CN111713517A - Plant source air disinfectant and preparation method thereof - Google Patents

Plant source air disinfectant and preparation method thereof Download PDF

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Publication number
CN111713517A
CN111713517A CN202010643755.9A CN202010643755A CN111713517A CN 111713517 A CN111713517 A CN 111713517A CN 202010643755 A CN202010643755 A CN 202010643755A CN 111713517 A CN111713517 A CN 111713517A
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parts
extract
oil
essential oil
air disinfectant
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CN202010643755.9A
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Inventor
徐德锋
陈秀竹
胡航
龚顺泽
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Taizhou Yunong Biotechnology Co.,Ltd.
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Nanjing Hope Pharm Co ltd
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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N25/00Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
    • A01N25/30Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests characterised by the surfactants
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N31/00Biocides, pest repellants or attractants, or plant growth regulators containing organic oxygen or sulfur compounds
    • A01N31/02Acyclic compounds
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • A01N65/12Asteraceae or Compositae [Aster or Sunflower family], e.g. daisy, pyrethrum, artichoke, lettuce, sunflower, wormwood or tarragon
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • A01N65/24Lauraceae [Laurel family], e.g. laurel, avocado, sassafras, cinnamon or camphor
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • A01N65/28Myrtaceae [Myrtle family], e.g. teatree or clove
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • A01N65/32Ranunculaceae [Buttercup family], e.g. hepatica, hydrastis or goldenseal
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/40Liliopsida [monocotyledons]
    • A01N65/48Zingiberaceae [Ginger family], e.g. ginger or galangal
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L9/00Disinfection, sterilisation or deodorisation of air
    • A61L9/01Deodorant compositions
    • A61L9/013Deodorant compositions containing animal or plant extracts, or vegetable material
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L2209/00Aspects relating to disinfection, sterilisation or deodorisation of air
    • A61L2209/20Method-related aspects
    • A61L2209/21Use of chemical compounds for treating air or the like

Abstract

The invention belongs to the technical field of daily chemicals, and particularly relates to a botanical air disinfectant and a preparation method thereof, wherein the botanical air disinfectant is prepared from the following raw materials in parts by weight: 2-5 parts of coptis chinensis extract, 1-3 parts of turmeric extract, 1-3 parts of water shield extract, 1-3 parts of eclipta extract, 0.2-1 part of patchouli essential oil, 0.2-1 part of mint oil, 0.2-1 part of cinnamon essential oil, 0.2-1 part of radix angelicae volatile oil, 0.2-1 part of eucalyptus oil, 0.1-0.5 part of nonionic surfactant, 30-50 parts of ethanol and 30-50 parts of purified water. The botanical air disinfectant disclosed by the invention is a botanical product, has no irritation and corrosivity, can effectively kill germs in the air, has aromatic smell, eliminates peculiar smell in the air, does not influence the normal life of people, is safe to use, wide in application range and has an obvious environment-friendly effect.

Description

Plant source air disinfectant and preparation method thereof
Technical Field
The invention relates to the technical field of daily chemicals, in particular to a botanical air disinfectant and a preparation method thereof.
Background
Indoor air pollution is 2-10 times higher than outdoor air pollution, and serious air pollution is even hundreds of times higher than outdoor air pollution. The indoor air pollutants mainly comprise gas pollutants and microbial pollutants, wherein the microbial pollutants comprise bacteria, viruses, pollen, dust mites and the like. Being in an air polluted room for a long time, the health care pillow is easy to cause lassitude, unsmooth breathing, inattention and reduction of metabolism capability, and serious people can also cause cancers. Especially children are in the development stage of the body, and the immune system is fragile and is more easily damaged by indoor air pollution, so that the indoor air disinfection is enhanced, the indoor air quality is improved, and the human health is promoted.
