CN105476892A - Multi-effect skin moisturizing cream containing lithospermum erythrorhizon and other vegetable oils, and preparation method thereof - Google Patents
Multi-effect skin moisturizing cream containing lithospermum erythrorhizon and other vegetable oils, and preparation method thereof Download PDFInfo
- Publication number
- CN105476892A CN105476892A CN201410471798.8A CN201410471798A CN105476892A CN 105476892 A CN105476892 A CN 105476892A CN 201410471798 A CN201410471798 A CN 201410471798A CN 105476892 A CN105476892 A CN 105476892A
- Authority
- CN
- China
- Prior art keywords
- oil
- extract
- vegetable oils
- carbon dioxide
- supercritical carbon
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Landscapes
- Medicines Containing Plant Substances (AREA)
Abstract
The present invention discloses a multi-effect skin moisturizing cream containing lithospermum erythrorhizon and other vegetable oils, wherein the components comprise 47.3-49.5% of olea europaea fruit oil, 24-33% of hydrogenated soybean oil, 4-12% of beeswax, 2-8% of ozocerite, 0.7-1% of vitamin E, 3-6% of a lithospermum erythrorhizon root extract, 1.1-0.5% of a ginger root extract, 1.8-0.5% of lavender oil, 1.2-0.5% of cymbopogon schoenanthus oil, 1.6-0.5% of peppermint leaf oil, and 1.3-0.5% of rosmarinus officinalis leaf oil. According to the present invention, the used vegetable oils are extracted by using supercritical carbon dioxide extraction; the non-toxic, readily available and inexpensive CO2 is adopted as the fluid to extract the functionally components of lithospermum erythrorhizon, lavender, cymbopogon schoenanthus, rosmarinus officinalis leaf and the like under the supercritical state so as to provide characteristics of good extraction effect, simple process, being suitable for large-scale production, short production cycle, and the like; and the vegetable oils extracted by using the supercritical carbon dioxide have high purity, and do not have the organic solvent residue problem so as to further ensure the function and the safety of the vegetable oils.
Description
Technical field
The invention belongs to cosmetic field, particularly relate to a kind of many effects skin lotion containing various plants oil such as Radix Arnebiae (Radix Lithospermi)s and preparation method thereof.
Background technology
Radix Arnebiae (Radix Lithospermi) is the parts of generic medicinal plants of China, sweet in the mouth, salty, cold in nature, GUIXIN, Liver Channel, and Radix Arnebiae (Radix Lithospermi) has removing heat from blood, invigorates blood circulation, the effect of rash of detoxifying, and contains, macule purple is black, measles without adequate eruption, skin infection, eczema, burn due to hot liquid or fire for heat in blood poison.Modern pharmacology research shows, Radix Arnebiae (Radix Lithospermi) has antibacterial, the effect such as antitumor, antiviral, antiinflammatory, antiallergic, the liver protecting and ALT lowering preferably, be the plant that a kind of medical value is very high, cause the very big attention of Chinese scholars in recent years, extensive use on clinical medicine.Along with the development of science and technology, Radix Arnebiae (Radix Lithospermi) is applied in skin care item gradually, and Radix Arnebiae (Radix Lithospermi) is applied in the skin lotion of child by the apis florea of the U.S., the profit basis of GuangZhou, China and Bei Yiner.In the forward position in epoch, Radix Arnebiae (Radix Lithospermi) is applied in skin lotion although these producers are walked, but in the extraction process of Oleum Radix Arnebiae (Oleum Radix Lithospermi), what adopt is oily immersion process, the Oleum Radix Arnebiae (Oleum Radix Lithospermi) purity that the method extracts is not high and have the residual of oils and fats, the efficacy exertion of Radix Arnebiae (Radix Lithospermi) not only can not be made to the limit, and there is the problem of organic solvent residual.For this reason, a kind of many effects skin lotion containing various plants oil such as Radix Arnebiae (Radix Lithospermi)s of ad hoc meter and preparation method thereof.
