CN104274634A - Compound plant essential oil for refreshing, restoring consciousness, diminishing swelling and relieving itching and preparation method of compound plant essential oil - Google Patents
Compound plant essential oil for refreshing, restoring consciousness, diminishing swelling and relieving itching and preparation method of compound plant essential oil Download PDFInfo
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Abstract
The invention discloses compound plant essential oil for refreshing, restoring consciousness, diminishing swelling and relieving itching and a preparation method of the compound plant essential oil. The compound plant essential oil is prepared by mixing the following components in parts by weight: 30-80 parts of simmondsia chinensis seed oil, 10-20 parts of peppermint leaf oil, 1-10 parts of eucalyptus globulus leaf oil, 1-10 parts of lavender oil, 1-10 parts of citrus aurantium bergamia fruit oil, 1-10 parts of hypericum perforatum oil, 1-10 parts of patchouli oil, 5-20 parts of natural menthol, 1-10 parts of borneol, 0.5-5 parts of tocopherol, 0.5-5 parts of natural bisabolol and 0.1-2 parts of aloe gel lyophilized powder. The compound plant essential oil has fresh and pleasant fragrance, is safe and mild, and is capable of refreshing, restoring consciousness, quickly diminishing swelling and relieving itching, and is an ideal product in summer.
Description
Technical field
The present invention relates to a kind of plants essential oil, particularly the compound plant essential oil and preparation method thereof of a kind of refreshment and repellent antipruritic.
Background technology
Modern life rhythm is fast, and work and study pressure is large, and especially business people, white collar and student, often can feel exhausted, have one's head in the clouds.Some people easily felt sleepy in spring, torridity summer, autumn, particularly human pilot, more need tired sleepy time refreshment, avoid danger.Be at present essential balm, white flower oil, refrigerant wet goods medicine for the main externally applied product of this market demand on the market, although can play a role, but mostly containing the composition that the chemosynthesis such as methyl salicylate, Camphora, safety are lower, abnormal smells from the patient is pungent, and mostly be low side consumer products, be difficult to meet middle and high end crowd and pursue natural, safe psychology.
A kind of compound essential Oil of refreshment of the disclosure of the invention of application number 200710303708.4, it is mixed according to certain ratio primarily of rosemary ethereal oil, clove oil, oil of Cymbopogon winterianus, tea tree ethereal oil, Peppermint essential oil, Herba Pogostemonis quintessence oil.Though this compound essential Oil can refreshment but do not have the function of repellent antipruritic, and is easy to quick volatilization when this compound essential Oil uses, cause a large amount of wastes of effective ingredient.
Summary of the invention
The object of the present invention is to provide the compound plant essential oil of a kind of refreshment and repellent antipruritic, have refrigerant, pleasant fragrance, safety is gentle, can refreshment, fast repellent antipruritic, is non-defective unit of aestivating.
Present invention also offers the preparation method of the compound plant essential oil of a kind of refreshment and repellent antipruritic, simple, be applicable to suitability for industrialized production.
The technical solution adopted for the present invention to solve the technical problems is:
A compound plant essential oil for refreshment and repellent antipruritic, is mixed by the component of following parts by weight: Jojoba seed oil 30-80 part, Herba Menthae leaf oil 10-20 part, Eucalyptus globulus Labill leaf oil 1-10 part, Oleum lavandula angustifolia 1-10 part, bergamot fruit oil 1-10 part, Herba Hyperici perforati oil 1-10 part, patchouli oil 1-10 part, natural menthol 5-20 part, natural Broneolum Syntheticum 1-10 part, tocopherol 0.5-5 part, neutral red bisabolol 0.5-5 part, Aloe gel lyophilized powder 0.1-2 part.
Sachet is that China is used for the mode of refreshing oneself the earliest, and it plays a role is exactly volatile ingredient based in these medical substances.The present invention with sachet for developing basis, give full play to motherland's TCM Features and in conjunction with modern pharmacology achievement in research, be equipped with natural, refrigerant, refreshment composition of having one's ideas straightened out, form compound essential Oil product, product has refrigerant, pleasant herbal aromatic, and energy quick sterilization is antipruritic, for the personage pursuing natural health provides another selection.
