CN110271249B - 一种全遮光窗帘面料的制备方法 - Google Patents

一种全遮光窗帘面料的制备方法 Download PDF

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CN110271249B
CN110271249B CN201910552900.XA CN201910552900A CN110271249B CN 110271249 B CN110271249 B CN 110271249B CN 201910552900 A CN201910552900 A CN 201910552900A CN 110271249 B CN110271249 B CN 110271249B
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layer
temperature
coating
stirring
reaction
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CN110271249A (zh
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施法元
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Zhejiang Yuanzheng Cloth Co ltd
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Zhejiang Yuanzheng Cloth Co ltd
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    • A—HUMAN NECESSITIES
    • A47—FURNITURE; DOMESTIC ARTICLES OR APPLIANCES; COFFEE MILLS; SPICE MILLS; SUCTION CLEANERS IN GENERAL
    • A47H—FURNISHINGS FOR WINDOWS OR DOORS
    • A47H23/00—Curtains; Draperies
    • A47H23/02—Shapes of curtains; Selection of particular materials for curtains
    • A47H23/08—Selection of particular materials
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Abstract

本发明公开了一种全遮光窗帘面料的制备方法，包括如下步骤：步骤1，将二甲基二氯硅烷加入至乙醚中搅拌均匀，然后滴加蒸馏水并低温搅拌反应1‑3h，得到粘稠的初步水解液；步骤2，将基底布料平铺，并喷洒无水乙醇中完全润湿，然后将初步水解液均匀涂覆在基底布料表面，得到一级镀膜层；步骤3，将钛酸正丁酯加入至无水乙醇中，并加入甲基纤维素搅拌均匀，得到分散钛醇液，然后将黑色竹炭纤维加入至钛醇液中，搅拌形成分散悬浊液；步骤4，将分散悬浊液均匀涂覆在一级镀膜层表面，得到二级镀膜层，然后依次将色浆层和复合纤维层平覆在二级镀膜层表面，得到镀膜面料；步骤5，将镀膜面料梯度恒温加压反应3‑5h，降压冷却后得到全遮光窗帘面料。

Description

一种全遮光窗帘面料的制备方法
技术领域
本发明属于窗帘领域，具体涉及一种全遮光窗帘面料的制备方法。
背景技术
遮光门帘不仅能够给人们的私人空间提供最大程度的保护，而且具有调节室内光线、阻挡强光以及紫外线的功效，对人的皮肤有缓解衰老的作用，也可以保护家具的寿命，与此同时，遮光门帘夏天隔热，防蚊，冬天保温，为消费者创造了一个良好的家具环境。
