CN102973977B - Air-freshening bacteriostatic agent and preparation method thereof - Google Patents
Air-freshening bacteriostatic agent and preparation method thereof Download PDFInfo
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- CN102973977B CN102973977B CN201210583250.3A CN201210583250A CN102973977B CN 102973977 B CN102973977 B CN 102973977B CN 201210583250 A CN201210583250 A CN 201210583250A CN 102973977 B CN102973977 B CN 102973977B
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Abstract
The invention discloses a traditional Chinese medicine air sterilization freshening agent and a preparation method thereof. The method provides a formula comprising components in parts by weight as follows: 10-20 parts of rheum officinale, 5-10 parts of officinal magnolia bark, 50-60 parts of atratylodes rhizome, 30-40 parts of honeysuckle, 30-35 parts of figwort roots, 5-15 parts of mint, 5-20 parts of orange peel, 0-10 parts of Chinese-date, 30-50 parts of licorice roots and 45-60 parts of wild chrysanthemum flower are immersed in an ethanol solution and extracted, a filtrate is collected for filling, and the air-freshening bacteriostatic agent is obtained. The air-freshening bacteriostatic agent can be used for preventing colds and treating respiratory diseases and the like, and can not only inhibit and kill harmful bacteria and viruses in the air, but also expel parasites, relieve itching and prevent virus colds.
Description
Technical field
The present invention relates to a kind of air fresh bacteriostat for fresh air, particularly relate to a kind of take the Chinese crude drug air fresh bacteriostat formulated as raw material extracts and the preparation method of this antibacterial.
Background technology
The insect aerosol of the air freshener of selling on market and the use that repels mosquitoes and flies, because containing a large amount of chemical compositions, all has certain toxicity to human body more.Widely used indoor insecticidal aerosol in the world for example, adopts a kind of insecticidal constituent of universally acknowledged safe pyrethroid exactly.Yet home and abroad environment toxicologist tests confirmation, pyrethroid insecticides also has obvious toxicity to people and animals' nervous system, and Long Term Contact can cause nervous system toxicity, causes the nervous symptoms such as the abnormal and dizziness headache of neural paralysis, sensory nerve.
High development along with social material civilization, air pollution is room air pollution particularly, in its degree, greatly increase, cause the ill frequency of some people respiratory tract disease to increase and occur dizzy, the tired symptom such as feel sick, bring puzzlement and worried to many people's work and life, the mankind healthy has been subject to increasing threat.How to eliminate and to prevent room air pollution to become the focus that people are concerned about, also the released one after another product of pure and fresh and disinfecting air of many producers, but these freshener exist larger problems and shortcomings in the market, the one, the overwhelming majority is chemicals, only adds some essence and is injected in and in air, just has aromatic odor and do not possess sterilizing effect; The 2nd, adopt chemical products as raw material, when doing pure and fresh sterilization like this, increased again new pollution; The 3rd, traditional medicine sterile products, although there is stronger sterilization, often the smell is awful (as lysol), common people are difficult to accept, or sterilize with fluoric acid, but all can not improve indoor air ambient completely.
Therefore, both at home and abroad well-known expert once advised, the duty ventilation of windowing, carrys out environment purification by fresh and salubrious natural air, is the first selection of fresh air; Another selection is that effective component extracting is made novel air freshener from natural plants.From relevant Chinese medicine, effective component extracting is made the air freshener of high-efficiency environment friendly, in current domestic and international market, still belongs to initiative industry project, has development prospect.For Chinese medicine air fresh bacteriostat, there is antibacterium and pathogenic dermatophytes, the present market of Chinese medicine air fresh bacteriostat of the effect such as Prevention eczema, skin pruritus, scabies is also rare.
Summary of the invention
The object of this invention is to provide and a kind ofly take pure Chinese medicine and extract preparation as raw material, can fresh air, repel mosquitoes and flies, again can prophylactic air fresh bacteriostat.
The preparation method of above-mentioned air fresh bacteriostat is provided, and is another goal of the invention of the present invention.
Chinese medicine air fresh bacteriostat of the present invention is that the component by following parts by weight is that raw material is made:
The further raw material components (parts by weight) of Chinese medicine air fresh bacteriostat of the present invention is:
The optimum raw material components (parts by weight) of Chinese medicine air fresh bacteriostat of the present invention is:
The present invention makes concentrating agents by above-mentioned Chinese medicine air-freshing bacteria inhibition liquid and uses.