Herba Menthae leaf oil: dispelling wind and heat pathogens, the clear sharp head.Eucalyptus globulus Labill leaf oil: dispelling wind to relieve the exterior syndrome, heat-clearing and toxic substances removing, killing parasites for relieving itching.Herba Hyperici perforati oil: heat-clearing and toxic substances removing, dispersing swelling and dissipating binds, dispelling wind and heat pathogens.Patchouli oil: eliminating turbid pathogen with aromatics, deliver expelling summer-heat.Menthol: refrigerant antipruritic.Tocopherol can reduce cell needs oxygen amount, the power that sustains life, endurance, endurance, and tocopherol has good oxidation resistance simultaneously, can extend the shelf life.Bisabolol has good antiinflammatory, bactericidal action, can subside a swelling.Borneolum Syntheticum: refreshment of having one's ideas straightened out, priming is up.Oleum lavandula angustifolia and bergamot fruit oil can releive pressure, alleviate headache, anti-inflammation and sterilization, novel aroma contributes to improving spirit, plays the effect of Synergistic.Jojoba oil contains abundant vitamin, very easily merges with skin, has the effect of nourishing softening skin, based on oil.Aloe gel lyophilized powder can make quintessence oil volatility reduce while repellent antipruritic, plays slow releasing, the effect that lasting is lasting.
Modern pharmacology research proves: Herba Hyperici perforati oil has obvious inhibitory action to gram positive bacteria.In Herba Pogostemonis, Pogostone is main antimicrobial component, all has certain inhibitory action, be obviously better than Bacterium entericum to staphylococcus aureus effect to Salmonella, escherichia coli, shigella, staphylococcus aureus etc.Menthol has obvious itching-relieving action, its effect with to antfhistamine effect with suppress the release of histamine relevant.Natural Broneolum Syntheticum safety is high, and drug effect is stronger, has the effect of anti-inflammation, pain relieving, protection nervus centralis, promotion agent permeates therethrough blood brain barrier.Aloe gel can killing parasites for relieving itching, detoxification sore treatment tinea, anti-inflammation and sterilization.
Volatile in order to solve quintessence oil series products, retention time is short, the problem that fragrance is lasting not, the present invention invents special interpolation Aloe gel lyophilized powder, while enhancing repellent antipruritic effect, can reduce quintessence oil volatility well, product onset is better, the fragrant breath of book on Chinese herbal medicine is obviously more lasting, and pro-skin experience effect is better.The each component of compound plant essential oil of the present invention is collaborative plays potentiation, and have refrigerant, pleasant fragrance, safety is gentle, can refreshment, fast repellent antipruritic, is non-defective unit of aestivating.
As preferably, described Herba Menthae leaf oil adopts carbon dioxide supercritical fluid extraction mentha leave and obtains, and the state modulator of carbon dioxide supercritical fluid extraction is: extracting pressure 8-10Mpa, extraction temperature 50-55 DEG C, carbon dioxide flow 25-30L/h, extraction time 1-1.5h.
As preferably, described Herba Hyperici perforati oil adopts carbon dioxide supercritical fluid extraction Herba Hyperici perforati and obtains, and the state modulator of carbon dioxide supercritical fluid extraction is: extracting pressure 20-22Mpa, extraction temperature 40-45 DEG C, carbon dioxide flow 25-30L/h, extraction time 1-1.5h.
As preferably, described patchouli oil adopts carbon dioxide supercritical fluid extraction Herba Pogostemonis and obtains, the state modulator of carbon dioxide supercritical fluid extraction is: extracting pressure 15-16Mpa, extraction temperature 40-42 DEG C, carbon dioxide flow 20-25L/h, mass concentration is the ethanol of 90-95% is entrainer, extraction time 2-2.5h.
Herba Menthae leaf oil of the present invention, Herba Hyperici perforati oil, patchouli oil adopt the extraction of carbon dioxide supercritical fluid extraction technology, operative temperature is low, in volatile oil thermal instability composition and oxidizable component survivable, the effective ingredient of acquisition more comprehensively, closer to natural component ratio.
