CN109988474A - A kind of early stage excellent water resistance water burnt-in sand multicolor finish - Google Patents
A kind of early stage excellent water resistance water burnt-in sand multicolor finish Download PDFInfo
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- CN109988474A CN109988474A CN201910267500.4A CN201910267500A CN109988474A CN 109988474 A CN109988474 A CN 109988474A CN 201910267500 A CN201910267500 A CN 201910267500A CN 109988474 A CN109988474 A CN 109988474A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D143/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and containing boron, silicon, phosphorus, selenium, tellurium, or a metal; Coating compositions based on derivatives of such polymers
- C09D143/04—Homopolymers or copolymers of monomers containing silicon
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- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/14—Paints containing biocides, e.g. fungicides, insecticides or pesticides
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/29—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes for multicolour effects
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
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- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/63—Additives non-macromolecular organic
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- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/65—Additives macromolecular
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2237—Oxides; Hydroxides of metals of titanium
- C08K2003/2241—Titanium dioxide
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
- C08L2205/025—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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Abstract
The invention discloses a kind of early stage excellent water resistance water burnt-in sand multicolor finishes; the preparation of preparation, base paint including protective glue, the preparation of water burnt-in sand multicolor finish continuous phase, the preparation of colorful particle, multicolor finish preparation step; it can effectively improve the early stage water resistance of water burnt-in sand multicolor finish; it can solve the problem of that is generated in practice of construction by Changes in weather whitens, changes colour very well.
Description
Technical field
The present invention relates to building coating field more particularly to a kind of early stage excellent water resistance water burnt-in sand multicolor finishes.
Background technique
Heat-proof water burnt-in sand multicolor finish is a kind of architectural decoration coating material, the decoration effect of decorative effect approximation lithotome
Fruit, have the characteristics that it is light, environmentally friendly, rich in color, can be used for high-rise outer wall decoration.Water burnt-in sand multicolor finish is used for decoration of exterior wall
When, operational procedure is usually: crowd putty layer → one of seal coat → one of priming paint → bis- in smooth, firm base
The water burnt-in sand multicolor finish → road 1-2 finish, priming paint, multicolor finish finish, when spraying, every one of interval time is at least for 24 hours
To guarantee the stemness of coating, it is just competent to take 7 day time coating after finish has been constructed for entire coating system under standard conditions
Thoroughly, 7 days or more can be dried without meeting rainy weather, water burnt-in sand multicolor finish by being difficult very guarantee system in practice of construction
Due to containing the hydrophilic aids such as cellulose, thickener, arrive in the meantime it is rainy will result in water burnt-in sand multicolor finish layer and whiten,
And it is difficult to restore.Therefore it is early stage water resistance problem that multicolor finish, which faces greatest problem, in practice of construction, i.e., colorful in water burnt-in sand
There is good water resistance after coating application for 24 hours, stand and drench with rain and non-whitening, discoloration.
Summary of the invention
It is an object of the present invention to overcome the above deficiencies, provides a kind of colorful painting of water burnt-in sand of early stage excellent water resistance
Material meets the case where water whitens to solve early water burnt-in sand multicolor finish.
The present invention realizes in the following way: its preparation step is as follows:
Step 1: the preparation of protective glue
The raw material and mass ratio of protective glue are as follows: 90~95 parts by weight of water, 5~10 parts by weight of hectorite are first added water and divide
Cylinder is dissipated, hectorite is added under 600~1500r/min stirring condition, is dispersed to abundant dissolution, it is spare to stand 2h for no granular sensation.
Step 2: the preparation of base paint
The raw material and mass ratio of base paint are as follows: 30~40 parts by weight of water；0.5~1.5 parts by weight of hydrophobically modified celluloses；It is anti-
Freeze 0.05~0.5 parts by weight of agent；Multi-functional dose of 0.05~0.2 parts by weight；0.2~0.5 parts by weight of dispersing agent；Defoaming agent 0.3~
0.7 parts by weight；0.5~1.0 parts by weight of coalescing agent；10~25 parts by weight of kaolin；1~2 parts by weight of titanium dioxide；Silicone acrylic emulsion
25~35 parts by weight；2~5 parts by weight of organic silicon emulsion；8~15 parts by weight of protective glue prepared by step 1；Preservative 0.2~0.5
Parts by weight；Successively addition above-mentioned raw materials are fully dispersed uniformly, and white basis paint is made.
