CN110318139B - 一种抗紫外功能的纤维面料的制备方法 - Google Patents
一种抗紫外功能的纤维面料的制备方法 Download PDFInfo
- Publication number
- CN110318139B CN110318139B CN201910618611.5A CN201910618611A CN110318139B CN 110318139 B CN110318139 B CN 110318139B CN 201910618611 A CN201910618611 A CN 201910618611A CN 110318139 B CN110318139 B CN 110318139B
- Authority
- CN
- China
- Prior art keywords
- fiber
- fiber fabric
- solution
- fabric
- temperature
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- D—TEXTILES; PAPER
- D03—WEAVING
- D03D—WOVEN FABRICS; METHODS OF WEAVING; LOOMS
- D03D15/00—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M10/00—Physical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. ultrasonic, corona discharge, irradiation, electric currents, or magnetic fields; Physical treatment combined with treatment with chemical compounds or elements
- D06M10/04—Physical treatment combined with treatment with chemical compounds or elements
- D06M10/06—Inorganic compounds or elements
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M10/00—Physical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. ultrasonic, corona discharge, irradiation, electric currents, or magnetic fields; Physical treatment combined with treatment with chemical compounds or elements
- D06M10/04—Physical treatment combined with treatment with chemical compounds or elements
- D06M10/08—Organic compounds
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
- D06M11/50—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with hydrogen peroxide or peroxides of metals; with persulfuric, permanganic, pernitric, percarbonic acids or their salts
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/152—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen having a hydroxy group bound to a carbon atom of a six-membered aromatic ring
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/244—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus
- D06M13/282—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus with compounds containing phosphorus