遮光布的材质主要有两种：一种是正面为原始的胚布，背面是PVC涂层。价格较低，但环保性能差；第二种为网格状胚布上加PVC布，背面也是涂层，类似塑料质地，比前一种厚，遮光效果较好，缺点是比较脆，手感发硬、哗哗作响，不隔音，不隔热。
发明内容
针对现有技术中的问题，本发明提供一种全遮光窗帘面料的制备方法，解决了遮光布材质差，无法满足需求的问题，通过以甲基有机硅作为复合粘结剂，将色浆层和复合层凝固在基底布料表面，不仅提升了粘结稳定性，同时也提高了韧性和耐候性、防水、防盐雾、防霉菌等特性。
为实现以上技术目的，本发明的技术方案是：
一种全遮光窗帘面料的制备方法，包括如下步骤：
步骤1，将二甲基二氯硅烷加入至乙醚中搅拌均匀，然后滴加蒸馏水并低温搅拌反应1-3h，得到粘稠的初步水解液；
步骤2，将基底布料平铺，并喷洒无水乙醇中完全润湿，然后将初步水解液均匀涂覆在基底布料表面，得到一级镀膜层；
步骤3，将钛酸正丁酯加入至无水乙醇中，并加入甲基纤维素搅拌均匀，得到分散钛醇液，然后将黑色竹炭纤维加入至钛醇液中，搅拌形成分散悬浊液；
步骤4，将分散悬浊液均匀涂覆在一级镀膜层表面，得到二级镀膜层，然后依次将色浆层和复合纤维层平覆在二级镀膜层表面，得到镀膜面料；
步骤5，将镀膜面料梯度恒温加压反应3-5h，降压冷却后得到全遮光窗帘面料。
所述步骤1中的二甲基二氯硅烷在乙醚中的浓度为100-200g/L，所述滴加的速度为1-3mL/min，所述低温搅拌反应的搅拌速度为500-1000r/min，温度为2-6℃。
所述步骤2中的无水乙醇的喷洒量为1-3mL/cm2，所述均匀涂覆的涂覆量为5-10mL/cm2。
所述步骤3中的钛酸正丁酯在无水乙醇中的浓度为20-80g/L，甲基纤维素的加入量是钛酸正丁酯质量的10-15%，搅拌均匀的搅拌速度为500-800r/min，所述黑色竹炭纤维的加入量是钛酸正丁酯质量的150-300%。
所述步骤4中的均匀涂覆的涂覆量是5-10mL/cm2。
所述步骤4中的色浆层采用发泡色浆涂料纺丝编织而成，所述复合纤维层采用纳米纤维网，且所述纳米纤维网的厚度为0.1-0.9mm。
所述色浆层的制备方法如下：
步骤A，将聚丙烯酸钠加入至蒸馏水中，加入高取代羟丙基纤维素和水溶性色料低温超声分散30-60min，得到聚丙烯酸钠分散液；
步骤B，将聚丙烯酸钠分散液加入至静电纺丝机中静电纺丝反应，然后编织成单层纤维网；
步骤C，将电气石粉加入球磨机中湿法球磨30-60min，烘干后加入无水乙醇中搅拌均匀，得到浆料；
步骤D，将浆料均匀涂覆在单层纤维网表面，然后覆盖单层纤维网，重复2-3次，得到多层纤维网；
步骤E，将多层纤维网加入至烘箱内恒温反应2-4h，得到色浆层。
所述步骤A中的聚丙烯酸钠在蒸馏水中的浓度为100-500g/L，所述高取代羟丙基纤维素的加入量是聚丙烯酸钠质量的20-40%，所述水溶性色料的加入量是聚丙烯酸钠质量的2-8%，所述低温超声分散的温度为10-15℃，超声频率为20-40kHz；所述步骤B中的静电纺丝参数为：溶液推进速率为0.7-1.2mL/h，纺丝电压为15-25kV，接收距离为18-25cm，温度为100-120℃；步骤C中的湿法球磨的温度为30-50℃，所述浆料的浓度为100-500g/L；所述步骤D中的涂覆量为2-6g/L；所述步骤E中的恒温反应的温度为80-90℃，压力为0.12-0.15MPa。
所述步骤5中的梯度恒温加压反应的程序如下：
温度 时间 压力
80-90℃ 20-30min 0.1-0.2MPa
110-140℃ 剩余时间 0.2-0.3MPa
步骤1将二甲基二氯硅烷加入至乙醚中，形成溶解液，然后滴加蒸馏水促进水解反应，同时低温搅拌能够利用低温条件下水解产物的低活性，阻止团聚反应的形成，搅拌能够保证蒸馏水与二甲基二氯硅烷的充分接触，保证水解反应的彻底进行，得到粘稠的初步水解液。
