CN103451032A - Safe and environment-friendly tea seed washing powder and preparation method thereof - Google Patents
Safe and environment-friendly tea seed washing powder and preparation method thereof Download PDFInfo
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Abstract
The invention discloses safe and environment-friendly tea seed washing powder and a preparation method thereof. The preparation method comprises the following steps: step 1, taking raw materials, namely, weighing the following raw materials in parts by mass: 60-70 parts of camellia seed, 15-30 parts of Chinese honey locust, 5-10 parts of cacumen biotae, 0.5-3 parts of cortex albiziae, 0.5-3 parts of pomegranate bark and 0.5-2.5 parts of natural borneol; step 2, crushing, namely, respectively crushing the weighed raw materials by using a crusher so as to obtain raw material powder; step 3, mixing, namely, mixing the raw material powder, and uniformly stirring the raw material powder; step 4, sterilizing, namely, sterilizing through ultraviolet ray or microwave, and further sealing and packaging so as to obtain the safe and environment-friendly tea seed washing powder. The safe and environment-friendly tea seed washing powder is high in active substance content, good in detergency, good in sterilizing effect, non-toxic, non-irritating, anti-anaphylaxis, low in foam and water-saving, so that the powder can be used as a safe and environment-friendly washing product which is ideal for washing food, utensils, tableware, vegetables and fruits in daily life of people.
Description
Technical field
The present invention relates to a kind of articles for washing and preparation method thereof, a kind of safety and environmental protection tea seed detergent powder and preparation method thereof particularly, it is mainly used in people's daily life washing, and its raw material is green plants, without any chemical industry composition, safety, environmental protection.
Background technology
Tea seed is after squeezing, extract technology extract, and residual bits, be referred to as camellia seed meal, and it contains 10% protein, 10% tea polysaccharide, 12% tea saponin, 50% Mierocrystalline cellulose and xylogen.
Gleditsia officinalis, have another name called the Chinese honey locust tree, is one of China distinctive Caesalpiniaceae Gleditsia seeds.Its Chinese honey locust of tying is rich in triterpene soap formula, the triterpenoid saponin more than 15%.
Tea saponin has another name called TS, belong to triterpene compound with triterpene soap formula, triterpenoid saponin, all a kind of pure natural nonionic surface active agent, there is emulsification, dispersion, wetting, decontamination, foaming, surely steep ability, and not affected by water hardness, also there are pathogenic bacterium in the Grain-negative intestines such as antibacterial and anti-inflammation functions, particularly intestinal bacteria, bacterium sonnei, Bacillus proteus, Corynebacterium diphtheriae, paratyphosum Bacterium, Pseudomonas aeruginosa, vibrio cholerae restraining effect is all arranged.People also have the tea oil cake that will contain tea saponin directly to use as washing product, although it is directly used and have certain washing functions as washing product, still there is the shortcoming that detergency is strong, antisepsis and anti-inflammation power is strong, active matter content is not high in it.
Existing cleaning product is mainly chemosynthesis in the market, although its detergency is strong, but there is chemical reagent in it, insecurity, the stimulation of life-time service to skin, cause pachylosis dry and cracked, clean not exclusively, residually cause endangering health, simultaneously because being difficult for decomposition, quite serious to the pollution of ambient soil and water body.
Summary of the invention
The objective of the invention is to overcome the above-mentioned deficiency of prior art and a kind of safety and environmental protection tea seed detergent powder is provided, its active matter content is high, detergent power good, sterilization effect is good, nontoxicity, nonirritant, without supersensitivity, low bubble, water-saving, can be used as the desirable safety and environmental protection washing products such as cleaning food Work tool, tableware and vegetables, fruit in people's daily life.
Another object of the present invention is to provide the preparation method of above-mentioned safety and environmental protection tea seed detergent powder, and its technique is simple, and raw material is common, cheap.
Technical scheme of the present invention is: a kind of safety and environmental protection tea seed detergent powder, it is to be made by the raw material of following proportion by weight: 60～70 parts of camellia seed meals, 15～30 parts, Chinese honey locust, 5～10 parts of Leafy twigs of Oriental Arborvitae, 0.5～3 part of Silktree Albizzia Bark, 0.5～3 part of pomegranate rind, 0.5～2.5 part of natural Broneolum Syntheticum.
The further preferred mass part of the present invention proportioning is: 60～67.5 parts of camellia seed meals, 15～26.3 parts, Chinese honey locust, 5～8.8 parts of Leafy twigs of Oriental Arborvitae, 0.5～2.4 part of Silktree Albizzia Bark, 0.5～2.4 part of pomegranate rind, 0.5～2 part of natural Broneolum Syntheticum.