- D06M13/292—Mono-, di- or triesters of phosphoric or phosphorous acids; Salts thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/35—Heterocyclic compounds
- D06M13/352—Heterocyclic compounds having five-membered heterocyclic rings
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/50—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with organometallic compounds; with organic compounds containing boron, silicon, selenium or tellurium atoms
- D06M13/51—Compounds with at least one carbon-metal or carbon-boron, carbon-silicon, carbon-selenium, or carbon-tellurium bond
- D06M13/513—Compounds with at least one carbon-metal or carbon-boron, carbon-silicon, carbon-selenium, or carbon-tellurium bond with at least one carbon-silicon bond
- D06M13/5135—Unsaturated compounds containing silicon atoms
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M16/00—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/04—Vegetal fibres
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/25—Resistance to light or sun, i.e. protection of the textile itself as well as UV shielding materials or treatment compositions therefor; Anti-yellowing treatments
-
- D—TEXTILES; PAPER
- D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2201/00—Cellulose-based fibres, e.g. vegetable fibres
- D10B2201/01—Natural vegetable fibres
-
- D—TEXTILES; PAPER
- D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2401/00—Physical properties
- D10B2401/13—Physical properties anti-allergenic or anti-bacterial
-
- D—TEXTILES; PAPER
- D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2401/00—Physical properties
- D10B2401/16—Physical properties antistatic; conductive
-
- D—TEXTILES; PAPER
- D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2401/00—Physical properties
- D10B2401/22—Physical properties protective against sunlight or UV radiation
Abstract
本发明涉及面料制备技术领域,特别涉及一种抗紫外功能的纤维面料的制备方法;在超声分散的作用下,PK‑抗静电剂能均匀分散到过硫酸铵溶液组成的无机相中,并均匀附着在甲壳素纤维的表面,后加入的4,4′‑二羟基二苯甲酮与甲壳素纤维表面的羟基、氨基相互作用,生成作用力较强的化学键,并将PK‑抗静电剂固定在甲壳素纤维和4,4′‑二羟基二苯甲酮组成的三维网络结构中,使得面料不仅具有强而持久的抗紫外功能;桑皮纤维和卡松以Y‑甲基丙烯酰氧基丙基三甲氧基硅烷作为连接的″桥梁″,使得卡松以化学键的形式牢牢固定在桑皮纤维的表面,提高了桑皮纤维的抗菌性能;纤维面料还能释放对人体健康有益的负离子和远红外,起到很好的保健和保暖的效果。
