CN104762136A - Compound tea tree essential oil with sterilization and disinfection effects and preparation method of compound tea tree essential oil - Google Patents
Compound tea tree essential oil with sterilization and disinfection effects and preparation method of compound tea tree essential oil Download PDFInfo
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Abstract
The invention discloses compound tea tree essential oil with sterilization and disinfection effects and a preparation method of the compound tea tree essential oil. The compound tea tree essential oil is prepared from the following raw materials in parts by mass: 5-12 parts of wild chrysanthemum flowers, 9-16 parts of fructus forsythia, 4-9 parts of scabrous mosla herb, 8-12 parts of lithospermum, 9-15 parts of Chinese angelica, 8-12 parts of croton, 5-10 parts of moutan bark and an appropriate amount of German chamomile essential oil, lavender essential oil, VE, rose fruit oil and tea tree essential oil. According to the compound tea tree essential oil, plant resources are sufficiently utilized, and traditional Chinese medicine extract is organically combined with the plant essential oil. Compared with chemical germicide and disinfectant, the compound tea tree essential oil is safe, environmentally friendly, pleasant in smell, and the like. A product prepared by the compound tea tree essential oil is convenient to use and wide in applicability, can be applied to sterilizing and disinfecting skin on different parts and an oral cavity of a person, and can also be used for sterilizing and disinfecting air and apparatuses.
Description
Technical field
The present invention relates to essential oil field, particularly relate to a kind of compound tea tree ethereal oil and the preparation method with sterilization and disinfection effect.
Background technology
Along with the expansion of people's scope of activity, and the diversity of mode of life, the mankind can generate a large amount of domestic refuses every day, and wherein containing a large amount of bacteriums and virus, some can be in the air floating with the flowing of air, threatens the health of people.Some refuse tip also can give out unpleasant peculiar smell, drastically influence the life of people.For the pathogenic micro-organism wherein serving as communication media, people's many employings sterilizing agent is killed it or is removed, to cut off the propagation of transmissible disease.The disinfection solution that market uses is mostly chemical synthesis preparation or fermentation preparation, and they all have stronger elimination effect to the harmful organism such as germ and insect.But these sterilizing agents of life-time service, the enhancing of germ tolerance can be caused, disinfection effect is died down gradually, and these disinfection sanitizers all have larger hormesis to the respiratory system of human body, skin and mucous membrane, improper use can cause certain injury to human body.Publication No. CN 102239893 A(application number 201110113813.8) Chinese patent literature disclose a kind of plant essential oil bactericidal disinfectant, be made up of the following raw material of weight percent: Oil of Eucalyptus 0.3%, tea tree oil 0.4%, mugwort oil 0.3%, rosemary oil 0.5%, bergamot oil 0.5%, lemon oil 0.5%, Oleum lavandula angustifolia 0.7%, Syzygium aromaticum stem oil 0.2%, thyme oil 0.4%, and the thinner of residue surplus.Publication No. CN 104255835 A(application number 201410434284.5) Chinese patent literature disclose a kind of indoor sterilizing agent and preparation method thereof, by the chamomile essential oil 1 ~ 3 part of weight part, spearmint oil 0.5 ~ 2 part, cinnamon essential oil 1 ~ 3 part, Japanese Honeysuckle 1 ~ 5 part, wrinkled giant hyssop 3 ~ 7 parts, taraxacum 5 ~ 10 parts, the coptis 8 ~ 15 parts, aloe 10 ~ 18 parts, the red sage root 10 ~ 18 parts, pure water 50 ~ 60 parts prepares.Publication No. CN 103478177A(application number 201310399260.6) Chinese patent literature disclose a kind of air disinfectant, comprise peach-pit extracting solution 20-50 part, root of Dahurain angelica extracting solution 10-20 part, pomegranate rind extracting solution 5-15 part, Cananga odorata quintessence oil 1-5 part, dehydrated alcohol 5-20 part, water 30-50 part.
Though existing disinfection sanitizer has good sterilization and disinfection effect, life-time service damages human body, and threat people's is healthy.Much research finds, plants essential oil has good germicidal action, therefore, can make full use of plant resources, develops by the composite disinfection sanitizer of plant milk extract.
Summary of the invention
For the problem of prior art, the object of this invention is to provide a kind of natural, non-stimulated compound tea tree ethereal oil with sterilization and disinfection effect and preparation method.
Technical scheme of the present invention is:
There is the compound tea tree ethereal oil of sterilization and disinfection effect, be prepared from primarily of following raw materials according, be mass parts: Wild Chrysanthemum 5-12, capsule of weeping forsythia 9-16, Scabrous Mosla Herb 4-9, Asian puccoon 8-12, Radix Angelicae Sinensis 9-15, crotons 8-12, Tree Peony Bark 5-10, German chamomile essential oil, Herba Lysimachiae foenumgraeci quintessence oil, VE, rose hip oil, tea tree ethereal oil are in right amount each.
In preferred scheme, Wild Chrysanthemum 7-10, capsule of weeping forsythia 11-14, Scabrous Mosla Herb 5-8, Asian puccoon 9-11, Radix Angelicae Sinensis 10-14, crotons 9-11, Tree Peony Bark 7-8, German chamomile essential oil, Herba Lysimachiae foenumgraeci quintessence oil, VE, rose hip oil, tea tree ethereal oil are in right amount each.
Be more preferably, Wild Chrysanthemum 8.5, the capsule of weeping forsythia 12.5, Scabrous Mosla Herb 6.5, Asian puccoon 10, Radix Angelicae Sinensis 12, crotons 10, Tree Peony Bark 7.5, German chamomile essential oil, Herba Lysimachiae foenumgraeci quintessence oil, VE, rose hip oil, tea tree ethereal oil are in right amount each.