Summary of the invention
For overcoming above-mentioned deficiency, the invention provides a kind of many effects skin lotion containing various plants oil such as Radix Arnebiae (Radix Lithospermi)s and preparation method thereof.
The technical solution adopted for the present invention to solve the technical problems is: a kind of many effects skin lotion containing various plants oil such as Radix Arnebiae (Radix Lithospermi)s, it is characterized in that being made up of following component and mass percentage thereof: Fructus oleae europaeae fruit oil 47.3 ~ 49.5%, oil with hydrogenated soybean 24 ~ 33%, Cera Flava 4 ~ 12%, ceresine 2 ~ 8%, vitamin E 0.7 ~ 1%, Radix Arnebiae (Radix Lithospermi) extract 3 ~ 6%, ginger-root extract 1.1 ~ 0.5%, Oleum lavandula angustifolia 1.8 ~ 0.5%, Andropogon schoenanthus oil 1.2 ~ 0.5%, Herba Menthae leaf oil 1.6 ~ 0.5%, Herba Rosmarini Officinalis leaf oil 1.3 ~ 0.5%, and each component percentages sum is absolutely,
The extraction separation method of described vegetable oil is all utilize supercritical carbon dioxide extraction method, supercritical carbon dioxide extraction method extracts the method for effective components in plants, it uses supercritical carbon dioxide extraction, with the root of plant, stem, leaf, flower for raw material, at pressure 10 ~ 40MPa and temperature 32 ~ 80 DEG C, using white oil as entrainer, extract 1 ~ 6 hour in the supercritical state, separating still I pressure is 5 ~ 10Mpa, temperature is 32 ~ 80 DEG C, separating still II pressure is 5 ~ 6Mpa, obtains the high-quality plant extract of safety non-pollution.
Vegetable oil used in the present invention all adopts supercritical carbon dioxide extraction, the method with nontoxic, be easy to get, cheap CO
2for fluid extracts the functional component of Radix Arnebiae (Radix Lithospermi), lavandula angustifolia, Herba Cymbopogonis Citrari, leaf of Herba Rosmarini Officinalis etc. in the supercritical state; have that extraction effect is good, technique is simple, be applicable to large-scale production; the feature such as with short production cycle; not only purity is high for the vegetable oil of employing supercritical carbon dioxide extraction; and there is not the problem of organic solvent residual, further ensure the both effectiveness of vegetable oil and safety.
Accompanying drawing illustrates:
Fig. 1 is preparation technology's schematic flow sheet of the present invention
1.CO
2steel cylinder; 2. filter; 3. fridge; 4.CO
2pump; 5. hot water machine; 6. extraction kettle; 7. separating still; 8. valve; 9. entrainer still;
Detailed description of the invention:
Example is below described in detail new method of the present invention, but does not mean that and limit the scope of the invention.
A kind of many effects skin lotion containing various plants oil such as Radix Arnebiae (Radix Lithospermi)s, be made up of following component and mass percentage thereof: Fructus oleae europaeae fruit oil 47.3 ~ 49.5%, oil with hydrogenated soybean 24 ~ 33%, Cera Flava 4 ~ 12%, ceresine 2 ~ 8%, vitamin E 0.7 ~ 1%, Radix Arnebiae (Radix Lithospermi) extract 3 ~ 6%, ginger-root extract 1.1 ~ 0.5%, Oleum lavandula angustifolia 1.8 ~ 0.5%, Andropogon schoenanthus oil 1.2 ~ 0.5%, Herba Menthae leaf oil 1.6 ~ 0.5%, Herba Rosmarini Officinalis leaf oil 1.3 ~ 0.5%, and each component percentages sum is absolutely.
