CN104721868B - Compound Radix et Rhizoma Gynurae divaricatae solid air freshening agent and preparation method thereof - Google Patents
Compound Radix et Rhizoma Gynurae divaricatae solid air freshening agent and preparation method thereof Download PDFInfo
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- CN104721868B CN104721868B CN201510181974.9A CN201510181974A CN104721868B CN 104721868 B CN104721868 B CN 104721868B CN 201510181974 A CN201510181974 A CN 201510181974A CN 104721868 B CN104721868 B CN 104721868B
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- radix
- gynurae divaricatae
- rhizoma gynurae
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Abstract
The present invention provides a kind of compound Radix et Rhizoma Gynurae divaricatae solid air freshening agent and preparation method thereof；Include each component of following number：130~170 parts of Radix et Rhizoma Gynurae divaricatae, 30~70 parts of cordate houttuynia, 80~120 parts of cloves, 40~80 parts of radix glycyrrhizae, 3~7 parts of menthol, 0.08~0.12 part of lemon yellow, 0.8~1.2 part of edible water-soluble champignon plants essential oil；Present invention additionally comprises above-mentioned preparation method.Gas freshener of the present invention uses Radix et Rhizoma Gynurae divaricatae, cordate houttuynia, cloves, radix glycyrrhizae, menthol, natural pigment and plants essential oil as raw material, using extraction by steam distillation extract, it is aided with agar, sodium carboxymethylcellulose prepares solid air freshening agent, the freshener have antibacterial, fresh air, it is pollution-free, have no toxic side effect, and store, carry it is easy to use.
Description
Technical field
The invention belongs to solid air freshening agent preparation method, is related to compound Radix et Rhizoma Gynurae divaricatae solid air freshening agent and its system
Preparation Method.
Background technology
In recent years, air quality declines increasingly, and pollution problem is increasingly severe.2015, National Meteorological Bureau was in whole year
In the competition of ten macroclimate events, haze is classified as a major issue for concerning the people's livelihood, reflecting that haze becomes can not currently escape
Social concern.The multiple cities in China, such as Beijing, Lanzhou, Taiyuan, Xi'an, Tianjin suffer from the invasion and attack of haze, and PM2.5 is dense
Degree is remained high, and largely inhalable particulate and noxious material, respiratory disease (infection of the upper respiratory tract, heavy breathing are left floating in air
Asthma, conjunctivitis, bronchitis etc.) incidence constantly increase.
Currently, common air sanitizer is mainly chemicals, such as Peracetic acid, lactic acid, hydrogen peroxide, formaldehyde, 84
Thimerosal, glutaraldehyde etc., the in addition also physical method such as ultraviolet irradiation, ozone generator.Above method can be killed effectively
Pathogenic microorganisms, effect is rapid, and valid density is low, and effect is preferable, but also there are it is certain the defects of, stimulated as Peracetic acid has
Property, there is very strong corrosivity to metal, and lasting effect is poor；Some disinfectants form pollutant, peculiar smell after disinfection again in itself
It cannot eliminate quickly, long-time service has human body the danger of accumulation of poisoning, influences health, such as formaldehyde to some extent；It is purple
All personnel must leave the theatre when outside line sterilizes, and operating system will have safeguard procedures；Ozone generator higher price, and it is not portable
Band.
And above problem one kind can remove can kill be harmful to pathogenic microorganism, but also with it is safe efficient, have no toxic side effect,
Storage and air freshener easy to use are by as the important topic of research.
The content of the invention
For in the prior art the defects of, the object of the present invention is to provide a kind of compound Radix et Rhizoma Gynurae divaricatae solid air freshening agent
And preparation method thereof.
The present invention is achieved by the following technical solutions：
In a first aspect, the present invention relates to a kind of compound Radix et Rhizoma Gynurae divaricatae solid air freshening agent, include each group of following number
Point：
Wherein, the number is mass fraction or volume parts.
Preferably, each component of following number is included：
Wherein, the number is mass fraction or volume parts.