The described preparation method with the compound tea tree ethereal oil of sterilization and disinfection effect is:
(1) get wheat bran to put into pot and heat, add clean crotons after smoldering, stir-fry 12-16 minute (preferred, to stir-fry 14 minutes), adds water and no crotons, after little fire decocts, pull out, remove wheat bran, dry;
(2) get Tree Peony Bark removing impurity and residual core, mix thoroughly with the yellow rice wine of Tree Peony Bark quality 0.3 times, be then placed in pot Steam by water bath saturating, take out, dry;
(3) Wild Chrysanthemum, the capsule of weeping forsythia, Scabrous Mosla Herb, Asian puccoon, Radix Angelicae Sinensis are cleaned removal of impurities, segment, put into frying pan, after slow fire stir-fries, take out, dry in the air cool, pulverize and sieve together with step (1) (2) made raw material, then drop into supercritical CO
2in the extraction kettle of abstraction instrument, at pressure 25MPa, temperature 60 C, CO
2flow is 0.3m
3extract under the condition of/h, obtain volatile oil 1;
(4) made for step (3) volatile oil 1 is joined in rose hip oil, stir evenly, then German chamomile essential oil, Herba Lysimachiae foenumgraeci quintessence oil, VE, tea tree ethereal oil is added successively, limit edged stirs, and mixes rear stopping and stirring, leave standstill 1 hour, centrifugal, rotating speed 3000r/min, gets supernatant liquor, obtains compound tea tree ethereal oil.
The described preparation method with the compound tea tree ethereal oil of sterilization and disinfection effect, the little fire of step (1) decocts 15-25 minute, and (preferred, little fire decocts 17-23 minute; Be more preferably, little fire decocts 20 minutes).
The described preparation method with the compound tea tree ethereal oil of sterilization and disinfection effect, step (3) slow fire stir-fries, and within 12-18 minute, (preferred, slow fire stir-fries 14-16 minute; Be more preferably, slow fire stir-fries 15 minutes).
The described preparation method with the compound tea tree ethereal oil of sterilization and disinfection effect, step (3) was pulverized 60-100 mesh sieve and (preferably, was pulverized 70-90 mesh sieve; Be more preferably, pulverized 80 mesh sieves).
The described preparation method with the compound tea tree ethereal oil of sterilization and disinfection effect, step (3) extraction time is 3-5 hour (preferably, extraction 3.5-4.5 hour; Be more preferably, extract 4 hours).
The described preparation method with the compound tea tree ethereal oil of sterilization and disinfection effect, step (4) centrifugal 10-16 minute (preferred, centrifugal 12-14 minute; Be more preferably, centrifugal 13 minutes).
The described preparation method with the compound tea tree ethereal oil of sterilization and disinfection effect, volatile oil 1 in step (4), Germany's chamomile essential oil, Herba Lysimachiae foenumgraeci quintessence oil, VE, the mass ratio of tea tree ethereal oil and rose hip oil is (0.3-0.7): (0.4-0.8): (0.7-1.1): (0.4-0.9): (0.8-1.2): (3.0-4.4) is (preferred, volatile oil 1, Germany's chamomile essential oil, Herba Lysimachiae foenumgraeci quintessence oil, VE, the mass ratio of tea tree ethereal oil and rose hip oil is (0.4-0.6): (0.5-0.7): (0.8-1.0): (0.5-0.8): (0.9-1.1): (3.4-4.0), be more preferably, the mass ratio of volatile oil 1, German chamomile essential oil, Herba Lysimachiae foenumgraeci quintessence oil, VE, tea tree ethereal oil and rose hip oil is 0.5:0.6:0.9:0.65:1.0:3.7).
The compound tea tree ethereal oil with sterilization and disinfection effect provided by the invention is prepared from by traditional Chinese medicine material and natural plant essential oils, safely, has no side effect, and has good sterilization and disinfection effect.In addition, excellent results of the present invention also shows:
1, the present invention makes full use of plant resources, Chinese medicinal material extract is organically combined with plants essential oil, with chemical sterilization sterilizing agent ratio, has the advantages such as safety and environmental protection, smell be pleasant;
2, products made thereby of the present invention is easy to use, and suitability is wide, can be applicable to the sterilization in individual different sites skin and oral cavity, also can be used for the sterilization of air and apparatus.
Embodiment
Describe technical scheme of the present invention in detail below in conjunction with embodiment and experimental example, but protection domain is not limited thereto.
embodiment 1there is the compound tea tree ethereal oil of sterilization and disinfection effect, be prepared from (every part of 10g) primarily of following raw materials according: Wild Chrysanthemum 5 parts, the capsule of weeping forsythia 9 parts, Scabrous Mosla Herb 4 parts, Asian puccoon 8 parts, Radix Angelicae Sinensis 9 parts, crotons 8 parts, Tree Peony Bark 5 parts, Germany's chamomile essential oil is (purchased from Qingdao Feng Ze Xin Jia commerce and trade limited liability company, specification 10ml, article No. AD21A01), Herba Lysimachiae foenumgraeci quintessence oil is (purchased from Lan Lan bio tech ltd, Qingdao, specification 30ml, commodity bar code 0701413813392), VE(is purchased from Jiahe, the Holy Land, Shandong biotechnology company limited, specification 1000 IU/g), rose hip oil is (purchased from Qingdao Feng Ze Xin Jia commerce and trade limited liability company, specification 100ml, article No. AK30I71), tea tree ethereal oil is (purchased from Guangzhou Chang Ju trade Co., Ltd, specification 500ml, article No. CA007) in right amount each.