The extraction separation method of vegetable oil is all utilize supercritical carbon dioxide extraction method, supercritical carbon dioxide extraction method extracts the method for effective components in plants, it uses supercritical carbon dioxide extraction, with the root of plant, stem, leaf, flower for raw material, at pressure 10 ~ 40MPa and temperature 32 ~ 80 DEG C, using white oil as entrainer, extract 1 ~ 6 hour in the supercritical state, separating still I pressure is 5 ~ 10Mpa, temperature is 32 ~ 80 DEG C, separating still II pressure is 5 ~ 6Mpa, obtains the high-quality plant extract of safety non-pollution.
Come in the gross weight of skin lotion: Oleum Radix Arnebiae (Oleum Radix Lithospermi) 1% ~ 5%, olive oil 40% ~ 60%, Oleum lavandula angustifolia 0.1% ~ 1%, Andropogon schoenanthus oil 0.1% ~ 1%, ginger-root extract 0.1% ~ 1%, Oleum menthae 0.1% ~ 1%, Herba Rosmarini Officinalis leaf oil 0.1% ~ 1%, solid-state basic skin moistening oils and fats, comprises oil with hydrogenated soybean, Cera Flava and ceresine 30% ~ 50%.
The vegetable oil used in the present invention as shown in Figure 1 all adopts supercritical carbon dioxide extraction, and for Radix Arnebiae (Radix Lithospermi), the concrete technology of this equipment is:
First by Radix Arnebiae (Radix Lithospermi) crushed after being dried to 4 ~ 100 order, insert in extraction kettle 6; In entrainer still 9, add white oil, carbon dioxide is from CO
2in steel cylinder 1 out, excessively CO is filtered through filter 2
2in impurity, through fridge 3, temperature is dropped to less than 0 DEG C and guarantees CO
2for liquid state, through CO
2pump 4, constantly pumps into extraction kettle 6 by liquid CO 2, makes liquid CO
2pressure reaches setting pressure (10 ~ 40MPa), now through hot water machine 5, and heating liquid CO
2, make its temperature reach design temperature (32 ~ 80 DEG C), now carbon dioxide reaches supercriticality in extraction kettle 6.Simultaneously under the effect of entrainer pump 10, the entrainer in entrainer still 9 is pumped into extraction kettle 6, at CO
2extract and separate effect under, the effective ingredient in sample is with supercritical CO
2enter in separating still 7 together, the pressure and temperature of setting separating still 7, makes CO
2be in non-supercritical state, then the effective ingredient dissolved wherein just parses, and lodges in separating still 7 and collects by valve 8, and CO
2then again recycled.
Example 1
Radix Arnebiae (Radix Lithospermi) powder 2kg about 10 orders of drying is put into extraction kettle.Setting extracting pressure is 40MPa, and extraction temperature is 32 DEG C, and separating still I temperature is 45 DEG C, pressure is 8MPa, and separating still II pressure is 4.5Mpa.Take white oil as entrainer, dynamic extraction 4h, can obtain the Oleum Radix Arnebiae (Oleum Radix Lithospermi) of 360mL.
Example 2
Extraction kettle is put into by with the Cortex seu Flos Hibisci taiwanenss root powder 2kg about moistening 40 orders of white oil.Setting extracting pressure is 15MPa, and extraction temperature is 45 DEG C, and separating still I temperature is 50 DEG C, pressure is 8MPa, and separating still II pressure is 4.5Mpa.Static extracting is after 1 hour, and take white oil as entrainer, dynamic extraction 3h, can obtain the Oleum Radix Arnebiae (Oleum Radix Lithospermi) of 390mL.
Example 3
Radix Arnebiae (Radix Lithospermi) powder 2kg about 100 orders of drying is put into extraction kettle.Setting extracting pressure is 25MPa, and extraction temperature is 75 DEG C, and separating still I temperature is 75 DEG C, pressure is 6MPa, and separating still II pressure is 5Mpa.Take white oil as entrainer, dynamic extraction 2h, can obtain the Oleum Radix Arnebiae (Oleum Radix Lithospermi) of 347mL.