步骤2将基底布料润湿，将布料形成浸液松软，打开布料丝线的空隙，通过均匀涂覆水解液的方式将水解产物均匀分布在布料表面，由于水与无水乙醇具有互溶特性，形成蒸馏水的快速渗透，进入丝线内，水解产物随着蒸馏水的渗透，充满丝线内部，形成丝线材料与水解产物的充分混合，得到充分渗透粘附的一级镀膜层。
步骤3将钛酸正丁酯加入至无水乙醇中，并采用甲基纤维素作为分散剂，搅拌均匀形成具有良好分散效果的钛醇液，然后将黑色竹炭纤维加入至钛醇液中搅拌均匀，由于甲基纤维素具有良好的分散体系，提升黑色竹炭纤维的分散效果。
步骤4将在悬浊液均匀涂覆在一级镀膜层表面，形成二级镀膜层，并在二级镀膜层上依次设置色浆层和复合纤维层，形成镀膜面料。
步骤5通过梯度恒温加压反应的方式促使一级镀膜层内的乙醚和蒸馏水、二级镀膜层内的无水乙醇快速去除，同时在镀膜过程中钛酸正丁酯遇水水解形成二氧化钛和丁酯，丁酯在反应过程中快速去除，而二氧化钛渗透至一级镀膜层内，加压过程能够一级镀膜层、二级镀膜层、色浆层和复合纤维层充分复合并固化，恒温反应还带来二甲基而氯硅烷的水解产物形成缩聚反应，达到立体网络结构，提升面料的稳定性，也保证了黑色竹炭纤维的均匀覆盖，达到全遮光效果。
步骤A将聚丙烯酸钠溶解在水中，因聚丙烯酸钠遇水膨胀，故此能够快速膨胀，形成水溶液胶体，将高取代羟丙基纤维素和水溶性色料加入溶液中，能够形成快速溶解，同时与胶体接触，达到渗透分散。
步骤B将聚丙烯酸钠分散液静电纺丝形成纤维纺丝，由于高取代羟丙基纤维素在静电纺丝中形成胶体固化，将蒸馏水转化为气态，形成良好的纺丝纤维，然后编织成单层纤维网，纤维丝内采用聚丙烯酸钠与高取代纤维素混合而成。
步骤C将电气石粉均匀球磨形成细粉颗粒，然后加入无水乙醇形成浆料。
步骤D将浆料均匀涂覆在单层纤维网表面，然后覆盖单层纤维网，重复几次，形成以浆料形成电气石粉膜为间隔层，以单层纤维网为固定层的多层纤维网，
步骤E将多层纤维网恒温反应，该过程中施加压力，确保多层纤维网形成加压，促使电气石粉挤压渗透至单层纤维网内，并且由于聚丙烯酸钠形成网络结构，能够对电气石粉形成固化，达到良好的紧密连接，不仅起到良好的色彩可控性，还能够释放负离子和杀菌。
从以上描述可以看出，本发明具备以下优点：
1.本发明解决了遮光布材质差，无法满足需求的问题，通过以甲基有机硅作为复合粘结剂，将色浆层和复合层凝固在基底布料表面，不仅提升了粘结稳定性，同时也提高了韧性和耐候性、防水、防盐雾、防霉菌等特性。
2.本发明以二甲基二氯硅烷为有机硅树脂的原材料，通过其水解产物缩聚固化过程与复合过程相结合，利用甲基硅树脂的立体网络结构形成渗透式固定，有效地提升了面料的牢固性与稳定性，同时提高了整体的弹性。
具体实施方式
结合实施例详细说明本发明，但不对本发明的权利要求做任何限定。
实施例1
一种全遮光窗帘面料的制备方法，包括如下步骤：
步骤1，将二甲基二氯硅烷加入至乙醚中搅拌均匀，然后滴加蒸馏水并低温搅拌反应1h，得到粘稠的初步水解液；
步骤2，将基底布料平铺，并喷洒无水乙醇中完全润湿，然后将初步水解液均匀涂覆在基底布料表面，得到一级镀膜层；
步骤3，将钛酸正丁酯加入至无水乙醇中，并加入甲基纤维素搅拌均匀，得到分散钛醇液，然后将黑色竹炭纤维加入至钛醇液中，搅拌形成分散悬浊液；
步骤4，将分散悬浊液均匀涂覆在一级镀膜层表面，得到二级镀膜层，然后依次将色浆层和复合纤维层平覆在二级镀膜层表面，得到镀膜面料；
步骤5，将镀膜面料梯度恒温加压反应3h，降压冷却后得到全遮光窗帘面料。
所述步骤1中的二甲基二氯硅烷在乙醚中的浓度为100g/L，所述滴加的速度为1mL/min，所述低温搅拌反应的搅拌速度为500r/min，温度为2℃。
所述步骤2中的无水乙醇的喷洒量为1mL/cm2，所述均匀涂覆的涂覆量为5mL/cm2。
