CN112352785A - Chlorine dioxide nano zinc disinfection and bacteriostasis tablet - Google Patents
Chlorine dioxide nano zinc disinfection and bacteriostasis tablet Download PDFInfo
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- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
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- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/36—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a singly bound oxygen or sulfur atom attached to the same carbon skeleton, this oxygen or sulfur atom not being a member of a carboxylic group or of a thio analogue, or of a derivative thereof, e.g. hydroxy-carboxylic acids
- A01N37/38—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a singly bound oxygen or sulfur atom attached to the same carbon skeleton, this oxygen or sulfur atom not being a member of a carboxylic group or of a thio analogue, or of a derivative thereof, e.g. hydroxy-carboxylic acids having at least one oxygen or sulfur atom attached to an aromatic ring system
- A01N37/40—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a singly bound oxygen or sulfur atom attached to the same carbon skeleton, this oxygen or sulfur atom not being a member of a carboxylic group or of a thio analogue, or of a derivative thereof, e.g. hydroxy-carboxylic acids having at least one oxygen or sulfur atom attached to an aromatic ring system having at least one carboxylic group or a thio analogue, or a derivative thereof, and one oxygen or sulfur atom attached to the same aromatic ring system
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- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
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- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
- A01N43/04—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
- A01N43/14—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
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- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
- A01N65/42—Aloeaceae [Aloe family] or Liliaceae [Lily family], e.g. aloe, veratrum, onion, garlic or chives
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
- A01N65/48—Zingiberaceae [Ginger family], e.g. ginger or galangal
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Abstract
The invention discloses a chlorine dioxide nano zinc disinfection bacteriostatic tablet which comprises, by weight, 15-25 parts of chlorine dioxide, 8-12 parts of nano zinc, 8-12 parts of chitosan, 1-4 parts of sodium bisulfate, 2.5-4.5 parts of ginger extract, 3-6 parts of aloe extract, 3.5-5.5 parts of citric acid, 2-5 parts of a stable forming agent, 1.5-3.5 parts of a drying agent, 0.5-1.5 parts of a preservative and 10-16 parts of deionized water. The chlorine dioxide nano zinc disinfection and bacteriostasis tablet has obvious purification assistance effect on water quality, can effectively purify water, inhibit toxic substances and prevent water eutrophication, is non-toxic and harmless, is simple to produce and prepare, is convenient to store and transport, and is safe and convenient to use.
Description
Technical Field
The invention relates to the technical field of disinfectants, in particular to a chlorine dioxide nano-zinc disinfection bacteriostatic tablet.
Background
The bacteriostatic agent is a substance capable of inhibiting the growth of bacteria, and the bacteriostatic agent can not kill the bacteria, but can inhibit the growth of the bacteria, so that the bacteria are prevented from breeding too much and endangering health, the application field of the bacteriostatic agent is wide, and the use requirement of the bacteriostatic agent is higher and higher along with the continuous development of the use requirements of different fields;
the traditional simple bacteriostatic component proportion is adopted in the conventional bacteriostatic agent, so that various demands are difficult to meet, for example, for the maintenance of water quality, the bacteriostatic agent does not have a corresponding disinfection effect while being simple, and the bacteriostatic agent is limited in use.
Disclosure of Invention
The invention mainly aims to provide a chlorine dioxide nano zinc disinfection and bacteriostasis tablet which has an obvious purification help function on water quality, has a quick disinfection and bacteriostasis effect, is convenient to store and transport, and can effectively solve the problems in the background technology.
In order to achieve the purpose, the invention adopts the technical scheme that: the chlorine dioxide nano zinc disinfection and bacteriostasis tablet comprises, by weight, 15-25 parts of chlorine dioxide, 8-12 parts of nano zinc, 8-12 parts of chitosan, 1-4 parts of sodium bisulfate, 2.5-4.5 parts of ginger extract, 3-6 parts of aloe extract, 3.5-5.5 parts of citric acid, 2-5 parts of a stable forming agent, 1.5-3.5 parts of a drying agent, 0.5-1.5 parts of a preservative and 10-16 parts of deionized water.