The preparation method of the pure Chinese medicine air fresh bacteriostat concentrating agents of the present invention is that Radix Et Rhizoma Rhei, Cortex Magnoliae Officinalis, Rhizoma Atractylodis, Flos Lonicerae, Radix Scrophulariae, Herba Menthae, Pericarpium Citri Reticulatae, Fructus Jujubae, Radix Glycyrrhizae, Flos Chrysanthemi Indici are mixed according to described parts by weight, with ethanol, soak extraction, collect rear fill in filtrate and make.
The concrete preparation method of the pure Chinese medicine air fresh bacteriostat concentrating agents of the present invention comprises the following steps:
(1) pretreatment of raw material: Radix Et Rhizoma Rhei, Cortex Magnoliae Officinalis, Rhizoma Atractylodis, Flos Lonicerae, Radix Scrophulariae, Herba Menthae, Pericarpium Citri Reticulatae, Fructus Jujubae, Radix Glycyrrhizae, Flos Chrysanthemi Indici are cleaned standby;
(2) alcohol extractions: by pretreated raw material according to the mixing of weighing of above-mentioned parts by weight, according to the volume of 8～10 times of raw material gross weights, prepare the ethanol of mass concentration 75%, first in mixed material, add the above-mentioned ethanol that accounts for whole volumes 1/2～2/3, under room temperature, soak after one week and filter, filtrate is left in fluid reservoir;
(3) secondary alcohol extraction: the filtering residue with remaining ethanol after to an alcohol extraction carries out soak at room temperature, soaks after one week and filters, and filtrate is mixed with an alcohol extraction filtrate;
(4) fill: filtrate is carried out to fill.
The present invention can also make above-mentioned Chinese medicine air-freshing bacteria inhibition liquid spray and use.
The concrete grammar that the present invention makes spray using Chinese medicine air fresh bacteriostat be in the Chinese medicine air fresh bacteriostat of fill directly filling compressed air as propellant, to enable to form vaporific, reach spray effect.Because the present invention adds the chemical propellant such as propane, butane or dimethyl ether, guaranteed that product life-time service of the present invention is also nontoxic to human body.
In the main raw material of Chinese medicine that Chinese medicine air fresh bacteriostat of the present invention is used, Radix Et Rhizoma Rhei has anti-bacteria and anti-virus effect, it can effectively suppress the antibacterials such as staphylococcus aureus, escherichia coli, dysentery bacterium, bacillus enteritidis, bacillus pyocyaneus, typhoid fever, and Hemolytic streptococcus, diphtheria corynebacterium, bacillus subtilis, Mycobacterium phlei, brucella, bacillus pestis, Salmonella paratyphi, deep shape bacillus, bacillus smegmatis, gonorrhea diplococcus etc. are all had to inhibitory action in various degree; Cortex Magnoliae Officinalis has bacteriostasis to streptococcus pneumoniae, diphtheria corynebacterium, Hemolytic streptococcus, bacillus subtilis, will Hayes and Amur dysentery bacterium, staphylococcus aureus etc., in Cavia porcellus body, anthrax bacillus is had to some antibacterial action; Some dermatophytess are had to inhibitory action in vitro; Experimental viral hepatitis is also improved to the effect of liver essence pathological changes; Rhizoma Atractylodis have the effect of the strongly fragrant table of noxious dampness, to eczema itch, impetigo, Keratoderma disease, tuberculosis and prevention and control malaria symptom all have positive effect.Rhizoma Atractylodis abnormal smells from the patient virtue is strong, therefore conventional dirty, epidemic prevention, diseases prevention and the disinfection of indoor air of driving among the people.Cloth bag as fragrant in Dragon Boat Festival child take Rhizoma Atractylodis as main note material, and Rhizoma Atractylodis and Folium Artemisiae Argyi are stifling can wipe out the flies and mosquitoes and indoor disinfection, and tubercule bacillus, streptococcus pneumoniae, staphylococcus aureus, large intestine, hay and bacillus pyocyaneus, fungus etc. are had to significant sterilization effect; Flos Lonicerae is monarch drug in side, and it is described as the good medicine of heat-clearing and toxic substances removing from ancient times.Flos Lonicerae has heat-clearing and toxic substances removing, liver heat removing and eyesight improving, removing heat from blood relieves summer heat, and promoting the production of body fluid to quench thirst, diseases prevention are antibacterial, antiviral, Weight-reducing and lipid-lowering, blood pressure lowering, improve the effects such as body immunity.Its property sweet cold, gas is fragrant, clearing away heat with drugs sweet in flavor and cold in nature and not injuring one's stomach, fragrance thoroughly reaches and can be eliminating evil.Flos Lonicerae is sweet cold, and both clearing heat in QI system can