所述步骤3中的钛酸正丁酯在无水乙醇中的浓度为20g/L，甲基纤维素的加入量是钛酸正丁酯质量的10%，搅拌均匀的搅拌速度为500r/min，所述黑色竹炭纤维的加入量是钛酸正丁酯质量的150%。
所述步骤4中的均匀涂覆的涂覆量是5mL/cm2。
所述步骤4中的色浆层采用发泡色浆涂料纺丝编织而成，所述复合纤维层采用纳米纤维网，且所述纳米纤维网的厚度为0.1mm。
所述色浆层的制备方法如下：
步骤A，将聚丙烯酸钠加入至蒸馏水中，加入高取代羟丙基纤维素和水溶性色料低温超声分散30min，得到聚丙烯酸钠分散液；
步骤B，将聚丙烯酸钠分散液加入至静电纺丝机中静电纺丝反应，然后编织成单层纤维网；
步骤C，将电气石粉加入球磨机中湿法球磨30min，烘干后加入无水乙醇中搅拌均匀，得到浆料；
步骤D，将浆料均匀涂覆在单层纤维网表面，然后覆盖单层纤维网，重复2次，得到多层纤维网；
步骤E，将多层纤维网加入至烘箱内恒温反应2h，得到色浆层。
所述步骤A中的聚丙烯酸钠在蒸馏水中的浓度为100g/L，所述高取代羟丙基纤维素的加入量是聚丙烯酸钠质量的20%，所述水溶性色料的加入量是聚丙烯酸钠质量的2%，所述低温超声分散的温度为10℃，超声频率为20kHz；所述步骤B中的静电纺丝参数为：溶液推进速率为0.7mL/h，纺丝电压为15kV，接收距离为18cm，温度为100℃；步骤C中的湿法球磨的温度为30℃，所述浆料的浓度为100g/L；所述步骤D中的涂覆量为2g/L；所述步骤E中的恒温反应的温度为80℃，压力为0.12MPa。
所述步骤5中的梯度恒温加压反应的程序如下：
温度 时间 压力
80℃ 20min 0.1MPa
110℃ 剩余时间 0.2MPa
实施例2
一种全遮光窗帘面料的制备方法，包括如下步骤：
步骤1，将二甲基二氯硅烷加入至乙醚中搅拌均匀，然后滴加蒸馏水并低温搅拌反应3h，得到粘稠的初步水解液；
步骤2，将基底布料平铺，并喷洒无水乙醇中完全润湿，然后将初步水解液均匀涂覆在基底布料表面，得到一级镀膜层；
步骤3，将钛酸正丁酯加入至无水乙醇中，并加入甲基纤维素搅拌均匀，得到分散钛醇液，然后将黑色竹炭纤维加入至钛醇液中，搅拌形成分散悬浊液；
步骤4，将分散悬浊液均匀涂覆在一级镀膜层表面，得到二级镀膜层，然后依次将色浆层和复合纤维层平覆在二级镀膜层表面，得到镀膜面料；
步骤5，将镀膜面料梯度恒温加压反应5h，降压冷却后得到全遮光窗帘面料。
所述步骤1中的二甲基二氯硅烷在乙醚中的浓度为200g/L，所述滴加的速度为3mL/min，所述低温搅拌反应的搅拌速度为1000r/min，温度为6℃。
所述步骤2中的无水乙醇的喷洒量为3mL/cm2，所述均匀涂覆的涂覆量为10mL/cm2。
所述步骤3中的钛酸正丁酯在无水乙醇中的浓度为80g/L，甲基纤维素的加入量是钛酸正丁酯质量的15%，搅拌均匀的搅拌速度为800r/min，所述黑色竹炭纤维的加入量是钛酸正丁酯质量的300%。
所述步骤4中的均匀涂覆的涂覆量是10mL/cm2。
所述步骤4中的色浆层采用发泡色浆涂料纺丝编织而成，所述复合纤维层采用纳米纤维网，且所述纳米纤维网的厚度为0.9mm。
所述色浆层的制备方法如下：
步骤A，将聚丙烯酸钠加入至蒸馏水中，加入高取代羟丙基纤维素和水溶性色料低温超声分散60min，得到聚丙烯酸钠分散液；
步骤B，将聚丙烯酸钠分散液加入至静电纺丝机中静电纺丝反应，然后编织成单层纤维网；
步骤C，将电气石粉加入球磨机中湿法球磨60min，烘干后加入无水乙醇中搅拌均匀，得到浆料；
步骤D，将浆料均匀涂覆在单层纤维网表面，然后覆盖单层纤维网，重3次，得到多层纤维网；
步骤E，将多层纤维网加入至烘箱内恒温反应4h，得到色浆层。