Description
技术领域
本发明涉及面料制备技术领域,特别涉及一种抗紫外功能的纤维面料的制备方法。
背景技术
面料就是用来制作服装的材料。作为服装三要素之一,面料不仅可以诠释服装的风格和特性,而且直接左右着服装的色彩、造型的表现效果。确分析识别面料性能并准确合理地运用于服装设计是每一个设计师需要掌握的基本知识,否则面料识别错误可能会导致整款服装的设计,制作,穿着或者洗涤等环节出现问题。服装面料的识别包括服装面料的原料识别,外观特征识别以及外观质量识别等。观察识别面料不仅要用视觉,而且要用听觉,触觉甚至嗅觉。如运用眼睛的视觉效应观看织物的光泽明暗,染色情况,表面粗细以及组织,纹路和纤维的外观特征,比如纯棉布光泽普通,外观不够细洁,粗糙甚至有棉结杂质,羊毛与涤纶混纺的呢绒光泽较亮,有闪色感,身骨略为搬硬而失之柔软,并随涤纶含量的增加而明显突出。缺乏柔和的柔润感,织物挺括。平整,光滑;运用手的触觉效应能够感觉到织物和纤维的软硬,光滑,粗细,弹性,冷暖等,用手还可以测出纤维中纱线的强度和伸长度。
不同的面料具有不同的透气性,吸湿性,保暖性等性能,比如棉织物具有良好的透气性和吸湿性,穿着舒适,保暖性好,是最理想的童装面料。选择面料时要确认面料的透气性,保温性,吸湿性,静电性等性能特征,再针对面料的挺括性,重量感,软硬度和悬垂性来考虑它适合做什么样的造型,做什么样的款式等。但是,现有的纤维面料的抗紫外功能较差,在长时间的太阳光的照射下其使用寿命缩短。
中国专利(CN108374223A)公开了一种可再生温敏纺织面料,将纤维经过含有抗静电悬浮液的温敏混合液浸泡作出得到相应的改性的经线和纬线,然后编织成具有温敏特性和抗静电的效果的面料。其虽然采用特定浸泡液进行改性处理得到具有特定效果的面料,但是因此得到面料不具备抗紫外性能,也不具备抗菌性能,而且纤维面料透气吸汗性能不好、舒适性不好;中国专利(CN108468134A)公开了一种抗菌防起毛面料的加工方法,将经线和纬线相互编织成所需的面料,经线由涤纶纤维和竹纤维混纺编织而成,然后将面料置于抗菌整理液液中浸扎处理得到。虽然其采用抗菌液浸扎处理具有抗菌效果的面料,但是并具备抗紫外、抗静电效果,而且透气吸汗性能差;中国专利(CN108642674A)公开了一种新型抗菌面料,该面料经线采用甲壳素抗菌纤维,纬线采用涤纶长丝纤维,这种面料抑菌除臭,防止静电,穿着更舒适。虽然其声称得到面料均匀抗菌、防静电效果,但是其抗菌、防静电效果并不明显,没有对经线和纬线经线特殊的改性处理,也不具备抗紫外的性能;中国专利(CN107881596A)一种抗静电纺织面料,其采用包覆有抗静电膜的经线和纬线编织而成,虽然也能得到具有抗静电性的面料,但是其透气性、舒适性差,而且不具备抗紫外、抗菌效果;中国专利(CN203137151U)公开了一种防紫外线泳衣面料,分为内外层,内层是由经纱和纬纱交织成,外层是防紫外线层。面料具有透气性好、舒适性好以及具有良好的抗紫外性,虽然其具备一定的抗紫外线性能,但是其专门设置抗紫外线层,导致面料柔性差,不适合作为休闲服饰用面料,而不具备抗静电和抗菌性能。
基于现有技术中的面料存在的各种问题,本发明提供一种新的抗紫外功能的纤维面料的制备方法。
发明内容
针对上述存在的问题,本发明提供了一种抗紫外功能的纤维面料的制备方法,用于解决背景技术中所提出的技术问题。
为了达到上述的目的,本发明采用以下的技术方案:
一种抗紫外功能的纤维面料的制备方法,包括以下步骤:
S1、室温下,将甲壳素纤维浸泡在氢氧化钠溶液中160~200min,然后用清水清洗干净,烘干备用;
S2、将S1中所得的甲壳素纤维浸泡在温度为40~55℃、浓度为1.2~1.8mol/L的过硫酸铵溶液中,并向其中加入质量为过硫酸铵溶液2.2~2.8%的PK-抗静电剂,超声分散30~45min后向其中加入质量为甲壳素纤维20~45%的4,4′-二羟基二苯甲酮,微波加热至温度为70~85℃,并持续向其中通入氮气约25~40min,保温静置160~200min;
S3、将S2中的甲壳素纤维捞出后在室温下进行纺丝,待自然凝固成型后,得改性甲壳素纤维;
S4、将桑皮纤维浸渍在温度为40~50℃的抗菌液中,浸渍时间为30~50min,然后将桑皮纤维捞出,并置于恒温干燥箱中在65~80℃的条件下对其进行干燥,得到改性桑皮纤维;
S5、以改性甲壳素纤维为纬线,改性桑皮纤维作为经线,利用喷气织机进行织造,制备纤维面料粗产品;
S6、量取适量的去离子水,并向其中分别加入质量为去离子水的6~9%的活性染料、14~20%的匀染剂;混合均匀后用冰醋酸调节pH至5~7,搅拌均匀得到染液,调节染液温度后备用;