The preparation method with the compound tea tree ethereal oil of sterilization and disinfection effect is:
(1) get wheat bran to put into pot and heat, add clean crotons, stir-fry 12 minutes, add water and do not have crotons after smoldering, little fire decocted after 15 minutes, pulled out, and removing wheat bran, dries;
(2) get Tree Peony Bark removing impurity and residual core, mix thoroughly with the yellow rice wine of Tree Peony Bark quality 0.3 times, be then placed in pot Steam by water bath saturating, take out, dry;
(3) Wild Chrysanthemum, the capsule of weeping forsythia, Scabrous Mosla Herb, Asian puccoon, Radix Angelicae Sinensis are cleaned removal of impurities, segment, put into frying pan, after slow fire stir-fries 12 minutes, take out, dry in the air cool, pulverized 60 mesh sieves together with step (1) (2) made raw material, then drop into supercritical CO
2in the extraction kettle of abstraction instrument, at pressure 25MPa, temperature 60 C, CO
2flow is 0.3m
3extract 3 hours under the condition of/h, obtain volatile oil 1;
(4) made for step (3) volatile oil 1 is joined in rose hip oil, stir evenly, then German chamomile essential oil, Herba Lysimachiae foenumgraeci quintessence oil, VE, tea tree ethereal oil (mass ratio of volatile oil 1, German chamomile essential oil, Herba Lysimachiae foenumgraeci quintessence oil, VE, tea tree ethereal oil and rose hip oil is 0.3:0.4:0.7:0.4:0.8:3.0) is added successively, limit edged stirs, and mixes rear stopping and stirring, leave standstill 1 hour, centrifugal 10 minutes, rotating speed 3000r/min, gets supernatant liquor, obtains compound tea tree ethereal oil.
embodiment 2there is the compound tea tree ethereal oil of sterilization and disinfection effect, be prepared from (every part of 10g) primarily of following raw materials according: Wild Chrysanthemum 12 parts, the capsule of weeping forsythia 16 parts, Scabrous Mosla Herb 9 parts, Asian puccoon 12 parts, Radix Angelicae Sinensis 15 parts, crotons 12 parts, Tree Peony Bark 10 parts, Germany's chamomile essential oil is (purchased from Qingdao Feng Ze Xin Jia commerce and trade limited liability company, specification 10ml, article No. AD21A01), Herba Lysimachiae foenumgraeci quintessence oil is (purchased from Lan Lan bio tech ltd, Qingdao, specification 30ml, commodity bar code 0701413813392), VE(is purchased from Jiahe, the Holy Land, Shandong biotechnology company limited, specification 1000 IU/g), rose hip oil is (purchased from Qingdao Feng Ze Xin Jia commerce and trade limited liability company, specification 100ml, article No. AK30I71), tea tree ethereal oil is (purchased from Guangzhou Chang Ju trade Co., Ltd, specification 500ml, article No. CA007) in right amount each.
The preparation method with the compound tea tree ethereal oil of sterilization and disinfection effect is:
(1) get wheat bran to put into pot and heat, add clean crotons, stir-fry 16 minutes, add water and do not have crotons after smoldering, little fire decocted after 25 minutes, pulled out, and removing wheat bran, dries;
(2) get Tree Peony Bark removing impurity and residual core, mix thoroughly with the yellow rice wine of Tree Peony Bark quality 0.3 times, be then placed in pot Steam by water bath saturating, take out, dry;
(3) Wild Chrysanthemum, the capsule of weeping forsythia, Scabrous Mosla Herb, Asian puccoon, Radix Angelicae Sinensis are cleaned removal of impurities, segment, put into frying pan, after slow fire stir-fries 18 minutes, take out, dry in the air cool, pulverized 100 mesh sieves together with step (1) (2) made raw material, then drop into supercritical CO
2in the extraction kettle of abstraction instrument, at pressure 25MPa, temperature 60 C, CO
2flow is 0.3m
3extract 5 hours under the condition of/h, obtain volatile oil 1;
(4) made for step (3) volatile oil 1 is joined in rose hip oil, stir evenly, then German chamomile essential oil, Herba Lysimachiae foenumgraeci quintessence oil, VE, tea tree ethereal oil (mass ratio of volatile oil 1, German chamomile essential oil, Herba Lysimachiae foenumgraeci quintessence oil, VE, tea tree ethereal oil and rose hip oil is 0.7:0.8:1.1:0.9:1.2:4.4) is added successively, limit edged stirs, and mixes rear stopping and stirring, leave standstill 1 hour, centrifugal 16 minutes, rotating speed 3000r/min, gets supernatant liquor, obtains compound tea tree ethereal oil.
embodiment 3there is the compound tea tree ethereal oil of sterilization and disinfection effect, be prepared from (every part of 10g) primarily of following raw materials according: Wild Chrysanthemum 7 parts, the capsule of weeping forsythia 11 parts, Scabrous Mosla Herb 5 parts, Asian puccoon 9 parts, Radix Angelicae Sinensis 10 parts, crotons 9 parts, Tree Peony Bark 7 parts, Germany's chamomile essential oil is (purchased from Qingdao Feng Ze Xin Jia commerce and trade limited liability company, specification 10ml, article No. AD21A01), Herba Lysimachiae foenumgraeci quintessence oil is (purchased from Lan Lan bio tech ltd, Qingdao, specification 30ml, commodity bar code 0701413813392), VE(is purchased from Jiahe, the Holy Land, Shandong biotechnology company limited, specification 1000 IU/g), rose hip oil is (purchased from Qingdao Feng Ze Xin Jia commerce and trade limited liability company, specification 100ml, article No. AK30I71), tea tree ethereal oil is (purchased from Guangzhou Chang Ju trade Co., Ltd, specification 500ml, article No. CA007) in right amount each.