The present invention further preferred mass part proportioning is: 62.5～70 parts of camellia seed meals, 18.8～30 parts, Chinese honey locust, 6.3～10 parts of Leafy twigs of Oriental Arborvitae, 1.2～3 parts of Silktree Albizzia Barks, 1.1～3 parts of pomegranate rinds, 1～2.5 part of natural Broneolum Syntheticum.
The present invention further preferred mass part proportioning is: 62.5～67.5 parts of camellia seed meals, 18.8～26.3 parts, Chinese honey locust, 6.3～8.8 parts of Leafy twigs of Oriental Arborvitae, 1.2～2.4 parts of Silktree Albizzia Barks, 1.1～2.4 parts of pomegranate rinds, 1～2 part of natural Broneolum Syntheticum.
The present invention also further preferred mass part proportioning is: 65 parts of camellia seed meals, 22.5 parts, Chinese honey locust, 7.5 parts of Leafy twigs of Oriental Arborvitae, 1.8 parts of Silktree Albizzia Barks, 1.7 parts of pomegranate rinds, 1.5 parts of natural Broneolum Syntheticums.
Another technical scheme of the present invention is: a kind of preparation method of safety and environmental protection tea seed detergent powder, it comprises the steps:
One, get raw material
Take raw material by following proportion by weight: 60～70 parts of camellia seed meals, 15～30 parts, Chinese honey locust, 5～10 parts of Leafy twigs of Oriental Arborvitae, 0.5～3 part of Silktree Albizzia Bark, 0.5～3 part of pomegranate rind, 0.5～2.5 part of natural Broneolum Syntheticum;
Two, pulverize
To obtain raw material and be pulverized by pulverizer respectively, obtain each raw material powder;
Three, mix
Each raw material powder is mixed, stir, obtain safety and environmental protection tea seed detergent powder.
The present invention further another technical scheme is: the raw material particle size after second step is pulverized is for crossing 40～50 mesh sieves.
The present invention further another technical scheme is: raw material preferred mass part proportioning that the first step takes is: 62.5～67.5 parts of camellia seed meals, 18.8～26.3 parts, Chinese honey locust, 6.3～8.8 parts of Leafy twigs of Oriental Arborvitae, 1.2～2.4 parts of Silktree Albizzia Barks, 1.1～2.4 parts of pomegranate rinds, 1～2 part of natural Broneolum Syntheticum.
The present invention further another technical scheme is: raw material preferred mass part proportioning that the first step takes is: 65 parts of camellia seed meals, 22.5 parts, Chinese honey locust, 7.5 parts of Leafy twigs of Oriental Arborvitae, 1.8 parts of Silktree Albizzia Barks, 1.7 parts of pomegranate rinds, 1.5 parts of natural Broneolum Syntheticums.
Also further another technical scheme of the present invention is: it also comprises step:
Four, sterilization
The safety and environmental protection tea seed detergent powder that the 3rd step is obtained is by ultraviolet ray or microwave disinfection, then packs.
Main symbol and name resolving that the present invention uses are as follows:
～: numerical range, for example 1～5 means 1 to 5.
The main raw material that the present invention uses is described as follows:
Camellia seed meal: camellia seed kernel is after squeezing, extract technology extract, and residual bits, be referred to as camellia seed meal, and it is containing having an appointment 10% protein, 10% tea polysaccharide, 12% tea saponin, 50% Mierocrystalline cellulose and xylogen.