A preparation method for the compound plant essential oil of refreshment and repellent antipruritic, comprises the following steps:
(1) natural menthol, natural Broneolum Syntheticum and Jojoba seed oil is taken in proportion, control temperature 20-25 DEG C, ultrasonic to solid-solution, then liquid is sucked hermetic container;
(2) in hermetic container, add Herba Menthae leaf oil, Eucalyptus globulus Labill leaf oil, Oleum lavandula angustifolia, bergamot fruit oil, Herba Hyperici perforati oil, patchouli oil, tocopherol and neutral red bisabolol, mix homogeneously obtains elementary quintessence oil;
(3) get the elementary quintessence oil accounting for elementary quintessence oil cumulative volume 15-25% and Aloe gel lyophilized powder ground and mixed even, then add the elementary quintessence oil mix homogeneously of residue, after homogenizer homogenizing, fill is in Ethereal oil bottle.
In production process of the present invention, have employed low temperature ultrasonic dissolving technology, avoid menthol, Borneolum Syntheticum adopts conventional heating dissolution mechanism and problem that the oils quality that causes declines, shorten the operating time, effectively reduce the volatilization of component, improve product quality.
The invention has the beneficial effects as follows:
1, be raw materials usedly natural plant extraction, without chemical raw material, safety is gentle, can life-time service, more meets natural, healthy consumption demand.
2, quintessence oil main component is micromolecular compound, very easily permeates in skin, and easily by Cell uptake, onset is rapid.Product fragrance walks string, refreshment of having one's ideas straightened out, by massage forehead, temple, the position such as after ear, can fast wake-up brain cell, and refreshment.Experience through the thousand routine personnel that go beyond what is acceptable or necessary (user is mainly driving personnel, stay up late overtime work personnel, student etc.), refreshment, for the repellent antipruritic effect after mosquito bite, total effective rate is more than 96%.
3, product odour is refrigerant, fresh and clean, has draft breath, brain centres can being regulated to respond to by inhaling the modes such as news, making human body produce refrigerant sensation of soothing the spirit.
4, because steam distillation is simple to operate, cost is lower, and the domestic and international extraction to quintessence oil at present adopts which more.But vapor distillation operative temperature is higher, in volatile oil, thermally labile component and oxidizable component are easily destroyed, and then affect product quality.By contrast test, effective ingredient component and ratio in paper examines oil yield and volatile oil, adopt carbon dioxide supercritical fluid extraction Herba Menthae leaf oil, oil yield 2.43%, is 2.1 times of steam distillation oil yield 1.15%.Herba Hyperici perforati oil adopts carbon dioxide supercritical fluid extraction Oleum menthae, and oil yield 3.39%, is 1.6 times of steam distillation oil yield 2.11%.Patchouli oil adopts carbon dioxide supercritical fluid extraction technology extraction oil yield 2.46%, is 1.6 times of steam distillation 1.56%.Carbon dioxide supercritical fluid extraction is applied to three kind of plant extractions in prescription, with the obvious advantage, there is not dissolvent residual, compared with steam distillation, because operative temperature is low, terpenes composition not easily loses, part high boiling point composition also can extract, and Total Product quality is more excellent.
5, the present invention adopts low temperature ultrasonic dissolving technology, avoids menthol, Borneolum Syntheticum routine adopts heating for dissolving method and the oils quality that causes declines, shorten the operating time, effectively reduce the volatilization of component, improve product quality.
6, the present invention adds Aloe gel lyophilized powder especially, and while enhancing repellent antipruritic effect, solve quintessence oil series products well volatile, retention time is short, the problem that fragrance is lasting not.Can make product volatile ingredient slow releasing, herbal fragrant breath is obviously more lasting, and pro-skin experience effect is better.
Detailed description of the invention
Below by specific embodiment, technical scheme of the present invention is described in further detail.
In the present invention, if not refer in particular to, the raw material adopted and equipment etc. all can be buied from market or this area is conventional.Method in following embodiment, if no special instructions, is the conventional method of this area.
