h are directly being detached Kettle outlet triangular flask collection volatile oil A, it is spare;
S5, by 7 parts by weight of elm bark, 5 parts by weight of cordate houttuynia, 4.5 parts by weight of corydlis bungeana, 3.5 parts by weight of agalloch eaglewood, 11 weight of camphorwood Part, 3 parts by weight of calamus are measured, 1.75 parts by weight of peppermint clean drying, put into micronizer be crushed to 70 mesh together, then add Deionized water is impregnated 6 hours, and amount of water is institute 6.5 times of immersion bulk pharmaceutical chemicals quality, is dispersed with stirring and mixes well, and obtained Chinese medicine mixes Object, it is spare;
S6, Traditional Chinese drug mixture made from step S5 is decocted 2 hours in 80 DEG C, collects distillate, and ether extraction, distillation is added The volume ratio of liquid and ether is 2:1, then plus anhydrous sodium sulfate drying upper oil phase is taken, obtains volatile oil B, it is spare;
S7, the made volatile oil A of step S4 and S6 and volatile oil B are mixed and mix well obtained miscella, then sequentially added while stirring Wheat malt essential oil, Geranium Essential, snow lotus herb soap essential oil, lemon and grapefruit essential oil are sufficiently stirred 35 minutes, stand 30 points Clock is sufficiently stirred and mixes well, and filtering and impurity removing is to get essential oil of traditional Chinese medicine, wherein the miscella and wheat malt essential oil, Geranium Essential, The mass ratio of snow lotus herb soap essential oil, lemon and grapefruit essential oil is 1.3:0.4:0.75:0.6:0.5:0.3.
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