Leafy twigs of Oriental Arborvitae: (formal name used at school: browse Platycladus orientalis (L.) Franco), the medicinal material Leafy twigs of Oriental Arborvitae has branch to Cupressaceae plant arbor-vitae more, little and different in size, is flakey.Color is sorrel.The visible leaf in surface is mutually to life, the section yellow-white.Quality is crisp, easily fractureed.The micro-perfume (or spice) of gas, a kind of in the blood-cooling hemostatic of bitter and puckery flavor Chinese medicine hemostatic drug, the effect that has hemostasis, black beard and hair, cough-relieving to breathe heavily.[medicine name] Leafy twigs of Oriental Arborvitae [another name] CedarLeaves, Japan cypress leaf, Cong Baiye.Branch and leaf that [medicinal material Ji Yuan] is Cupressaceae plant arbor-vitae.[section's genus] Cupressaceae.[nature and flavor] hardship; Puckery; Cold nature.[return through] lung; Liver; Large intestine channel.[effect] cooling blood for hemostasis; Cough-relieving apophlegmatic; Wind-damp dispelling; Loose pyogenic infections.[effect classification] blood-cooling hemostatic; Medicine for rheumatism.[curing mainly] controls spitting of blood; Spit blood; Bleeding from five sense organs or subcutaneous tissue; Hematuria; Bloody flux; Discharging fresh blood stool; Uterine bleeding is more than; Coughing with a lot of sputum; Rheumatic arthralgia; Erysipelas; Mumps, scald.[attention] " property of medicine opinion ": suitable with wine." book on Chinese herbal medicine is stated ": many foods also can fall stomach.Chemical composition: containing volatile oil, be mainly fenchone (fenchone), camphor, Bornyl acetate, terpene alcohol in oil; And containing juniperic acid (juniperic acid) Quercetin, poplar luteoxanthin (myricetin), kaempferol, hinokiflavone (hinokiflavone), wax etc.; In Leafy twigs of Oriental Arborvitae, containing volatile oil 0.26%, in oil, main component is α-thujone, thujene, fenchone etc.; Other is still containing flavones ingredient, as aromadendrin, Quercetin, myricetin, hinokiflavone etc.; Also contain the trace elements such as potassium, sodium, nitrogen, phosphorus, calcium, magnesium, manganese and zinc in leaf.Pharmacological action: the Leafy twigs of Oriental Arborvitae decoction can obviously shorten bleeding time and clotting time, and its hemostasis effective constituent is Quercetin and tannin.In addition, effects such as antibechic still being arranged, eliminate the phlegm, relieving asthma, be calm; Experiment in vitro shows, these product all have restraining effect to streptococcus aureus, micrococcus catarrhalis, dysentery bacterium, Corynebacterium diphtheriae, diphtheria corynebacterium etc.
Silktree Albizzia Bark: the dry bark for pulse family (Legumin0sae) plant silk tree is curling tubular or half tubular, long 40～80cm, thick Silktree Albizzia Bark 0.1～0.3cm.The outside surface taupe brown is to beige, and nature and flavor are sweet, flat.The merit that Xie Yu and blood, the peaceful heart, subduing inflammation are arranged.English name: Silktree Albizia Bark; Latin literary fame: Cortex Albiziae; Another name: close confused skin (Thousand Golden Prescriptions), CORTEX ALBIZIAE (" side of walking alone "), albizzia skin (" detailed outline ").The effect of Silktree Albizzia Bark: the bark that Silktree Albizzia Bark is the leguminous plants silk tree, Silktree Albizzia Bark another name closes confused skin, night platform skin, albizzia skin, Silktree Albizzia Bark has the Xie Yu that calms the nerves, the effect of carbuncle of disappearing of invigorating blood circulation, Silktree Albizzia Bark has the effect of confused and worried, melancholy, the egersis for the treatment of, inside and outside large carbuncle, wound, Peptic Ulcers and gastritis sufferer be careful takes Silktree Albizzia Bark, and wind-heat spontaneous perspiration, diseases caused by external factors egersis person prohibit and take Silktree Albizzia Bark.
Chinese honey locust: " Chinese medicine voluminous dictionary " record: Chinese honey locust, [different name] chicken son (" wide will) of dwelling }), Chinese honey locust (" Handbook of Prescriptions for Emergencies "), large Chinese honey locust (" prescriptions worth thousand gold "), long Chinese honey locust (" Bencao Tujing "), outstanding cutter (" outer red book on Chinese herbal medicine "), long Chinese honey locust (" side of directing at ").Fruit or sterile fruit that [base is former] is pulse family Gleditsia plant Chinese honey locust.The former claims Chinese honey locust, and the latter claims Fructus Gleditsiae Abnormalis.[processing of gathering] cultivates after 5～6 years is result, during autumn fruit maturation blackening, plucks, and dries.[pharmacology] be phlegm-dispelling functions 1., and this product can stimulate gastric mucosa containing saponin(e, causes that reflectingly the respiratory mucosa secretion increases.Belong to nauseous expectorant.2. anti-microbial effect, the Chinese honey locust preserved material has restraining effect to trichophyton, star-shaped nocardia and some dermatophytes in vitro.
Pomegranate rind: be the pericarp of Punicaceae plant pomegranate.Autumn, the pomegranate fruit maturation, plucked during the cracking of top, removes seed and reach every flesh, and valve cutting is dried, or low baking temperature is dried.Function cures mainly: puckery intestines, hemostasis, expelling parasite.Control for a long time and rush down, protracted dysentery, have blood in stool, prolapse of the anus, and involuntary emission, uterine bleeding, under band, abdominal pain due to worm stagnation, mange.