Second aspect, it is described the invention further relates to the preparation method of foregoing compound Radix et Rhizoma Gynurae divaricatae solid air freshening agent
Method and step is as follows：
Step 1：Radix et Rhizoma Gynurae divaricatae is weighed by the number, cordate houttuynia, cloves, radix glycyrrhizae, puts in round-bottomed flask, adds distilled water
500mL, soaks 1h, is heated to 70 DEG C with electric jacket, continuously extracts 4h, collect the distillation of certain volume；
Step 2：Tween-80 1mL drops are added in distillation to shake up, addition menthol, glass bar is stirred to being completely dissolved,
Obtain solution 1；
Step 3：Take agar 1.0g, sodium cellulose glycolate 0.5g to put in beaker, distilled water 50mL is added, on electromagnetic oven
Heating is boiled to being completely dissolved, and obtains solution 2；
Step 4：1 to 60 DEG C or so of the solution is put, adds the solution 2, adds lemon yellow, edible water-soluble champignon
Plants essential oil, stirs evenly；
Step 5：Pour into clean vessel, got product after cooling, solidification.
Preferably, in step 1, the distillation is aqueous and volatile oil.
Preferably, each component of following number is included：
Wherein, the number is mass fraction or volume parts；
Or include each component of following number：
Wherein, the number is mass fraction or volume parts.
The Radix et Rhizoma Gynurae divaricatae is national new resource food, its is edible for each different stages of growth, each growth and development stage
Part belongs to level-one vegetables scope, is the medical and edible dual purpose plant among the people commonly used.Indoor placement also has sterilizing and purifying air
Effect.Research shows that Radix et Rhizoma Gynurae divaricatae has a variety of works such as hypoglycemic, lowering blood pressure and blood fat, liver protection, protection stomach lining, anti-oxidant
With.
The cordate houttuynia is medical and edible dual purpose plant, and among the people edible with a long history, its preparation has the stronger disease-resistant micro- life of original
Thing acts on, and inside and outside is to a variety of gram positive bacterias such as staphylococcus aureus, hemolytic streptococcus, pneumococcus, tubercle bacillus
Etc. inhibited.Meanwhile decanoy acetaldehyde also has anti-inflammatory, suppresses influenza virus, antidiarrheal, treatment acute upper respiratory infection etc.
Effect.
The cloves acrid flavour, it is warm-natured, have middle benefit gas drop inverse, the effect of tonifying the kidney and support yang.Volatile oil in cloves have antibacterial,
Anti-inflammatory, antiviral and other effects, eugenol also has efficient acaricidal action in its volatile oil.
The radix glycyrrhizae is sweet in flavor, mild-natured, can coordinating the drug actions of a prescription.
The menthol is a kind of cyclic alcohol of the saturation obtained in peppermint, has the special aroma of peppermint, to large intestine
The inhibitory action such as bacillus, staphylococcus aureus are preferable, and fragrant odour.
Compared with prior art, the present invention has following beneficial effect：
(1) present invention uses natural plant extracts, and prepare makes with resisting pathogenic microbes, fresh air, storage carrying
Prospect is had a vast market with convenient Traditional Chinese drug air refreshing agent.
(2) the method for the present invention uses Radix et Rhizoma Gynurae divaricatae, cordate houttuynia, cloves, radix glycyrrhizae, menthol, natural pigment and plants essential oil
For raw material, using extraction by steam distillation extract, it is aided with agar, sodium carboxymethylcellulose prepares solid air freshening agent,
The freshener have antibacterial, fresh air, it is pollution-free, have no toxic side effect, and store, carry it is easy to use.
Brief description of the drawings
Upon reading the detailed description of non-limiting embodiments with reference to the following drawings, further feature of the invention,
Objects and advantages will become more apparent upon：
Fig. 1 is the preparation method flow chart of the present invention.