Preferably, the preservative comprises, by weight, 18-22 parts of chlorine dioxide, 9-11 parts of nano zinc, 9-11 parts of chitosan, 2-3 parts of sodium bisulfate, 3-4 parts of ginger extract, 4-5 parts of aloe extract, 4-5 parts of citric acid, 3-4 parts of a stabilizing and forming agent, 2-3 parts of a drying agent, 1 part of a preservative and 12-14 parts of deionized water.
Preferably, the preparation method of the chlorine dioxide nano-zinc disinfection bacteriostatic tablet comprises the following steps:
the method comprises the following steps: taking chlorine dioxide solution as a substrate, and mixing with deionized water for 8-10 min;
step two: sequentially adding nano zinc, chitosan, ginger extract, aloe extract and citric acid into the mixed solution, and mixing to obtain a further mixed solution;
step three: sequentially adding sodium bisulfate and a stable forming agent into the mixed solution obtained in the second step, mixing, standing and reacting for 15-25 min;
step four: finally, adding a drying agent and a preservative into the mixed solution after the standing reaction, and mixing to obtain the required chlorine dioxide nano-zinc disinfection and bacteriostasis solution;
step five: and (4) performing mould tabletting on the disinfection and bacteriostasis solution in the step four to obtain the required chlorine dioxide nano zinc disinfection and bacteriostasis tablet.
Preferably, the stable forming agent is a mixture of sodium sulfate and sodium chloride, and the mass ratio of the sodium sulfate to the sodium chloride is 0.8: 1.2.
Preferably, the drying agent is a mixture of calcium chloride and calcium sulfate, and the mass ratio of the calcium chloride to the calcium sulfate is 1: 1.5.
Preferably, the preservative is one of phenoxyethanol, methylparaben, sodium benzoate and potassium sorbate, preferably phenoxyethanol.
Preferably, the preparation method of the aloe extract comprises the following steps:
taking 500g of aloe leaves, cleaning the aloe leaves with clear water, airing the aloe leaves, and naturally drying the aloe leaves to remove residual moisture on the surface;
peeling the air-dried aloe leaves longitudinally from the middle, extruding the pulp in the peeling process to drip the aloe juice, wherein the extruding operation can be repeatedly carried out, the collection amount of the aloe juice is increased, and a glass container is selected for collection;
heating the collected aloe juice at 45-55 deg.C for 5-8 min;
and (3) simply filtering the heated juice by using a fine filter screen to remove redundant floating foam, thus obtaining the required aloe extracting solution.
Preferably, the preparation method of the citric acid comprises the following steps:
taking 150g of orange juice and plum juice, mixing and precipitating for 15-25min, filtering the upper layer juice twice, and removing the bottom layer impurities;
heating the filtered juice at 75-85 deg.C to obtain mixed juice;
adding 15g of calcium carbonate milk into the mixed juice, continuously heating to 100 ℃, and keeping for 15-20 min;
standing and precipitating the heated mixed solution for 35-45min to obtain calcium citrate;
the calcium citrate is desalted, acidolyzed and decolored, and is firstly heated and cleaned by using clear water, the cleaning temperature is 80-85 ℃, 45 percent sulfuric acid is added after cleaning, and the heating is continuously carried out to 100 ℃;
adding 1-2% active carbon into the mixed solution, mixing, reacting for 15-25min, and drying for 4-6min to obtain colorless clear liquid;
and (3) concentrating the colorless clear liquid until the clear liquid is in a solid state, standing for reaction to obtain citric acid crystals, and finally drying for 25-35min to obtain the required citric acid.
The invention has the following beneficial effects:
the chlorine dioxide nano-zinc disinfection bacteriostatic tablet has a remarkable purification assisting effect on water quality, and can effectively purify water, inhibit toxic substances and prevent water eutrophication.