Natural Broneolum Syntheticum: another name: d-Bomeol, English name: BORNEOLUM, the fresh branch that this product is canella camphor tree Cinnamomumcamphora (L.) Presl, the crystallization that leaf is processed into through extraction, this product is containing d-Bomeol (C
10h
18o) must not be less than 95.0%.[nature and flavor] are hot, bitter, cool.[function with the cure mainly] inducing resuscitation of having one's ideas straightened out, clearing away heat to and alleviating pain.For pyreticosis coma, convulsion, faint, apoplexy coma due to blocking of the respiratory system, frightened epilepsy phlegm fan, larynx numbness dentalgia, aphtha large carbuncle, hot eyes.
" Chinese medicine voluminous dictionary ": " Chinese medicine voluminous dictionary " second edition is write by Nanjing University of Traditional Chinese Medicine, and Shanghai Century publishes limited-liability company and Shanghai science tech publishing house publishes and distributes.
Usage and dosage:
1. consumption.The aqueous solution that preparation concentration is about 0.117g/ml, can be for cleaning food Work tool, tableware and vegetables, fruit etc.
2. common usage.Approximately soup ladle safety and environmental protection tea of the present invention seed detergent powder adds slightly wetting mixing well of suitable quantity of water, then is stained with rag tablewares such as a bit cleaning dish, and then clear water washes down; Or directly be poured into water stirring, immersion, after washing with rag, then wash with Qing Shui Red; If, when dish is too oily, available safety and environmental protection tea seed detergent powder of the present invention is directly scrubbed, then clear water washes down.
The present invention compared with prior art has following features:
1. the safety and environmental protection tea seed detergent powder of the present invention of 0.117g/ml concentration is best detergency concentration, and the detersive power of the safety and environmental protection tea seed detergent powder of the present invention of same concentration is distilled water 1.4～2.5 times, for 1.3～1.7 times of camellia seed meal, the detergency of safety and environmental protection tea seed detergent powder of the present invention is than simple camellia seed meal much better than (detergency that also shows any one single raw material that the detergency of the safety and environmental protection tea seed detergent powder of the present embodiment adopts than it all is eager to excel) simultaneously, each feed composition of safety and environmental protection tea seed detergent powder of the present invention has been to have formed synergistic effect on detergency, detergency of the present invention is the mean value of not all component detergency not only, and the detergency higher than any component, be that the present invention has produced beyond thought detergent power.
2. safety and environmental protection tea seed detergent powder of the present invention is after use, it is pleasant, lubricated that hand is felt, the care of its any one single raw material that ratio adopts or other current chemical washing product is eager to excel (in using practice, testing crew has all confirmed this advantage, but not concrete index and the detection data of detecting).
Safety and environmental protection tea seed detergent powder of the present invention have advantages of that active matter content is high, detersive power good, nontoxic.
Safety and environmental protection tea seed detergent powder of the present invention to the antibacterial of Salmonella typhi, staphylococcus epidermidis, streptococcus aureus, beta hemolytic streptococcus with and germicidal action be better than camellia seed meal, that is to say that safety and environmental protection tea seed detergent powder of the present invention has improved germicidal action with respect to its main raw material camellia seed meal, safety and environmental protection tea seed detergent powder of the present invention is better as the washes disinfectant properties than using separately camellia seed meal.
5. safety and environmental protection tea seed detergent powder of the present invention is without obvious animal toxicity, harmless, safety.
6. safety and environmental protection tea seed detergent powder percutaneous drug delivery of the present invention, to complete normal skin and the equal nonirritant of damaged skin, environmental protection.
7. safety and environmental protection tea seed detergent powder of the present invention is without supersensitivity.
Safety and environmental protection tea seed detergent powder active matter content of the present invention is high in sum, detergent power good, sterilization effect good, nontoxicity, nonirritant, without supersensitivity, it adopts natural vegetation as raw material fully, not containing any Chemicals, the biological decomposition degree is high, low bubble, water-saving, hand is not hindered in washing, after washing, can not cause what pollution to environment yet, and soil is played to improving effect, can be used as safety and environmental protection washing product desirable in people's daily life and use.
In order to be illustrated more clearly in the present invention, enumerate following examples and detect test situation, but it to be without any restrictions to scope of invention.