Embodiment 1:
The compound plant essential oil of a kind of refreshment and repellent antipruritic, be mixed by the component of following parts by weight: Jojoba seed oil (commercially available) 30 parts, Herba Menthae leaf oil 10 parts, Eucalyptus globulus Labill leaf oil (commercially available) 1 part, Oleum lavandula angustifolia (commercially available) 1 part, bergamot fruit oil (commercially available) 1 part, Herba Hyperici perforati oil 1 part, patchouli oil 10 parts, natural menthol (commercially available) 20 parts, natural Broneolum Syntheticum (commercially available) 1 part, tocopherol (commercially available) 0.5 part, neutral red bisabolol (commercially available) 0.5 part, Aloe gel lyophilized powder (commercially available) 0.1 part.
Herba Menthae leaf oil adopts carbon dioxide supercritical fluid extraction mentha leave and obtains, and extract after mentha leave drying and crushing, the state modulator of carbon dioxide supercritical fluid extraction is: extracting pressure 8Mpa, extraction temperature 50 DEG C, carbon dioxide flow 25L/h, extraction time 1.5h.
Herba Hyperici perforati oil adopts carbon dioxide supercritical fluid extraction Herba Hyperici perforati and obtains, and extract after Herba Hyperici perforati drying and crushing, the state modulator of carbon dioxide supercritical fluid extraction is: extracting pressure 20Mpa, extraction temperature 40 DEG C, carbon dioxide flow 25L/h, extraction time 1.5h.
Patchouli oil adopts carbon dioxide supercritical fluid extraction Herba Pogostemonis and obtains, extract after Herba Pogostemonis drying and crushing, the state modulator of carbon dioxide supercritical fluid extraction is: extracting pressure 15Mpa, extraction temperature 40 DEG C, carbon dioxide flow 20L/h, mass concentration be 90% ethanol be entrainer, extraction time 2.5h.
Preparation method, comprises the following steps:
(1) natural menthol, natural Broneolum Syntheticum and Jojoba seed oil is taken in proportion, control temperature 20 DEG C, ultrasonic to solid-solution, then liquid is sucked hermetic container;
(2) in hermetic container, add Herba Menthae leaf oil, Eucalyptus globulus Labill leaf oil, Oleum lavandula angustifolia, bergamot fruit oil, Herba Hyperici perforati oil, patchouli oil, tocopherol and neutral red bisabolol, mix homogeneously obtains elementary quintessence oil;
(3) get the elementary quintessence oil accounting for elementary quintessence oil cumulative volume 15% and Aloe gel lyophilized powder ground and mixed even, then add the elementary quintessence oil mix homogeneously of residue, after homogenizer homogenizing, fill is in Ethereal oil bottle.
Embodiment 2:
The compound plant essential oil of a kind of refreshment and repellent antipruritic, be mixed by the component of following parts by weight: Jojoba seed oil (commercially available) 80 parts, Herba Menthae leaf oil 20 parts, Eucalyptus globulus Labill leaf oil (commercially available) 10 parts, Oleum lavandula angustifolia (commercially available) 10 parts, bergamot fruit oil (commercially available) 10 parts, Herba Hyperici perforati oil 10 parts, patchouli oil 1 part, natural menthol (commercially available) 5 parts, natural Broneolum Syntheticum (commercially available) 10 parts, tocopherol (commercially available) 5 parts, neutral red bisabolol (commercially available) 5 parts, Aloe gel lyophilized powder (commercially available) 2 parts.
Herba Menthae leaf oil adopts carbon dioxide supercritical fluid extraction mentha leave and obtains, and extract after mentha leave drying and crushing, the state modulator of carbon dioxide supercritical fluid extraction is: extracting pressure 10Mpa, extraction temperature 55 DEG C, carbon dioxide flow 30L/h, extraction time 1h.
Herba Hyperici perforati oil adopts carbon dioxide supercritical fluid extraction Herba Hyperici perforati and obtains, and extract after Herba Hyperici perforati drying and crushing, the state modulator of carbon dioxide supercritical fluid extraction is: extracting pressure 22Mpa, extraction temperature 45 DEG C, carbon dioxide flow 30L/h, extraction time 1h.
Patchouli oil adopts carbon dioxide supercritical fluid extraction Herba Pogostemonis and obtains, and extract after Herba Pogostemonis drying and crushing, the state modulator of carbon dioxide supercritical fluid extraction is: extracting pressure 16Mpa, extraction temperature 42 DEG C, carbon dioxide flow 25L/h, mass concentration be 95% ethanol be entrainer, extraction time 2h.