Embodiment
With reference to specific embodiment, the present invention is described in detail.Following embodiments will be helpful to the technology of this area
Personnel further understand the present invention, but the invention is not limited in any way.It should be pointed out that the ordinary skill to this area
For personnel, without departing from the inventive concept of the premise, various modifications and improvements can be made.These belong to the present invention
Protection domain.
Embodiment 1~5
The present embodiment 1~5 is related to the preparation method of compound Radix et Rhizoma Gynurae divaricatae solid air freshening agent, each component such as following table
Shown in 1：
The preparation method of above-described embodiment 1~5 is as shown in Figure 1, it includes the following steps：
Step 1：Radix et Rhizoma Gynurae divaricatae is weighed by the number, cordate houttuynia, cloves, radix glycyrrhizae, puts in round-bottomed flask, adds distilled water
500mL, soaks 1h, is heated to 70 DEG C with electric jacket, continuously extracts 4h, collect the distillation of certain volume；
Step 2：Tween-80 1mL drops are added in distillation to shake up, addition menthol, glass bar is stirred to being completely dissolved,
Obtain solution 1；
Step 3：Take agar 1.0g, sodium cellulose glycolate 0.5g to put in beaker, distilled water 50mL is added, on electromagnetic oven
Heating is boiled to being completely dissolved, and obtains solution 2；
Step 4：1 to 60 DEG C or so of the solution is put, adds the solution 2, adds lemon yellow, edible water-soluble champignon
Plants essential oil, stirs evenly；
Step 5：Pour into clean vessel, got product after cooling, solidification.
Implementation result：Above-described embodiment 1~5 prepare solid air freshening agent using Radix et Rhizoma Gynurae divaricatae, cordate houttuynia, cloves,
Radix glycyrrhizae, menthol, natural pigment and plants essential oil are raw material, using extraction by steam distillation extract, are aided with agar, carboxylic first
Base sodium cellulosate prepares solid air freshening agent, the freshener have antibacterial, fresh air, it is pollution-free, have no toxic side effect, and store
Deposit, carry it is easy to use.
The specific embodiment of the present invention is described above.It is to be appreciated that the invention is not limited in above-mentioned
Particular implementation, those skilled in the art can make various deformations or amendments within the scope of the claims, this not shadow
Ring the substantive content of the present invention.
Claims (6)
1. a kind of compound Radix et Rhizoma Gynurae divaricatae solid air freshening agent, it is characterised in that include each component of the following raw material number：
Wherein, the raw material number is mass fraction or volume parts,
The compound Radix et Rhizoma Gynurae divaricatae solid air freshening agent is prepared by following steps：
Step 1：Radix et Rhizoma Gynurae divaricatae is weighed by the raw material number, cordate houttuynia, cloves, radix glycyrrhizae, puts in round-bottomed flask, adds distilled water
500mL, soaks 1h, is heated to 70 DEG C with electric jacket, continuously extracts 4h, collect the distillation of certain volume；
Step 2：Tween-80 1mL is added in distillation to shake up, and adds menthol, glass bar is stirred to being completely dissolved, obtained molten
Liquid 1；
Step 3：Take agar 1.0g, sodium cellulose glycolate 0.5g to put in beaker, add distilled water 50mL, heated on electromagnetic oven
Boil to being completely dissolved, obtain solution 2；
Step 4：The solution 1 is set to 60 DEG C, adds the solution 2, adds lemon yellow, edible water-soluble champignon plant essence
Oil, stirs evenly；
Step 5：Pour into clean vessel, got product after cooling, solidification.
2. compound Radix et Rhizoma Gynurae divaricatae solid air freshening agent as claimed in claim 1, it is characterised in that including the following raw material number
Each component：
Wherein, the raw material number is mass fraction or volume parts.