Embodiment
embodiment 1
Get 65 kilograms of camellia seed meals, 22.5 kilograms, Chinese honey locust, 7.5 kilograms of Leafy twigs of Oriental Arborvitae, 1.8 kilograms of Silktree Albizzia Barks, 1.7 kilograms of pomegranate rinds, 1.5 kilograms of natural Broneolum Syntheticums;
To obtain raw material and be pulverized by pulverizer respectively, cross 40～50 mesh sieves, obtain each raw material powder;
Each raw material powder is put into to stirred pot, mix and blend, churning time is 20～40min, obtains mixing meal;
Gained mixing meal is packed after by ultraviolet or microwave disinfection, obtain safety and environmental protection tea seed detergent powder.
embodiment 2-12
As shown in Table 1 below, its preparation method is identical with embodiment 1 for the raw material that embodiment 2-12 is used and quality; Following table 1 shows concrete raw material and the quality that embodiment 1-12 is used.
Table 1
detect and test
The applicant delivers to by the safety and environmental protection tea seed detergent powder of various embodiments of the present invention detection and the test that special detection mechanism has carried out system, and it is as follows that it mainly detects test-results.
One. by the safety and environmental protection tea seed detergent powder of above each embodiment gained, by check active matter content, detergent power (GB 9985-2000 detection) etc., obtain the detected result shown in following table 2:
Table 2
From above table 2 can find out the safety and environmental protection tea seed detergent powder of various embodiments of the present invention have advantages of that active matter content is high, detersive power good, nontoxic.
Two. anti-microbial effect detects
1. antibacterial range detects (mensuration of inhibition zone diameter size)
Purpose: the utilization agar diffusion method detects the safety and environmental protection tea seed detergent powder (concentration is 0.5g/ml) of various embodiments of the present invention and camellia seed meal is wide to distributing in environment, resistibility is strong, can cause that the pathogenic bacterium of food spoilage, food poisoning, pyogenic infection have anti-microbial effect, clear and definite its antibacterial range.
Method: cut-off footpath 12cm plate, impouring substratum 15ml, the cotton swab with sterilizing after condensation dips the test organisms bacterium liquid for the logarithmic phase of specialized range density, is uniformly coated on media surface.Then be put in flat board with aseptic nipper gripping sterilizing Oxford cup, add safety and environmental protection tea seed detergent powder (concentration the is 0.5g/ml) 200ul of various embodiments of the present invention in each Oxford cup, and carry out three parallel tests.Take out after 24 hours of 37 ℃ of cultivations, survey inhibition zone diameter, and obtain the mean value of the inhibition zone diameter of three parallel tests.Adopt same method to carry out comparison and detection to camellia seed meal.
Result: see the following form shown in 3.
The comparison and detection result of table 3. antibacterial range (mm,
± s)
2. antibiotic degree detecting (MIC; The mensuration of MBC)
Purpose: the antibiotic degree of pathogenic bacterium that utilization liquid diluting method detects the safety and environmental protection tea seed detergent powder of various embodiments of the present invention and 8 above different concns points of camellia seed meal are wide to distributing in environment, resistibility is strong, can cause food spoilage, food poisoning, pyogenic infection, detect minimum inhibitory concentration (MIC) and minimum bactericidal concentration (MBC), clear and definite its antibiotic degree.
Method: get some of sterile test tube, after doubly diluting the safety and environmental protection tea seed detergent powder (concentration is 0.5g/ml) of various embodiments of the present invention with liquid nutrient medium etc., each pipe adds 0.1ml for examination bacterium liquid, establish substratum control tube and bacterium liquid control tube simultaneously, take out and see result after 37 ℃ of cultivation 24h, in the satisfactory situation of control tube, observe one by one each developmental tube, take can inhibition test the high dilution of safety and environmental protection tea seed detergent powder (concentration is 0.5g/ml) of various embodiments of the present invention of bacteria growing be minimum inhibitory concentration (MIC), and the culture in the test tube of each asepsis growth is forwarded on the agar plate of corresponding substratum, take out and see result after 37 ℃ of cultivation 24h, the high dilution of safety and environmental protection tea seed detergent powder (concentration is 0.5g/ml) of the various embodiments of the present invention of killing 99.9% test organisms thalline of take is minimum bactericidal concentration (MBC).Adopt same method to carry out comparison and detection to camellia seed meal.
Result: see the following form shown in 4.
The comparison and detection result (mg/mL) of the antibiotic degree of table 4.
