CN109942802A - 具有自修复功能的共聚聚碳酸酯及其制备方法 - Google Patents
具有自修复功能的共聚聚碳酸酯及其制备方法 Download PDFInfo
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- CN109942802A CN109942802A CN201910234541.3A CN201910234541A CN109942802A CN 109942802 A CN109942802 A CN 109942802A CN 201910234541 A CN201910234541 A CN 201910234541A CN 109942802 A CN109942802 A CN 109942802A
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- self
- repair function
- preparation
- copolymerization polycarbonate
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- 239000004417 polycarbonate Substances 0.000 title claims abstract description 39
- 229920000515 polycarbonate Polymers 0.000 title claims abstract description 39
- 238000007334 copolymerization reaction Methods 0.000 title claims abstract description 27
- 238000002360 preparation method Methods 0.000 title claims abstract description 21
- 238000006243 chemical reaction Methods 0.000 claims abstract description 17
- 239000003054 catalyst Substances 0.000 claims abstract description 16
- QYMFNZIUDRQRSA-UHFFFAOYSA-N dimethyl butanedioate;dimethyl hexanedioate;dimethyl pentanedioate Chemical compound COC(=O)CCC(=O)OC.COC(=O)CCCC(=O)OC.COC(=O)CCCCC(=O)OC QYMFNZIUDRQRSA-UHFFFAOYSA-N 0.000 claims abstract description 14
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 13
- 238000000034 method Methods 0.000 claims abstract description 8
- 150000002921 oxetanes Chemical class 0.000 claims abstract description 7
- 238000009413 insulation Methods 0.000 claims abstract description 5
- KWYUFKZDYYNOTN-UHFFFAOYSA-M potassium hydroxide Substances [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims description 10
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 claims description 8
- 239000008103 glucose Substances 0.000 claims description 8
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 4
- IISBACLAFKSPIT-UHFFFAOYSA-N bisphenol A Chemical compound C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 IISBACLAFKSPIT-UHFFFAOYSA-N 0.000 claims description 4
- 239000007789 gas Substances 0.000 claims description 4
- 230000001681 protective effect Effects 0.000 claims description 4
- -1 galactolipin Chemical compound 0.000 claims description 3
- AHHWIHXENZJRFG-UHFFFAOYSA-N oxetane Chemical compound C1COC1 AHHWIHXENZJRFG-UHFFFAOYSA-N 0.000 claims description 3
- OWEGMIWEEQEYGQ-UHFFFAOYSA-N 100676-05-9 Natural products OC1C(O)C(O)C(CO)OC1OCC1C(O)C(O)C(O)C(OC2C(OC(O)C(O)C2O)CO)O1 OWEGMIWEEQEYGQ-UHFFFAOYSA-N 0.000 claims description 2
- RRRHGMRCVIZIRT-UHFFFAOYSA-N 3-(bromomethyl)-3-ethyloxetane Chemical compound CCC1(CBr)COC1 RRRHGMRCVIZIRT-UHFFFAOYSA-N 0.000 claims description 2
- RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 claims description 2
- 229930091371 Fructose Natural products 0.000 claims description 2
- 239000005715 Fructose Substances 0.000 claims description 2
- GUBGYTABKSRVRQ-QKKXKWKRSA-N Lactose Natural products OC[C@H]1O[C@@H](O[C@H]2[C@H](O)[C@@H](O)C(O)O[C@@H]2CO)[C@H](O)[C@@H](O)[C@H]1O GUBGYTABKSRVRQ-QKKXKWKRSA-N 0.000 claims description 2
- GUBGYTABKSRVRQ-PICCSMPSSA-N Maltose Natural products O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@@H](CO)OC(O)[C@H](O)[C@H]1O GUBGYTABKSRVRQ-PICCSMPSSA-N 0.000 claims description 2
- 239000003513 alkali Substances 0.000 claims description 2
- 239000002585 base Substances 0.000 claims description 2
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 claims description 2
- 229940106691 bisphenol a Drugs 0.000 claims description 2
- ROORDVPLFPIABK-UHFFFAOYSA-N diphenyl carbonate Chemical group C=1C=CC=CC=1OC(=O)OC1=CC=CC=C1 ROORDVPLFPIABK-UHFFFAOYSA-N 0.000 claims description 2
- 239000008101 lactose Substances 0.000 claims description 2