The current common air disinfection methods comprise an ozone method, an ultraviolet irradiation method and a chemical disinfection method, and the disinfection methods can kill pathogenic microorganisms, have high action speed and low effective concentration and obtain better disinfection effect. However, the disinfection methods have the problems of high toxicity, strong corrosiveness, high irritation and the like; improper use can seriously affect the health. All the personnel are required to leave the site during the ozone disinfection and the ultraviolet irradiation disinfection, and protective measures are required in the operation process; chemical disinfectants such as peroxyacetic acid, lactic acid, hydrogen peroxide and the like can not eliminate peculiar smell quickly after being disinfected, and have the risk of accumulation poisoning and the like on human bodies after being used for a long time. The traditional medicinal plants have good antibacterial and antiviral effects, can be used for preparing a plant source air disinfectant, can disinfect indoors in an environment-friendly and pollution-free manner, and has important social significance in research and development of the plant source air disinfectant.
Coptis chinensis Franch (Coptis chinensis Franch.) belongs to Ranunculaceae and Coptis chinensis is a perennial herb, and is a traditional Chinese medicinal material in Shennong Ben Cao Jing. Is bitter in taste and cold in nature, and has the effects of purging fire, detoxifying, clearing heat, eliminating dampness and the like. The main active components of the coptis chinensis comprise alkaloids such as berberine, coptisine, methyl coptisine, tetrandrine and the like, and the coptis chinensis has good antibacterial effect.
Turmeric (Curcuma longa L.) is a traditional Chinese medicinal material in China, and has the effects of resisting inflammation, resisting virus, resisting oxidation, reducing blood fat, protecting liver, benefiting gallbladder, resisting cancer and the like. The main active molecule in the turmeric is curcumin, and researches show that the turmeric curcumin and derivatives thereof can resist various viruses such as influenza virus, enveloped virus, coronavirus, respiratory syndrome virus and the like,
chinese invention patent publication No. CN 104255835A discloses that chamomile essential oil, peppermint oil, cinnamon essential oil, honeysuckle, patchouli essential oil, dandelion, coptis, aloe, salvia miltiorrhiza and the like are taken as raw materials to prepare a disinfectant in an air chamber, and Chinese invention patent publication No. CN 104604956A discloses an air chamber disinfectant prepared by taking patchouli essential oil, phellodendron, scutellaria, angelica dahurica, fructus cnidii, sophora flavescens, coptis, folium artemisiae argyi, astragalus membranaceus, magnolia officinalis, fructus forsythiae, liquorice, white, honeysuckle and the like as raw materials, and the disinfectant has the conditions of multiple traditional Chinese medicine components, complex process, unstable product quality and the like. Through patent search, no relevant research report that the coptis chinensis extract, the turmeric extract and the like are used as main components for producing the air indoor disinfectant is found at present.
Disclosure of Invention
Technical problem to be solved
Aiming at the defects of the prior art, the invention provides a botanical air disinfectant and a preparation method thereof, and solves the problems of high toxicity, strong corrosivity, high irritation and the like of the existing chemical air disinfectant; compared with the traditional Chinese medicine disinfectant in the prior art, the Chinese goldthread, the water shield, the turmeric and the eclipta are simultaneously selected, the antibacterial ranges of the Chinese goldthread, the water shield, the turmeric and the eclipta are complementary, and various pathogenic bacteria can be killed; the mint oil, the cinnamon essential oil, the angelica dahurica volatile oil and the eucalyptus oil are selected to have strong fragrance, and the effect of refreshing air can be achieved.
The invention has obvious bacteriostasis and sterilization effects, is safe and nontoxic, can be used as an air freshener, and improves the air quality of the working and learning environment of people.
(II) technical scheme
In order to solve the technical problems, the invention adopts a technical scheme that: the plant source air disinfectant and the preparation method thereof are provided, and are characterized in that the plant source air disinfectant is prepared from the following raw materials in parts by weight:
2-6 parts of coptis chinensis extract, 1-3 parts of turmeric extract, 1-3 parts of water shield extract, 1-3 parts of eclipta extract, 0.2-1 part of patchouli essential oil, 0.2-1 part of mint oil, 0.2-1 part of cinnamon essential oil, 0.2-1 part of radix angelicae volatile oil, 0.2-1 part of eucalyptus oil, 0.1-0.5 part of nonionic surfactant, 30-50 parts of ethanol and 30-50 parts of purified water.