Conclusion: can find out from table 3,4, the safety and environmental protection tea seed detergent powder of various embodiments of the present invention to the antibacterial of Salmonella typhi, staphylococcus epidermidis, streptococcus aureus, beta hemolytic streptococcus with and germicidal action be better than camellia seed meal, the safety and environmental protection tea seed detergent powder that is to say various embodiments of the present invention has improved germicidal action with respect to its main raw material camellia seed meal, and the safety and environmental protection tea seed detergent powder of various embodiments of the present invention is better as the washes disinfectant properties than using separately camellia seed meal.
Three. detergent action detects
Purpose: by preparing safety and environmental protection tea seed detergent powder solution of the present invention and the camellia seed meal solution of different concns, test its detergent power.
Method: with water extraction, prepare respectively concentration and be the extracting solution of the safety and environmental protection tea seed detergent powder of 0.117g/ml, concentration are 0.235g/ml, concentration is 0.47g/ml camellia seed meal and various embodiments of the present invention, by GB GB9985-2000 method, measure detergent power.
Result: see the following form shown in 5.
The comparison and detection result (N=6, %) of table 5. detergent action
Conclusion: as can be seen from Table 5, the detergency of the safety and environmental protection tea seed detergent powder 0.117g/ml concentration of various embodiments of the present invention is better than the detergency of 0.235g/ml concentration and the detergency of 0.47g/ml concentration, and the detergency of 0.117g/ml concentration is strong, and the detersive power of the safety and environmental protection tea seed detergent powder of each embodiment of same concentration is distilled water 1.4～2.5 times, for 1.3～1.7 times of camellia seed meal, the detergency of testing the safety and environmental protection tea seed detergent powder that also shows various embodiments of the present invention is more much better than than simple camellia seed meal, this each feed composition that absolutely proves the safety and environmental protection tea seed detergent powder of various embodiments of the present invention has been to have formed synergistic effect on detergency, the detergency of the safety and environmental protection tea seed detergent powder of various embodiments of the present invention is the mean value of not all component detergency not only, and the detergency higher than any component, if each component of the safety and environmental protection tea seed detergent powder of various embodiments of the present invention does not form collaborative de-sludging effect, the detergent power of each component mixture of so same quality can be lower than the detergent power of the camellia seed meal of the same quality of high detergent power in each component, be that the present invention has produced beyond thought detergent power.
Four. animal toxicity test
Purpose: observe rabbit intact skin and damaged skin and contact in a short time the toxic reaction produced after tested material (the safety and environmental protection tea seed detergent powders of various embodiments of the present invention), so that the security foundation to be provided.
Method: select 12 of white new zealand rabbits, be divided at random 3 groups, 4 every group.A group: intact skin group, B group: damaged skin group, C group: blank group.The test position is skin of back, control group is to distilled water, the tested material group is to the safety and environmental protection tea seed detergent powder of various embodiments of the present invention, directly be coated on intact skin and damaged skin, Tu Houfu is with polyethylene film, then gauze is fixed, guarantee itself and skin contact 24 hours, be coated with examination after 24 hours, as be not poisoned to death, available warm water or other nonirritant solvents go tested material.Continuous Observation 7 days, observe and record whole body poisoning manifestations and death condition to animal after tested material every day, comprises the variation of the weight of animals, skin, hair, eyes and mucous membrane, the variation of breathing, circulation, central nervous system, four limbs activity etc.
Result: white new zealand rabbit gives to have no whole body poisoning manifestations and death condition after the safety and environmental protection tea seed detergent powder of various embodiments of the present invention, and the weight of animals increases, on breathing, circulation, central nervous system, four limbs activity etc. without impact.The indivedual animals of damaged skin are had to slight erythema and without oedema, after drug withdrawal, 24h disappears, medication district drug residue free spot.
Conclusion: the safety and environmental protection tea seed detergent powder of various embodiments of the present invention to white new zealand rabbit intact skin and damaged skin without obvious toxic reaction.
Five. irritation test
Purpose: detect the skin irritation reaction of the safety and environmental protection tea seed detergent powder of various embodiments of the present invention, for clinical application provides the security foundation.
Method: carry out according to the relevant requirements in " irritation test and skin allergy test governing principle ".Rabbit skin gives safety and environmental protection tea seed detergent powder, the distilled water of various embodiments of the present invention, observes the skin irritation reaction.
Result: after rabbit skin gives the safety and environmental protection tea seed detergent powder of various embodiments of the present invention, intact skin and damaged skin are showed no to the skin irritation reactions such as erythema, oedema.
Conclusion: the safety and environmental protection tea seed detergent powder percutaneous drug delivery of various embodiments of the present invention, to complete normal skin and the equal nonirritant of damaged skin.