- 229910052757 nitrogen Inorganic materials 0.000 claims description 2
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Substances [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 claims description 2
- 229910000027 potassium carbonate Inorganic materials 0.000 claims description 2
- UKLWXKWTXHHMFK-UHFFFAOYSA-N 3-(chloromethyl)-3-ethyloxetane Chemical compound CCC1(CCl)COC1 UKLWXKWTXHHMFK-UHFFFAOYSA-N 0.000 claims 1
- GUBGYTABKSRVRQ-XLOQQCSPSA-N Alpha-Lactose Chemical compound O[C@@H]1[C@@H](O)[C@@H](O)[C@@H](CO)O[C@H]1O[C@@H]1[C@@H](CO)O[C@H](O)[C@H](O)[C@H]1O GUBGYTABKSRVRQ-XLOQQCSPSA-N 0.000 claims 1
- WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical compound [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 claims 1
- GUBGYTABKSRVRQ-QUYVBRFLSA-N beta-maltose Chemical compound OC[C@H]1O[C@H](O[C@H]2[C@H](O)[C@@H](O)[C@H](O)O[C@@H]2CO)[C@H](O)[C@@H](O)[C@@H]1O GUBGYTABKSRVRQ-QUYVBRFLSA-N 0.000 claims 1
- GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Substances BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 claims 1
- 229910052794 bromium Inorganic materials 0.000 claims 1
- 125000004218 chloromethyl group Chemical group [H]C([H])(Cl)* 0.000 claims 1
- 239000000463 material Substances 0.000 abstract description 8
- 230000007613 environmental effect Effects 0.000 abstract description 4
- 238000004519 manufacturing process Methods 0.000 abstract description 4
- 230000006870 function Effects 0.000 description 8
- 230000035876 healing Effects 0.000 description 7
- 238000002474 experimental method Methods 0.000 description 4
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 4
- 238000010792 warming Methods 0.000 description 4
- 230000000630 rising effect Effects 0.000 description 3
- 239000000758 substrate Substances 0.000 description 3
- WAGBGDXBSUHBSB-UHFFFAOYSA-N 2-(1-bromopropan-2-yl)oxirane Chemical compound CC(CBr)C1CO1 WAGBGDXBSUHBSB-UHFFFAOYSA-N 0.000 description 2
- HFUODXIIBUADCY-UHFFFAOYSA-N 2-(1-chloropropan-2-yl)oxirane Chemical compound ClCC(C)C1CO1 HFUODXIIBUADCY-UHFFFAOYSA-N 0.000 description 2
- 238000012661 block copolymerization Methods 0.000 description 2
- FJDQFPXHSGXQBY-UHFFFAOYSA-L caesium carbonate Chemical compound [Cs+].[Cs+].[O-]C([O-])=O FJDQFPXHSGXQBY-UHFFFAOYSA-L 0.000 description 2
- 229910000024 caesium carbonate Inorganic materials 0.000 description 2
- 150000001720 carbohydrates Chemical class 0.000 description 2
- 235000014633 carbohydrates Nutrition 0.000 description 2
- NEHMKBQYUWJMIP-UHFFFAOYSA-N chloromethane Chemical compound ClC NEHMKBQYUWJMIP-UHFFFAOYSA-N 0.000 description 2
- 239000011248 coating agent Substances 0.000 description 2
- 238000000576 coating method Methods 0.000 description 2
- 229910003460 diamond Inorganic materials 0.000 description 2
- 239000010432 diamond Substances 0.000 description 2
- 150000002148 esters Chemical class 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 229920001228 polyisocyanate Polymers 0.000 description 2
- 239000005056 polyisocyanate Substances 0.000 description 2
- 229920000642 polymer Polymers 0.000 description 2
- MCZYEFODKAZWIH-UHFFFAOYSA-N 3-(chloromethyl)-3-methyloxetane Chemical class ClCC1(C)COC1 MCZYEFODKAZWIH-UHFFFAOYSA-N 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 125000005997 bromomethyl group Chemical group 0.000 description 1
- 239000002041 carbon nanotube Substances 0.000 description 1
- 229910021393 carbon nanotube Inorganic materials 0.000 description 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-N carbonic acid Chemical compound OC(O)=O BVKZGUZCCUSVTD-UHFFFAOYSA-N 0.000 description 1