In a preferred embodiment of the invention, the following raw materials are prepared in parts by weight:
3-5 parts of coptis chinensis extract, 1.5-2.5 parts of turmeric extract, 1.5-2.5 parts of water shield extract, 1.5-2.5 parts of eclipta extract, 0.4-0.8 part of patchouli essential oil, 0.4-0.8 part of mint oil, 0.4-0.8 part of cinnamon essential oil, 0.4-0.8 part of angelica dahurica volatile oil, 0.4-0.8 part of eucalyptus oil, 0.2-0.4 part of nonionic surfactant, 35-45 parts of ethanol and 35-45 parts of purified water.
In a preferred embodiment of the invention, the following raw materials are prepared in parts by weight: 4 parts of coptis extract, 2 parts of turmeric extract, 2 parts of water shield extract, 2 parts of eclipta extract, 0.6 part of patchouli essential oil, 0.6 part of peppermint oil, 0.6 part of cinnamon essential oil, 0.6 part of angelica volatile oil, 0.6 part of eucalyptus oil, 0.3 part of nonionic surfactant, 40 parts of ethanol and 40 parts of purified water.
Preferably, the coptis chinensis extract, the turmeric extract, the water shield extract and the eclipta extract are all extracts obtained by sequentially cleaning, refining and concentrating fresh coptis chinensis, turmeric, water shield and eclipta raw materials.
The nonionic surfactant is one or more of lauryl oleyl alcohol, palmityl alcohol, polyoxyethylene lauryl amine fatty acid ester, polyoxyethylene laurate, dodecyl phenol polyoxyethylene ether and tween-80;
firstly, adding a nonionic surfactant and water into a mixing kettle, and stirring and mixing for 15-30min at the temperature of 20-35 ℃ and the rotating speed of 800r/min at 400-;
secondly, sequentially adding the coptis extract, the turmeric extract, the water shield extract and the eclipta extract into a mixing kettle, adding alcohol, stirring and mixing for 15-30min at 65-75 ℃ and the rotating speed of 400-;
thirdly, adding the plant extract essential oil prepared in the second step into the active water prepared in the first step, stirring and mixing for 15-30min at the temperature of 20-35 ℃ and the rotating speed of 400-800r/min, then sequentially adding the selected patchouli essential oil, the mint oil, the cinnamon essential oil, the angelica volatile oil and the eucalyptus oil into a mixing kettle, stirring and mixing for 1-2h at the temperature of 20-35 ℃ and the rotating speed of 400-800r/min, and fully mixing the mixtures to obtain a finished product of the plant source air disinfectant;
and fourthly, detecting, filling and packaging the finished product of the plant-source air disinfectant prepared in the third step to obtain a marketable product of the plant-source air disinfectant.
(III) advantageous effects
The invention has the beneficial effects that the plant source air disinfectant and the preparation method thereof are provided, the air disinfectant prepared from the berberine, the curcumin, the brasenia schreberi polysaccharide and the vanillic ether compound has better antibacterial disinfection effect, and the natural aromatic odor and the antibacterial effect of essential oil of patchouli, mint, cinnamon, angelica dahurica and the like which are natural sources can be fully utilized to achieve the effect of refreshing air.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below, and these examples are only illustrative of the present invention and do not limit the scope of the present invention.
The first embodiment is as follows:
the plant source air disinfectant and the preparation method thereof are provided, and the preparation raw materials comprise the following components in parts by weight: 6 parts of coptis extract, 3 parts of turmeric extract, 3 parts of water shield extract, 3 parts of eclipta extract, 1 part of patchouli essential oil, 1 part of peppermint oil, 0.2 part of cinnamon essential oil, 1 part of angelica volatile oil, 0.2 part of eucalyptus oil, 0.5 part of nonionic surfactant (0.3 part of lauryl alcohol and 0.2 part of dodecyl phenol polyoxyethylene ether), 50 parts of ethanol and 30 parts of purified water.