Six. skin allergy test
Purpose: the anaphylaxis of the intact skin of the safety and environmental protection tea seed detergent powder of detection various embodiments of the present invention, for clinical application provides the security foundation.
Method: carry out according to the relevant requirements in " irritation test and skin allergy test governing principle ", the cavy sensitization contact and excite the contact detection various embodiments of the present invention safety and environmental protection tea seed detergent powder, distilled water and positive control medicine 2, the 4-dinitrochlorobenzene, observe the skin hypersensitivity reaction.
Result: after the safety and environmental protection tea seed detergent powder that cavy gives various embodiments of the present invention is detected, do not find that the anaphylaxis such as erythema, oedema appear in the local skin of tested cavy.
Conclusion: the safety and environmental protection tea seed detergent powder of various embodiments of the present invention without supersensitivity.
Claims (10)
1. a safety and environmental protection tea seed detergent powder, it is characterized in that: it is to be made by the raw material of following proportion by weight: 60～70 parts of camellia seed meals, 15～30 parts, Chinese honey locust, 5～10 parts of Leafy twigs of Oriental Arborvitae, 0.5～3 part of Silktree Albizzia Bark, 0.5～3 part of pomegranate rind, 0.5～2.5 part of natural Broneolum Syntheticum.
2. safety and environmental protection tea seed detergent powder according to claim 1, it is characterized in that: it is to be made by the raw material of following proportion by weight: 60～67.5 parts of camellia seed meals, 15～26.3 parts, Chinese honey locust, 5～8.8 parts of Leafy twigs of Oriental Arborvitae, 0.5～2.4 part of Silktree Albizzia Bark, 0.5～2.4 part of pomegranate rind, 0.5～2 part of natural Broneolum Syntheticum.
3. safety and environmental protection tea seed detergent powder according to claim 1, it is characterized in that: it is to be made by the raw material of following proportion by weight: 62.5～70 parts of camellia seed meals, 18.8～30 parts, Chinese honey locust, 6.3～10 parts of Leafy twigs of Oriental Arborvitae, 1.2～3 parts of Silktree Albizzia Barks, 1.1～3 parts of pomegranate rinds, 1～2.5 part of natural Broneolum Syntheticum.
4. according to claim 1 or 2 or 3 described safety and environmental protection tea seed detergent powders, it is characterized in that: it is to be made by the raw material of following proportion by weight: 62.5～67.5 parts of camellia seed meals, 18.8～26.3 parts, Chinese honey locust, 6.3～8.8 parts of Leafy twigs of Oriental Arborvitae, 1.2～2.4 parts of Silktree Albizzia Barks, 1.1～2.4 parts of pomegranate rinds, 1～2 part of natural Broneolum Syntheticum.
5. according to claim 1 or 2 or 3 or 4 described safety and environmental protection tea seed detergent powders, it is characterized in that: it is to be made by the raw material of following proportion by weight: 65 parts of camellia seed meals, 22.5 parts, Chinese honey locust, 7.5 parts of Leafy twigs of Oriental Arborvitae, 1.8 parts of Silktree Albizzia Barks, 1.7 parts of pomegranate rinds, 1.5 parts of natural Broneolum Syntheticums.
6. the preparation method of a safety and environmental protection tea seed detergent powder, it is characterized in that: it comprises the steps:
One, get raw material
Take raw material by following proportion by weight: 60～70 parts of camellia seed meals, 15～30 parts, Chinese honey locust, 5～10 parts of Leafy twigs of Oriental Arborvitae, 0.5～3 part of Silktree Albizzia Bark, 0.5～3 part of pomegranate rind, 0.5～2.5 part of natural Broneolum Syntheticum;
Two, pulverize
To obtain raw material and be pulverized by pulverizer respectively, obtain each raw material powder;
Three, mix
Each raw material powder is mixed, stir, obtain safety and environmental protection tea seed detergent powder.
7. the preparation method of safety and environmental protection tea seed detergent powder according to claim 6, it is characterized in that: it also comprises step:
Four, sterilization
The safety and environmental protection tea seed detergent powder that the 3rd step is obtained is by ultraviolet ray or microwave disinfection, then packs.
8. according to the preparation method of the described safety and environmental protection tea of claim 6 or 7 seed detergent powder, it is characterized in that: the raw material particle size after second step is pulverized is for crossing 40～50 mesh sieves.