The preparation method with the compound tea tree ethereal oil of sterilization and disinfection effect is:
(1) get wheat bran to put into pot and heat, add clean crotons, stir-fry 12 minutes, add water and do not have crotons after smoldering, little fire decocted after 17 minutes, pulled out, and removing wheat bran, dries;
(2) get Tree Peony Bark removing impurity and residual core, mix thoroughly with the yellow rice wine of Tree Peony Bark quality 0.3 times, be then placed in pot Steam by water bath saturating, take out, dry;
(3) Wild Chrysanthemum, the capsule of weeping forsythia, Scabrous Mosla Herb, Asian puccoon, Radix Angelicae Sinensis are cleaned removal of impurities, segment, put into frying pan, after slow fire stir-fries 14 minutes, take out, dry in the air cool, pulverized 70 mesh sieves together with step (1) (2) made raw material, then drop into supercritical CO
2in the extraction kettle of abstraction instrument, at pressure 25MPa, temperature 60 C, CO
2flow is 0.3m
3extract 3.5 hours under the condition of/h, obtain volatile oil 1;
(4) made for step (3) volatile oil 1 is joined in rose hip oil, stir evenly, then German chamomile essential oil, Herba Lysimachiae foenumgraeci quintessence oil, VE, tea tree ethereal oil (mass ratio of volatile oil 1, German chamomile essential oil, Herba Lysimachiae foenumgraeci quintessence oil, VE, tea tree ethereal oil and rose hip oil is 0.4:0.5:0.8:0.5:0.9:3.4) is added successively, limit edged stirs, and mixes rear stopping and stirring, leave standstill 1 hour, centrifugal 12 minutes, rotating speed 3000r/min, gets supernatant liquor, obtains compound tea tree ethereal oil.
embodiment 4there is the compound tea tree ethereal oil of sterilization and disinfection effect, be prepared from (every part of 10g) primarily of following raw materials according: Wild Chrysanthemum 10 parts, the capsule of weeping forsythia 14 parts, Scabrous Mosla Herb 8 parts, Asian puccoon 11 parts, Radix Angelicae Sinensis 14 parts, crotons 11 parts, Tree Peony Bark 8 parts, Germany's chamomile essential oil is (purchased from Qingdao Feng Ze Xin Jia commerce and trade limited liability company, specification 10ml, article No. AD21A01), Herba Lysimachiae foenumgraeci quintessence oil is (purchased from Lan Lan bio tech ltd, Qingdao, specification 30ml, commodity bar code 0701413813392), VE(is purchased from Jiahe, the Holy Land, Shandong biotechnology company limited, specification 1000 IU/g), rose hip oil is (purchased from Qingdao Feng Ze Xin Jia commerce and trade limited liability company, specification 100ml, article No. AK30I71), tea tree ethereal oil is (purchased from Guangzhou Chang Ju trade Co., Ltd, specification 500ml, article No. CA007) in right amount each.
The preparation method with the compound tea tree ethereal oil of sterilization and disinfection effect is:
(1) get wheat bran to put into pot and heat, add clean crotons, stir-fry 16 minutes, add water and do not have crotons after smoldering, little fire decocted after 23 minutes, pulled out, and removing wheat bran, dries;
(2) get Tree Peony Bark removing impurity and residual core, mix thoroughly with the yellow rice wine of Tree Peony Bark quality 0.3 times, be then placed in pot Steam by water bath saturating, take out, dry;
(3) Wild Chrysanthemum, the capsule of weeping forsythia, Scabrous Mosla Herb, Asian puccoon, Radix Angelicae Sinensis are cleaned removal of impurities, segment, put into frying pan, after slow fire stir-fries 16 minutes, take out, dry in the air cool, pulverized 90 mesh sieves together with step (1) (2) made raw material, then drop into supercritical CO
2in the extraction kettle of abstraction instrument, at pressure 25MPa, temperature 60 C, CO
2flow is 0.3m
3extract 4.5 hours under the condition of/h, obtain volatile oil 1;
(4) made for step (3) volatile oil 1 is joined in rose hip oil, stir evenly, then German chamomile essential oil, Herba Lysimachiae foenumgraeci quintessence oil, VE, tea tree ethereal oil (mass ratio of volatile oil 1, German chamomile essential oil, Herba Lysimachiae foenumgraeci quintessence oil, VE, tea tree ethereal oil and rose hip oil is 0.6:0.7:1.0:0.8:1.1:4.0) is added successively, limit edged stirs, and mixes rear stopping and stirring, leave standstill 1 hour, centrifugal 14 minutes, rotating speed 3000r/min, gets supernatant liquor, obtains compound tea tree ethereal oil.
Typical case: xxx, man, 10 years old.Play when running, accidentally fall, two knee epidermis galls, and bleeds, be afraid of head of a family's punishment, oneself to irrigate surperficial earth with clear water, has then smeared the compound tea tree ethereal oil that the present embodiment gained has sterilization and disinfection effect, wound pain is alleviated, and wound healing after four days, the surface of a wound does not infect.
embodiment 5there is the compound tea tree ethereal oil of sterilization and disinfection effect, be prepared from (every part of 10g) primarily of following raw materials according: Wild Chrysanthemum 8.5 parts, the capsule of weeping forsythia 12.5 parts, Scabrous Mosla Herb 6.5 parts, Asian puccoon 10 parts, Radix Angelicae Sinensis 12 parts, crotons 10 parts, Tree Peony Bark 7.5 parts, Germany's chamomile essential oil is (purchased from Qingdao Feng Ze Xin Jia commerce and trade limited liability company, specification 10ml, article No. AD21A01), Herba Lysimachiae foenumgraeci quintessence oil is (purchased from Lan Lan bio tech ltd, Qingdao, specification 30ml, commodity bar code 0701413813392), VE(is purchased from Jiahe, the Holy Land, Shandong biotechnology company limited, specification 1000 IU/g), rose hip oil is (purchased from Qingdao Feng Ze Xin Jia commerce and trade limited liability company, specification 100ml, article No. AK30I71), tea tree ethereal oil is (purchased from Guangzhou Chang Ju trade Co., Ltd, specification 500ml, article No. CA007) in right amount each.