- 150000004651 carbonic acid esters Chemical class 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000004035 construction material Substances 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000004132 cross linking Methods 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- MAHNFPMIPQKPPI-UHFFFAOYSA-N disulfur Chemical compound S=S MAHNFPMIPQKPPI-UHFFFAOYSA-N 0.000 description 1
- 229920006351 engineering plastic Polymers 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 230000009442 healing mechanism Effects 0.000 description 1
- 230000002427 irreversible effect Effects 0.000 description 1
- IQPQWNKOIGAROB-UHFFFAOYSA-N isocyanate group Chemical group [N-]=C=O IQPQWNKOIGAROB-UHFFFAOYSA-N 0.000 description 1
- 230000003902 lesion Effects 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 229920005668 polycarbonate resin Polymers 0.000 description 1
- 239000004431 polycarbonate resin Substances 0.000 description 1
- 239000002861 polymer material Substances 0.000 description 1
- 229920005862 polyol Polymers 0.000 description 1
- 150000003077 polyols Chemical class 0.000 description 1
- 239000004814 polyurethane Substances 0.000 description 1
- 229920002635 polyurethane Polymers 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 238000012113 quantitative test Methods 0.000 description 1
- 230000008439 repair process Effects 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G64/00—Macromolecular compounds obtained by reactions forming a carbonic ester link in the main chain of the macromolecule
- C08G64/20—General preparatory processes
- C08G64/30—General preparatory processes using carbonates
- C08G64/307—General preparatory processes using carbonates and phenols
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
- C08G63/64—Polyesters containing both carboxylic ester groups and carbonate groups
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G64/00—Macromolecular compounds obtained by reactions forming a carbonic ester link in the main chain of the macromolecule
- C08G64/04—Aromatic polycarbonates
- C08G64/06—Aromatic polycarbonates not containing aliphatic unsaturation
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G64/00—Macromolecular compounds obtained by reactions forming a carbonic ester link in the main chain of the macromolecule
- C08G64/16—Aliphatic-aromatic or araliphatic polycarbonates
- C08G64/1608—Aliphatic-aromatic or araliphatic polycarbonates saturated
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G64/00—Macromolecular compounds obtained by reactions forming a carbonic ester link in the main chain of the macromolecule
- C08G64/18—Block or graft polymers
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G2230/00—Compositions for preparing biodegradable polymers
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Polyesters Or Polycarbonates (AREA)
Abstract
Description
Claims (10)
Priority Applications (3)
Application Number | Priority Date | Filing Date | Title |
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CN201910234541.3A CN109942802B (zh) | 2019-03-26 | 2019-03-26 | 具有自修复功能的共聚聚碳酸酯及其制备方法 |
PCT/CN2020/077931 WO2020192381A1 (zh) | 2019-03-26 | 2020-03-05 | 具有自修复功能的共聚聚碳酸酯及其制备方法 |
US16/812,465 US11136433B2 (en) | 2019-03-26 | 2020-03-09 | Self-healing copolymerized polycarbonate and preparation method therefor |
Applications Claiming Priority (1)
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CN201910234541.3A CN109942802B (zh) | 2019-03-26 | 2019-03-26 | 具有自修复功能的共聚聚碳酸酯及其制备方法 |
Publications (2)
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CN109942802A true CN109942802A (zh) | 2019-06-28 |
CN109942802B CN109942802B (zh) | 2020-11-20 |