S7、将S5所得的纤维面料粗产品置于等离子体仪中,并向其中充入氧气,处理时间为70~100s;
S8、将S7中的纤维面料粗产品取出并立即浸入S6中所得的染液中浸泡,浸泡时间为35~55min;然后取出纤维面料,烘焙3~7min;然后再经水洗和烘干定型,得到纤维面料成品。
优选的,所述S1中氢氧化钠溶液的浓度为3~5%。
抗菌液的制备方法为:取适量的去离子水,并用醋酸调节pH至3.5~4.8,然后向其中加入一定量的γ-甲基丙烯酰氧基丙基三甲氧基硅烷和卡松,混合搅拌均匀,然后向其中滴加浓度为6~8%的氨水溶液,调节pH至8.3~9.5,即得抗菌液成品。
优选的,所述S6中的匀染剂选用平平加O-25。
优选的,所述S7中充入氧气的速度为70~90mL/min。
优选的,所述S8中浸泡纤维粗面料产品时的浴比1∶30~40。
优选的,所述S8中的烘焙温度为70~85℃。
采用上述的技术方案,本发明达到的有益效果是:
1、本发明通过将甲壳素纤维浸泡在过硫酸铵溶液中,然后通过向其中加入PK-抗静电剂和4,4′-二羟基二苯甲酮,在超声分散的作用下,PK-抗静电剂能均匀分散到过硫酸铵溶液组成的无机相中,并均匀附着在甲壳素纤维的表面,后加入的4,4′-二羟基二苯甲酮与甲壳素纤维表面的羟基、氨基相互作用,生成作用力较强的化学键,并将PK-抗静电剂固定在甲壳素纤维和4,4′-二羟基二苯甲酮组成的三维网络结构中,使得面料不仅具有强而持久的抗紫外功能,而且具有很强的抗静电功能,延长了纤维面料的使用寿命。
2、将桑皮纤维浸渍在抗菌液中,其中抗菌液中的Y-甲基丙烯酰氧基丙基三甲氧基硅烷和卡松三者之间产生化学作用,即桑皮纤维和卡松以Y-甲基丙烯酰氧基丙基三甲氧基硅烷作为连接的″桥梁″,使得卡松以化学键的形式牢牢固定在桑皮纤维的表面,从而提高了桑皮纤维的抗菌性能。
3、本发明采用改性甲壳素和改性桑皮纤维作为制备纤维面料的原料,所制备的纤维面料不仅具有很好的抗紫外、抗静电和抗菌性。同时其还具有很好的透气吸汗性能,穿着十分地舒适。更为重要的是本发明所制备的纤维面料还能释放对人体健康有益的负离子和远红外,起到很好的保健和保暖的效果。
具体实施方式
为使本发明实施例的目的、技术方案和优点更加清楚,下面将结合本发明实施例,对本发明实施例中的技术方案进行清楚、完整地描述。基于本发明的实施例,本领域普通技术人员在没有作出创造性劳动前提下所获得的所有其他实施例,都属于本发明保护的范围。
实施例1:
一种抗紫外功能的纤维面料的制备方法,包括以下步骤:
S1、室温下,将甲壳素纤维浸泡在氢氧化钠溶液中160min,然后用清水清洗干净,烘干备用;
S2、将S1中所得的甲壳素纤维浸泡在温度为40~55℃、浓度为1.2mol/L的过硫酸铵溶液中,并向其中加入质量为过硫酸铵溶液2.2%的PK-抗静电剂,超声分散30min后向其中加入质量为甲壳素纤维20%的4,4′-二羟基二苯甲酮,微波加热至温度为70℃,并持续向其中通入氮气约25min,保温静置160min;
S3、将S2中的甲壳素纤维捞出后在室温下进行纺丝,待自然凝固成型后,得改性甲壳素纤维;
S4、将桑皮纤维浸渍在温度为40℃的抗菌液中,浸渍时间为30min,然后将桑皮纤维捞出,并置于恒温干燥箱中在65℃的条件下对其进行干燥,得到改性桑皮纤维;
S5、以改性甲壳素纤维为纬线,改性桑皮纤维作为经线,利用喷气织机进行织造,制备纤维面料粗产品;
S6、量取适量的去离子水,并向其中分别加入质量为去离子水的6%的活性染料、14%的匀染剂;混合均匀后用冰醋酸调节pH至5,搅拌均匀得到染液,调节染液温度后备用;
S7、将S5所得的纤维面料粗产品置于等离子体仪中,并向其中充入氧气,处理时间为70s;
S8、将S7中的纤维面料粗产品取出并立即浸入S6中所得的染液中浸泡,浸泡时间为35min;然后取出大豆纤维面料,烘焙3min;然后再经水洗和烘干定型,得到纤维面料成品。
所述S1中氢氧化钠溶液的浓度为3%。
抗菌液的制备方法为:取适量的去离子水,并用醋酸调节pH至3.5,然后向其中加入一定量的γ-甲基丙烯酰氧基丙基三甲氧基硅烷和卡松,混合搅拌均匀,然后向其中滴加浓度为6%的氨水溶液,调节pH至8.3,即得抗菌液成品。
所述S7中充入氧气的速度为70mL/min。
所述S8中浸泡纤维粗面料产品时的浴比1∶30。
所述S8中的烘焙温度为70℃。
实施例2:
一种抗紫外功能的纤维面料的制备方法,包括以下步骤:
S1、室温下,将甲壳素纤维浸泡在氢氧化钠溶液中180min,然后用清水清洗干净,烘干备用;
S2、将S1中所得的甲壳素纤维浸泡在温度为40~55℃、浓度为1.5mol/L的过硫酸铵溶液中,并向其中加入质量为过硫酸铵溶液2.5%的PK-抗静电剂,超声分散35min后向其中加入质量为甲壳素纤维30%的4,4′-二羟基二苯甲酮,微波加热至温度为75℃,并持续向其中通入氮气约30min,保温静置180min;