purify the blood again minute hot, and among heat clearing away, have again the merit that slight a surname is loose, thus can control affection due to external wind and heat or epidemic febrile disease from the beginning of the disease that table disease is not separated, interior-heat is contained again.Flos Lonicerae can dispelling wind-heat, kind removing summer-heat blood poison also, and for various febrile diseases, as fever of the body, dermexanthesis, send out the cards such as speckle, pyretic toxicity carbuncle sore, laryngopharynx swelling and pain, all effect is remarkable.In the hall random notes > > of < < Chongqing, in the clear network of Flos Lonicerae, wind-fire is damp and hot, separates the dirty filthy heresy of pestilence; Radix Scrophulariae and Herba Menthae are ministerial drug in side.Radix Scrophulariae cold nature, sweet in the mouth, hardship, salty, return lung, stomach, kidney channel.There is clearing away heat and cooling blood, nourishing YIN to lower pathogenic fire, the effect of detoxicating and resolving stagnation of pathogens.For heat, enter nutrient blood, maculae caused by violent heat pathogen, consumption of YIN caused by febrile disease, crimson tongue excessive thirst, constipation is hindered in Tianjin, hectic fever due to YIN-deficiency chronic cough, conjunctival congestion, pharyngalgia, diphtheria, scrofula, carbuncle sore tumefacting virus.Radix Scrophulariae is successful aspect treatment laryngopharynx swelling and pain especially, has the effect that strengthens monarch drug removing summer-heat blood poison, helps monarch drug to alleviate the symptom of pharyngalgia simultaneously.Herba Menthae acrid in the mouth cool in nature, pungent to disperse, cool to heat clearing away, clear light cool loose, be the conventional product of dispelling wind and heat pathogens; Pericarpium Citri Reticulatae and Fructus Jujubae are adjuvant drug in side.Pericarpium Citri Reticulatae bitter in the mouth, pungent, warm in nature, temperature can circulation of qi promoting, and pungent can dispersing is bitter and sluice.There is regulating qi-flowing for strengthening spleen, the merit of drying dampness to eliminate phlegm, for distension and fullness in the abdomen, lack of appetite and vomiting, cough with copious phlegm.Fructus Jujubae sweet in the mouth, warm in nature.There is invigorating the spleen and replenishing QI, the merit of nourishing blood to tranquillize the mind, for insufficiency of the spleen lack of appetite, weak loose stool, married woman is dirty dry; Radix Glycyrrhizae makes medicine at Fang Zhongwei, coordinating the actions of various ingredients in a prescription.Radix Glycyrrhizae sweet in the mouth is flat, has invigorating the spleen and replenishing QI, heat-clearing and toxic substances removing, and expelling phlegm for arresting cough, relieving spasm to stop pain, the effect of coordinating the actions of various ingredients in a prescription, for weakness of the spleen and stomach, fatigue and weakness, shortness of breath and palpitation, cough with copious phlegm, gastral cavity abdomen, the anxious pain of extremity contraction, carbuncle sore tumefacting virus; Flos Chrysanthemi Indici containing can be widely used in treatment furuncle carbuncle, laryngopharynx swelling and pain, wind-fire acute conjunctivitis, the disease such as dizzy of having a headache.There is again good hypotensive effect, can be used for the auxiliary treatment of hypertension simultaneously.
The present invention selects fragrant odour, and the natural Chinese medicine with sterilizing fungistatic effect is raw material, extracts its effective ingredient and makes air fresh bacteriostat, and filling compressed air is as propellant, not only production method is simple, easy to use, and after using to human body without any murder by poisoning.
Through the results show, product of the present invention has powerful dissipation effect to harmful bacterias such as staphylococcus aureus, influenza virus, escherichia coli, can effectively prevent the generation of influenza and epidemic disease, can substitute chemosynthesis air freshener and insect aerosol in the market, the place that the crowd is dense, easily cause cross infection such as be widely used in hotel, office building, room, army, school, hospital, car.
The specific embodiment
Below in conjunction with embodiment, further set forth the present invention.Should be understood that these embodiment are only not used in and limit the scope of the invention for the present invention is described.In addition should be understood that those skilled in the art can make various changes or modifications the present invention after having read the content of the present invention's instruction, these equivalent form of values fall within the application's appended claims limited range equally.