The chlorine dioxide nano-zinc disinfection and bacteriostasis tablet has the advantages of high dissolution efficiency, quick disinfection and bacteriostasis effect and wide application field.
The chlorine dioxide nano zinc disinfection and bacteriostasis tablet is nontoxic and harmless, simple to produce and prepare, convenient to store and transport, and safe and convenient to use.
Of course, it is not necessary for any product in which the invention is practiced to achieve all of the above-described advantages at the same time.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below, and it should be understood that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example 1
The chlorine dioxide nano zinc disinfection and bacteriostasis tablet comprises, by weight, 15-25 parts of chlorine dioxide, 8-12 parts of nano zinc, 8-12 parts of chitosan, 1-4 parts of sodium bisulfate, 2.5-4.5 parts of ginger extract, 3-6 parts of aloe extract, 3.5-5.5 parts of citric acid, 2-5 parts of a stable forming agent, 1.5-3.5 parts of a drying agent, 0.5-1.5 parts of a preservative and 10-16 parts of deionized water.
The preservative comprises, by weight, 18-22 parts of chlorine dioxide, 9-11 parts of nano zinc, 9-11 parts of chitosan, 2-3 parts of sodium bisulfate, 3-4 parts of ginger extract, 4-5 parts of aloe extract, 4-5 parts of citric acid, 3-4 parts of a stabilizing and forming agent, 2-3 parts of a drying agent, 1 part of a preservative and 12-14 parts of deionized water.
The preparation method of the chlorine dioxide nano-zinc disinfection bacteriostatic tablet comprises the following steps:
the method comprises the following steps: taking chlorine dioxide solution as a substrate, and mixing with deionized water for 8-10 min;
step two: sequentially adding nano zinc, chitosan, ginger extract, aloe extract and citric acid into the mixed solution, and mixing to obtain a further mixed solution;
step three: sequentially adding sodium bisulfate and a stable forming agent into the mixed solution obtained in the second step, mixing, standing and reacting for 15-25 min;
step four: finally, adding a drying agent and a preservative into the mixed solution after the standing reaction, and mixing to obtain the required chlorine dioxide nano-zinc disinfection and bacteriostasis solution;
step five: and (4) performing mould tabletting on the disinfection and bacteriostasis solution in the step four to obtain the required chlorine dioxide nano zinc disinfection and bacteriostasis tablet.
The stable forming agent is a mixture of sodium sulfate and sodium chloride, and the use mass ratio of the sodium sulfate to the sodium chloride is 0.8: 1.2.
The drying agent is a mixture of calcium chloride and calcium sulfate, and the use mass ratio of the calcium chloride to the calcium sulfate is 1: 1.5.
Wherein the antiseptic is one of phenoxyethanol, methyl p-hydroxybenzoate, sodium benzoate and potassium sorbate, preferably phenoxyethanol.
The preparation method of the aloe extract comprises the following steps:
taking 500g of aloe leaves, cleaning the aloe leaves with clear water, airing the aloe leaves, and naturally drying the aloe leaves to remove residual moisture on the surface;
peeling the air-dried aloe leaves longitudinally from the middle, extruding the pulp in the peeling process to drip the aloe juice, wherein the extruding operation can be repeatedly carried out, the collection amount of the aloe juice is increased, and a glass container is selected for collection;
heating the collected aloe juice at 45-55 deg.C for 5-8 min;
and (3) simply filtering the heated juice by using a fine filter screen to remove redundant floating foam, thus obtaining the required aloe extracting solution.