S3、将S2中的甲壳素纤维捞出后在室温下进行纺丝,待自然凝固成型后,得改性甲壳素纤维;
S4、将桑皮纤维浸渍在温度为45℃的抗菌液中,浸渍时间为40min,然后将桑皮纤维捞出,并置于恒温干燥箱中在75℃的条件下对其进行干燥,得到改性桑皮纤维;
S5、以改性甲壳素纤维为纬线,改性桑皮纤维作为经线,利用喷气织机进行织造,制备纤维面料粗产品;
S6、量取适量的去离子水,并向其中分别加入质量为去离子水的7%的活性染料、18%的匀染剂;混合均匀后用冰醋酸调节pH至6,搅拌均匀得到染液,调节染液温度后备用;
S7、将S5所得的纤维面料粗产品置于等离子体仪中,并向其中充入氧气,处理时间为90s;
S8、将S7中的纤维面料粗产品取出并立即浸入S6中所得的染液中浸泡,浸泡时间为50min;然后取出大豆纤维面料,烘焙5min;然后再经水洗和烘干定型,得到纤维面料成品。
所述S1中氢氧化钠溶液的浓度为4%。
抗菌液的制备方法为:取适量的去离子水,并用醋酸调节pH至4.5,然后向其中加入一定量的γ-甲基丙烯酰氧基丙基三甲氧基硅烷和卡松,混合搅拌均匀,然后向其中滴加浓度为7%的氨水溶液,调节pH至9.0,即得抗菌液成品。
所述S7中充入氧气的速度为80mL/min。
所述S8中浸泡纤维粗面料产品时的浴比1∶35。
所述S8中的烘焙温度为75℃。
实施例3:
一种抗紫外功能的纤维面料的制备方法,包括以下步骤:
S1、室温下,将甲壳素纤维浸泡在氢氧化钠溶液中200min,然后用清水清洗干净,烘干备用;
S2、将S1中所得的甲壳素纤维浸泡在温度为55℃、浓度为1.8mol/L的过硫酸铵溶液中,并向其中加入质量为过硫酸铵溶液2.8%的PK-抗静电剂,超声分散45min后向其中加入质量为甲壳素纤维45%的4,4′-二羟基二苯甲酮,微波加热至温度为85℃,并持续向其中通入氮气约40min,保温静置200min;
S3、将S2中的甲壳素纤维捞出后在室温下进行纺丝,待自然凝固成型后,得改性甲壳素纤维;
S4、将桑皮纤维浸渍在温度为40~50℃的抗菌液中,浸渍时间为50min,然后将桑皮纤维捞出,并置于恒温干燥箱中在80℃的条件下对其进行干燥,得到改性桑皮纤维;
S5、以改性甲壳素纤维为纬线,改性桑皮纤维作为经线,利用喷气织机进行织造,制备纤维面料粗产品;
S6、量取适量的去离子水,并向其中分别加入质量为去离子水的9%的活性染料、20%的匀染剂;混合均匀后用冰醋酸调节pH至7,搅拌均匀得到染液,调节染液温度后备用;
S7、将S5所得的纤维面料粗产品置于等离子体仪中,并向其中充入氧气,处理时间为100s;
S8、将S7中的纤维面料粗产品取出并立即浸入S6中所得的染液中浸泡,浸泡时间为55min;然后取出大豆纤维面料,烘焙7min;然后再经水洗和烘干定型,得到纤维面料成品。
所述S1中氢氧化钠溶液的浓度为5%。
抗菌液的制备方法为:取适量的去离子水,并用醋酸调节pH至4.8,然后向其中加入一定量的γ-甲基丙烯酰氧基丙基三甲氧基硅烷和卡松,混合搅拌均匀,然后向其中滴加浓度为8%的氨水溶液,调节pH至9.5,即得抗菌液成品。
所述S7中充入氧气的速度为90mL/min。
所述S8中浸泡纤维粗面料产品时的浴比1∶40。
所述S8中的烘焙温度为85℃。
产品性能检测:
分别对市售的纤维布料(对比例)和本发明中实施例1、实施例2、实施例3制备的纤维布料的性能进行测试,所得数据如下表所示:
项目名称 | UPF | 抗菌性/% | 吸湿率(g/g) |
实施例1 | 485 | 86.74 | 0.853 |
实施例2 | 476 | 83.27 | 0.894 |
实施例3 | 469 | 85.85 | 0.864 |
对比例 | 256 | 45.72 | 0.653 |
由上表可见,本发明制备的纤维面料的抗紫外功能、抗菌性和吸湿率均优于对比例。表明本发明制备的产品整体性能比对比例更好,具有更广阔的前景,更值得推广。
Claims (7)
1.一种抗紫外功能的纤维面料的制备方法,其特征在于,包括以下步骤:
S1、室温下,将甲壳素纤维浸泡在氢氧化钠溶液中160~200min,然后用清水清洗干净,烘干备用;
S2、将S1中所得的甲壳素纤维浸泡在温度为40~55℃、浓度为1.2~1.8mol/L的过硫酸铵溶液中,并向其中加入质量为过硫酸铵溶液2.2~2.8%的PK-抗静电剂,超声分散30~45min后向其中加入质量为甲壳素纤维20~45%的4,4′-二羟基二苯甲酮,微波加热至温度为70~85℃,并持续向其中通入氮气25~40min,保温静置160~200min;
S3、将S2中的甲壳素纤维捞出后在室温下进行纺丝,待自然凝固成型后,得改性甲壳素纤维;