The first composition of the present invention is that Radix Arnebiae (Radix Lithospermi) has removing heat from blood, invigorates blood circulation, the effect of rash of detoxifying, contain for heat in blood poison, macule purple is black, measles without adequate eruption, skin infection, eczema, burn due to hot liquid or fire, modern pharmacology research shows, Radix Arnebiae (Radix Lithospermi) has antibacterial, the effect such as antitumor, antiviral, antiinflammatory, antiallergic, the liver protecting and ALT lowering preferably, it is the plant that a kind of medical value is very high, cause the very big attention of Chinese scholars in recent years, extensive use on clinical medicine.
The second composition of the present invention is that olive oil is rich in the Squalene splendid with skin affinity and essential fatty acid, absorbs rapidly, effectively keeps skin elasticity with moist; Monounsaturated fatty acid contained abundant in olive oil and vitamin E, K, A, D etc. and phenols antioxidant, facial wrinkles can be eliminated, there is the effect such as skin or hair care and control rhagadia manus et pedis, be the cosmetics and skincare product that can " eat ", smear skin energy ultraviolet rays resistance with olive oil in addition and prevent skin carcinoma.
The third composition of the present invention is Oleum lavandula angustifolia is one of oil that in aromatic essential oil, purposes is the widest, family's essential items.Its character is gentle, and fragrant odour, has and soothe the spirit, and meticulously, pain relieving, helps sleep, pressure of releiving, and promotes cell regeneration, balance skin secretion, physical therapy scald and mosquito bite; Prevent and improve hair quality; The diffusion of fragrance thereupon, the cation in air increases, the nervous system of further mediator, blood circulation promoting, enhancing immunity and body energy.
4th kind of composition of the present invention is the most important characteristic of Andropogon schoenanthus oil is exactly anthelmintic, be adapted at most being used for summer spraying or incense is quite well-known anthelmintic quintessence oil, and it is harmless, abnormal smells from the patient is warm, and warm tranquil draft abnormal smells from the patient is also applicable to assisting weak crowd and providing the psychology of infant safety to console.Can purify and improve emotion, can express and separate depressed mood.Warm draft taste, make people be filled with simple and natural fragrant fragrant environment, Buddhist of walking back and forth stays the Miscanthus hilltop, can purify and improve mood, dissolves confusion secularity.Regulation of skin, balance oiliness its deodorization of skin quality and the characteristic of excitation, can make that skin is pure and fresh vigor.
5th kind of composition of the present invention is that ginger-root extract can effective inflammation-inhibiting medium PGE2, has irritation, antiinflammatory, calmness, antibacterial, antioxidative effect.
6th kind of composition of the present invention is Herba Menthae is one of Chinese conventional Chinese medicine, and it is pungent cool property sweating antipyretic medicine.External can training the mind dysmenorrhoea, skin pruritus, erythra and eczema etc.Herba Menthae contains menthol, and this material can fresh breath have the multiple property of medicine, has antisepsis and sterilization, diuresis, reduces phlegm, stomach invigorating and the effect such as aid digestion, often contains menthol in the various ointment being used for the treatment of headache and myalgia.
7th kind of composition of the present invention has a kind of material being carnosol in Herba Rosmarini Officinalis, and its moistening effect is remarkable.Experiment shows, smear skin after two weeks with the astringent containing this material, the moisture of skin can rise to 63% from 44%, and water evaporation quantity then drops to less than 13% from 21%, just as adding one natural cover for defense to skin, decrease much due to skin problem that hydropenia causes.Herba Rosmarini Officinalis extract has unique antioxygenic property-safe, efficient, heat-resisting because of it, and becomes one of emphasis of food antioxidant research and development in recent years.