所述步骤A中的聚丙烯酸钠在蒸馏水中的浓度为500g/L，所述高取代羟丙基纤维素的加入量是聚丙烯酸钠质量的40%，所述水溶性色料的加入量是聚丙烯酸钠质量的8%，所述低温超声分散的温度为15℃，超声频率为40kHz；所述步骤B中的静电纺丝参数为：溶液推进速率为1.2mL/h，纺丝电压为25kV，接收距离为25cm，温度为120℃；步骤C中的湿法球磨的温度为50℃，所述浆料的浓度为500g/L；所述步骤D中的涂覆量为6g/L；所述步骤E中的恒温反应的温度为90℃，压力为0.15MPa。
所述步骤5中的梯度恒温加压反应的程序如下：
温度 时间 压力
90℃ 30min 0.2MPa
140℃ 剩余时间 0.3MPa
实施例3
一种全遮光窗帘面料的制备方法，包括如下步骤：
步骤1，将二甲基二氯硅烷加入至乙醚中搅拌均匀，然后滴加蒸馏水并低温搅拌反应2h，得到粘稠的初步水解液；
步骤2，将基底布料平铺，并喷洒无水乙醇中完全润湿，然后将初步水解液均匀涂覆在基底布料表面，得到一级镀膜层；
步骤3，将钛酸正丁酯加入至无水乙醇中，并加入甲基纤维素搅拌均匀，得到分散钛醇液，然后将黑色竹炭纤维加入至钛醇液中，搅拌形成分散悬浊液；
步骤4，将分散悬浊液均匀涂覆在一级镀膜层表面，得到二级镀膜层，然后依次将色浆层和复合纤维层平覆在二级镀膜层表面，得到镀膜面料；
步骤5，将镀膜面料梯度恒温加压反应4h，降压冷却后得到全遮光窗帘面料。
所述步骤1中的二甲基二氯硅烷在乙醚中的浓度为150g/L，所述滴加的速度为2mL/min，所述低温搅拌反应的搅拌速度为800r/min，温度为4℃。
所述步骤2中的无水乙醇的喷洒量为2mL/cm2，所述均匀涂覆的涂覆量为8mL/cm2。
所述步骤3中的钛酸正丁酯在无水乙醇中的浓度为60g/L，甲基纤维素的加入量是钛酸正丁酯质量的12%，搅拌均匀的搅拌速度为700r/min，所述黑色竹炭纤维的加入量是钛酸正丁酯质量的250%。
所述步骤4中的均匀涂覆的涂覆量是8mL/cm2。
所述步骤4中的色浆层采用发泡色浆涂料纺丝编织而成，所述复合纤维层采用纳米纤维网，且所述纳米纤维网的厚度为0.5mm。
所述色浆层的制备方法如下：
步骤A，将聚丙烯酸钠加入至蒸馏水中，加入高取代羟丙基纤维素和水溶性色料低温超声分散50min，得到聚丙烯酸钠分散液；
步骤B，将聚丙烯酸钠分散液加入至静电纺丝机中静电纺丝反应，然后编织成单层纤维网；
步骤C，将电气石粉加入球磨机中湿法球磨50min，烘干后加入无水乙醇中搅拌均匀，得到浆料；
步骤D，将浆料均匀涂覆在单层纤维网表面，然后覆盖单层纤维网，重复3次，得到多层纤维网；
步骤E，将多层纤维网加入至烘箱内恒温反应3h，得到色浆层。
所述步骤A中的聚丙烯酸钠在蒸馏水中的浓度为300g/L，所述高取代羟丙基纤维素的加入量是聚丙烯酸钠质量的30%，所述水溶性色料的加入量是聚丙烯酸钠质量的6%，所述低温超声分散的温度为13℃，超声频率为30kHz；所述步骤B中的静电纺丝参数为：溶液推进速率为0.9mL/h，纺丝电压为20kV，接收距离为20cm，温度为110℃；步骤C中的湿法球磨的温度为40℃，所述浆料的浓度为300g/L；所述步骤D中的涂覆量为4g/L；所述步骤E中的恒温反应的温度为85℃，压力为0.14MPa。
所述步骤5中的梯度恒温加压反应的程序如下：
温度 时间 压力
85℃ 25min 0.2MPa
130℃ 剩余时间 0.2MPa
综上所述，本发明具有以下优点：
1.本发明解决了遮光布材质差，无法满足需求的问题，通过以甲基有机硅作为复合粘结剂，将色浆层和复合层凝固在基底布料表面，不仅提升了粘结稳定性，同时也提高了韧性和耐候性、防水、防盐雾、防霉菌等特性。
2.本发明以二甲基二氯硅烷为有机硅树脂的原材料，通过其水解产物缩聚固化过程与复合过程相结合，利用甲基硅树脂的立体网络结构形成渗透式固定，有效地提升了面料的牢固性与稳定性，同时提高了整体的弹性。
可以理解的是，以上关于本发明的具体描述，仅用于说明本发明而并非受限于本发明实施例所描述的技术方案。本领域的普通技术人员应当理解，仍然可以对本发明进行修改或等同替换，以达到相同的技术效果；只要满足使用需要，都在本发明的保护范围之内。