Embodiment 1
Take that to manufacture the spray product that 10,000 bottles of net capacity are 400mL be example, according to following weight, be ready to raw material of Chinese medicine: Radix Et Rhizoma Rhei 15Kg, Cortex Magnoliae Officinalis 5Kg, Rhizoma Atractylodis 60Kg, Flos Lonicerae 40Kg, Radix Scrophulariae 33Kg, Herba Menthae 10Kg, Pericarpium Citri Reticulatae 8Kg, Fructus Jujubae 8Kg, Radix Glycyrrhizae 35Kg, Flos Chrysanthemi Indici 48Kg.
Radix Et Rhizoma Rhei, Cortex Magnoliae Officinalis, Rhizoma Atractylodis, Flos Lonicerae, Radix Scrophulariae, Herba Menthae, Pericarpium Citri Reticulatae, Fructus Jujubae, Radix Glycyrrhizae, Flos Chrysanthemi Indici are mixed, add the ethanol 1500L of mass concentration 75%, under room temperature, airtight immersion, after one week, filters out filtrate, leaves in fluid reservoir stand-by.The ethanol 1000L that adds again mass concentration 75% in filtering residue, under room temperature, airtight immersion is one week, filters out filtrate, mixes with an alcohol extraction filtrate, obtains altogether alcohol extract 2000L.
Add 40% ethanol 2000L again, obtain containing the alcohol extract 4000L that alcohol mass concentration is 58%, dress is filled with, and filling compressed air in tank, packs and put in storage after the assay was approved simultaneously.
Embodiment 2
Take that to manufacture the concentrating agents product that 10,000 bottles of net capacity are 500mL be example, according to following weight, be ready to raw material of Chinese medicine: Radix Et Rhizoma Rhei 14Kg, Cortex Magnoliae Officinalis 6Kg, Rhizoma Atractylodis 55Kg, Flos Lonicerae 35Kg, Radix Scrophulariae 32Kg, Herba Menthae 9Kg, Pericarpium Citri Reticulatae 8Kg, Fructus Jujubae 6Kg, Radix Glycyrrhizae 40Kg, Flos Chrysanthemi Indici 50Kg.
Radix Et Rhizoma Rhei, Cortex Magnoliae Officinalis, Rhizoma Atractylodis, Flos Lonicerae, Radix Scrophulariae, Herba Menthae, Pericarpium Citri Reticulatae, Fructus Jujubae, Radix Glycyrrhizae, Flos Chrysanthemi Indici are mixed, add the ethanol 1500L of mass concentration 75%, under room temperature, airtight immersion, after one week, filters out filtrate, leaves in fluid reservoir stand-by.In filtering residue, add 75% ethanol 1000L, under room temperature, airtight immersion is one week, filters out filtrate again, mixes with an alcohol extraction filtrate, obtains altogether alcohol extract 2000L.
The ethanol 2000L that adds again mass concentration 40%, obtains containing the alcohol extract 4000L that alcohol mass concentration concentration is 58%, and dress is filled with, after the assay was approved packing warehouse-in.
The present invention is according to < < disinfection technology standard > > (version in 2002), under testing conditions separately, the bacteriostasis property to Chinese medicine air fresh bacteriostat of the present invention detects respectively, and concrete testing result is as follows.
The ethanol dilution liquid of A, Chinese medicine air fresh bacteriostat of the present invention 5% is 3.76 * 10 to concentration
4bacteria suspension effect 2min for the coli test of cfu/mL, each the equal > 97% of bacteriostasis rate, product has bacteriostasis for escherichia coli.
The ethanol dilution liquid of B, Chinese medicine air fresh bacteriostat mass concentration 5% of the present invention is 1.80 * 10 to concentration
4the staphylococcus aureus of cfu/mL bacteria suspension effect 2min for test, each the equal > 96% of bacteriostasis rate, product has stronger bacteriostasis for staphylococcus aureus.
The ethanol dilution liquid of C, Chinese medicine air fresh bacteriostat mass concentration 5% of the present invention is 2.02 * 10 to concentration
4the clostridium tetani of cfu/mL bacteria suspension effect 2min for test, each the equal > 94% of bacteriostasis rate, product has bacteriostasis for clostridium tetani.