Claims (1)
1. the many effects skin lotion containing various plants oil such as Radix Arnebiae (Radix Lithospermi)s, it is characterized in that being made up of following component and mass percentage thereof: Fructus oleae europaeae fruit oil 47.3 ~ 49.5%, oil with hydrogenated soybean 24 ~ 33%, Cera Flava 4 ~ 12%, ceresine 2 ~ 8%, vitamin E 0.7 ~ 1%, Radix Arnebiae (Radix Lithospermi) extract 3 ~ 6%, ginger-root extract 1.1 ~ 0.5%, Oleum lavandula angustifolia 1.8 ~ 0.5%, Andropogon schoenanthus oil 1.2 ~ 0.5%, Herba Menthae leaf oil 1.6 ~ 0.5%, Herba Rosmarini Officinalis leaf oil 1.3 ~ 0.5%, and each component percentages sum is absolutely;
The extraction separation method of described vegetable oil is all utilize supercritical carbon dioxide extraction method, supercritical carbon dioxide extraction method extracts the method for effective components in plants, it uses supercritical carbon dioxide extraction, with the root of plant, stem, leaf, flower for raw material, at pressure 10 ~ 40MPa and temperature 32 ~ 80 DEG C, using white oil as entrainer, extract 1 ~ 6 hour in the supercritical state, separating still I pressure is 5 ~ 10Mpa, temperature is 32 ~ 80 DEG C, separating still II pressure is 5 ~ 6Mpa, obtains the high-quality plant extract of safety non-pollution.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410471798.8A CN105476892A (en) | 2014-09-17 | 2014-09-17 | Multi-effect skin moisturizing cream containing lithospermum erythrorhizon and other vegetable oils, and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410471798.8A CN105476892A (en) | 2014-09-17 | 2014-09-17 | Multi-effect skin moisturizing cream containing lithospermum erythrorhizon and other vegetable oils, and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105476892A true CN105476892A (en) | 2016-04-13 |
Family
ID=55664412
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410471798.8A Pending CN105476892A (en) | 2014-09-17 | 2014-09-17 | Multi-effect skin moisturizing cream containing lithospermum erythrorhizon and other vegetable oils, and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN105476892A (en) |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106265346A (en) * | 2016-09-20 | 2017-01-04 | 无比滴（广东）药业有限公司 | A kind of both effectiveness external preparation containing Radix Arnebiae (Radix Lithospermi) extract |
| CN108420771A (en) * | 2018-06-08 | 2018-08-21 | 康柏利科技（苏州）有限公司 | A kind of zicao soft plaster and preparation method thereof |
| CN111544564A (en) * | 2020-04-29 | 2020-08-18 | 娇时日化（杭州）股份有限公司 | Ointment for treating infantile diaper dermatitis and preparation method thereof |
| CN111560289A (en) * | 2020-04-15 | 2020-08-21 | 青岛市妇女儿童医院（青岛市妇幼保健院、青岛市残疾儿童医疗康复中心、青岛市新生儿疾病筛查中心） | Method for preparing lithospermum oil by ultrasonic-assisted supercritical fluid extraction |
| CN113143804A (en) * | 2021-04-28 | 2021-07-23 | 广州亦妆生物科技有限公司 | Plant composition and application thereof |
| US11547734B2 (en) * | 2018-07-03 | 2023-01-10 | Mary Kay Inc. | Topical muscle relaxation compositions and methods |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20040131704A1 (en) * | 2003-01-03 | 2004-07-08 | Tammy Morse | A method of organic and all natural treatment, prevention and relief of diaper dermatitis and other related skin irritations. |
| CN103386215A (en) * | 2013-07-29 | 2013-11-13 | 嘉文丽（福建）化妆品有限公司 | Method for continuously extracting active components of Hibiscus taiwanensis by utilizing supercritical carbon dioxide |
-
2014
- 2014-09-17 CN CN201410471798.8A patent/CN105476892A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20040131704A1 (en) * | 2003-01-03 | 2004-07-08 | Tammy Morse | A method of organic and all natural treatment, prevention and relief of diaper dermatitis and other related skin irritations. |