The preparation method with the compound tea tree ethereal oil of sterilization and disinfection effect is:
(1) get wheat bran to put into pot and heat, add clean crotons, stir-fry 14 minutes, add water and do not have crotons after smoldering, little fire decocted after 20 minutes, pulled out, and removing wheat bran, dries;
(2) get Tree Peony Bark removing impurity and residual core, mix thoroughly with the yellow rice wine of Tree Peony Bark quality 0.3 times, be then placed in pot Steam by water bath saturating, take out, dry;
(3) Wild Chrysanthemum, the capsule of weeping forsythia, Scabrous Mosla Herb, Asian puccoon, Radix Angelicae Sinensis are cleaned removal of impurities, segment, put into frying pan, after slow fire stir-fries 15 minutes, take out, dry in the air cool, pulverized 80 mesh sieves together with step (1) (2) made raw material, then drop into supercritical CO
2in the extraction kettle of abstraction instrument, at pressure 25MPa, temperature 60 C, CO
2flow is 0.3m
3extract 4 hours under the condition of/h, obtain volatile oil 1;
(4) made for step (3) volatile oil 1 is joined in rose hip oil, stir evenly, then German chamomile essential oil, Herba Lysimachiae foenumgraeci quintessence oil, VE, tea tree ethereal oil (mass ratio of volatile oil 1, German chamomile essential oil, Herba Lysimachiae foenumgraeci quintessence oil, VE, tea tree ethereal oil and rose hip oil is 0.5:0.6:0.9:0.65:1.0:3.7) is added successively, limit edged stirs, and mixes rear stopping and stirring, leave standstill 1 hour, centrifugal 13 minutes, rotating speed 3000r/min, gets supernatant liquor, obtains compound tea tree ethereal oil.
The pharmacology of the present invention's main Chinese medicine material used is as follows:
Wild Chrysanthemum: base is former: be the head inflorescence of feverfew mother chrysanthemum, HERBA CHRYSANTHEMI LAVANDULAEFOLII or lavandulaleaf dendranthema herb.Nature and flavor: bitter, pungent, are slightly cold.Gui Jing: return liver, the heart channel of Hang-Shaoyin.Function cures mainly: clearing heat and detoxicating.Swell for furunculosis carbuncle, conjunctival congestion with pain and swelling of the eye, has a headache dizzy.
The capsule of weeping forsythia: base is former: be the fruit of the Oleaceae plants capsule of weeping forsythia.Nature and flavor: bitter, are slightly cold.Gui Jing: return lung, the heart, small intestinl channel.Function cures mainly: clearing heat and detoxicating, dispersing swelling and dissipating binds.For ulcer, scrofula, acute mastitis, erysipelas, common cold due to wind-heat, warm disease from the beginning of, warmly join the army, high hot polydipsia, coma sends out spot, and heat drenches renal shutdown.
Scabrous Mosla Herb: base is former: be the herb of Labiatae Scabrous Mosla Herb platymiscium Scabrous Mosla Herb.Nature and flavor: pungent, bitter, cool.Function cures mainly: expelling wind and removing dampness wind, summer heat clearing toxin resolving.Cure mainly cold headache, cough, hot summer weather, hot miliaria, rubella, eczema, the ringworm of the foot, enteritis, dysentery, She Chong bites, hemorrhoid blood, metrorrhagia.
Asian puccoon: base is former: be the root of comfrey Asian puccoon, the false Asian puccoon in Xinjiang-Tibet or Onosma paniculatum.Nature and flavor: sweet, salty, cold.Gui Jing: the thoughts of returning home, Liver Channel.Function cures mainly: cool blood, invigorates blood circulation, removing toxic substances promoting eruption.Contain for blood-head poison, macula purple is black, measles without adequate eruption, sore, eczema, burn due to hot liquid or fire.
Radix Angelicae Sinensis: base is former: be the root of umbelliferae angelica.Nature and flavor: sweet, acrid, warm.Gui Jing: return liver, the heart, the spleen channel.Function cures mainly: enrich blood and invigorate blood circulation, and menstruction regulating and pain relieving relaxes bowel.Sallow for the deficiency of blood, dizzy palpitaition, menoxenia, through closing dysmenorrhoea, asthenia cold abdominalgia, the dry constipation of intestines, rheumatic arthralgia, injury from falling down, ulcer sores.Radix Angelicae Sinensis (processed with wine) promoting blood circulation to restore menstrual flow.For through closing dysmenorrhoea, rheumatic arthralgia, injury from falling down.
Crotons: base is former: be the seed of euphorbia plant crotons.Nature and flavor: seed: pungent, heat; Very toxic.Root, leaf: pungent, warm.Poisonous.Gui Jing: seed: return stomach, large intestine channel.Function cures mainly: seed: dispel under rushing down long-pending, detumescence of relieving oedema or abdominal distension through diuresis or purgation.For cold long-pending stagnation, distension and fullness of the chest and abdomen; External application erosion blister.For disliking sore mange, wart mole, diphtheria, malaria, intestinal obstruction.Root: warming spleen and stomach for dispelling cold, dispelling, collateral-activating.For rheumatic arthritis, treating swelling and pain by traumatic injury, venomous snake bite.Leaf: external application treating chilblain, and can infanticide Jue, fly maggot.
Tree Peony Bark: base is former: be the root skin of ranunculaceae peony.Nature and flavor: bitter, pungent, are slightly cold.Gui Jing: the thoughts of returning home, liver, kidney channel.Function cures mainly: clearing heat and cooling blood, promoting blood circulation and removing blood stasis.For maculae caused by violent heat pathogen, hematemesis and epistaxis, night fever abating at dawn, lossless hectic fever due to yin, through closing dysmenorrhoea, carbuncle sore tumefacting virus, falls and flutters the pain of injury.