Firstly, adding 0.3 part of lauryl alcohol oleyl alcohol, 0.2 part of dodecyl phenol polyoxyethylene ether, and 30 parts of non-ionic surfactant and purified water into a mixing kettle, and stirring and mixing for 15min at 35 ℃ and 800r/min to prepare active water for later use;
secondly, sequentially adding 6 parts of coptis extract, 3 parts of turmeric extract, 3 parts of water shield extract and 3 parts of eclipta extract into a mixing kettle, adding 50 parts of alcohol, stirring and mixing for 15min at 75 ℃ and at the rotating speed of 800r/min with 400-;
thirdly, adding the plant extract essential oil prepared in the second step into the active water prepared in the first step, stirring and mixing for 15min at 35 ℃ and at the rotating speed of 800r/min, then sequentially adding 1 part of patchouli essential oil, 1 part of peppermint oil, 0.2 part of cinnamon essential oil, 1 part of radix angelicae volatile oil and 0.2 part of eucalyptus oil into a mixing kettle, stirring and mixing for 1h at 35 ℃ and at the rotating speed of 800r/min, and fully mixing the mixtures until uniform liquid is formed, thus obtaining a plant source air disinfectant finished product;
and fourthly, detecting, filling and packaging the finished product of the plant-source air disinfectant prepared in the third step to obtain a marketable product of the plant-source air disinfectant.
The nonionic surfactant is a mixture of lauryl alcohol oleyl alcohol and dodecyl phenol polyoxyethylene ether.
Example 2
The plant source air disinfectant and the preparation method thereof are provided, and the preparation raw materials comprise the following components in parts by weight: 3 parts of coptis extract, 1.5 parts of turmeric extract, 1.5 parts of water shield extract, 1.5 parts of eclipta extract, 0.4 part of patchouli essential oil, 0.4 part of peppermint oil, 0.8 part of cinnamon essential oil, 0.4 part of angelica volatile oil, 0.4 part of eucalyptus oil, 0.4 part of nonionic surfactant (0.2 part of palmityl alcohol and 0.4 part of tween-800.2), 35 parts of ethanol and 45 parts of purified water.
Firstly, adding 0.2 part of palmityl alcohol, 0.78 part of tween-800.2 part of nonionic surfactant and 45 parts of purified water into a mixing kettle, and stirring and mixing for 30min at the temperature of 25 ℃ and the rotating speed of 400r/min to prepare active water for later use;
secondly, sequentially adding 3 parts of coptis chinensis extract, 1.5 parts of turmeric extract, 1.5 parts of water shield extract and 1.5 parts of eclipta extract into a mixing kettle, adding 35 parts of alcohol, stirring and mixing for 30min at 65 ℃ and the rotating speed of 400r/min, cooling to room temperature, and filtering insoluble substances to obtain plant extract essential oil for later use;
thirdly, adding the plant extract essential oil prepared in the second step into the active water prepared in the first step, stirring and mixing for 30min at 25 ℃ and the rotating speed of 400r/min, then sequentially adding 0.4 part of pogostemon cablin essential oil, 0.4 part of peppermint oil, 0.8 part of cinnamon essential oil, 0.4 part of angelica dahurica volatile oil and 0.4 part of eucalyptus oil into a mixing kettle, stirring and mixing for 2h at 25 ℃ and the rotating speed of 400r/min, and fully mixing all the mixtures until uniform liquid is formed, thus obtaining a finished product of the botanical air disinfectant;
and fourthly, detecting, filling and packaging the finished product of the plant-source air disinfectant prepared in the third step to obtain a marketable product of the plant-source air disinfectant.
The non-ionic surfactant is a mixture of palm alcohol and tween-80.
Example 3
The plant source air disinfectant and the preparation method thereof are provided, and the preparation raw materials comprise the following components in parts by weight: 4 parts of coptis extract, 2 parts of turmeric extract, 2 parts of water shield extract, 2 parts of eclipta extract, 0.6 part of patchouli essential oil, 0.6 part of peppermint oil, 0.6 part of cinnamon essential oil, 0.6 part of angelica volatile oil, 0.6 part of eucalyptus oil, 0.3 part of nonionic surfactant (0.1 part of polyoxyethylene lauryl amine fatty acid ester, 0.1 part of polyoxyethylene laurate and 0.1 part of dodecylphenol polyoxyethylene ether), 40 parts of ethanol and 40 parts of purified water.