The ethanol dilution liquid of D, Chinese medicine air fresh bacteriostat mass concentration 5% of the present invention is after 45 ℃ are incubated 90 days, bacteria suspension effect 2min for staphylococcus aureus is tested, each the equal > 97% of bacteriostasis rate, bacteria suspension effect 2min for escherichia coli, clostridium tetani are tested, each the equal > 95% of bacteriostasis rate, there is no significant difference with the fungistatic effect before depositing, show the fungistatic effect of escherichia coli, staphylococcus aureus, clostridium tetani stable.
Actual case
Inventor selects certain liang kindergarten to do drug study contrast of the present invention, experimental group and matched group have respectively 50 4-6 year children, experimental group is used Chinese medicine air fresh bacteriostat of the present invention every day in classroom, and matched group is not used any air fresh bacteriostat.At swine flu, hold in journey in explosive autumn, use Chinese medicine air fresh bacteriostat of the present invention, no one flu.And have 26 people in matched group, there is flu-like symptom.
Claims (3)
1. a Chinese medicine air fresh bacteriostat, is characterized in that being made by the preparation method comprising the steps:
(1) pretreatment of raw material: Radix Et Rhizoma Rhei, Cortex Magnoliae Officinalis, Rhizoma Atractylodis, Flos Lonicerae, Radix Scrophulariae, Herba Menthae, Pericarpium Citri Reticulatae, Fructus Jujubae, Radix Glycyrrhizae, Flos Chrysanthemi Indici are cleaned standby; The parts by weight of above-mentioned raw materials are:
(2) alcohol extractions: by pretreated raw material according to the mixing of weighing of above-mentioned parts by weight, according to raw material gross weight 8-10 volume doubly, prepare the ethanol of mass concentration 75%, first in mixed material, add the above-mentioned ethanol that accounts for whole volume 1/2-2/3, under room temperature, soak after one week and filter, filtrate is left in fluid reservoir;
(3) secondary alcohol extraction: the filtering residue with remaining ethanol after to an alcohol extraction carries out soak at room temperature, soaks after one week and filters, and filtrate is mixed with an alcohol extraction filtrate;
(4) fill: filtrate is carried out to fill.
2. Chinese medicine air fresh bacteriostat according to claim 1, is characterized in that the parts by weight of described raw material are:
3. Chinese medicine air fresh bacteriostat according to claim 2, is characterized in that the parts by weight of described raw material are:
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Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105169448A (en) * | 2015-09-10 | 2015-12-23 | 潘福昆 | Refrigerator deodorant |
| CN105340990A (en) * | 2015-11-06 | 2016-02-24 | 丁民修 | Application of rhubarb as mosquito repellent |
| CN108186428A (en) * | 2016-12-08 | 2018-06-22 | 成都中医药大学 | A kind of Cortex Magnoliae Officinalis floral water and preparation method thereof |
| CN107668093A (en) * | 2017-08-08 | 2018-02-09 | 深圳沃海森科技有限公司 | Environment-friendly long-life type air conditioner filter element bacteriostatic agent and preparation method thereof |
| CN109805039A (en) * | 2017-11-20 | 2019-05-28 | 柳州市皇之品贸易有限公司 | A kind of bacteriostatic agent of air containing medicinal herb components |
| CN107912467A (en) * | 2017-12-16 | 2018-04-17 | 柳州市晟铂贸易有限公司 | A kind of high effect nontoxic bacteriostatic agent |
| CN111296508A (en) * | 2020-03-20 | 2020-06-19 | 呼和浩特市万登环境科技有限公司 | Disinfectant for indoor air disinfection |
| CN111838213A (en) * | 2020-07-30 | 2020-10-30 | 海南医学院 | Traditional Chinese medicine air purification spray and preparation method thereof |
| CN112998033A (en) * | 2021-03-19 | 2021-06-22 | 大连耀灸生物科技有限公司 | Traditional Chinese medicine incense |
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| CN101391108B (en) * | 2008-10-31 | 2013-05-08 | 山西振东制药股份有限公司 | Traditional Chinese medicine air fresh bacteriostat and preparation method thereof |
| CN101530112A (en) * | 2009-03-23 | 2009-09-16 | 深圳市武大金球中药现代化工程技术研究中心 | An air sterilization freshener, a preparation method and a using method thereof |
| CN101990913A (en) * | 2009-08-29 | 2011-03-30 | 夏焰明 | Chinese medical drug air sanitizing preparation and preparation method thereof |
| CN101690503A (en) * | 2009-10-12 | 2010-04-07 | 何丹凤 | Chinese herbal medicine health-care joss stick |
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