Germany Flos Matricariae chamomillae: distribute the faint scent as straw, color blackish green, moderate tack.Effect: make calmly, relax, clear smooth respiratory system, can maintenance sensitivity, redness, eczema, pimples skin.Ant insect bite wound can also be treated.Can to releive headache, gastritis, diarrhoea, with myalgia, dysmenorrhoea, toothache etc., also to have good effectiveness for liver, anaemia and immunity system problem.
Herba Lysimachiae foenumgraeci quintessence oil: effect: clearing heat and detoxicating, cleaning skin, controls oil content, freckle removing and whitening, the tender skin of anti-wrinkle, eye haustra-dsipelling, promotes that damaged tissue regeneration recovery waits skin-protecting function, stimulates circulation, strengthening immunity and function vigor.
Rose hip oil: deep yellow or filbert, light bitter taste.Main component is made up of a-linolic acid and linolenic acid.Effect: enhanced tissue effect, produces active function of organization, easily permeates skin corium, moisturizing, promotes effect of the smooth whitening of skin.To cell regeneration, maintenance and healing have splendid effect.It can make skin pigment desalinate, and reappears homogeneous hue, makes skin level and smooth.It can keep skin clean, soft, soft, moistening, deflation, solid, the effect of high resilience, Feng Li.
VE (vitamin-E): have another name called tocopherol, delays cell aging because of oxidation, oxygen in donor, and vitamin A one works, and resists topsoil, protection lungs; Prevent blood coagulation; Lessen fatigue; Be externally applied agent (can pass through skin to be absorbed) and the medicine for oral administration of locality wound, all can prevent scar; Accelerate the rehabilitation of burning; With diuretic(s) be used for reduce blood pressure; Prevent miscarriage; Contribute to alleviating the situation had a cramp in the leg with charley horse; Reduce the chance suffering from ischemic heart disease.
Tea tree ethereal oil: smell is pungent and pungent, color is very light, viscosity as water quality.Topmost chemical composition is ethene, Dipentine, Limonene, cineol, sesame oil brain, anisoxide.Have bactericidal antiphlogistic, convergence pore, treatment Common Cold, cough, rhinitis, asthma, improve dysmenorrhoea, menoxenia and genital infection.Be applicable to oiliness and acne-prone skin, treatment suppurative wound and burn, tan severely, tinea pedis and dandruff.Also can clear the head, rejuvenate, anti-dejected.
test example 1for checking gained of the present invention has the disinfection effect of the compound tea tree ethereal oil (embodiment 5) of sterilization and disinfection effect, We conducted the mensuration of bacteriostatic activity:
Test materials: bacterial strain: streptococcus aureus, subtilis, bacillus coli, Pseudomonas aeruginosa, Salmonella typhimurium, bacterial strain is purchased from Institute of Microorganism, Academia Sinica.Reagent agent: products obtained therefrom of the present invention and potassium sorbate.
Test method: 1, the mensuration of inhibition zone adopts agar diffusion method, and every plate adds 0.1ml bacterium liquid, and (bacterial concentration is 1.0 × 10
5cfu/ml), coat whole media surface, 30 DEG C, adsorb 30 minutes.Then the aseptic stainless steel Oxford cup that 4 diameters are about 6mm is evenly placed above, then in hole, add with liquid-transfering gun the reagent agent 200 μ l that concentration is 10mg/L, at 30 DEG C after constant temperature culture 24h, the diameter of survey record inhibition zone, each process repetition 3 times, averages.Products obtained therefrom treatment group of the present invention is experimental group, and potassium sorbate treatment group is control group.
2, the mensuration of minimum inhibitory concentration adopts tube dilution method, get 11 test tubes, respectively add 1ml broth culture, then add the reagent agent solution 1ml of the 1-10mg/L for preparing totally 10 series concentration respectively, 11st test tube is as blank group, in each pipe, add the bacterium liquid 0.1ml of corrected concentrations again, mixing, at placing 30 DEG C, constant temperature culture 24h, observe statistics, each process repeats 3 times, averages.Products obtained therefrom treatment group of the present invention is experimental group, and potassium sorbate treatment group is control group.
Test-results: the bacteriostatic activity of experimental group and control group is in table 1, therefrom known, under same treatment concentration (10mg/L), experimental group and control group all have certain restraining effect to for examination bacterium.Record the display of two groups of minimum inhibitory concentration results (seeing table 2), experimental group to the minimum inhibitory concentration of streptococcus aureus, subtilis, bacillus coli, Pseudomonas aeruginosa and Salmonella typhimurium all lower than control group.Illustrate that the virulence of products made thereby of the present invention to these five kinds of bacteriums is better than potassium sorbate.
a table 1 liang group bacteriostatic activity compares (
± s)
Table 2 liang group minimum inhibitory concentration
The present invention selects there is clearing heat and detoxicating Wild Chrysanthemum, the capsule of weeping forsythia of dispersing swelling and dissipating binds, detoxify the Scabrous Mosla Herb of clear heat, the Asian puccoon of cooling and activating blood, the Radix Angelicae Sinensis of menstruction regulating and pain relieving, relieve oedema or abdominal distension through diuresis or purgation detumescence crotons, the Tree Peony Bark of clearing heat and cooling blood, alleviate the chamomile essential oil of headache, the Herba Lysimachiae foenumgraeci quintessence oil of cleaning skin, the rose hip oil of enhanced tissue, oxidation resistant VE, the tea tree ethereal oil of bactericidal antiphlogistic, Chinese medicine material extract and essential oil reasonably combined, not only safety, non-stimulated, the sterilization and disinfection that also can give full play to wherein activeconstituents is active, protection human body is from bacterium, the infringement of virus, enhancing body immunizing power, be worthy to be popularized.