Firstly, adding 0.1 part of polyoxyethylene lauryl amine fatty acid ester, 0.1 part of polyoxyethylene laurate, 0.1 part of dodecyl phenol polyoxyethylene ether, and 40 parts of purified water into a mixing kettle, and stirring and mixing for 30min at 25 ℃ and the rotating speed of 400r/min to prepare active water for later use;
secondly, sequentially adding 4 parts of coptis chinensis extract, 2 parts of turmeric extract, 2 parts of water shield extract and 2 parts of eclipta extract into a mixing kettle, adding 40 parts of alcohol, stirring and mixing for 25min at 70 ℃ and at the rotating speed of 600r/min, cooling to room temperature, and filtering insoluble substances to obtain plant extract essential oil for later use;
thirdly, adding the plant extract essential oil prepared in the second step into the active water prepared in the first step, stirring and mixing for 20min at the temperature of 30 ℃ and the rotating speed of 600r/min, then sequentially adding 0.6 part of patchouli essential oil, 0.6 part of peppermint oil, 0.6 part of cinnamon essential oil, 0.6 part of angelica volatile oil and 0.6 part of eucalyptus oil into a mixing kettle, stirring and mixing for 1.5h at the temperature of 30 ℃ and the rotating speed of 600r/min, and fully mixing the mixtures until uniform liquid is formed, thus obtaining a finished product of the plant source air disinfectant;
and fourthly, detecting, filling and packaging the finished product of the plant-source air disinfectant prepared in the third step to obtain a marketable product of the plant-source air disinfectant.
The nonionic surfactant is a mixture of polyoxyethylene lauryl amine fatty acid ester, polyoxyethylene laurate and dodecyl phenol polyoxyethylene ether.
EXAMPLE 4 laboratory Sterilization test for air disinfectants
The plant source air disinfectant prepared in the embodiment 1-3 is subjected to a sterilization experiment at room temperature, and the result shows that the plant source air disinfectant prepared by the invention acts for 2min, and the average killing log values of staphylococcus aureus and escherichia coli are all more than 5.0; the results are shown in Table 1.
TABLE 1 Effect of botanical air disinfectants on bacteria
Figure RE-GDA0002606623880000061
Note that log kill value (KL) is log mean viable concentration of control group (N0) -log mean viable concentration of experimental group (NX).
EXAMPLE 5 indoor Sterilization test with air disinfectant
Selecting a room with approximately same volume and capable of being sealed, and respectively spraying 84% disinfectant and 30% disinfectantThe spraying amount of the alcohol solution and the plant source air disinfectant obtained in the examples 1-3 is 2mL/m3. And (3) sealing the room after spraying, keeping 1 person in the room, measuring the settled bacteria every 30min before and after spraying, respectively arranging a sampling point in the diagonal line and the middle of each room, wherein each group of bacteria and mould culture dishes are respectively 3, the sampling points are arranged at the positions 1.2 m higher than the ground, and the culture dishes with the diameter of 90mm are used for sampling for 15 min. After sampling, culturing for 48h at 30 e-35 e and culturing for 72h at 23 e-28 e respectively, repeating the test for 1 time every other week, and recording the colony number of each group. Colony count (cfu/m) using the formula3) 50000N/AT, wherein A is the area of the culture dish (cm)2) T is the exposure time (min) of the culture dish, N is the average colony count (cfu/dish) of the culture dish, i.e., (cfu/m)3) 52.4N, calculate cfu/m3
Thus, when the air disinfectant reaches 100g/m in 1 hour by the dosage of each cubic meter3The bactericidal effect test is shown in table 2.
TABLE 2 indoor sterilizing effect of botanical air disinfectant
Figure RE-GDA0002606623880000071
Therefore, the plant source air disinfectant prepared by the invention overcomes the problems of irritation, corrosivity and the like of the existing chemical disinfectant, is a plant source product, can effectively kill germs in the air, has aromatic smell, eliminates peculiar smell in the air, and does not influence the normal life of people.
The foregoing description of specific embodiments of the present invention has been presented. It is to be understood that the present invention is not limited to the specific embodiments described above, and that various changes and modifications may be made by one skilled in the art within the scope of the appended claims without departing from the spirit of the invention.