S4、将桑皮纤维浸渍在温度为40~50℃的抗菌液中,浸渍时间为30~50min,然后将桑皮纤维捞出,并置于恒温干燥箱中在65~80℃的条件下对其进行干燥,得到改性桑皮纤维;
S5、以改性甲壳素纤维为纬线,改性桑皮纤维作为经线,利用喷气织机进行织造,制备纤维面料粗产品;
S6、量取适量的去离子水,并向其中分别加入质量为去离子水的6~9%的活性染料、14~20%的匀染剂;混合均匀后用冰醋酸调节pH至5~7,搅拌均匀得到染液,调节染液温度后备用;
S7、将S5所得的纤维面料粗产品置于等离子体仪中,并向其中充入氧气,处理时间为70~100s;
S8、将S7中的纤维面料粗产品取出并立即浸入S6中所得的染液中浸泡,浸泡时间为35~55min;然后取出纤维面料,烘焙3~7min;然后再经水洗和烘干定型,得到纤维面料成品。
2.根据权利要求1所述的一种抗紫外功能的纤维面料的制备方法,其特征在于:所述S1中氢氧化钠溶液的浓度为3~5%。
3.根据权利要求1所述的一种抗紫外功能的纤维面料的制备方法,其特征在于,所述S4中的抗菌液的制备方法为:取适量的去离子水,并用醋酸调节pH至3.5~4.8,然后向其中加入一定量的Y-甲基丙烯酰氧基丙基三甲氧基硅烷和卡松,混合搅拌均匀,然后向其中滴加浓度为6~8%的氨水溶液,调节pH至8.3~9.5,即得抗菌液成品。
4.根据权利要求1所述的一种抗紫外功能的纤维面料的制备方法,其特征在于:所述S6中的匀染剂选用平平加O-25。
5.根据权利要求1所述的一种抗紫外功能的纤维面料的制备方法,其特征在于:所述S7中充入氧气的速度为70~90mL/min。
6.根据权利要求1所述的一种抗紫外功能的纤维面料的制备方法其特征在于:所述S8中浸泡纤维粗面料产品时的浴比1∶30~40。
7.根据权利要求1所述的一种抗紫外功能的纤维面料的制备方法,其特征在于:所述S8中的烘焙温度为70~85℃。
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201910618611.5A CN110318139B (zh) | 2019-07-10 | 2019-07-10 | 一种抗紫外功能的纤维面料的制备方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201910618611.5A CN110318139B (zh) | 2019-07-10 | 2019-07-10 | 一种抗紫外功能的纤维面料的制备方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN110318139A CN110318139A (zh) | 2019-10-11 |
CN110318139B true CN110318139B (zh) | 2020-08-11 |
Family
ID=68123304
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201910618611.5A Active CN110318139B (zh) | 2019-07-10 | 2019-07-10 | 一种抗紫外功能的纤维面料的制备方法 |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN110318139B (zh) |
Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN112921444B (zh) * | 2021-03-09 | 2023-02-03 | 无锡市世纪风服饰有限公司 | 一种抗紫外功能纤维及其制备工艺 |
CN112981933B (zh) * | 2021-04-13 | 2022-03-29 | 东莞市帝诺电子材料有限公司 | 一种高强度黑色导电无纺布的制备方法 |
Family Cites Families (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2013177746A1 (zh) * | 2012-05-28 | 2013-12-05 | Zhu Yulan | 透气性能优异的家纺用布 |
CN105586686A (zh) * | 2014-10-24 | 2016-05-18 | 天津市兰纳针织服饰有限公司 | 一种可净化空气的绿色环保面料 |
CN106245193A (zh) * | 2016-08-24 | 2016-12-21 | 江苏中孚达科技股份有限公司 | 一种抗紫外线杀菌面料 |
CN108193481A (zh) * | 2017-12-30 | 2018-06-22 | 绍兴恒钧环保科技有限公司 | 抗菌抗紫外线锦棉面料制备方法 |