It should be pointed out that embodiment is the more representational example of the present invention, obvious technical scheme of the present invention is not limited to above-described embodiment, can also have a lot of distortion.Those of ordinary skill in the art, with the present invention clear and definite disclosed or according to undoubted the obtaining of the written description of file, the claimed scope of this patent all should be thought.
Claims (10)
1. there is the compound tea tree ethereal oil of sterilization and disinfection effect, it is characterized in that, be prepared from primarily of following raw materials according, be mass parts: Wild Chrysanthemum 5-12, capsule of weeping forsythia 9-16 Scabrous Mosla Herb 4-9, Asian puccoon 8-12, Radix Angelicae Sinensis 9-15, crotons 8-12, Tree Peony Bark 5-10, German chamomile essential oil, Herba Lysimachiae foenumgraeci quintessence oil, VE, rose hip oil, tea tree ethereal oil are in right amount each.
2. there is the compound tea tree ethereal oil of sterilization and disinfection effect as claimed in claim 1, it is characterized in that, Wild Chrysanthemum 7-10, capsule of weeping forsythia 11-14, Scabrous Mosla Herb 5-8, Asian puccoon 9-11, Radix Angelicae Sinensis 10-14, crotons 9-11, Tree Peony Bark 7-8, German chamomile essential oil, Herba Lysimachiae foenumgraeci quintessence oil, VE, rose hip oil, tea tree ethereal oil are in right amount each.
3. there is the compound tea tree ethereal oil of sterilization and disinfection effect as claimed in claim 1, it is characterized in that, Wild Chrysanthemum 8.5, the capsule of weeping forsythia 12.5; Scabrous Mosla Herb 6.5, Asian puccoon 10, Radix Angelicae Sinensis 12, crotons 10, Tree Peony Bark 7.5, German chamomile essential oil, Herba Lysimachiae foenumgraeci quintessence oil, VE, rose hip oil, tea tree ethereal oil are in right amount each.
4. the preparation method with the compound tea tree ethereal oil of sterilization and disinfection effect as described in as arbitrary in claim 1-3, it is characterized in that, step is:
(1) get wheat bran to put into pot and heat, add clean crotons after smoldering, stir-fry 12-16 minute (preferred, to stir-fry 14 minutes), adds water and no crotons, after little fire decocts, pull out, remove wheat bran, dry;
(2) get Tree Peony Bark removing impurity and residual core, mix thoroughly with the yellow rice wine of Tree Peony Bark quality 0.3 times, be then placed in pot Steam by water bath saturating, take out, dry;
(3) Wild Chrysanthemum, the capsule of weeping forsythia, Scabrous Mosla Herb, Asian puccoon, Radix Angelicae Sinensis are cleaned removal of impurities, segment, put into frying pan, after slow fire stir-fries, take out, dry in the air cool, pulverize and sieve together with step (1) (2) made raw material, then drop into supercritical CO
2in the extraction kettle of abstraction instrument, at pressure 25MPa, temperature 60 C, CO
2flow is 0.3m
3extract under the condition of/h, obtain volatile oil 1;
(4) made for step (3) volatile oil 1 is joined in rose hip oil, stir evenly, then German chamomile essential oil, Herba Lysimachiae foenumgraeci quintessence oil, VE, tea tree ethereal oil is added successively, limit edged stirs, and mixes rear stopping and stirring, leave standstill 1 hour, centrifugal, rotating speed 3000r/min, gets supernatant liquor, obtains compound tea tree ethereal oil.
5. have the preparation method of the compound tea tree ethereal oil of sterilization and disinfection effect as claimed in claim 4, it is characterized in that, the little fire of step (1) decocts 15-25 minute, and (preferred, little fire decocts 17-23 minute; Be more preferably, little fire decocts 20 minutes).
6. have the preparation method of the compound tea tree ethereal oil of sterilization and disinfection effect as claimed in claim 4, it is characterized in that, step (3) slow fire stir-fries, and within 12-18 minute, (preferred, slow fire stir-fries 14-16 minute; Be more preferably, slow fire stir-fries 15 minutes).
7. have the preparation method of the compound tea tree ethereal oil of sterilization and disinfection effect as claimed in claim 4, it is characterized in that, step (3) was pulverized 60-100 mesh sieve and (preferably, was pulverized 70-90 mesh sieve; Be more preferably, pulverized 80 mesh sieves).
8. have the preparation method of the compound tea tree ethereal oil of sterilization and disinfection effect as claimed in claim 4, it is characterized in that, step (3) extraction time is 3-5 hour (preferably, extraction 3.5-4.5 hour; Be more preferably, extract 4 hours).
9. there is the preparation method of the compound tea tree ethereal oil of sterilization and disinfection effect as claimed in claim 4, it is characterized in that, step (4) centrifugal 10-16 minute (preferred, centrifugal 12-14 minute; Be more preferably, centrifugal 13 minutes).
10. there is the preparation method of the compound tea tree ethereal oil of sterilization and disinfection effect as claimed in claim 4, it is characterized in that, volatile oil 1 in step (4), Germany's chamomile essential oil, Herba Lysimachiae foenumgraeci quintessence oil, VE, the mass ratio of tea tree ethereal oil and rose hip oil is (0.3-0.7): (0.4-0.8): (0.7-1.1): (0.4-0.9): (0.8-1.2): (3.0-4.4) is (preferred, volatile oil 1, Germany's chamomile essential oil, Herba Lysimachiae foenumgraeci quintessence oil, VE, the mass ratio of tea tree ethereal oil and rose hip oil is (0.4-0.6): (0.5-0.7): (0.8-1.0): (0.5-0.8): (0.9-1.1): (3.4-4.0), be more preferably, the mass ratio of volatile oil 1, German chamomile essential oil, Herba Lysimachiae foenumgraeci quintessence oil, VE, tea tree ethereal oil and rose hip oil is 0.5:0.6:0.9:0.65:1.0:3.7).