Preparation method, comprises the following steps:
(1) natural menthol, natural Broneolum Syntheticum and Jojoba seed oil is taken in proportion, control temperature 25 DEG C, ultrasonic to solid-solution, then liquid is sucked hermetic container;
(2) in hermetic container, add Herba Menthae leaf oil, Eucalyptus globulus Labill leaf oil, Oleum lavandula angustifolia, bergamot fruit oil, Herba Hyperici perforati oil, patchouli oil, tocopherol and neutral red bisabolol, mix homogeneously obtains elementary quintessence oil;
(3) get the elementary quintessence oil accounting for elementary quintessence oil cumulative volume 25% and Aloe gel lyophilized powder ground and mixed even, then add the elementary quintessence oil mix homogeneously of residue, after homogenizer homogenizing, fill is in Ethereal oil bottle.
Embodiment 3:
The compound plant essential oil of a kind of refreshment and repellent antipruritic, be mixed by the component of following parts by weight: Jojoba seed oil (commercially available) 50 parts, Herba Menthae leaf oil 15 parts, Eucalyptus globulus Labill leaf oil (commercially available) 5 parts, Oleum lavandula angustifolia (commercially available) 5 parts, bergamot fruit oil (commercially available) 5 parts, Herba Hyperici perforati oil 5 parts, patchouli oil 5 parts, natural menthol (commercially available) 10 parts, natural Broneolum Syntheticum (commercially available) 5 parts, tocopherol (commercially available) 2 parts, neutral red bisabolol (commercially available) 3 parts, Aloe gel lyophilized powder (commercially available) 1 part.
Herba Menthae leaf oil adopts carbon dioxide supercritical fluid extraction mentha leave and obtains, and extract after mentha leave drying and crushing, the state modulator of carbon dioxide supercritical fluid extraction is: extracting pressure 9Mpa, extraction temperature 52 DEG C, carbon dioxide flow 30L/h, extraction time 1.5h.
Herba Hyperici perforati oil adopts carbon dioxide supercritical fluid extraction Herba Hyperici perforati and obtains, and extract after Herba Hyperici perforati drying and crushing, the state modulator of carbon dioxide supercritical fluid extraction is: extracting pressure 21Mpa, extraction temperature 42 DEG C, carbon dioxide flow 25L/h, extraction time 1.5h.
Patchouli oil adopts carbon dioxide supercritical fluid extraction Herba Pogostemonis and obtains, and extract after Herba Pogostemonis drying and crushing, the state modulator of carbon dioxide supercritical fluid extraction is: extracting pressure 15Mpa, extraction temperature 40 DEG C, carbon dioxide flow 25L/h, mass concentration be 90% ethanol be entrainer, extraction time 2h.
Preparation method, comprises the following steps:
(1) natural menthol, natural Broneolum Syntheticum and Jojoba seed oil is taken in proportion, control temperature 22 DEG C, ultrasonic to solid-solution, then liquid is sucked hermetic container;
(2) in hermetic container, add Herba Menthae leaf oil, Eucalyptus globulus Labill leaf oil, Oleum lavandula angustifolia, bergamot fruit oil, Herba Hyperici perforati oil, patchouli oil, tocopherol and neutral red bisabolol, mix homogeneously obtains elementary quintessence oil;
(3) get the elementary quintessence oil accounting for elementary quintessence oil cumulative volume 20% and Aloe gel lyophilized powder ground and mixed even, then add the elementary quintessence oil mix homogeneously of residue, after homogenizer homogenizing, fill is in Ethereal oil bottle.
Essential oil product main component of the present invention is micromolecular compound, very easily permeates in skin, and easily by Cell uptake, onset is rapid.Product fragrance walks string, refreshment of having one's ideas straightened out, by massage forehead, temple, the position such as after ear, can fast wake-up brain cell, and refreshment.Experience through the thousand routine personnel that go beyond what is acceptable or necessary (user is mainly driving personnel, stay up late overtime work personnel, student etc.), refreshment, for the repellent antipruritic effect after mosquito bite, total effective rate is more than 96%.