The preparation method of the citric acid comprises the following steps:
taking 150g of orange juice and plum juice, mixing and precipitating for 15-25min, filtering the upper layer juice twice, and removing the bottom layer impurities;
heating the filtered juice at 75-85 deg.C to obtain mixed juice;
adding 15g of calcium carbonate milk into the mixed juice, continuously heating to 100 ℃, and keeping for 15-20 min;
standing and precipitating the heated mixed solution for 35-45min to obtain calcium citrate;
the calcium citrate is desalted, acidolyzed and decolored, and is firstly heated and cleaned by using clear water, the cleaning temperature is 80-85 ℃, 45 percent sulfuric acid is added after cleaning, and the heating is continuously carried out to 100 ℃;
adding 1-2% active carbon into the mixed solution, mixing, reacting for 15-25min, and drying for 4-6min to obtain colorless clear liquid;
and (3) concentrating the colorless clear liquid until the clear liquid is in a solid state, standing for reaction to obtain citric acid crystals, and finally drying for 25-35min to obtain the required citric acid.
Example 2
The chlorine dioxide nano zinc disinfection and bacteriostasis tablets prepared by the embodiment are used for carrying out a water purification experiment in aquaculture, a control object is disinfection and bacteriostasis to pollutants in water, such as residual baits and various metabolites, the reference object is a culture water area without using the disinfection and bacteriostasis tablet product, four culture ponds with the same water condition and area are selected and respectively expressed as an experiment group, a control group 1, a control group 2 and a control group 3, wherein the experiment group uses the disinfection and bacteriostasis tablets of the product to combine and match 100%, the control group 1 uses the proportion of 60%, the control group 2 uses the proportion of 30%, the control group 3 does not use the bacteriostasis tablets of the product, the four culture water areas are respectively sampled and detected after the same use time, and the water purification efficiency (%) in aquaculture is calculated, and the experiment results are shown in the following table:
the first table shows the control conditions of the tablet combination with each content ratio on water quality in different time intervals:
| group of | 3 days | 7 days | 15 days | 30 days |
| Experimental group | 43.6％ | 74.7％ | 91.2％ | 90.5％ |
| Control group 1 | 29.9％ | 57.6％ | 74.8％ | 71.3％ |
| Control group 2 | 18.2％ | 37.1％ | 55.5％ | 51.8％ |
| Control group 3 | 6.7％ | 8.4％ | 4.9％ | 7.2％ |
As can be seen from the table I, the chlorine dioxide nano zinc disinfection and bacteriostasis tablet has an obvious effect on water purification in aquaculture, has a considerable help effect on aquaculture, and is suitable for farmers to popularize and use for a long time.
In the description herein, references to the description of "one embodiment," "an example," "a specific example" or the like are intended to mean that a particular feature, structure, material, or characteristic described in connection with the embodiment or example is included in at least one embodiment or example of the invention. In this specification, the schematic representations of the terms used above do not necessarily refer to the same embodiment or example. Furthermore, the particular features, structures, materials, or characteristics described may be combined in any suitable manner in any one or more embodiments or examples.
The preferred embodiments of the invention disclosed above are intended to be illustrative only. The preferred embodiments are not intended to be exhaustive or to limit the invention to the precise embodiments disclosed. Obviously, many modifications and variations are possible in light of the above teaching. The embodiments were chosen and described in order to best explain the principles of the invention and the practical application, to thereby enable others skilled in the art to best utilize the invention. The invention is limited only by the claims and their full scope and equivalents.
Claims (8)
1. The chlorine dioxide nano-zinc disinfection bacteriostatic tablet is characterized in that: the preservative comprises, by weight, 15-25 parts of chlorine dioxide, 8-12 parts of nano zinc, 8-12 parts of chitosan, 1-4 parts of sodium bisulfate, 2.5-4.5 parts of ginger extract, 3-6 parts of aloe extract, 3.5-5.5 parts of citric acid, 2-5 parts of a stable forming agent, 1.5-3.5 parts of a drying agent, 0.5-1.5 parts of a preservative and 10-16 parts of deionized water.
2. The chlorine dioxide nano-zinc disinfection bacteriostatic tablet of claim 1, which is characterized in that: the preservative comprises, by weight, 18-22 parts of chlorine dioxide, 9-11 parts of nano zinc, 9-11 parts of chitosan, 2-3 parts of sodium bisulfate, 3-4 parts of ginger extract, 4-5 parts of aloe extract, 4-5 parts of citric acid, 3-4 parts of a stabilizing and forming agent, 2-3 parts of a drying agent, 1 part of a preservative and 12-14 parts of deionized water.