Step 3: the preparation of water burnt-in sand multicolor finish continuous phase:
The raw material and weight ratio of water burnt-in sand multicolor finish continuous phase are as follows: 10~20 parts by weight of water；0.2~0.5 weight of preservative
Measure part；3~4 parts by weight of coalescing agent；0.2~0.5 parts by weight of antifreezing agent；0.2~0.5 parts by weight of multifunctional assistant；The third cream of silicon
75~80 parts by weight of liquid；0.2~0.5 parts by weight of thickener；2~5 parts by weight of organic silicon emulsion；0.1~0.2 weight of defoaming agent
Part；It is fully dispersed uniformly successively to add above-mentioned raw material, water burnt-in sand multicolor finish continuous phase is made.
Step 4: the preparation of granulation liquid:
The raw material and weight ratio of granulation liquid are as follows: 50~70 parts by weight of water；0.4 parts by weight of preservative；Bentonite 0.5~0.8
Parts by weight；30~50 parts by weight of protective glue prepared by step 1；Successively addition above-mentioned raw materials are fully dispersed uniformly at translucent liquid
Granulation liquid is made in body.
Step 5: the preparation of colorful particle:
The raw material and weight ratio of colorful particle are as follows: 25~50 parts by weight of base paint prepared in step 2；Quartz sand 25~50
Parts by weight；0.05~0.5 parts by weight of mill base；30~40 parts by weight of granulation liquid prepared in step 4；Quartz is added in base paint
Sand is then added with color paste toning and is granulated granulation in liquid, prepared colorful particle.
Step 6: the preparation of multicolor finish:
The raw material and weight ratio of multicolor finish are as follows: 70~85 parts by weight of colorful particle prepared by step 5；Prepared by step 3
15~30 parts by weight of water burnt-in sand multicolor finish continuous phase；Successively addition above-mentioned raw materials are uniformly mixed, and multicolor finish is made.
Further, the antifreezing agent is ethylene glycol or propylene glycol；Described multi-functional dose is AMP95；The dispersion
Agent is multi-component copolymer acrylic acid ammonium salt；The defoaming agent is mineral oil antifoam agent or organic silicon defoamer；The film forming helps
Agent is one of 12 ester alcohols, butyl glycol ether, propylene glycol monomethyl ether, dipropylene glycol methyl ether；The preservative be Kathon CG or
Preservative MC；The thickener is one of ASE60, TT935, RM-8W.
Water burnt-in sand multicolor finish of the invention is effectively improved using organic silicon emulsion, hectorite, hydrophobically modified celluloses
The water resistance of multicolor finish, makes it have excellent early stage water resistance, can solve very well because of Changes in weather in practice of construction, and
The problem of whitening, change colour of generation.Water burnt-in sand multicolor finish of the invention, in air drying its water resistance for 24 hours are as follows: 25 DEG C of room temperature
Soak 15 days non-whitenings, non-discolouring, 70 DEG C of water temperatures non-whitening, non-discolouring for 24 hours.It can satisfy the water-fast of water burnt-in sand multicolor finish
Property.
Specific embodiment
Below by specific embodiment, the present invention will be further described in detail:
Embodiment one
Step 1: the preparation of protective glue
The raw material and mass ratio of protective glue are as follows: first dispersion cylinder is added in water by 91.8 parts by weight of water, 8 parts by weight of hectorite,
Hectorite is added under 600~1500r/min stirring condition, is dispersed to abundant dissolution, it is spare to stand 2h for no granular sensation.
Step 2: the preparation of base paint
The raw material and mass ratio of base paint are as follows: 40 parts by weight of water；1.5 parts by weight of hydrophobically modified celluloses；0.5 weight of antifreezing agent
Measure part；Multi-functional dose of 0.1 parts by weight；0.4 parts by weight of dispersing agent；0.5 parts by weight of defoaming agent；0.6 parts by weight of coalescing agent；Kaolinite
Native 15 parts by weight；1 parts by weight of titanium dioxide；26 parts by weight of silicone acrylic emulsion；2 parts by weight of organic silicon emulsion；Protective glue prepared by step 1
12 parts by weight；0.3 parts by weight of preservative；Successively addition above-mentioned raw materials are fully dispersed uniformly, and white basis paint is made.