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105567431A (en) * | 2016-01-15 | 2016-05-11 | 广东净霸科技有限公司 | Plant essential oil for clearing away heat and toxic materials and preparation method thereof |
| CN106214578A (en) * | 2016-08-31 | 2016-12-14 | 安徽省东至茶树良种繁殖示范场 | A kind of compound recipe tea tree ethereal oil with skin-care effect |
| CN108264972A (en) * | 2016-12-30 | 2018-07-10 | 北京绿伞化学股份有限公司 | A kind of tea tree ethereal oil concentrated detergent China liquid and preparation method thereof |
| CN109247343A (en) * | 2018-11-20 | 2019-01-22 | 娇时日化（杭州）股份有限公司 | A kind of thimerosal and preparation method thereof containing tea tree ethereal oil |
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Citations (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1703959A (en) * | 2004-05-31 | 2005-12-07 | 汕头市双骏生物工程有限公司 | Preparation capable of killing virus and bacteria and its preparation process |
| CN101199690A (en) * | 2007-12-21 | 2008-06-18 | 北京中科雍和医药技术有限公司 | Compound essential oil of releasing skin pruritus |
| CN101352235A (en) * | 2008-08-21 | 2009-01-28 | 许向梅 | Plant essential oil capsules and preparation method thereof |
| CN101428080A (en) * | 2008-12-10 | 2009-05-13 | 黄杰 | Health care essential oil of magnolia flower |
| KR20100082755A (en) * | 2010-06-25 | 2010-07-19 | 이경현 | Natural plant oil composition containing rose oil and jasmine oil for relieving menstrual pains and vaginal discharge symptom |
| CN102239893A (en) * | 2011-05-04 | 2011-11-16 | 云南同方科技有限公司 | Plant essential oil bactericidal disinfectant |
| CN102349991A (en) * | 2011-05-29 | 2012-02-15 | 王红芳 | Composition for killing virus and preventing influenza and cold prevention plaster prepared by composition |
| CN102512490A (en) * | 2012-01-10 | 2012-06-27 | 唐嗣信 | Aromatherapy essential oil for treating gynecological inflammation and essential oil aromatherapy patch |
| CN103478177A (en) * | 2013-09-05 | 2014-01-01 | 杨振生 | Air disinfectant |
| CN104255835A (en) * | 2014-08-29 | 2015-01-07 | 成都顺发消洗科技有限公司 | Indoor disinfectant and preparation method thereof |
-
2015
- 2015-04-07 CN CN201510159682.5A patent/CN104762136A/en active Pending
Patent Citations (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1703959A (en) * | 2004-05-31 | 2005-12-07 | 汕头市双骏生物工程有限公司 | Preparation capable of killing virus and bacteria and its preparation process |
| CN101199690A (en) * | 2007-12-21 | 2008-06-18 | 北京中科雍和医药技术有限公司 | Compound essential oil of releasing skin pruritus |
| CN101352235A (en) * | 2008-08-21 | 2009-01-28 | 许向梅 | Plant essential oil capsules and preparation method thereof |
| CN101428080A (en) * | 2008-12-10 | 2009-05-13 | 黄杰 | Health care essential oil of magnolia flower |
| KR20100082755A (en) * | 2010-06-25 | 2010-07-19 | 이경현 | Natural plant oil composition containing rose oil and jasmine oil for relieving menstrual pains and vaginal discharge symptom |
| CN102239893A (en) * | 2011-05-04 | 2011-11-16 | 云南同方科技有限公司 | Plant essential oil bactericidal disinfectant |
| CN102349991A (en) * | 2011-05-29 | 2012-02-15 | 王红芳 | Composition for killing virus and preventing influenza and cold prevention plaster prepared by composition |
| CN102512490A (en) * | 2012-01-10 | 2012-06-27 | 唐嗣信 | Aromatherapy essential oil for treating gynecological inflammation and essential oil aromatherapy patch |
| CN103478177A (en) * | 2013-09-05 | 2014-01-01 | 杨振生 | Air disinfectant |
| CN104255835A (en) * | 2014-08-29 | 2015-01-07 | 成都顺发消洗科技有限公司 | Indoor disinfectant and preparation method thereof |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105567431A (en) * | 2016-01-15 | 2016-05-11 | 广东净霸科技有限公司 | Plant essential oil for clearing away heat and toxic materials and preparation method thereof |
| CN106214578A (en) * | 2016-08-31 | 2016-12-14 | 安徽省东至茶树良种繁殖示范场 | A kind of compound recipe tea tree ethereal oil with skin-care effect |
| CN108264972A (en) * | 2016-12-30 | 2018-07-10 | 北京绿伞化学股份有限公司 | A kind of tea tree ethereal oil concentrated detergent China liquid and preparation method thereof |
| CN109247343A (en) * | 2018-11-20 | 2019-01-22 | 娇时日化（杭州）股份有限公司 | A kind of thimerosal and preparation method thereof containing tea tree ethereal oil |
| CN110352988A (en) * | 2019-07-31 | 2019-10-22 | 西藏阿木达草本科技有限公司 | A kind of plant type air bacteriostatic agent and preparation method |
| CN112494578A (en) * | 2020-12-16 | 2021-03-16 | 广州源美生物科技发展有限公司 | Chamomile fermentation liquor antibacterial gel and preparation method thereof |
| CN116870082A (en) * | 2023-08-29 | 2023-10-13 | 蓝音(兰州)生物科技有限公司 | Chinese angelica essential oil for repairing facial acne and compound essential oil containing same |
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