CN109440461B (zh) * | 2018-11-08 | 2021-06-15 | 珠海鑫康源新材料科技有限公司 | 新型抗菌防辐射银渗固纤维面料及其制备方法 |
-
2019
- 2019-07-10 CN CN201910618611.5A patent/CN110318139B/zh active Active
Also Published As
Publication number | Publication date |
---|---|
CN110318139A (zh) | 2019-10-11 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN103141975B (zh) | 一种竹纤维双点衬布的生产工艺 | |
CN102767083B (zh) | 一种免烫服装面料的加工方法 | |
CN107287754B (zh) | 一种仿棉全消光经编绒织物及其生产方法 | |
WO2021243940A1 (zh) | 抗菌防螨有机棉复合纤维面料及其加工工艺 | |
CN107858831B (zh) | 吸水透气性面料的制备方法 | |
CN106859265A (zh) | 一种防油、防污、防水的由高分子材料制成的窗帘及其加工工艺 | |
CN107268157A (zh) | 一种纺织毛巾面料 | |
CN103126140A (zh) | 一种羊绒衬布的生产工艺 | |
CN105926134A (zh) | 涤棉竹混纺机织面料 | |
CN110318139B (zh) | 一种抗紫外功能的纤维面料的制备方法 | |
CN104213305A (zh) | 一种新型仿棉床上纺织品面料及其制备方法 | |
WO2021097886A1 (zh) | 一种涤纶仿棉色织面料、及其制造方法和应用 | |
CN101942736A (zh) | 一种防透防紫外线弹性织物及其生产方法 | |
CN110356059B (zh) | 一种抗菌防紫外线面料 | |
CN104480610A (zh) | 一种含牛奶纤维的毛织物及其加工工艺 | |
CN110714265A (zh) | 一种竹纤维耐磨抗菌型罗纹针织布及其加工方法 | |
CN108625025B (zh) | 一种仿棉机织面料 | |
CN114318638B (zh) | 一种珍珠护肤高弹液氨棉多功能双面面料及其制备方法和应用 | |
CN214088824U (zh) | 一种醋涤变化芦席斜纹面料 | |
CN110760974A (zh) | 一种立体组织面料及其制备方法 | |
CN104611818A (zh) | 一种吸水柔软面料的生产工艺 | |
CN112064182B (zh) | 一种铜氨纤维的无缝形体保养内衣的生产方法 | |
CN212194512U (zh) | 一种顺滑光泽型高弹棉锦交织面料 | |
CN103710818A (zh) | 一种混纺机织衬衬布及其制备工艺 | |
CN209456651U (zh) | 一种生态超柔面料 |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
PB01 | Publication | ||
PB01 | Publication | ||
SE01 | Entry into force of request for substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
TA01 | Transfer of patent application right |
Effective date of registration: 20200717 Address after: 515000 north of Guangshan highway, Liannan village, Xiashan street, Chaonan District, Shantou City, Guangdong Province Applicant after: SHANTOU XUEGUO GARMENTS INDUSTRIAL Co.,Ltd. Address before: 325000 No. 8 Jiangbin Middle Road, Lucheng District, Wenzhou City, Zhejiang Province Applicant before: Wu Baoqin |
|
TA01 | Transfer of patent application right | ||
GR01 | Patent grant | ||
GR01 | Patent grant |