According to " cosmetics health specification " (version in 2007), carry out wholesomeness test to the present invention, result of the test shows: the equal compliant requirement of micro-biology experiment, hygienic chemistry index.Repeatedly irritation test result is: nonirritant.Assay is as follows:
Micro biological Tests result
| Inspection item | Assay | Limit value |
| Total plate count (CFU/g or CFU/mL) | <10 | ≤1000 |
| Yeast and mold sum (CFU/g or CFU/mL) | <10 | ≤100 |
| Excrement colibacillus group/g (or mL) | Do not detect | Must not detect |
| Staphylococcus aureus/g (or mL) | Do not detect | Must not detect |
| Pseudomonas aeruginosa/g (or mL) | Do not detect | Must not detect |
Health chemical testing result
| Inspection item | Unit | Assay | The method of inspection | Method concentrations | Limit value |
| Hydrargyrum | mg/kg | 0.049 | Hydride generation atomic fluorescence photometry | 0.006 | ≤1 |
| Arsenic | mg/kg | <0.04 | Hydride generation atomic fluorescence photometry | 0.04 | ≤10 |
| Plumbous | mg/kg | <5 | Atomic absorption spectrophotometry | 5 | ≤40 |
Above-described embodiment is one of the present invention preferably scheme, not does any pro forma restriction to the present invention, also has other variant and remodeling under the prerequisite not exceeding the technical scheme described in claim.
Claims (5)
1. a compound plant essential oil for refreshment and repellent antipruritic, is characterized in that, is mixed by the component of following parts by weight: Jojoba seed oil 30-80 part, Herba Menthae leaf oil 10-20 part, Eucalyptus globulus Labill leaf oil 1-10 part, Oleum lavandula angustifolia 1-10 part, bergamot fruit oil 1-10 part, Herba Hyperici perforati oil 1-10 part, patchouli oil 1-10 part, natural menthol 5-20 part, natural Broneolum Syntheticum 1-10 part, tocopherol 0.5-5 part, neutral red bisabolol 0.5-5 part, Aloe gel lyophilized powder 0.1-2 part.
2. compound plant essential oil according to claim 1, it is characterized in that: described Herba Menthae leaf oil adopts carbon dioxide supercritical fluid extraction mentha leave and obtains, the state modulator of carbon dioxide supercritical fluid extraction is: extracting pressure 8-10Mpa, extraction temperature 50-55 DEG C, carbon dioxide flow 25-30L/h, extraction time 1-1.5h.
3. compound plant essential oil according to claim 1 and 2, it is characterized in that: described Herba Hyperici perforati oil adopts carbon dioxide supercritical fluid extraction Herba Hyperici perforati and obtains, the state modulator of carbon dioxide supercritical fluid extraction is: extracting pressure 20-22Mpa, extraction temperature 40-45 DEG C, carbon dioxide flow 25-30L/h, extraction time 1-1.5h.
4. compound plant essential oil according to claim 1 and 2, it is characterized in that: described patchouli oil adopts carbon dioxide supercritical fluid extraction Herba Pogostemonis and obtains, the state modulator of carbon dioxide supercritical fluid extraction is: extracting pressure 15-16Mpa, extraction temperature 40-42 DEG C, carbon dioxide flow 20-25L/h, mass concentration is the ethanol of 90-95% is entrainer, extraction time 2-2.5h.
5. the preparation method of the compound plant essential oil of a kind of refreshment as claimed in claim 1 and repellent antipruritic, is characterized in that, comprise the following steps:
(1) natural menthol, natural Broneolum Syntheticum and Jojoba seed oil is taken in proportion, control temperature 20-25 DEG C, ultrasonic to solid-solution, then liquid is sucked hermetic container;
(2) in hermetic container, add Herba Menthae leaf oil, Eucalyptus globulus Labill leaf oil, Oleum lavandula angustifolia, bergamot fruit oil, Herba Hyperici perforati oil, patchouli oil, tocopherol and neutral red bisabolol, mix homogeneously obtains elementary quintessence oil;
(3) get the elementary quintessence oil accounting for elementary quintessence oil cumulative volume 15-25% and Aloe gel lyophilized powder ground and mixed even, then add the elementary quintessence oil mix homogeneously of residue, after homogenizer homogenizing, fill is in Ethereal oil bottle.
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