| CN103386215A (en) * | 2013-07-29 | 2013-11-13 | 嘉文丽（福建）化妆品有限公司 | Method for continuously extracting active components of Hibiscus taiwanensis by utilizing supercritical carbon dioxide |
Non-Patent Citations (1)
| Title |
|---|
| 佚名: ""Burt’s bees RES-Q ointment"", 《COSDNA网站》 * |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106265346A (en) * | 2016-09-20 | 2017-01-04 | 无比滴（广东）药业有限公司 | A kind of both effectiveness external preparation containing Radix Arnebiae (Radix Lithospermi) extract |
| CN108420771A (en) * | 2018-06-08 | 2018-08-21 | 康柏利科技（苏州）有限公司 | A kind of zicao soft plaster and preparation method thereof |
| US11547734B2 (en) * | 2018-07-03 | 2023-01-10 | Mary Kay Inc. | Topical muscle relaxation compositions and methods |
| CN111560289A (en) * | 2020-04-15 | 2020-08-21 | 青岛市妇女儿童医院（青岛市妇幼保健院、青岛市残疾儿童医疗康复中心、青岛市新生儿疾病筛查中心） | Method for preparing lithospermum oil by ultrasonic-assisted supercritical fluid extraction |
| CN111544564A (en) * | 2020-04-29 | 2020-08-18 | 娇时日化（杭州）股份有限公司 | Ointment for treating infantile diaper dermatitis and preparation method thereof |
| CN113143804A (en) * | 2021-04-28 | 2021-07-23 | 广州亦妆生物科技有限公司 | Plant composition and application thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN105476892A (en) | Multi-effect skin moisturizing cream containing lithospermum erythrorhizon and other vegetable oils, and preparation method thereof | |
| CN103479775B (en) | Scraping liniment and preparation method thereof | |
| CN104292985B (en) | A kind of anion lavender fragrance wax crayon | |
| CN104382786A (en) | Hair loss prevention hair-blacking agent and preparation method thereof | |
| CN1943382B (en) | Tea capsule and its preparing method | |
| CN108392445B (en) | Herbal antipruritic lotion | |
| CN106265147A (en) | A kind of floral water containing natural plant essential oils and preparation method thereof | |
| CN103223010A (en) | Preparation method of traditional Chinese medicine spray with anti-mosquito function | |
| CN109464320A (en) | A kind of baby baths liquid and preparation method thereof | |
| CN105062726A (en) | Medicated soap for conditioning skin and weakening melanin | |
| CN103830440A (en) | Health care essential oil with sedative effect | |
| CN103735468A (en) | Cosmetics containing mosquito-expelling composition microcapsules | |
| CN103393801A (en) | Traditional Chinese medicine composite extract with effect of removing acnes, and preparation method and application thereof | |
| CN104906005A (en) | Production method of wet tissue | |
| CN107184483A (en) | High penetration camellia massage essential oil promoting blood circulation and removing obstruction in channels and preparation method thereof | |
| CN104721633A (en) | Clinical nursing incense with sterilizing and inflammation diminishing effects and preparation method of clinical nursing incense | |
| CN104839246A (en) | Bacteriostatic disinfection liquid for clinical laboratory and preparation method thereof | |
| CN106619373A (en) | Garlicin hand cream | |
| CN105147567A (en) | Papaya soothing cream containing various plant components | |
| CN103432040B (en) | Lavender skin cream | |
| CN102872240A (en) | Compound essential oil for relaxing and activating collaterals | |
| CN102860942A (en) | Nursing compound essential oil for eyes | |
| CN105079760A (en) | Lavender massaging cream for soothing channels and activating collaterals | |
| CN105641668A (en) | Traditional Chinese medicine composition for foot bathing and body bathing | |
| CN102860939B (en) | Breast fitness conditioning compound essential oil |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20160413 |
|
| WD01 | Invention patent application deemed withdrawn after publication |