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CN201910234541.3A Active CN109942802B (zh) | 2019-03-26 | 2019-03-26 | 具有自修复功能的共聚聚碳酸酯及其制备方法 |
Country Status (3)
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US (1) | US11136433B2 (zh) |
CN (1) | CN109942802B (zh) |
WO (1) | WO2020192381A1 (zh) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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WO2020192381A1 (zh) * | 2019-03-26 | 2020-10-01 | 北京濮源新材料技术研究院(普通合伙) | 具有自修复功能的共聚聚碳酸酯及其制备方法 |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104725656A (zh) * | 2015-03-10 | 2015-06-24 | 长安大学 | 一种受损聚氨酯材料的修复方法 |
CN107793908A (zh) * | 2016-09-01 | 2018-03-13 | 纳米及先进材料研发院有限公司 | 涂料组合物及向衬底赋予自愈合等特性的方法 |
JP2018172690A (ja) * | 2015-04-01 | 2018-11-08 | サムヤン コーポレイション | ポリウレタン、その製造方法及び用途 |
Family Cites Families (9)
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---|---|---|---|---|
DE10201761A1 (de) * | 2002-01-18 | 2003-07-31 | Bayer Ag | Folie als Dielektrikum in Kondensatoren und Verfahren zu ihrer Herstellung |
CN100432119C (zh) * | 2003-06-16 | 2008-11-12 | 帝人株式会社 | 聚碳酸酯及其制备方法 |
KR101247819B1 (ko) * | 2007-12-12 | 2013-03-26 | 미쓰비시 가가꾸 가부시키가이샤 | 폴리카보네이트의 제조 방법 및 폴리카보네이트 성형물 |
US8658786B2 (en) * | 2009-04-20 | 2014-02-25 | The University Of Southern Mississippi | Self-repairing cyclic oxide-substituted chitosan polyurethane networks |
CN102470656B (zh) * | 2009-08-21 | 2015-11-25 | 帝人株式会社 | 嵌件成型品 |
JP5644623B2 (ja) * | 2010-03-25 | 2014-12-24 | 宇部興産株式会社 | 分子末端にオキセタンを有するポリカーボネート及びその製造方法 |
US20160235650A1 (en) * | 2013-03-15 | 2016-08-18 | Avon Products, Inc | Cosmetic Formulation Incorporating a UV-Triggered Self-Healing Material |
EP3414276A1 (en) * | 2016-02-12 | 2018-12-19 | SABIC Global Technologies B.V. | Inherently healing polycarbonate resins |
CN109942802B (zh) * | 2019-03-26 | 2020-11-20 | 北京濮源新材料技术研究院(普通合伙) | 具有自修复功能的共聚聚碳酸酯及其制备方法 |
-
2019
- 2019-03-26 CN CN201910234541.3A patent/CN109942802B/zh active Active
-
2020
- 2020-03-05 WO PCT/CN2020/077931 patent/WO2020192381A1/zh active Application Filing
- 2020-03-09 US US16/812,465 patent/US11136433B2/en active Active
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104725656A (zh) * | 2015-03-10 | 2015-06-24 | 长安大学 | 一种受损聚氨酯材料的修复方法 |
JP2018172690A (ja) * | 2015-04-01 | 2018-11-08 | サムヤン コーポレイション | ポリウレタン、その製造方法及び用途 |
CN107793908A (zh) * | 2016-09-01 | 2018-03-13 | 纳米及先进材料研发院有限公司 | 涂料组合物及向衬底赋予自愈合等特性的方法 |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2020192381A1 (zh) * | 2019-03-26 | 2020-10-01 | 北京濮源新材料技术研究院(普通合伙) | 具有自修复功能的共聚聚碳酸酯及其制备方法 |
Also Published As
Publication number | Publication date |
---|---|
US20200308345A1 (en) | 2020-10-01 |
US11136433B2 (en) | 2021-10-05 |
CN109942802B (zh) | 2020-11-20 |
WO2020192381A1 (zh) | 2020-10-01 |
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Denomination of invention: Copolymer polycarbonate with self-healing function and its preparation method Effective date of registration: 20230720 Granted publication date: 20201120 Pledgee: China Petroleum Finance Co.,Ltd. Pledgor: PUYANG SHENGTONGJUYUAN ADVANCED MATERIALS Co.,Ltd. Registration number: Y2023980048997 |
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Granted publication date: 20201120 Pledgee: China Petroleum Finance Co.,Ltd. Pledgor: PUYANG SHENGTONGJUYUAN ADVANCED MATERIALS Co.,Ltd. Registration number: Y2023980048997 |
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PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: Copolymer polycarbonate with self-healing function and its preparation method Granted publication date: 20201120 Pledgee: China Petroleum Finance Co.,Ltd. Pledgor: PUYANG SHENGTONGJUYUAN ADVANCED MATERIALS Co.,Ltd. Registration number: Y2024980021619 |