3. The method for preparing chlorine dioxide nano zinc disinfection bacteriostatic tablets as claimed in claim 1 or 2, which is characterized in that:
the method comprises the following steps: taking chlorine dioxide solution as a substrate, and mixing with deionized water for 8-10 min;
step two: sequentially adding nano zinc, chitosan, ginger extract, aloe extract and citric acid into the mixed solution, and mixing to obtain a further mixed solution;
step three: sequentially adding sodium bisulfate and a stable forming agent into the mixed solution obtained in the second step, mixing, standing and reacting for 15-25 min;
step four: finally, adding a drying agent and a preservative into the mixed solution after the standing reaction, and mixing to obtain the required chlorine dioxide nano-zinc disinfection and bacteriostasis solution;
step five: and (4) performing mould tabletting on the disinfection and bacteriostasis solution in the step four to obtain the required chlorine dioxide nano zinc disinfection and bacteriostasis tablet.
4. The nano zinc chloride dioxide disinfectant bacteriostatic tablet according to any one of claims 1-3, which is characterized in that: the stable forming agent is a mixture of sodium sulfate and sodium chloride, and the use mass ratio of the sodium sulfate to the sodium chloride is 0.8: 1.2.
5. The nano zinc chloride dioxide disinfectant bacteriostatic tablet according to any one of claims 1-3, which is characterized in that: the drying agent is a mixture of calcium chloride and calcium sulfate, and the use mass ratio of the calcium chloride to the calcium sulfate is 1: 1.5.
6. The nano zinc chloride dioxide disinfectant bacteriostatic tablet according to any one of claims 1-3, which is characterized in that: the preservative is one of phenoxyethanol, methyl p-hydroxybenzoate, sodium benzoate and potassium sorbate, preferably phenoxyethanol.
7. The nano zinc chloride dioxide disinfectant bacteriostatic tablet according to any one of claims 1 to 3, wherein the preparation method of the aloe extract comprises the following steps:
taking 500g of aloe leaves, cleaning the aloe leaves with clear water, airing the aloe leaves, and naturally drying the aloe leaves to remove residual moisture on the surface;
peeling the air-dried aloe leaves longitudinally from the middle, extruding the pulp in the peeling process to drip the aloe juice, wherein the extruding operation can be repeatedly carried out, the collection amount of the aloe juice is increased, and a glass container is selected for collection;
heating the collected aloe juice at 45-55 deg.C for 5-8 min;
and (3) simply filtering the heated juice by using a fine filter screen to remove redundant floating foam, thus obtaining the required aloe extracting solution.
8. The nano zinc chloride dioxide disinfectant bacteriostatic tablet according to any one of claims 1-3, which is characterized in that: the preparation method of the citric acid comprises the following steps:
taking 150g of orange juice and plum juice, mixing and precipitating for 15-25min, filtering the upper layer juice twice, and removing the bottom layer impurities;
heating the filtered juice at 75-85 deg.C to obtain mixed juice;
adding 15g of calcium carbonate milk into the mixed juice, continuously heating to 100 ℃, and keeping for 15-20 min;
standing and precipitating the heated mixed solution for 35-45min to obtain calcium citrate;
the calcium citrate is desalted, acidolyzed and decolored, and is firstly heated and cleaned by using clear water, the cleaning temperature is 80-85 ℃, 45 percent sulfuric acid is added after cleaning, and the heating is continuously carried out to 100 ℃;
adding 1-2% active carbon into the mixed solution, mixing, reacting for 15-25min, and drying for 4-6min to obtain colorless clear liquid;
and (3) concentrating the colorless clear liquid until the clear liquid is in a solid state, standing for reaction to obtain citric acid crystals, and finally drying for 25-35min to obtain the required citric acid.
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