9. according to the preparation method of the described safety and environmental protection tea of claim 6 or 7 seed detergent powder, it is characterized in that: raw material preferred mass part proportioning that the first step takes is: 62.5～67.5 parts of camellia seed meals, 18.8～26.3 parts, Chinese honey locust, 6.3～8.8 parts of Leafy twigs of Oriental Arborvitae, 1.2～2.4 parts of Silktree Albizzia Barks, 1.1～2.4 parts of pomegranate rinds, 1～2 part of natural Broneolum Syntheticum.
10. the preparation method of safety and environmental protection tea seed detergent powder according to claim 8, it is characterized in that: raw material preferred mass part proportioning that the first step takes is: 65 parts of camellia seed meals, 22.5 parts, Chinese honey locust, 7.5 parts of Leafy twigs of Oriental Arborvitae, 1.8 parts of Silktree Albizzia Barks, 1.7 parts of pomegranate rinds, 1.5 parts of natural Broneolum Syntheticums.
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Cited By (9)
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| CN104531389A (en) * | 2014-12-13 | 2015-04-22 | 张慧娜 | Natural tea seed powder added cleanser |
| CN106978281A (en) * | 2017-03-30 | 2017-07-25 | 柳州立洁科技有限公司 | A kind of acidic cleaner and preparation method thereof |
| CN108822978A (en) * | 2018-08-28 | 2018-11-16 | 湖南大三湘茶油股份有限公司 | Cleaning packet and preparation method thereof |
| CN108865517A (en) * | 2018-08-28 | 2018-11-23 | 赖琼玮 | Clean treasured and preparation method thereof |
| CN108913403A (en) * | 2018-08-28 | 2018-11-30 | 湖南大三湘茶油股份有限公司 | Detergent and preparation method thereof |
| CN109055042A (en) * | 2018-08-28 | 2018-12-21 | 湖南天华油茶科技股份有限公司 | Cleanser and preparation method thereof |
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Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104531389A (en) * | 2014-12-13 | 2015-04-22 | 张慧娜 | Natural tea seed powder added cleanser |
| CN106978281A (en) * | 2017-03-30 | 2017-07-25 | 柳州立洁科技有限公司 | A kind of acidic cleaner and preparation method thereof |
| CN108822978A (en) * | 2018-08-28 | 2018-11-16 | 湖南大三湘茶油股份有限公司 | Cleaning packet and preparation method thereof |
| CN108865517A (en) * | 2018-08-28 | 2018-11-23 | 赖琼玮 | Clean treasured and preparation method thereof |
| CN108913403A (en) * | 2018-08-28 | 2018-11-30 | 湖南大三湘茶油股份有限公司 | Detergent and preparation method thereof |
| CN109055042A (en) * | 2018-08-28 | 2018-12-21 | 湖南天华油茶科技股份有限公司 | Cleanser and preparation method thereof |
| CN111154555A (en) * | 2020-02-24 | 2020-05-15 | 深圳市凡兵生态科技有限公司 | Liquid detergent prepared by using tea seed cake powder and fruit peel as stock solution |
| JP2021134252A (en) * | 2020-02-26 | 2021-09-13 | 株式会社 Mtg | Detergent |
| JP7535859B2 (en) | 2020-02-26 | 2024-08-19 | 株式会社 Mtg | Cleaning agents |
| CN114129581A (en) * | 2021-02-24 | 2022-03-04 | 徐州医科大学 | Application of tea saponin in preparing medicine for treating shigella infectious enteritis and medicinal preparation thereof |
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Inventor after: Lu Fangguo Inventor after: Yang Yaoxue Inventor after: Huang Gui Inventor after: Liu Haicheng Inventor after: Zeng Qin Inventor after: Duan Wenxiu Inventor after: Lai Qiongwei Inventor after: Tian Hua Inventor after: Li Ling Inventor after: Pei Jianru Inventor after: Wen Lexi Inventor after: Kong Yingge Inventor after: Chen Jinsong Inventor after: Yu Dejun Inventor before: Lu Fangguo Inventor before: Lai Qiongwei Inventor before: Li Ling Inventor before: Wen Lexi Inventor before: Tian Hua Inventor before: Kong Yingge Inventor before: Pei Jianru Inventor before: Chen Jinsong |
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Address after: 421311 Hengnan City, Hunan province gathered in the industrial park, Hengyang Patentee after: Hunan Dasanxiang Camellia Oil Technology Co., Ltd. Address before: 421311 Hengnan City, Hunan province gathered in the industrial park, Hengyang Patentee before: Hunan Great Sanxiang Camellia Technology Co., Ltd. |