Claims (9)

1.一种全遮光窗帘面料的制备方法，其特征在于，包括如下步骤：
步骤1，将二甲基二氯硅烷加入至乙醚中搅拌均匀，然后滴加蒸馏水并低温搅拌反应1-3h，得到粘稠的初步水解液；
步骤2，将基底布料平铺，并喷洒无水乙醇中完全润湿，然后将初步水解液均匀涂覆在基底布料表面，得到一级镀膜层；
步骤3，将钛酸正丁酯加入至无水乙醇中，并加入甲基纤维素搅拌均匀，得到分散钛醇液，然后将黑色竹炭纤维加入至钛醇液中，搅拌形成分散悬浊液；
步骤4，将分散悬浊液均匀涂覆在一级镀膜层表面，得到二级镀膜层，然后依次将色浆层和复合纤维层平覆在二级镀膜层表面，得到镀膜面料；
步骤5，将镀膜面料梯度恒温加压反应3-5h，降压冷却后得到全遮光窗帘面料。
2.根据权利要求1所述的全遮光窗帘面料的制备方法，其特征在于：所述步骤1中的二甲基二氯硅烷在乙醚中的浓度为100-200g/L，所述滴加的速度为1-3mL/min，所述低温搅拌反应的搅拌速度为500-1000r/min，温度为2-6℃。
3.根据权利要求1所述的全遮光窗帘面料的制备方法，其特征在于：所述步骤2中的无水乙醇的喷洒量为1-3mL/cm2，所述均匀涂覆的涂覆量为5-10mL/cm2。
4.根据权利要求1所述的全遮光窗帘面料的制备方法，其特征在于：所述步骤3中的钛酸正丁酯在无水乙醇中的浓度为20-80g/L，甲基纤维素的加入量是钛酸正丁酯质量的10-15%，搅拌均匀的搅拌速度为500-800r/min，所述黑色竹炭纤维的加入量是钛酸正丁酯质量的150-300%。
5.根据权利要求1所述的全遮光窗帘面料的制备方法，其特征在于：所述步骤4中的均匀涂覆的涂覆量是5-10mL/cm2。
6.根据权利要求1所述的全遮光窗帘面料的制备方法，其特征在于：所述步骤4中的色浆层采用发泡色浆涂料纺丝编织而成，所述复合纤维层采用纳米纤维网，且所述纳米纤维网的厚度为0.1-0.9mm。
7.根据权利要求1所述的全遮光窗帘面料的制备方法，其特征在于：所述色浆层的制备方法如下：
步骤A，将聚丙烯酸钠加入至蒸馏水中，加入高取代羟丙基纤维素和水溶性色料低温超声分散30-60min，得到聚丙烯酸钠分散液；
步骤B，将聚丙烯酸钠分散液加入至静电纺丝机中静电纺丝反应，然后编织成单层纤维网；
步骤C，将电气石粉加入球磨机中湿法球磨30-60min，烘干后加入无水乙醇中搅拌均匀，得到浆料；
步骤D，将浆料均匀涂覆在单层纤维网表面，然后覆盖单层纤维网，重复2-3次，得到多层纤维网；
步骤E，将多层纤维网加入至烘箱内恒温反应2-4h，得到色浆层。
8.根据权利要求7所述的全遮光窗帘面料的制备方法，其特征在于：所述步骤A中的聚丙烯酸钠在蒸馏水中的浓度为100-500g/L，所述高取代羟丙基纤维素的加入量是聚丙烯酸钠质量的20-40%，所述水溶性色料的加入量是聚丙烯酸钠质量的2-8%，所述低温超声分散的温度为10-15℃，超声频率为20-40kHz；所述步骤B中的静电纺丝参数为：溶液推进速率为0.7-1.2mL/h，纺丝电压为15-25kV，接收距离为18-25cm，温度为100-120℃；步骤C中的湿法球磨的温度为30-50℃，所述浆料的浓度为100-500g/L；所述步骤D中的涂覆量为2-6g/L；所述步骤E中的恒温反应的温度为80-90℃，压力为0.12-0.15MPa。
9.根据权利要求1所述的全遮光窗帘面料的制备方法，其特征在于：所述步骤5中的梯度恒温加压反应的程序如下：
第一阶段，反应温度80-90℃，时间20-30min，压力0.1-0.2MPa;第二阶段，反应温度110-140℃，时间：剩余时间，压力0.2-0.3Mpa。
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