3. a kind of preparation method of compound Radix et Rhizoma Gynurae divaricatae solid air freshening agent as claimed in claim 1 or 2, its feature exist
In the method step is as follows：
Step 1：Radix et Rhizoma Gynurae divaricatae is weighed by the raw material number, cordate houttuynia, cloves, radix glycyrrhizae, puts in round-bottomed flask, adds distilled water
500mL, soaks 1h, is heated to 70 DEG C with electric jacket, continuously extracts 4h, collect the distillation of certain volume；
Step 2：Tween-80 1mL is added in distillation to shake up, and adds menthol, glass bar is stirred to being completely dissolved, obtained molten
Liquid 1；
Step 3：Take agar 1.0g, sodium cellulose glycolate 0.5g to put in beaker, add distilled water 50mL, heated on electromagnetic oven
Boil to being completely dissolved, obtain solution 2；
Step 4：The solution 1 is set to 60 DEG C, adds the solution 2, adds lemon yellow, edible water-soluble champignon plant essence
Oil, stirs evenly；
Step 5：Pour into clean vessel, got product after cooling, solidification.
4. the preparation method of compound Radix et Rhizoma Gynurae divaricatae solid air freshening agent as claimed in claim 3, it is characterised in that step 1
In, the distillation is aqueous and volatile oil.
5. the preparation method of compound Radix et Rhizoma Gynurae divaricatae solid air freshening agent as claimed in claim 3, it is characterised in that including such as
The each component of lower raw material number：
Wherein, the raw material number is mass fraction or volume parts.
6. the preparation method of compound Radix et Rhizoma Gynurae divaricatae solid air freshening agent as claimed in claim 3, it is characterised in that including such as
The each component of lower raw material number：
Wherein, the raw material number is mass fraction or volume parts.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510181974.9A CN104721868B (en) | 2015-04-16 | 2015-04-16 | Compound Radix et Rhizoma Gynurae divaricatae solid air freshening agent and preparation method thereof |
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|---|---|---|---|
| CN201510181974.9A CN104721868B (en) | 2015-04-16 | 2015-04-16 | Compound Radix et Rhizoma Gynurae divaricatae solid air freshening agent and preparation method thereof |
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| CN104721868A CN104721868A (en) | 2015-06-24 |
| CN104721868B true CN104721868B (en) | 2018-05-08 |
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| CN106729872A (en) * | 2016-12-10 | 2017-05-31 | 钦州学院 | A kind of air freshener and preparation method thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP4201222B2 (en) * | 1998-09-30 | 2008-12-24 | ネイチャーテクノロジー株式会社 | Filamentous growth inhibiting composition and filamentous growth inhibiting agent |
| CN102423026A (en) * | 2011-11-28 | 2012-04-25 | 黄珊珊 | Micronized Stahlianthus involucratus jelly |
| CN103041424A (en) * | 2012-12-28 | 2013-04-17 | 青岛润鑫伟业科贸有限公司 | Novel air freshener prepared from composite gas raw materials |
| CN103191039A (en) * | 2013-04-10 | 2013-07-10 | 江苏华生安颐生物科技有限公司 | Mouthwash as well as preparation method and application thereof |
| CN103349789A (en) * | 2013-06-18 | 2013-10-16 | 上海市静安区教育学院附属学校 | Solid air freshening agent and its preparation method |
-
2015
- 2015-04-16 CN CN201510181974.9A patent/CN104721868B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP4201222B2 (en) * | 1998-09-30 | 2008-12-24 | ネイチャーテクノロジー株式会社 | Filamentous growth inhibiting composition and filamentous growth inhibiting agent |
| CN102423026A (en) * | 2011-11-28 | 2012-04-25 | 黄珊珊 | Micronized Stahlianthus involucratus jelly |
| CN103041424A (en) * | 2012-12-28 | 2013-04-17 | 青岛润鑫伟业科贸有限公司 | Novel air freshener prepared from composite gas raw materials |
| CN103191039A (en) * | 2013-04-10 | 2013-07-10 | 江苏华生安颐生物科技有限公司 | Mouthwash as well as preparation method and application thereof |
| CN103349789A (en) * | 2013-06-18 | 2013-10-16 | 上海市静安区教育学院附属学校 | Solid air freshening agent and its preparation method |
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