Step 3: the preparation of water burnt-in sand multicolor finish continuous phase:
The raw material and weight ratio of water burnt-in sand multicolor finish continuous phase are as follows: 12 parts by weight of water；0.4 parts by weight of preservative；Film forming
3.5 parts by weight of auxiliary agent；0.25 parts by weight of antifreezing agent；0.2 parts by weight of multifunctional assistant；80 parts by weight of silicone acrylic emulsion；Thickener 0.4
Parts by weight；2 parts by weight of organic silicon emulsion；0.1 parts by weight of defoaming agent；It is fully dispersed uniformly successively to add above-mentioned raw material, is made
Water burnt-in sand multicolor finish continuous phase.
Step 4: the preparation of granulation liquid:
The raw material and weight ratio of granulation liquid are as follows: 64 parts by weight of water；0.4 parts by weight of preservative；0.6 parts by weight of bentonite；Step
35 parts by weight of protective glue of rapid 1 preparation；Successively addition above-mentioned raw materials are fully dispersed uniformly at translucent liquid, and granulation liquid is made.
Step 5: the preparation of colorful particle:
The raw material and weight ratio of colorful particle are as follows: 37 parts by weight of base paint prepared in step 2；37 parts by weight of quartz sand；
0.1 parts by weight of mill base；30 parts by weight of granulation liquid prepared in step 4；Quartz sand is added in base paint, with color paste toning, then
It is added and is granulated granulation in liquid, prepare colorful particle.
Step 6: the preparation of multicolor finish:
The raw material and weight ratio of multicolor finish are as follows: 80 parts by weight of colorful particle prepared by step 5；Water packet prepared by step 3
20 parts by weight of sand multicolor finish continuous phase；Successively addition above-mentioned raw materials are uniformly mixed, and multicolor finish is made.
Further, the antifreezing agent is ethylene glycol；Described multi-functional dose is AMP95；The dispersing agent is polynary
Co-polypropylene acid ammonium salt；The defoaming agent is organic silicon defoamer；The coalescing agent is 12 ester alcohols；The anti-corrosion
Agent is Kathon CG；The thickener is ASE60.
1 water burnt-in sand multicolor finish testing result of table
As shown in Table 1, the water burnt-in sand multicolor finish that prepared by embodiment one can satisfy performance indicator, water burnt-in sand of the invention
The major advantage of multicolor finish is the ability of early stage water resistance.Water resistance test the result is as follows:
The testing result that 2 water burnt-in sand coating of table dry early stage for 24 hours is water-fast
| Test item | Case 1 |
| 25 DEG C of water of resistance to room temperature | Nothing is whitened within 15 days |
| Resistance to 70 DEG C of hot water | 30h non-whitening |
By Tables 1 and 2 it is found that the indices of water burnt-in sand multicolor finish prepared by the embodiment of the present invention one are all satisfied and want
It asks, the water resistance of multicolor finish is effectively improved by organic silicon emulsion, hectorite, hydrophobically modified celluloses, it can be fine
Solve the problems, such as early stage meet water whiten.
It should be appreciated that embodiments of the present invention are not limited by the following examples, any shape that the present invention is done
Accommodation and/or change in formula fall within the scope of the present invention.