Claims (6)

1. A plant source air disinfectant and a preparation method thereof are characterized by comprising the following preparation raw materials in parts by weight: 2-5 parts of coptis chinensis extract, 1-3 parts of turmeric extract, 1-3 parts of water shield extract, 1-3 parts of eclipta extract, 0.2-1 part of patchouli essential oil, 0.2-1 part of mint oil, 0.2-1 part of cinnamon essential oil, 0.2-1 part of radix angelicae volatile oil, 0.2-1 part of eucalyptus oil, 0.1-0.5 part of nonionic surfactant, 30-50 parts of ethanol and 30-50 parts of purified water.
The preparation method of the plant source air disinfectant comprises the following steps:
firstly, adding a nonionic surfactant and water into a mixing kettle, and stirring and mixing for 15-30min at the temperature of 20-35 ℃ and the rotating speed of 800r/min at 400-;
secondly, sequentially adding the coptis extract, the turmeric extract, the water shield extract and the eclipta extract into a mixing kettle, adding alcohol, stirring and mixing for 15-30min at 65-75 ℃ and the rotating speed of 400-;
thirdly, adding the plant extract essential oil prepared in the second step into the active water prepared in the first step, stirring and mixing for 15-30min at the temperature of 20-35 ℃ and the rotating speed of 400-800r/min, then sequentially adding the selected patchouli essential oil, the mint oil, the cinnamon essential oil, the angelica volatile oil and the eucalyptus oil into a mixing kettle, stirring and mixing for 1-2h at the temperature of 20-35 ℃ and the rotating speed of 400-800r/min, and fully mixing the mixtures to obtain a finished product of the plant source air disinfectant;
and fourthly, detecting, filling and packaging the finished product of the plant-source air disinfectant prepared in the third step to obtain a marketable product of the plant-source air disinfectant.
2. The botanical air disinfectant as claimed in claim 1, wherein the preferable conditions include, by weight, 3-5 parts of coptis chinensis extract, 1.5-2.5 parts of turmeric extract, 1.5-2.5 parts of water shield extract, 1.5-2.5 parts of eclipta extract, 0.4-0.8 part of patchouli essential oil, 0.4-0.8 part of peppermint oil, 0.4-0.8 part of cinnamon essential oil, 0.4-0.8 part of angelica volatile oil, 0.4-0.8 part of eucalyptus oil, 0.2-0.4 part of nonionic surfactant, 35-45 parts of ethanol and 35-45 parts of purified water.
3. The botanical air disinfectant as claimed in claim 1, wherein the preferred conditions include, by weight, 4 parts of coptis chinensis extract, 2 parts of turmeric extract, 2 parts of brasenia schreberi extract, 2 parts of eclipta alba extract, 0.6 part of pogostemon cablin essential oil, 0.6 part of peppermint oil, 0.6 part of cinnamon essential oil, 0.6 part of angelica dahurica volatile oil, 0.6 part of eucalyptus oil, 0.3 part of nonionic surfactant, 40 parts of ethanol and 40 parts of purified water.
4. The botanical air disinfectant as claimed in claim 1, wherein the coptis root extract, the turmeric extract, the water shield extract and the eclipta extract are all extracts obtained by selecting fresh coptis root, turmeric, water shield and eclipta raw materials and sequentially performing cleaning, refining and concentrating processes.
5. The botanical air disinfectant and preparation method thereof as claimed in claim 1, wherein said non-ionic surfactant is one or more of lauryl oleyl alcohol, palmityl alcohol, polyoxyethylene lauryl amine fatty acid ester, polyoxyethylene laurate, polyoxyethylene dodecylphenol ether, and tween-80.
6. The botanical air disinfectant and preparation method thereof as claimed in claim 1, wherein said ethanol is 95% medicinal ethanol.
CN202010643755.9A 2020-07-07 2020-07-07 Plant source air disinfectant and preparation method thereof Pending CN111713517A (en)

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Publication number Priority date Publication date Assignee Title
CN112587682A (en) * 2020-11-20 2021-04-02 福建傲农生物科技集团股份有限公司 Method for removing aerosol pollution in laboratory
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CN115119848A (en) * 2021-10-19 2022-09-30 湖南坤源生物科技有限公司 Disinfectant for livestock and poultry and preparation method thereof

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