CN102336651A - Citric acid and its preparation method - Google Patents
Citric acid and its preparation method Download PDFInfo
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- CN102336651A CN102336651A CN2010102313712A CN201010231371A CN102336651A CN 102336651 A CN102336651 A CN 102336651A CN 2010102313712 A CN2010102313712 A CN 2010102313712A CN 201010231371 A CN201010231371 A CN 201010231371A CN 102336651 A CN102336651 A CN 102336651A
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- citric acid
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- hydrocerol
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Abstract
The invention relates to citric acid and a preparation method, which belongs to the food processing technical field. The invention is characterized in that citric acid uses the fruits of lemon, orange, plum, apricot, peach and the like, and the raw materials are carried out the processes of clearing, filtering, neutralizing, decolouring, concentrating and the like to obtain a citric acid product. The citric acid can be widely utilized in the food processing industry, is an important food organic acidity, and is an additive for beverage, candy and caned food, the market prospect is wide and the citric acid processing is capable of raising the income of the peasants.
Description
Technical field
The present invention relates to a kind of Hydrocerol A and preparation method thereof, belong to food processing technology field.
Background technology
Hydrocerol A is present at occurring in nature in the fruit such as lemon, oranges and tangerines, plum, plum, peach, and is more with acid content in the immature fruit, but industries such as widespread use food, medicine, daily use chemicals.Its process for extracting is all comparatively complicated at present, needs certain experimental installation and technician.
Summary of the invention
The objective of the invention is provides a kind of Hydrocerol A and preparation method thereof for overcoming the weak point of above-mentioned prior art, through raw material clarification filtration, neutralization, decolouring, step such as concentrate and obtain the Hydrocerol A product.Described Hydrocerol A can be widely used in food-processing industry, is a kind of important food organic acid, is the additive of beverage, candy, tinned pre-, and market outlook are wide, and the processing Hydrocerol A can improve peasant household's income.
The present invention realizes with following technical scheme: a kind of Hydrocerol A and preparation method thereof is characterized in that: carry out as follows:
(1) raw material clarification filtration: contain many pectin and impurity in orange juice, the plum juice, need clarify, promote contamination precipitation, use the pressure filter press filtration then;
(2) neutralization: orange juice, when plum juice is heated to 75 ℃, adding lime carbonate serum continues heating 2 hours, is dark green to solution, accomplishes neutralization reaction, staticly settles to be calcium citrate malate;
(3) desalination: calcium citrate malate washs with clear water, is heated to 70-80 ℃, and the repeated multiple times after drying is for use;
(4) acidolysis decolouring: the citrate of lime slurries are heated to 60-70 ℃, seethe with excitement 3 hours, staticly settle, and supernatant liquid is a citric acid solution;
(5) concentrate, behind the partial crystallization, centrifugal, dry, under 75 ℃, be dried to water cut and reach below 1%, through sieve, classification, packing warehouse-in.
Advantage of the present invention is: this Hydrocerol A utilizes fruit such as lemon, oranges and tangerines, plum, plum, peach, through raw material clarification filtration, neutralization, decolouring, step such as concentrate and obtain the Hydrocerol A product.Described Hydrocerol A can be widely used in food-processing industry, is a kind of important food organic acid, is the additive of beverage, candy, tinned pre-, and market outlook are wide, and the processing Hydrocerol A can improve peasant household's income.
Embodiment
Embodiment,
A kind of Hydrocerol A and preparation method thereof is characterized in that: carry out as follows:
(1) raw material clarification filtration: contain many pectin and impurity in orange juice, the plum juice, need clarify, promote contamination precipitation, use the pressure filter press filtration then;
(2) neutralization: orange juice, when plum juice is heated to 75 ℃, adding lime carbonate serum continues heating 2 hours, is dark green to solution, accomplishes neutralization reaction, staticly settles to be calcium citrate malate;
(3) desalination: calcium citrate malate washs with clear water, is heated to 70-80 ℃, and the repeated multiple times after drying is for use;
(4) acidolysis decolouring: the citrate of lime slurries are heated to 60-70 ℃, seethe with excitement 3 hours, staticly settle, and supernatant liquid is a citric acid solution;
(5) concentrate, behind the partial crystallization, centrifugal, dry, under 75 ℃, be dried to water cut and reach below 1%, through sieve, classification, packing warehouse-in.
Claims (1)
1. Hydrocerol A and preparation method thereof is characterized in that: carry out as follows:
(1) raw material clarification filtration: contain many pectin and impurity in orange juice, the plum juice, need clarify, promote contamination precipitation, use the pressure filter press filtration then;
(2) neutralization: orange juice, when plum juice is heated to 75 ℃, adding lime carbonate serum continues heating 2 hours, is dark green to solution, accomplishes neutralization reaction, staticly settles to be calcium citrate malate;
(3) desalination: calcium citrate malate washs with clear water, is heated to 70-80 ℃, and the repeated multiple times after drying is for use;
(4) acidolysis decolouring: the citrate of lime slurries are heated to 60-70 ℃, seethe with excitement 3 hours, staticly settle, and supernatant liquid is a citric acid solution;
(5) concentrate, behind the partial crystallization, centrifugal, dry, under 75 ℃, be dried to water cut and reach below 1%, through sieve, classification, packing warehouse-in.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN2010102313712A CN102336651A (en) | 2010-07-17 | 2010-07-17 | Citric acid and its preparation method |
Applications Claiming Priority (1)
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CN2010102313712A CN102336651A (en) | 2010-07-17 | 2010-07-17 | Citric acid and its preparation method |
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CN102336651A true CN102336651A (en) | 2012-02-01 |
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CN2010102313712A Pending CN102336651A (en) | 2010-07-17 | 2010-07-17 | Citric acid and its preparation method |
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Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105495069A (en) * | 2014-10-29 | 2016-04-20 | 张湉 | Preparation method of citric acid |
CN106835317A (en) * | 2017-02-27 | 2017-06-13 | 合肥中科富华新材料有限公司 | A kind of method that fish skin collagen is self-assembled into fiber |
CN110897962A (en) * | 2019-12-24 | 2020-03-24 | 沈阳君元生物科技有限公司 | Essential oil and preparation method thereof |
CN112352785A (en) * | 2020-10-29 | 2021-02-12 | 青岛翼科新程生物科技有限公司 | Chlorine dioxide nano zinc disinfection and bacteriostasis tablet |
CN114159956A (en) * | 2021-12-15 | 2022-03-11 | 淄博睿泽环保工程有限公司 | Deodorant formulation |
-
2010
- 2010-07-17 CN CN2010102313712A patent/CN102336651A/en active Pending
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105495069A (en) * | 2014-10-29 | 2016-04-20 | 张湉 | Preparation method of citric acid |
CN106835317A (en) * | 2017-02-27 | 2017-06-13 | 合肥中科富华新材料有限公司 | A kind of method that fish skin collagen is self-assembled into fiber |
CN110897962A (en) * | 2019-12-24 | 2020-03-24 | 沈阳君元生物科技有限公司 | Essential oil and preparation method thereof |
CN112352785A (en) * | 2020-10-29 | 2021-02-12 | 青岛翼科新程生物科技有限公司 | Chlorine dioxide nano zinc disinfection and bacteriostasis tablet |
CN114159956A (en) * | 2021-12-15 | 2022-03-11 | 淄博睿泽环保工程有限公司 | Deodorant formulation |
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Legal Events
Date | Code | Title | Description |
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C06 | Publication | ||
PB01 | Publication | ||
WD01 | Invention patent application deemed withdrawn after publication | ||
WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20120201 |