Claims (2)
1. a kind of early stage excellent water resistance water burnt-in sand multicolor finish, it is characterised in that: preparation methods steps are as follows:
Step 1: the preparation of protective glue
The raw material and mass ratio of protective glue are as follows: first dispersion cylinder is added in water by 90~95 parts by weight of water, 5~10 parts by weight of hectorite,
Hectorite is added under 600~1500r/min stirring condition, is dispersed to abundant dissolution, it is spare to stand 2h for no granular sensation；
Step 2: the preparation of base paint
The raw material and mass ratio of base paint are as follows: 30~40 parts by weight of water；0.5~1.5 parts by weight of hydrophobically modified celluloses；Antifreezing agent
0.05~0.5 parts by weight；Multi-functional dose of 0.05~0.2 parts by weight；0.2~0.5 parts by weight of dispersing agent；0.3~0.7 weight of defoaming agent
Measure part；0.5~1.0 parts by weight of coalescing agent；10~25 parts by weight of kaolin；1~2 parts by weight of titanium dioxide；Silicone acrylic emulsion 25~
35 parts by weight；2~5 parts by weight of organic silicon emulsion；8~15 parts by weight of protective glue prepared by step 1；0.2~0.5 weight of preservative
Part；Successively addition above-mentioned raw materials are fully dispersed uniformly, and white basis paint is made；
Step 3: the preparation of water burnt-in sand multicolor finish continuous phase:
The raw material and weight ratio of water burnt-in sand multicolor finish continuous phase are as follows: 10~20 parts by weight of water；0.2~0.5 parts by weight of preservative；
3~4 parts by weight of coalescing agent；0.2~0.5 parts by weight of antifreezing agent；0.2~0.5 parts by weight of multifunctional assistant；Silicone acrylic emulsion 75~
80 parts by weight；0.2~0.5 parts by weight of thickener；2~5 parts by weight of organic silicon emulsion；0.1~0.2 parts by weight of defoaming agent；Successively
It is fully dispersed uniformly to add above-mentioned raw material, water burnt-in sand multicolor finish continuous phase is made；
Step 4: the preparation of granulation liquid:
The raw material and weight ratio of granulation liquid are as follows: 50~70 parts by weight of water；0.4 parts by weight of preservative；0.5~0.8 weight of bentonite
Part；30~50 parts by weight of protective glue prepared by step 1；Successively addition above-mentioned raw materials are fully dispersed uniformly at translucent liquid, system
Obtain granulation liquid；
Step 5: the preparation of colorful particle:
The raw material and weight ratio of colorful particle are as follows: 25~50 parts by weight of base paint prepared in step 2；25~50 weight of quartz sand
Part；0.05~0.5 parts by weight of mill base；30~40 parts by weight of granulation liquid prepared in step 4；Quartz sand is added in base paint, uses
Color paste toning is then added and is granulated granulation in liquid, prepares colorful particle；
Step 6: the preparation of multicolor finish:
The raw material and weight ratio of multicolor finish are as follows: 70~85 parts by weight of colorful particle prepared by step 5；Water packet prepared by step 3
15~30 parts by weight of sand multicolor finish continuous phase；Successively addition above-mentioned raw materials are uniformly mixed, and multicolor finish is made.
2. a kind of early stage excellent water resistance water burnt-in sand multicolor finish according to claim 1, it is characterised in that: described antifreeze
Agent is ethylene glycol or propylene glycol；
Described multi-functional dose is AMP95；
The dispersing agent is multi-component copolymer acrylic acid ammonium salt；
The defoaming agent is mineral oil antifoam agent or organic silicon defoamer；
The coalescing agent is one of 12 ester alcohols, butyl glycol ether, propylene glycol monomethyl ether, dipropylene glycol methyl ether；
The preservative is Kathon CG or preservative MC；
The thickener is one of ASE60, TT935, RM-8W.
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| CN201910267500.4A CN109988474A (en) | 2019-04-03 | 2019-04-03 | A kind of early stage excellent water resistance water burnt-in sand multicolor finish |
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| CN201910267500.4A CN109988474A (en) | 2019-04-03 | 2019-04-03 | A kind of early stage excellent water resistance water burnt-in sand multicolor finish |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113667332A (en) * | 2021-09-03 | 2021-11-19 | 福建省三棵树新材料有限公司 | Liquid inorganic silicate paint for color-adjustable inner wall and preparation method thereof |
| CN113773694A (en) * | 2021-09-26 | 2021-12-10 | 北京莱恩斯新材料科技有限公司 | Suspended granulating liquid and preparation method thereof, stone-like coating and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113667332A (en) * | 2021-09-03 | 2021-11-19 | 福建省三棵树新材料有限公司 | Liquid inorganic silicate paint for color-adjustable inner wall and preparation method thereof |
| CN113773694A (en) * | 2021-09-26 | 2021-12-10 | 北京莱恩斯新材料科技有限公司 | Suspended granulating liquid and preparation method thereof, stone-like coating and preparation method thereof |
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Application publication date: 20190709 |
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